Refreshing essence composition containing platycladus orientalis essential oil as well as preparation method and application of refreshing essence composition

Abstract

The invention relates to the technical field of raw materials of skin care products, and particularly discloses a refreshing essence composition containing platycladus orientalis essential oil as well as a preparation method and application of the refreshing essence composition. The refreshing essence composition containing the platycladus orientalis essential oil is prepared by compounding the platycladus orientalis essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil and zanthoxylum oil. The method has the advantage that the refreshing effect is further improved.

Description

Technical Field

[0001] The present invention relates to the field of skin care product raw materials, and in particular to a refreshing fragrance composition containing Platycladus orientalis essential oil, a preparation method thereof, and an application thereof. Background Art

[0002] In the fast-paced modern life, people often face the problems of insufficient energy, drowsiness and fatigue whether in the working, learning or living scenarios. Whether it is long-term work overtime, high-intensity study for exams, or the exhaustion of daily commuting, effective refreshing methods are urgently needed to maintain a clear mind and good mental state. At present, the common refreshing products on the market mainly include coffee, functional beverages and some daily chemical products containing irritating ingredients. However, long-term consumption of coffee and functional beverages may cause problems such as palpitations and gastrointestinal discomfort, and their action time is limited; most traditional daily chemical refreshing products add artificially synthesized irritating ingredients, which not only have a pungent smell, but also have potential irritation risks to the skin and respiratory tract. At the same time, there are disadvantages such as short and non-persistent refreshing effects. Therefore, natural and green plant essential oils are beginning to be selected in refreshing products to bring a safer refreshing effect. However, the refreshing effect of the existing refreshing products added with plant essential oils is still relatively average, and it is difficult to achieve a quick refreshing effect. Therefore, there is still room for improvement. Summary of the Invention

[0003] In order to further improve the refreshing effect, the present application provides a refreshing fragrance composition containing Platycladus orientalis essential oil, a preparation method thereof, and an application thereof.

[0004] In the first aspect, the present application provides a refreshing fragrance composition containing Platycladus orientalis essential oil, adopting the following technical solution: A refreshing fragrance composition containing Platycladus orientalis essential oil is compounded from Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil.

[0005] By adopting the above technical solution, by compounding Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil, the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil can cooperate with each other to achieve a significant refreshing effect, enabling people to quickly regain their spirits. Moreover, under the interaction of Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil, the fragrance composition can have a relatively long fragrance retention time, so that the daily chemical products prepared can continuously emit fragrance during use, and thus the refreshing effect is relatively persistent.

[0006] Preferably, the mass ratio of the Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil is 38-42:2-4:14-16:14-16:24-26:2-4.

[0007] By adopting the above technical solution, by specifically selecting the mass ratios of Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil, the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil can be better combined in a specific ratio, and the synergistic effect is more significant.

[0008] In a second aspect, the present application provides a method for preparing a refreshing fragrance composition containing Platycladus orientalis essential oil, adopting the following technical solution: A method for preparing a refreshing fragrance composition containing Platycladus orientalis essential oil as described above, comprising the following steps: Step 1), mixing Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil evenly to obtain a mixture; Step 2), allowing the mixture to stand for 7 - 9 days to obtain a refreshing fragrance composition containing Platycladus orientalis essential oil.

[0009] By adopting the above technical solution, by allowing the mixture to stand for 7 - 9 days after mixing, the effect of the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil cooperating with each other is better, and the refreshing effect is better.

[0010] Preferably, in step 2), the mixture is kept at a constant temperature of 40 - 45 °C and allowed to stand for 7 - 9 days.

[0011] By adopting the above technical solution, by allowing the mixture to stand at a constant temperature of 40 - 45 °C, the effect of the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil cooperating with each other is further improved, and the refreshing effect is better.

[0012] Preferably, in step 2), in a nitrogen atmosphere, the mixture is kept at a constant temperature of 40 - 45 °C and allowed to stand for 7 - 9 days.

[0013] By adopting the above technical solution, by allowing the mixture to stand in a nitrogen atmosphere, oxidation by oxygen is reduced, and the product quality is more stable.

[0014] Preferably, in step 2), in a nitrogen atmosphere, under a constant pressure of 2 - 3 MPa, the mixture is kept at a constant temperature of 40 - 45 °C and allowed to stand for 7 - 9 days.

[0015] By adopting the above technical solution, by allowing the mixture to stand under high pressure, the effect of the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil cooperating with each other can be further improved, and the refreshing effect of the fragrance composition takes effect faster and is more significant.

[0016] In a third aspect, the present application provides an application of a refreshing fragrance composition containing Platycladus orientalis essential oil, adopting the following technical solution: Application of a preparation method of the above-mentioned refreshing essence composition containing Platycladus orientalis essential oil, wherein the refreshing essence composition containing Platycladus orientalis essential oil is added to a daily chemical product for preparing a daily chemical product with a refreshing effect.

