Deer-horn glue ancient nine-grid polymer and preparation method thereof

Abstract

The invention relates to the field of skin care product preparation, and discloses a deer-horn glue ancient method nine-grid polymer and a preparation method thereof.The deer-horn glue ancient method nine-grid polymer is prepared from, by weight, 30-40 parts of water, 15-25 parts of deer-horn glue, 5-10 parts of ligusticum wallichii, 5-10 parts of radix asparagi, 5-10 parts of radix ophiopogonis, 3-7 parts of bamboo shavings, 3-7 parts of radix angelicae, 3-7 parts of astragalus membranaceus, 3-7 parts of rhizoma atractylodis macrocephalae and 3-7 parts of almonds. The deer-horn glue is rich in collagen, amino acid and mineral substances, so that the lost collagen of the skin can be directly supplemented, and the skin elasticity is enhanced; various traditional Chinese medicinal materials such as radix asparagi, radix ophiopogonis and almonds provide comprehensive nutrient substances for the skin through the effects of nourishing yin, moistening dryness, nourishing and preserving moisture and the like, and the components have a synergistic effect, go deep into the bottom layer of the skin and improve the problems of dry and rough skin and the like, so that the skin becomes soft, fine and glossy, deep nourishing of the skin is realized, and metabolism of skin cells is promoted.

Description

Technical Field

[0001] The present invention relates to the technical field of skin care product preparation, and particularly to a traditional nine-square polymer of deer horn glue and a preparation method thereof. Background Art

[0002] Skin care products, which are products used to care for the skin, play an important role in people's daily lives. Nowadays, they are no longer luxury goods but have become a powerful assistant for the public to enhance their image and confidence. With the improvement of people's living standards and the increasing attention to their own health and beauty, consumers' demands for skin care products are becoming increasingly diversified and refined.

[0003] Traditional skin care products mainly use common moisturizers such as glycerol and sodium hyaluronate as core ingredients. Glycerol maintains the humidity of the skin surface by absorbing moisture in the air, and sodium hyaluronate forms a hydration film on the skin surface with its strong water absorption ability to play a moisturizing role. They can relieve skin dryness to a certain extent, but their functions are relatively single and they cannot nourish and repair the skin. Summary of the Invention

[0004] Aiming at the deficiencies of the prior art, the present invention provides a traditional nine-square polymer of deer horn glue and a preparation method thereof, which solves the problems that traditional skin care products have relatively single functions and cannot nourish and repair the skin.

[0005] To achieve the above object, the present invention is realized through the following technical solutions: A traditional nine-square polymer of deer horn glue comprises the following raw materials in parts by weight: 30-40 parts of water, 15-25 parts of deer horn glue, 5-10 parts of chuanxiong, 5-10 parts of asparagus root, 5-10 parts of dwarf lilyturf tuber, 3-7 parts of bamboo shavings, 3-7 parts of angelica dahurica, 3-7 parts of astragalus membranaceus, 3-7 parts of atractylodes macrocephala, and 3-7 parts of almond.

[0006] By adopting the above technical solutions, since deer horn glue is rich in collagen and various nutrients, it can directly supplement the substances required by the skin and enhance skin elasticity; chuanxiong promotes blood circulation in the skin and transports nutrients to cells; asparagus root and dwarf lilyturf tuber nourish yin and moisten dryness, and cooperate with raw materials such as almond to provide sufficient moisture and nourishment for the skin; bamboo shavings, angelica dahurica, astragalus membranaceus, etc. have anti-inflammatory, antibacterial and antioxidant effects, reducing skin inflammation and oxidative damage. These raw materials cooperate with each other to achieve multi-dimensional nourishment and repair of the skin, covering multiple effects such as moisturizing, enhancing elasticity, promoting metabolism, anti-inflammatory and antioxidant, and solving the problems that traditional skin care products have relatively single functions and cannot nourish and repair the skin.

