Relieving essential oil composition containing honeysuckle flower oil as well as preparation method and application of soothing essential oil composition

Abstract

The invention relates to the technical field of daily chemical raw materials, and particularly discloses a soothing essential oil composition containing honeysuckle flower oil as well as a preparation method and application thereof. The soothing essential oil composition containing the honeysuckle flower oil is prepared by compounding the honeysuckle flower oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacol, bergamot oil, green orange oil and spikenard oil. The traditional Chinese medicine composition has the advantage that the effect of relieving the emotion is quicker.

Description

Technical Field

[0001] The present invention relates to the field of daily chemical raw materials, and particularly to a soothing essential oil composition containing honeysuckle oil, a preparation method thereof, and an application thereof. Background Art

[0002] Soothing essential oils are products used to soothe negative emotions such as anxiety and irritability. They emit aromas through volatile substances, and after being absorbed by the human body, they can regulate the human mood, thereby achieving the effect of soothing negative emotions such as anxiety and irritability.

[0003] Existing soothing products mainly use chemically synthesized substances. Although such raw materials have significant soothing effects, chemically synthesized substances pose certain potential safety hazards to human health. Therefore, more and more natural plant ingredients are being applied to soothing products. However, although natural plant ingredients are almost harmless to the human body, the soothing effects of existing soothing products containing natural plant ingredients are relatively average, and it is difficult to quickly relieve anxiety and irritability, making it difficult to meet the needs of consumers. Therefore, there is still room for improvement. Summary of the Invention

[0004] In order to make the soothing effect take effect faster, the present application provides a soothing essential oil composition containing honeysuckle oil, a preparation method thereof, and an application thereof.

[0005] In a first aspect, the present application provides a soothing essential oil composition containing honeysuckle oil, adopting the following technical solution: A soothing essential oil composition containing honeysuckle oil is compounded from honeysuckle oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and nardostachys jatamansi oil.

[0006] By adopting the above technical solution, by compounding honeysuckle oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and nardostachys jatamansi oil, the volatile components cooperate with each other to produce a synergistic effect, which can achieve the effect of quickly soothing the mood. Moreover, with the mutual cooperation of honeysuckle oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and nardostachys jatamansi oil, the fragrance retention time of the essential oil composition can be longer, and the efficacy can be exerted more persistently, having a higher economic value.

[0007] Preferably, the mass ratio of the honeysuckle oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and nardostachys jatamansi oil is 38 - 42:2 - 4:2 - 4:14 - 16:7 - 9:33 - 37:2 - 4:2 - 4.

[0008] By adopting the above technical solution, by specifically selecting the mass ratios of honeysuckle oil, schisandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, calamondin oil, and nardostachys jatamansi oil, the volatile components can be better combined in a specific ratio, so that the effect of relieving emotions is more significant and the effect takes effect faster.

[0009] In a second aspect, the present application provides a method for preparing a soothing essential oil composition containing honeysuckle oil, adopting the following technical solution: A method for preparing a soothing essential oil composition containing honeysuckle oil as described above, comprising the following steps: Step 1), mix honeysuckle oil, schisandra chinensis oil, and michelia alba flower oil evenly to obtain a premix; Step 2), add cypress oil, guaiacwood oil, and bergamot oil to the premix and mix evenly to obtain a mixture; Step 3), add calamondin oil and nardostachys jatamansi oil to the mixture and mix evenly to obtain a soothing essential oil composition containing honeysuckle oil.

[0010] By adopting the above technical solution, through step-by-step mixing, the volatile components in each raw material can better play a synergistic role, so as to form volatile substances that can quickly relieve emotions, and further achieve a significant effect of relieving emotions.

[0011] Preferably, in the said step 1), honeysuckle oil, schisandra chinensis oil, and michelia alba flower oil are stirred at 50 - 60 °C for 30 - 40 min.

[0012] By adopting the above technical solution, by specifically selecting to stir and mix at 50 - 60 °C, the effect of the cooperation of each component is better, and it can play a better role in relieving emotions.

[0013] Preferably, in the said step 2), the premix is cooled to 40 - 45 °C, cypress oil, guaiacwood oil, and bergamot oil are added, and it is kept at a constant temperature of 40 - 45 °C and stirred for 30 - 40 min.