[0017] By adopting the above technical solution, by adding the refreshing essence composition containing Platycladus orientalis essential oil to a daily chemical product, the daily chemical product can have a better refreshing effect.

[0018] Preferably, the daily chemical product is one of a reed diffuser, a fragrance, a perfume, an air freshener, and a body wash.

[0019] By adopting the above technical solution, by selecting the daily chemical product as one of a reed diffuser, a fragrance, a perfume, an air freshener, and a body wash, the effect of the essence composition can be better exerted, and the refreshing effect is more remarkable.

[0020] In summary, the present application has the following beneficial effects: 1. Since the present application uses Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil for compounding, the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil can cooperate with each other to achieve a remarkable refreshing effect, enabling people to quickly regain their spirits. Moreover, under the interaction of Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil, the fragrance retention time of the essence composition can be longer, so that the prepared daily chemical product can continuously emit fragrance during use, and the refreshing effect is more lasting.

[0021] 2. In the present application, preferably, by specifically selecting the mass ratio of Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil, the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil can better cooperate in a specific ratio, and the synergistic effect exerted is more remarkable.

[0022] 3. By the method of the present application, after mixing and standing for 7 - 9 days, the effect of the volatile components in Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil cooperating with each other is better, and the refreshing effect is better. Detailed Embodiments

[0023] The following further elaborates on the present application in conjunction with embodiments.

[0024] Embodiment 1 A refreshing essence composition containing Platycladus orientalis essential oil is compounded from Platycladus orientalis essential oil, Mentha piperita oil, clove oil, Pinus massoniana Lamb. oil, lime oil, and Zanthoxylum bungeanum oil.

[0025] The Platycladus orientalis essential oil is purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0026] The peppermint oil was purchased from Jishui Hongxing Natural Medicinal Spice Oil Factory.

[0027] The clove oil was purchased from Wuhan Huajiu Pharmaceutical Technology Co., Ltd.

[0028] The pine needle oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0029] The lime oil was purchased from Wuhan Lana White Medicinal and Chemical Industry Co., Ltd.

[0030] The prickly ash oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0031] The preparation method of the refreshing essence composition containing Platycladus orientalis essential oil comprises the following steps: Step 1), put 38 kg of Platycladus orientalis essential oil, 2 kg of peppermint oil, 14 kg of clove oil, 14 kg of pine needle oil, 24 kg of lime oil, and 2 kg of prickly ash oil into the reaction kettle, with a rotation speed of 200 r / min, stir for 30 min, mix evenly to obtain a mixture.

[0032] Step 2), inject nitrogen into the reaction kettle to discharge air. After the air is discharged, seal the reaction kettle, continue to inject nitrogen until the pressure in the reaction kettle increases to 2 MPa, keep the pressure constant at 2 MPa, raise the temperature, keep the temperature constant at 40 °C, and let the mixture stand for 7 days to obtain the refreshing essence composition containing Platycladus orientalis essential oil.

[0033] Example 2 A refreshing essence composition containing Platycladus orientalis essential oil is compounded from Platycladus orientalis essential oil, peppermint oil, clove oil, pine needle oil, lime oil, and prickly ash oil.

[0034] The Platycladus orientalis essential oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0035] The peppermint oil was purchased from Jishui Hongxing Natural Medicinal Spice Oil Factory.

[0036] The clove oil was purchased from Wuhan Huajiu Pharmaceutical Technology Co., Ltd.

[0037] The pine needle oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0038] The lime oil was purchased from Wuhan Lana White Medicinal and Chemical Industry Co., Ltd.

[0039] The prickly ash oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0040] The preparation method of the refreshing essence composition containing Platycladus orientalis essential oil comprises the following steps: Step 1): Put 40 kg of Platycladus orientalis essential oil, 3 kg of Mentha piperita oil, 15 kg of clove oil, 15 kg of pine needle oil, 25 kg of lime oil, and 3 kg of Zanthoxylum bungeanum oil into a reaction kettle, with a rotation speed of 200 r / min, stir for 30 min, and mix evenly to obtain a mixture.

[0041] Step 2): Inject nitrogen into the reaction kettle to expel air. After the air is expelled, seal the reaction kettle, continue to inject nitrogen until the pressure in the reaction kettle increases to 2.5 MPa, keep the pressure constant at 2.5 MPa, raise the temperature, keep the temperature constant at 42.5 °C, and let the mixture stand for 8 days to obtain a refreshing essence composition containing Platycladus orientalis essential oil.