[0007] A preparation method of a traditional nine-square polymer of deer horn glue, applied to the above-mentioned traditional nine-square polymer of deer horn glue, comprises the following steps: S1. Pretreatment: After drying deer horn glue at low temperature by weight parts, it is successively subjected to coarse crushing and ultrafine crushing to obtain ultrafine powder of deer horn glue. Chuanxiong, Tianmen Dong, Maidong, Zhuru, Baizhi, Huangqi, Baizhu, and Xingren are selected, washed, vacuum dried, and ultrafinely crushed to obtain ultrafine powder of Chinese medicinal materials; S2. Water extraction: Add water by weight parts to a multi-functional extraction tank, heat and stir in ultrafine powder of deer horn glue until dissolved, add ultrafine powder of Chinese medicinal materials, and start the condensing reflux device for extraction to obtain an extract; S3. Solid-liquid separation: The extract is successively subjected to coarse filtration, centrifugal separation, and fine filtration through a filter membrane to obtain a clarified extract; S4. Concentration: The clarified extract is conveyed to a vacuum concentration tank for concentration. When its relative density reaches 1.15 - 1.2 at 60 °C, stop concentration to obtain a concentrated solution; S5. Drying and forming: When preparing a solid powder product, spray dry the concentrated solution, and then sieve and size it to obtain a solid powder polymer. When preparing a paste product, reduce the pressure of the concentrated solution to concentrate it until its relative density reaches 1.3 - 1.35 at 60 °C, and then perform homogenization treatment to obtain a paste polymer; S6. Packaging and storage: The solid powder polymer is hermetically packaged using an aluminum foil bag, and the paste polymer is packaged using a glass bottle and stored in a warehouse.

[0008] Preferably, in S1, the temperature for low-temperature drying of deer horn glue is 40 °C, the drying time is 2 hours, the conditions for vacuum drying are 60 °C and -0.08 MPa, and the drying time is 6 hours. The particle sizes of both the ultrafine powder of deer horn glue and the ultrafine powder of Chinese medicinal materials are 300 mesh.

[0009] Preferably, in S2, the water is deionized water with a conductivity not exceeding 2 μS / cm at 25 °C, the heating temperature is 90 °C, the stirring and adding rate is 150 r / min, and the extraction is carried out at 80 °C and 120 r / min for 8 hours. During this period, the content of the active ingredient is detected every 2 hours, and stop extraction when it reaches a stable value.

[0010] Preferably, in S3, a plate and frame filter press is used for coarse filtration, the centrifugal separation rate is 4000 r / min, the time is 20 minutes, and the micropore diameter of the filter membrane is 0.45 μm.

[0011] Preferably, in S4, the concentration is carried out under the conditions of -0.09 MPa and 50 °C.

[0012] Preferably, in step S5, the inlet air temperature for spray drying is 180 - 200°C, the outlet air temperature is 80 - 90°C, the atomization pressure is 0.2 - 0.3 MPa, the sieving and granulation use an 80 - mesh sieve, and the pressure for homogenization treatment is 20 - 30 MPa.

[0013] Preferably, in step S6, the temperature in the warehouse is 10 - 20°C, and the relative humidity is 40% - 60%.

[0014] The present invention provides a traditional - method nine - palace polymer of deer - horn glue and its preparation method. It has the following beneficial effects: 1. Since the deer - horn glue in the present invention is rich in collagen, amino acids, and minerals, it can directly supplement the collagen lost by the skin and enhance skin elasticity; various Chinese medicinal materials such as asparagus root, dwarf lilyturf root, and almond respectively provide comprehensive nutrients for the skin through functions such as nourishing yin and moistening dryness, nourishing and moisturizing. These components work synergistically, penetrate deep into the bottom layer of the skin, improve problems such as skin dryness and roughness, make the skin soft, delicate, and shiny, and achieve multiple effects such as deep nourishment of the skin, promotion of skin cell metabolism, enhancement of skin elasticity, regulation of skin water - oil balance, and improvement of skin antioxidant capacity, solving the problem that traditional skin - care products have relatively single functions and cannot nourish and repair the skin.

[0015] 2. By using chuanxiong as a raw material in the present invention, its active ingredient tetramethylpyrazine has the effect of promoting blood circulation and removing blood stasis, can dilate the skin blood vessels, and promote blood circulation in the skin. Good blood circulation can transport sufficient oxygen and nutrients to skin cells, and at the same time take away metabolic wastes in time, thereby improving the skin color, reducing problems such as dullness and skin spots, and making the skin show a healthy, rosy complexion.

[0016] 3. The antioxidant components in Chinese medicinal materials such as asparagus root, dwarf lilyturf root, and bamboo shavings in the present invention, such as polysaccharides and flavonoids, can scavenge free radicals in the skin, reduce the damage of oxidative stress to skin cells, astragalus membranaceus enhances skin immunity, promotes cell growth and repair, and atractylodes macrocephala regulates skin water metabolism. Multiple components jointly regulate skin metabolism, accelerate cell renewal, delay the skin aging process, reduce the generation of wrinkles, and keep the skin in a young state.