[0014] By adopting the above technical solution, by specifically selecting to stir and mix at 40 - 45 °C after adding cypress oil, guaiacwood oil, and bergamot oil, the effect of the cooperation of each component is better, and at the same time, the oxidation of components caused by high temperature is reduced, making the quality of the composition more stable.

[0015] Preferably, in the said step 3), the mixture is cooled to 30 - 35 °C, calamondin oil and nardostachys jatamansi oil are added, sealed, increased to 3 - 4 MPα, and stirred for 50 - 60 min.

[0016] By adopting the above technical solution, through specifically selecting to add green mandarin oil and spikenard oil and then performing high-pressure stirring and mixing, the effect of the mutual cooperation of each component can be further improved, and each component is made relatively stable and not easily oxidized, and the product quality is better.

[0017] In a third aspect, the present application provides an application of a soothing essential oil composition containing honeysuckle oil, adopting the following technical solution: An application of the above-mentioned soothing essential oil composition containing honeysuckle oil, wherein the soothing essential oil composition containing honeysuckle oil is added to daily chemical products for preparing daily chemical products containing the soothing essential oil composition of honeysuckle oil.

[0018] By adopting the above technical solution, after adding the soothing essential oil composition containing honeysuckle oil to daily chemical products, the daily chemical products can also have a good effect of soothing emotions, so that the application scenario of the soothing essential oil composition containing honeysuckle oil is relatively wide and has a high economic value.

[0019] Preferably, the daily chemical product is one of a reed diffuser, a fragrance, a body wash, and a shampoo.

[0020] By adopting the above technical solution, after adding the soothing essential oil composition containing honeysuckle oil to one of a reed diffuser, a fragrance, a body wash, and a shampoo, the soothing effect of the soothing essential oil composition containing honeysuckle oil can be better exerted, and the formula compatibility of the soothing essential oil composition containing honeysuckle oil with the reed diffuser, the fragrance, the body wash, and the shampoo is relatively high, and the processing cost is relatively low, and it has a high economic value.

[0021] In summary, the present application has the following beneficial effects: 1. Since the present application performs compounding with honeysuckle oil, schizandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and spikenard oil, the volatile components cooperate with each other to produce a synergistic effect, which can achieve the effect of quickly soothing emotions. Moreover, under the mutual cooperation of honeysuckle oil, schizandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and spikenard oil, the fragrance retention time of the essential oil composition can be longer, and the effect can be exerted more persistently, having a high economic value.

[0022] 2. In the present application, preferably, by specifically selecting the mass ratio of honeysuckle oil, schizandra chinensis oil, michelia alba flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and spikenard oil, the volatile components can be better combined in a specific ratio, so that the effect of soothing emotions is more significant and the effect is faster.

[0023] 3. The method of the present application enables the volatile components in each raw material to better exert their synergistic effects through step-by-step mixing, thereby forming volatile substances that can quickly soothe emotions, and further achieving a significant effect of soothing emotions. Detailed Embodiments

[0024] The present application will be further described in detail below in conjunction with embodiments.

[0025] Embodiment 1 A soothing essential oil composition containing honeysuckle oil is compounded from honeysuckle oil, schizandra oil, magnolia denudata oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and nardostachys jatamansi oil.

[0026] The honeysuckle oil is purchased from Jiangxi Jingwang Natural Spice Co., Ltd.

[0027] The schizandra oil is purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0028] The magnolia denudata oil is purchased from Ji'an Borui Spice Oil Co., Ltd.

[0029] The cypress oil is purchased from Hubei Xinghengye Technology Co., Ltd.

[0030] The guaiacwood oil is purchased from Zhongshan Dixin Chemical Co., Ltd.

[0031] The bergamot oil is purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0032] The green mandarin oil is purchased from Jingzhou Yinjie Chemical Co., Ltd.

[0033] The nardostachys jatamansi oil is purchased from Wuhan Lvjingfenghua Biotechnology Co., Ltd.

[0034] The preparation method of the soothing essential oil composition containing honeysuckle oil includes the following steps: Step 1), put 38 kg of honeysuckle oil, 2 kg of schizandra oil, and 2 kg of magnolia denudata oil into a stirring kettle, keep the temperature at 50 °C, stir for 30 min, and mix evenly to obtain a premix.

[0035] Step 2), cool the premix to 40 °C, then add 14 kg of cypress oil, 7 kg of guaiacwood oil, and 33 kg of bergamot oil to the premix, keep the temperature at 40 °C, stir for 30 min, and mix evenly to obtain a mixture.