[0042] Example 3 A refreshing essence composition containing Platycladus orientalis essential oil is compounded from Platycladus orientalis essential oil, Mentha piperita oil, clove oil, pine needle oil, lime oil, and Zanthoxylum bungeanum oil.

[0043] The Platycladus orientalis essential oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0044] The Mentha piperita oil was purchased from Jishui Hongxing Natural Medicinal Spice Oil Factory.

[0045] The clove oil was purchased from Wuhan Huajiu Pharmaceutical Technology Co., Ltd.

[0046] The pine needle oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0047] The lime oil was purchased from Wuhan Lanaibai Pharmaceutical and Chemical Co., Ltd.

[0048] The Zanthoxylum bungeanum oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0049] The preparation method of the refreshing essence composition containing Platycladus orientalis essential oil includes the following steps: Step 1): Put 42 kg of Platycladus orientalis essential oil, 4 kg of Mentha piperita oil, 16 kg of clove oil, 16 kg of pine needle oil, 26 kg of lime oil, and 4 kg of Zanthoxylum bungeanum oil into a reaction kettle, with a rotation speed of 200 r / min, stir for 30 min, and mix evenly to obtain a mixture.

[0050] Step 2): Inject nitrogen into the reaction kettle to expel air. After the air is expelled, seal the reaction kettle, continue to inject nitrogen until the pressure in the reaction kettle increases to 3 MPa, keep the pressure constant at 3 MPa, raise the temperature, keep the temperature constant at 45 °C, and let the mixture stand for 9 days to obtain a refreshing essence composition containing Platycladus orientalis essential oil.

[0051] Comparative Example 1 A refreshing essence composition containing Platycladus orientalis essential oil, compared with Example 2, the difference is only that: Rosemary essential oil is used to replace Platycladus orientalis essential oil in equal amount.

[0052] The rosemary essential oil was purchased from Hebei Qiansheng Biotechnology Co., Ltd.

[0053] Comparative Example 2 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Basil essential oil was used to replace peppermint oil in equal amounts.

[0054] The basil essential oil was purchased from Jishui Jianmin Natural Spice Oil Factory.

[0055] Comparative Example 3 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Thyme essential oil was used to replace clove oil in equal amounts.

[0056] The thyme essential oil was purchased from Jiangsu Bost Chemical Technology Co., Ltd.

[0057] Comparative Example 4 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Nigella sativa seed oil was used to replace pine needle oil in equal amounts.

[0058] The Nigella sativa seed oil was purchased from Jiangxi Chuanhui Herb Biotechnology Co., Ltd.

[0059] Comparative Example 5 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Ylang-ylang essential oil was used to replace lime oil in equal amounts.

[0060] The ylang-ylang essential oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0061] Comparative Example 6 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Coriander seed essential oil was used to replace prickly ash oil in equal amounts.

[0062] The coriander seed essential oil was purchased from Jishui Hongxing Natural Medicinal Spice Oil Factory.

[0063] Comparative Example 7 A refreshing fragrance composition containing thuja essential oil, compared with Example 2, the difference is only that: Rosemary essential oil was used to replace thuja essential oil, basil essential oil was used to replace peppermint oil in equal amounts, thyme essential oil was used to replace clove oil in equal amounts, Nigella sativa seed oil was used to replace pine needle oil in equal amounts, ylang-ylang essential oil was used to replace lime oil in equal amounts, and coriander seed essential oil was used to replace prickly ash oil in equal amounts.

[0064] The rosemary essential oil was purchased from Hebei Qiansheng Biotechnology Co., Ltd.

[0065] The basil essential oil was purchased from Jianmin Natural Spice Oil Factory in Jishui County.

[0066] The thyme essential oil was purchased from Jiangsu Bost Chemical Technology Co., Ltd.

[0067] The black cumin seed oil was purchased from Jiangxi Chuanhui Herbal Biotechnology Co., Ltd.

[0068] The ylang-ylang essential oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0069] The coriander seed essential oil was purchased from Hongxing Natural Medicinal Spice Oil Factory in Jishui County.

[0070] Experiment 1 Preparation of test samples: Mix 10 g of the refreshing fragrance composition containing thuja essential oil and 90 g of olive oil evenly to prepare the test aromatherapy sample.

[0071] Recruit a number of volunteers, with 20 people in each group.

[0072] Test method: Before and during the continuous sniffing of the test aromatherapy sample, electroencephalograms are measured. The proportion data of β waves in the electroencephalogram channels of F3 (left frontal lobe) and F4 (right frontal lobe) are taken for statistical analysis.

[0073] Test equipment: Digital electroencephalogram topographic map instrument, XL-998C, 16 channels, Jiangsu Mutai Medical Technology Co., Ltd.

[0074] Environmental conditions: Temperature 20 - 25 °C, humidity 50 - 60% RH.