[0017] 4. Raw materials such as bamboo shavings, dahurian angelica root, and astragalus membranaceus in the present invention have anti - inflammatory and antibacterial effects, can inhibit the growth of harmful bacteria on the skin surface, reduce skin inflammatory reactions, have a good improvement effect on skin inflammation problems such as acne and acne, and at the same time, enhance skin resistance, reduce the risk of skin allergy and infection, maintain the healthy state of the skin, and create a good growth environment for the skin.

[0018] 5. By using natural ingredients such as deer antler glue and various traditional Chinese medicinal herbs, this product significantly reduces skin irritation compared to the chemically synthesized ingredients commonly used in traditional skincare products. This avoids the adverse reactions that chemically synthesized ingredients can cause, such as allergies, redness, and damage to the skin barrier, reducing the burden on the skin. It is suitable for all skin types, especially those with sensitive skin. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 This is a flow chart of the method for preparing the ancient nine-palace polymer of deer antler glue proposed in the present invention. DETAILED DESCRIPTION

[0020] The following will clearly and completely describe the technical solution of the present invention in conjunction with the accompanying drawings. Obviously, the embodiments described are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0021] The embodiment of the present invention provides an ancient nine-palace polymer of deer antler glue, comprising the following raw materials in parts by weight: 30-40 parts of water, 15-25 parts of deer antler glue, 5-10 parts of Chuanxiong, 5-10 parts of Asparagus cochinchinensis, 5-10 parts of Ophiopogon japonicus, 3-7 parts of Rhizoma Anemarrhenae, 3-7 parts of Angelica dahurica, 3-7 parts of Astragalus membranaceus, 3-7 parts of Atractylodes macrocephala, and 3-7 parts of Apricot kernel.

[0022] Specifically, water is a good solvent for various nutrients, providing a medium for the dispersion and dissolution of other ingredients. It is also crucial for maintaining the normal physiological functions of the skin, replenishing moisture, increasing its water content, and keeping it hydrated. It improves dry, dehydrated skin, making it softer and smoother, and reducing the dry lines and roughness caused by dehydration. Deer antler glue is rich in collagen, various amino acids, and minerals. Collagen is a crucial component of skin structure. With aging, collagen is gradually lost from the skin, leading to sagging and wrinkles. The collagen in the deer antler glue used in this invention directly replenishes the skin's needs and enhances its elasticity. Amino acids participate in skin cell metabolism, providing raw materials for cell growth and repair. Minerals regulate the osmotic pressure inside and outside skin cells, maintaining normal cellular function and promoting skin self-repair. Ligustrazine, the main active ingredient in Chuanxiong, has significant blood circulation and blood stasis-removing effects. Skin metabolism relies on good blood circulation. A sufficient blood supply delivers oxygen and nutrients to skin cells while removing metabolic waste. Ligustrazine can dilate skin blood vessels, improve local blood circulation, accelerate skin metabolism, enable skin cells to obtain nutrients in a timely manner and excrete toxins, thereby improving skin color and reducing dullness, pigmentation and other problems.

[0023] Asparagus contains components such as asparagus polysaccharide and asparagine. Asparagus polysaccharide has excellent moisturizing properties and can form a water-retaining film on the skin surface, reducing water evaporation and maintaining the moist state of the skin; asparagine can regulate the water balance within skin cells and enhance the water-retaining ability of the skin. In addition, the antioxidant components in asparagus can scavenge free radicals in the skin, reduce the damage of free radicals to skin cells, and delay skin aging. Ophiopogon japonicus is rich in substances such as ophiopogon saponins and ophiopogon polysaccharides. Ophiopogon saponins have anti-inflammatory and antioxidant effects, can reduce skin inflammatory reactions, and protect the skin from damage by external stimuli; ophiopogon polysaccharides can promote the proliferation and differentiation of skin cells, accelerate the renewal rate of skin cells, and keep the skin in a youthful state. At the same time, ophiopogon polysaccharides also have good moisturizing effects and cooperate with other moisturizing components to jointly maintain the water content of the skin. Bamboo shavings contain components such as bamboo shavings polysaccharide and flavonoids. Bamboo shavings polysaccharide has antibacterial and anti-inflammatory effects, can inhibit the growth of harmful bacteria on the skin surface, and reduce the occurrence of skin inflammations such as acne and acne; flavonoid components have antioxidant properties, can scavenge free radicals in the skin, and reduce the damage of oxidative stress to the skin. In addition, bamboo shavings can also regulate the sebum secretion of the skin. For oily skin, it can reduce excessive sebum secretion and keep the skin fresh.