[0036] Step 3), cool the mixture to 30 °C, add 2 kg of green mandarin oil and 2 kg of nardostachys jatamansi oil to the mixture, seal it, increase the pressure to 3 MPa, stir for 50 min, and mix evenly to obtain the soothing essential oil composition containing honeysuckle oil.

[0037] Embodiment 2 A soothing essential oil composition containing honeysuckle oil is compounded from honeysuckle oil, schizandra oil, white magnolia flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and spikenard oil.

[0038] The honeysuckle oil was purchased from Jiangxi Jingwang Natural Flavors Co., Ltd.

[0039] The schizandra oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0040] The white magnolia flower oil was purchased from Ji'an Borui Flavor Oil Co., Ltd.

[0041] The cypress oil was purchased from Hubei Xinghengye Technology Co., Ltd.

[0042] The guaiacwood oil was purchased from Zhongshan Dixin Chemical Industry Co., Ltd.

[0043] The bergamot oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0044] The green mandarin oil was purchased from Jingzhou Yinjie Chemical Industry Co., Ltd.

[0045] The spikenard oil was purchased from Wuhan Lvjingfenghua Biotechnology Co., Ltd.

[0046] The preparation method of the soothing essential oil composition containing honeysuckle oil includes the following steps: Step 1), Put 40 kg of honeysuckle oil, 3 kg of schizandra oil, and 3 kg of white magnolia flower oil into a stirring kettle, keep the temperature at 55 °C, stir for 35 min, and mix evenly to obtain a premix.

[0047] Step 2), Cool the premix to 42.5 °C, then add 15 kg of cypress oil, 8 kg of guaiacwood oil, and 35 kg of bergamot oil to the premix, keep the temperature at 42.5 °C, stir for 35 min, and mix evenly to obtain a mixture.

[0048] Step 3), Cool the mixture to 32.5 °C, add 3 kg of green mandarin oil and 3 kg of spikenard oil to the mixture, seal it, increase the pressure to 3.5 MPα, stir for 55 min, and mix evenly to obtain the soothing essential oil composition containing honeysuckle oil.

[0049] Example 3 A soothing essential oil composition containing honeysuckle oil is compounded from honeysuckle oil, schizandra oil, white magnolia flower oil, cypress oil, guaiacwood oil, bergamot oil, green mandarin oil, and spikenard oil.

[0050] The honeysuckle oil was purchased from Jiangxi Jingwang Natural Flavors Co., Ltd.

[0051] The schizandra oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Bioproducts Factory.

[0052] Magnolia flower oil was purchased from Ji'an Borui Spice Oil Co., Ltd.

[0053] Cypress oil was purchased from Hubei Xinghengye Technology Co., Ltd.

[0054] Guaiacwood oil was purchased from Zhongshan Dixin Chemical Co., Ltd.

[0055] Bergamot oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0056] Tangerine oil was purchased from Jingzhou Yinjie Chemical Co., Ltd.

[0057] Spikenard oil was purchased from Wuhan Lvjing Fenghua Biotechnology Co., Ltd.

[0058] The preparation method of the soothing essential oil composition containing honeysuckle oil comprises the following steps: Step 1), put 42 kg of honeysuckle oil, 4 kg of schisandra oil, and 4 kg of magnolia flower oil into a stirring kettle, keep the temperature at 60 °C, stir for 40 min, and mix evenly to obtain a premix.

[0059] Step 2), cool the premix to 45 °C, then add 16 kg of cypress oil, 9 kg of guaiacwood oil, and 37 kg of bergamot oil to the premix, keep the temperature at 45 °C, stir for 40 min, and mix evenly to obtain a mixture.

[0060] Step 3), cool the mixture to 35 °C, add 4 kg of tangerine oil and 4 kg of spikenard oil to the mixture, seal it, increase the pressure to 4 MPa, stir for 60 min, and mix evenly to obtain the soothing essential oil composition containing honeysuckle oil.

[0061] Comparative Example 1 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Lavender oil is used to replace honeysuckle oil in equal amount.

[0062] Lavender oil was purchased from Jinan Yunuo Chemical Co., Ltd.

[0063] Comparative Example 2 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Neroli oil is used to replace schisandra oil in equal amount.