[0075] Test procedure: Registration of subject information, completion of understanding and signing of the informed consent form, enrollment after meeting the inclusion and exclusion criteria: Rest in the environment at 20 - 25 °C for 15 min; Wear the electroencephalogram monitoring equipment, monitor for 5 minutes, continuously sniff the test substance with an aromatherapy clip for 10 minutes, and monitor for 10 minutes simultaneously.

[0076] Data statistics: Take the proportion data of β waves in the electroencephalogram channels of F3 (left frontal lobe) and F4 (right frontal lobe) for descriptive statistics; Take the proportion data of β waves in the electroencephalogram channels of F3 (left frontal lobe) and F4 (right frontal lobe) for normal distribution test. If it is a normal distribution, paired T-test is used for statistical analysis; if the test data is non-normal distribution, the rank sum test method is used for statistical analysis. The above statistical analyses are all two-tailed tests, with a significance level of α = 0.05.

[0077] Result judgment: P < 0.05, there is a significant difference; P < 0.01, there is a highly significant difference; P > 0.05, there is no significant difference.

[0078] △If the proportion of β waves is >0, there is a refreshing effect; if the proportion of β waves is ≤0, there is no refreshing effect.

[0079] Experiment 2 Preparation of test samples: 10 g of a refreshing fragrance composition containing Platycladus orientalis essential oil and 90 g of olive oil were evenly mixed to prepare an aromatherapy sample to be tested.

[0080] Take 1 ml of the aromatherapy sample to be tested and drop it on the filter paper to make the paper sample to be tested.

[0081] The test paper sample is placed in a ventilated place and 10 perfumers smell it every 30 minutes. When all 10 perfumers judge that the test paper sample has no fragrance, the elapsed time is recorded as the fragrance retention time.

[0082] The specific experimental data of Experiment 1-2 are shown in Table 1.

[0083] Table 1 According to the data comparison of each embodiment and the comparative example in Table 1, the proportion of △β waves in each embodiment is significantly higher than that in each comparative example, which proves that the aromatherapy samples prepared in each embodiment can achieve a faster refreshing effect. Although the proportion of △β waves in each comparative example is also ≥0, which proves that each comparative example can also achieve a certain improvement effect, the special compounding system of cypress essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil and prickly ash oil in the embodiment is destroyed, resulting in a significant reduction in the synergistic effect of each plant essential oil, resulting in a significantly weaker refreshing effect than that in the embodiment.

[0084] In addition, the fragrance retention time of each embodiment is significantly longer than that of each comparative example, which proves that the compounding of arborvitae essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil and prickly ash oil can not only significantly improve the refreshing effect, but also prolong the fragrance retention time, so that the daily chemical products made of the fragrance composition can have a long-lasting refreshing effect and well meet the needs of consumers.

[0085] This specific embodiment is merely an explanation of the present application and is not a limitation of the present application. After reading this specification, those skilled in the art may make modifications to the present embodiment without any creative contribution as needed, but such modifications are protected by the patent law as long as they are within the scope of the claims of the present application.

Claims

1. A refreshing flavor composition containing Platycladus orientalis essential oil, characterized in that: It is compounded from arborvitae essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil and Zanthoxylum bungeanum oil.

2. A refreshing flavor composition containing arborvitae essential oil according to claim 1, characterized in that: The mass ratio of the arborvitae essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil and prickly ash oil is 38-42:2-4:14-16:14-16:24-26:2-4.

3. A method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 1 or 2, characterized in that: The following steps are involved: Step 1), evenly mix arborvitae essential oil, peppermint oil, clove oil, pine needle oil, white lemon oil, and prickly ash oil to obtain a mixture; Step 2), the mixture is left to stand for 7-9 days to obtain a refreshing flavor composition containing Platycladus orientalis essential oil.

4. The method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 3, characterized in that: In the step 2), the mixture is kept at a constant temperature of 40-45° C. and allowed to stand for 7-9 days.

5. The method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 4, characterized in that: In the step 2), the mixture is kept at a constant temperature of 40-45° C. under a nitrogen atmosphere and allowed to stand for 7-9 days.

6. The method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 5, characterized in that: In the step 2), the mixture is kept at a constant temperature of 40-45° C. under a nitrogen atmosphere at a constant pressure of 2-3 MPa and allowed to stand for 7-9 days.

7. An application of the method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 1 or 2, characterized in that: The refreshing fragrance composition containing arborvitae essential oil is added into daily chemical products for preparing daily chemical products with refreshing effects.

8. The application of the method for preparing a refreshing flavor composition containing arborvitae essential oil according to claim 7, characterized in that: The daily chemical product is one of fireless aromatherapy, fragrance, perfume, air freshener and shower gel.

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