[0024] The coumarin components contained in Angelica dahurica, such as angelicin and isoimperatorin, have whitening effects. These components can inhibit the activity of tyrosinase, reduce the synthesis of melanin, thereby fading skin spots and brightening the skin tone. At the same time, Angelica dahurica also has certain anti-inflammatory and antibacterial effects, can protect the skin from external pathogens, and promote the repair of damaged skin. The main active components of Astragalus membranaceus, such as astragaloside IV and astragalus polysaccharides, have immunomodulatory effects. As the body's first line of defense, the immune function of the skin is crucial for resisting the invasion of external pathogens. Astragalus membranaceus can enhance the immunity of the skin, improve the resistance of skin cells, and reduce the occurrence of skin problems such as allergies and infections. In addition, astragalus polysaccharides can also promote the growth and repair of skin cells, accelerate wound healing, and keep the skin in a healthy state. Atractylodes macrocephala contains volatile oils, atractylodes macrocephala polysaccharides and other components. Atractylodes macrocephala polysaccharides can regulate the water metabolism of the skin, promote the excretion of excess water, and reduce skin edema; the volatile oil components have certain antibacterial and anti-inflammatory effects, can improve the inflammatory state of the skin. At the same time, Atractylodes macrocephala can also provide nutrition for the skin, promote the normal metabolism of skin cells, and enhance the elasticity and luster of the skin. Almonds are rich in nutrients such as unsaturated fatty acids and vitamin E. Unsaturated fatty acids can moisturize the skin, form a protective film on the skin surface, prevent water loss, and make the skin soft and smooth; vitamin E is a powerful antioxidant, can protect skin cells from damage by free radicals, delay skin aging, and reduce the generation of wrinkles. In addition, vitamin E can also promote the repair and regeneration of skin cells, and accelerate the healing of damaged skin.

[0025] The combination of various ingredients creates a synergistic system that conditions and improves the skin from multiple perspectives. It not only replenishes the skin's essential moisture, nutrients, and collagen, enhancing its elasticity and radiance, but also regulates its metabolism, blood circulation, oil secretion, and immune function, reducing inflammation, pigmentation, dryness, and sagging. This addresses the problem of traditional skincare products, which are limited in their functionality and incapable of nourishing and repairing the skin. It provides a natural and effective skincare solution that helps improve overall skin quality and maintain a healthy, youthful appearance.

[0026] A method for preparing a antler glue ancient method nine-palace polymer, which is applied to the above-mentioned antler glue ancient method nine-palace polymer, comprises the following steps: S1. Pretreatment: After low-temperature drying, the antler glue is coarsely crushed and ultrafinely crushed in sequence according to weight to obtain antler glue ultrafine powder; Chuanxiong, Asparagus cochinchinensis, Radix Ophiopogonis, Rhizoma Anemarrhenae, Angelica dahurica, Astragalus membranaceus, Atractylodes macrocephala, and Apricot kernel are selected, cleaned, vacuum-dried, and ultrafinely crushed to obtain ultrafine Chinese medicinal material powder; in S1, the low-temperature drying temperature of the antler glue is 40° C., and the drying time is 2 hours; the vacuum drying conditions are 60° C., -0.08 MPa, and the drying time is 6 hours; the particle size of the antler glue ultrafine powder and the Chinese medicinal material ultrafine powder are both 300 mesh.

[0027] Specifically, deer antler glue is placed in a low-temperature drying oven at 40°C for 2 hours to remove moisture from the surface of the glue. Deer antler glue easily absorbs moisture from the air during storage. If it is not dried, it will easily clump during the subsequent crushing process, affecting the crushing effect. After drying, it is first coarsely crushed through a conventional grinder to break it into smaller particles, and then ultrafinely crushed using a jet mill to achieve a particle size of 300 mesh. Ultrafine grinding technology can significantly increase the specific surface area of ​​deer antler glue, allowing the active ingredients to dissolve into water more quickly and fully during the subsequent water extraction process, thereby improving extraction efficiency.