[0064] Neroli oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0065] Comparative Example 3 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Ylang-ylang oil is used to replace magnolia flower oil in equal amount.

[0066] Ylang ylang oil was purchased from Xi'an Shilin Biotechnology Co., Ltd.

[0067] Comparative Example 4 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Cedarwood oil is used to replace cypress oil in equal amount.

[0068] Cedarwood oil was purchased from Hubei Xingheng Industry Technology Co., Ltd.

[0069] Comparative Example 5 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Frankincense oil is used to replace guaiacwood oil in equal amount.

[0070] Frankincense oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Biological Products Factory.

[0071] Comparative Example 6 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Melissa oil is used to replace bergamot oil in equal amount.

[0072] Melissa oil was purchased from Jiangxi Chuanhui Herb Biotechnology Co., Ltd.

[0073] Comparative Example 7 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Jasmine oil is used to replace tangerine oil in equal amount.

[0074] Jasmine oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Biological Products Factory.

[0075] Comparative Example 8 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Sandalwood oil is used to replace spikenard oil in equal amount.

[0076] Sandalwood oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0077] Comparative Example 9 A soothing essential oil composition containing honeysuckle oil, compared with Example 2, the difference is only that: Lavender oil is used to replace honeysuckle oil, neroli oil is used to replace schisandra oil, ylang ylang oil is used to replace michelia alba flower oil, cedarwood oil is used to replace cypress oil, frankincense oil is used to replace guaiacwood oil, melissa oil is used to replace bergamot oil, jasmine oil is used to replace tangerine oil, sandalwood oil is used to replace spikenard oil.

[0078] Lavender oil was purchased from Jinan Yunuo Chemical Co., Ltd.

[0079] The neroli oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0080] The ylang-ylang oil was purchased from Xi'an Shilin Biotechnology Co., Ltd.

[0081] The cedarwood oil was purchased from Hubei Xingheng Industry Technology Co., Ltd.

[0082] The frankincense oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Biological Products Factory.

[0083] The lemon balm oil was purchased from Jiangxi Chuanhui Herb Biotechnology Co., Ltd.

[0084] The jasmine oil was purchased from Ji'an Huatianbao Chinese Herbal Medicine Biological Products Factory.

[0085] The sandalwood oil was purchased from Jiangxi Xuesong Natural Medicinal Oil Co., Ltd.

[0086] Experiment 1 Preparation of test samples: 10 g of the soothing essential oil composition containing honeysuckle oil was mixed evenly with 90 g of olive oil to prepare the aromatherapy test sample.

[0087] A number of volunteers were recruited and divided into groups of 20.

[0088] Test method: When the test aromatherapy sample was inhaled before and during continuous olfactory inhalation, electroencephalograms were measured, and the percentage of alpha waves in the electroencephalogram channels of O1 (left occipital lobe) and O2 (right occipital lobe) were taken for statistical analysis.

[0089] Test equipment: Digital electroencephalogram topographic instrument, XL-998C, 16 channels, Jiangsu Mutai Medical Technology Co., Ltd.

[0090] Environmental conditions: Temperature 20 - 25 °C, humidity 50 - 60% RH.

[0091] Test procedure: Registration of subject information, completion of understanding and signing of the informed consent form, enrollment after meeting the inclusion and exclusion criteria; resting in an environment of 20 - 25 °C for 15 min; wearing the electroencephalogram monitoring equipment, monitoring for 5 minutes, continuously inhaling the test aromatherapy sample by aromatherapy button for 10 minutes while monitoring for 10 minutes.

[0092] Data statistics: Descriptive statistics were taken for the percentage of alpha waves in the electroencephalogram channels of O1 (left occipital lobe) and O2 (right occipital lobe); The data of the proportion of alpha waves in the EEG channels of O1 (left occipital lobe) and O2 (right occipital lobe) were tested for normal distribution. If the data were normally distributed, the paired T test was used for statistical analysis; if the test data were non-normally distributed, the rank sum test method was used for statistical analysis. The above statistical analyses were all two-tailed tests, with a significance level of α = 0.05.

[0093] Result judgment: P<0.05, there is a significant difference; P<0.01, there is a very significant difference; P>0.05, there is no significant difference If the proportion of △α waves is >0, there is a soothing effect; if the proportion of △α waves is ≤0, there is no soothing effect.

