A method for rapidly detecting BaP in edible oil based on LLE-SERS modified silver nanomaterial

By combining CTAB-modified silver nanomaterials with liquid-liquid extraction and surface-enhanced Raman spectroscopy, the problems of rapid, low-cost, and high-sensitivity detection of BaP in edible oils have been solved, enabling a simple detection of BaP.

CN119985442BActive Publication Date: 2026-01-13XIAMEN UNIV
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Patent Information

Application Number
CN202510159888.1
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-02-13
Publication Date
2026-01-13
Estimated Expiration
2045-02-13

AI Technical Summary

Technical Problem

Existing technologies make it difficult to achieve rapid, low-cost, and highly sensitive on-site detection of BaP in edible oils. Traditional methods require complex pretreatment processes and are costly.

Method used

By combining CTAB-modified silver nanomaterials with liquid-liquid extraction and surface-enhanced Raman spectroscopy (LLE-SERS), BaP can be rapidly enriched and detected using CTAB-functionalized Ag nanoparticles, avoiding interference from the oil matrix.

Benefits of technology

This technology enables rapid, simple, and sensitive detection of BaP in edible oils, reducing detection costs and improving detection efficiency and accuracy.

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Abstract

The application belongs to the technical field of food safety detection, and specifically discloses a method for detecting BaP in edible oil by using CTAB modified silver nanomaterial based on LLE-SERS, which comprises the following steps: preparing Ag nanoparticle sol, preparing CTAB functionalized Ag nanoparticle sol, SERS detection of BaP standard aqueous solution with different concentrations, fitting a standard curve, extracting BaP and performing SERS detection. The synthetic raw materials of the surface CTAB functionalized Ag nanoparticles used in the application are simple, and the coverage degree of the ligand molecules CTAB on the surface of the Ag nanoparticles can be controlled and adjusted. The CTAB as the surface ligand can directly capture and enrich BaP molecules. The detection method is high in stability, and can effectively avoid the problem that different batches of samples produce different effects in the Raman test.
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