[0028] Chuanxiong, Asparagus cochinchinensis, Radix Ophiopogonis, Rhizoma Anemarrhenae, Angelica dahurica, Astragalus membranaceus, Atractylodes macrocephala, and Apricot kernel are rigorously selected to remove impurities, mold, and insect-damaged parts to ensure raw material quality. The herbs are then rinsed 3-5 times with running deionized water to remove surface contaminants such as mud and sand. The washed herbs are placed in a vacuum drying oven and dried at 60°C and -0.08 MPa for 6 hours. Vacuum drying reduces the drying temperature, preventing the decomposition or inactivation of heat-sensitive ingredients in the herbs at high temperatures. It also accelerates water evaporation and improves drying efficiency. After drying, each herb is individually pulverized to 300 mesh using ultrafine grinding technology. This is also intended to increase the specific surface area of the herbs, allowing for better release of the active ingredients into the water during the water extraction process.

[0029] S2. Water extraction: Add water to a multi-functional extraction tank by weight, heat it, and then stir in ultrafine powder of deer horn glue until dissolved. Add ultrafine powder of traditional Chinese medicinal materials, and start the condensation reflux device for extraction to obtain an extract. The water in S2 is deionized water, and its conductivity does not exceed 2 μS / cm at 25 °C. The heating temperature is 90 °C, the stirring and adding rate is 150 r / min, and the extraction is carried out at 80 °C and 120 r / min for 8 hours. During this period, the content of active ingredients is detected every 2 hours, and the extraction is stopped when the stable value is reached.

[0030] Specifically, add 30 - 40 parts of deionized water with a conductivity not exceeding 2 μS / cm at 25 °C to the multi-functional extraction tank. The deionized water has high purity and does not contain impurity ions, which can avoid the influence of impurities on the extraction process and product quality. Heat the water to 90 °C. At this time, the water temperature is relatively high, which is conducive to the rapid dissolution of the ultrafine powder of deer horn glue. Slowly add the ultrafine powder of deer horn glue at a stirring speed of 150 r / min and continuously stir for 45 minutes to ensure that the deer horn glue is completely dissolved in water. The stirring process can make the deer horn glue fully contact with water and accelerate the dissolution process.

[0031] After the deer horn glue is dissolved, add the ultrafine powder of each traditional Chinese medicinal material in sequence and start the condensation reflux device. The condensation reflux device can condense the evaporated solvent (water) and reflux it to the extraction tank, preventing solvent loss, ensuring that the extraction process is carried out under a constant solvent volume, and at the same time avoiding the loss of active ingredients with the volatilization of the solvent. Control the temperature in the extraction tank at 80 °C and extract at a stirring speed of 120 r / min for 8 hours. At this temperature and stirring speed, it can not only ensure the full dissolution and extraction of active ingredients, but also avoid the decomposition of active ingredients caused by too high temperature. During the extraction process, use a high performance liquid chromatograph (HPLC) to detect the content of active ingredients in the extract every 2 hours. When the content of active ingredients reaches a stable value, it means that the active ingredients in the raw materials have been basically extracted completely. At this time, stop the extraction to avoid energy waste and possible component degradation caused by over-extraction.

[0032] S3. Solid-liquid separation: Subject the extract to rough filtration, centrifugal separation, and fine filtration through a filter membrane in sequence to obtain a clarified extract. In S3, the rough filtration uses a plate and frame filter press, the centrifugal separation rate is 4000 r / min, the time is 20 minutes, and the micropore diameter of the filter membrane is 0.45 μm.

[0033] Specifically, first, pass the extract through a plate and frame filter press for rough filtration. The plate and frame filter press utilizes the filtering effect of the filter cloth to remove large solid impurities such as medicinal residue particles in the extract, and initially realizes solid-liquid separation. The extract after rough filtration still contains some fine impurities and precipitates, which need further treatment.

[0034] Next, use a centrifuge at 4000 rpm for 20 minutes. Centrifugal separation utilizes centrifugal force to create different centrifugal accelerations for materials of varying densities within the centrifugal field, thereby achieving solid-liquid separation. Under high-speed centrifugation, fine impurity particles settle to the bottom of the centrifuge tube, while the clarified liquid remains above. This clarified liquid can be separated by decantation or siphoning.

[0035] Finally, fine filtration is performed using a 0.45μm microporous membrane. The microporous membrane has a uniform microporous structure that can intercept impurities such as tiny particles and bacteria with a diameter larger than 0.45μm, further improving the clarity and purity of the extract, resulting in a clarified extract that provides high-quality raw materials for subsequent concentration and other operations.

[0036] S4, concentration: the clarified extract is transported to a vacuum concentration tank for concentration. When the relative density reaches 1.15-1.2 at 60°C, the concentration is stopped to obtain a concentrated solution. The concentration in S4 is carried out at -0.09 MPa and 50°C.