[0094] Experiment 2 Preparation of test samples: 10 g of the soothing essential oil composition containing honeysuckle oil and 90 g of olive oil were evenly mixed to prepare an aromatherapy sample to be tested.

[0095] Take 1 ml of the aromatherapy sample to be tested and drop it on the filter paper to make the paper sample to be tested.

[0096] The test paper sample is placed in a ventilated place and 10 perfumers smell it every 30 minutes. When all 10 perfumers judge that the test paper sample has no fragrance, the elapsed time is recorded as the fragrance retention time.

[0097] The specific experimental data of Experiment 1-2 are shown in Table 1.

[0098] Table 1 According to the data comparison of each embodiment and the comparative example in Table 1, after inhaling the aromatherapy sample for 10 minutes, the proportion of △α waves in each embodiment is significantly higher than that in each comparative example. Although the change rate of the proportion of △α waves in each comparative example is ≥0, it proves that each comparative example also has a certain effect of soothing emotions, but the effect of soothing emotions in each embodiment is significantly better than that in each comparative example, which proves that only when honeysuckle oil, schisandra oil, white magnolia oil, cypress oil, guaiac wood oil, bergamot oil, green tangerine oil and spikenard oil are used in combination, can a more significant effect of quickly soothing emotions be achieved.

[0099] In addition, the fragrance retention time of each embodiment is significantly longer than that of each comparative example. It can be seen that each embodiment can not only quickly relieve emotions, but also through the compounding of honeysuckle oil, schisandra oil, magnolia oil, cypress oil, guaiac oil, bergamot oil, green tangerine oil, and spikenard oil, the volatile components inhibit each other, thereby significantly extending the fragrance retention time, making the aromatherapy prepared by the composition of each embodiment more durable.

[0100] This specific embodiment is only an interpretation of the present application and does not limit the present application. After reading this specification, those skilled in the art can make modifications to this embodiment without creative contributions as needed, but as long as it is within the scope of the claims of the present application, it is protected by the patent law.

Claims

1. A soothing essential oil composition containing honeysuckle oil, characterized in that: It is made from honeysuckle oil, schisandra oil, white magnolia oil, cypress oil, guaiac wood oil, bergamot oil, green tangerine oil and spikenard oil.

2. A soothing essential oil composition containing honeysuckle oil according to claim 1, characterized in that: The mass ratio of the honeysuckle oil, schisandra oil, white magnolia oil, cypress oil, guaiac oil, bergamot oil, green mandarin oil and spikenard oil is 38-42: 2-4: 2-4: 14-16: 7-9: 33-37: 2-4: 2-4.

3. A method for preparing a soothing essential oil composition containing honeysuckle oil according to claim 1 or 2, characterized in that: The following steps are involved: Step 1), mixing honeysuckle oil, schisandra oil and magnolia oil evenly to obtain a premix; Step 2), adding cypress oil, guaiac wood oil and bergamot oil to the premix, and mixing evenly to obtain a mixture; Step 3), add green tangerine oil and spikenard oil to the mixture, mix evenly, and obtain a soothing essential oil composition containing honeysuckle oil.

4. The method for preparing a soothing essential oil composition containing honeysuckle oil according to claim 3, characterized in that: In the step 1), the honeysuckle oil, schisandra oil and magnolia oil are stirred at 50-60° C. for 30-40 minutes.

5. The method for preparing a soothing essential oil composition containing honeysuckle oil according to claim 4, characterized in that: In the step 2), the premix is ​​cooled to 40-45° C., cypress oil, guaiac wood oil and bergamot oil are added, the temperature is kept at 40-45° C., and stirred for 30-40 minutes.

6. The method for preparing a soothing essential oil composition containing honeysuckle oil according to claim 5, characterized in that: In the step 3), the mixture is cooled to 30-35° C., green tangerine oil and spikenard oil are added, the mixture is sealed, the temperature is increased to 3-4 MPa, and stirred for 50-60 minutes.

7. The use of a soothing essential oil composition containing honeysuckle oil according to claim 1 or 2, characterized in that: The soothing essential oil composition containing honeysuckle oil is added into daily chemical products to prepare the daily chemical products containing the soothing essential oil composition containing honeysuckle oil.

8. The use of a soothing essential oil composition containing honeysuckle oil according to claim 7, characterized in that: The daily chemical product is one of fire-free aromatherapy, fragrance, shower gel and shampoo.

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