[0037] Specifically, the clarified extract is transferred to a vacuum concentration tank and concentrated at -0.09 MPa and 50°C. Vacuum concentration involves performing an evaporation operation at a pressure lower than atmospheric pressure, which lowers the boiling point of the solution. This allows for evaporation of the solvent at a lower temperature, thus preventing decomposition of the active ingredients at high temperatures. The relative density of the concentrate is monitored in real time via an online monitoring system. Concentration is stopped when the relative density reaches 1.15-1.2 at 60°C. At this point, the concentration of the active ingredients in the concentrate has reached an appropriate range, ensuring the content of the active ingredients while avoiding problems such as over-concentration leading to the precipitation of active ingredients or unsuitable product viscosity, resulting in a concentrated solution.

[0038] S5, drying and molding: When preparing a solid powder product, the concentrated liquid is spray-dried and then sieved and granulated to obtain a solid powder polymer. When preparing a paste product, the concentrated liquid is decompressed and concentrated to a relative density of 1.3-1.35 at 60°C, and then homogenized to obtain a paste polymer. The inlet air temperature of the spray drying in S5 is 180-200°C, the outlet air temperature is 80-90°C, the atomization pressure is 0.2-0.3 MPa, the sieving and granulating uses an 80-mesh screen, and the pressure of the homogenization treatment is 20-30 MPa.

[0039] Specifically, when preparing a solid powder product, the concentrated solution is spray-dried. Spray drying disperses the concentrated solution into fine droplets through an atomizer, which are fully contacted with hot air, and the moisture in the droplets quickly evaporates to obtain dry powder. The inlet air temperature is controlled at 180 - 200 °C, the outlet air temperature is 80 - 90 °C, and the atomization pressure is 0.2 - 0.3 MPa. A suitable inlet air temperature can quickly dry the droplets and prevent the active ingredients from decomposing due to excessive residence time at high temperatures; the outlet air temperature affects the water content and particle morphology of the powder; the atomization pressure determines the size of the droplets, which in turn affects the particle size and drying effect of the powder. There may be some caking in the powder after spray drying, and it is sieved and sized through an 80-mesh sieve to remove larger particles and caking, making the powder particle size uniform, and obtaining a solid powder polymer.

[0040] If a paste product is to be prepared, the concentrated solution is continuously concentrated under reduced pressure to a relative density of 1.3 - 1.35 at 60 °C. At this time, the viscosity and concentration of the concentrated solution are already suitable for making a paste product, but in order to make the paste texture more delicate and uniform, homogenization treatment is required. The concentrated solution is homogenized using a homogenizer at a pressure of 20 - 30 MPa. The homogenization process can further refine the particles in the concentrated solution and make the dispersion more uniform, obtaining a paste polymer.

[0041] S6. Packaging and storage: The solid powder polymer is hermetically packaged using an aluminum foil bag, and the paste polymer is packaged using a glass bottle and stored in a warehouse. The temperature of the warehouse in S6 is 10 - 20 °C, and the relative humidity is 40% - 60%.

[0042] Specifically, for the solid powder polymer, it is hermetically packaged using an aluminum foil bag. The aluminum foil bag has good barrier properties and can effectively prevent the influence of external factors such as moisture, oxygen, and light on the product, maintaining the quality stability of the product. For the paste polymer, it is packaged using a glass bottle. The glass bottle has the advantages of good chemical stability and strong sealing performance, which can prevent chemical reactions between the paste product and the packaging material and avoid product contamination during storage and use.

[0043] The packaged products are stored in a warehouse with a temperature of 10 - 20 °C and a relative humidity of 40% - 60%. Appropriate temperature and humidity conditions can prevent problems such as the decomposition and deterioration of the active ingredients due to too high or too low temperature, and caking and mildew due to too high humidity, ensuring that the products maintain good quality during storage.

[0044] The following is a further introduction in combination with specific examples: Example 1: Thirty volunteers were selected, and their states before use were counted: their skin color was relatively dull, there was pigmentation around the eyes, dark circles were obvious, the skin around the eyes was dull, there were fine lines. The polymer of this embodiment was used once in the morning and once in the evening every day, twice a day. The skin state results were counted respectively after using it for 15 days / 30 days / 45 days / 60 days: After using this polymer, the glossiness was increased by about 20%, the skin color difference was increased by 30%, the skin color brightness was increased by 30%, the melanin content was reduced by 40%, the yellow and black spots were reduced by 30%, the cell repair was 35%, the water content of skin cells was 30%, the elasticity of skin tissue was 25%, and the pore diameter was decreased by 25%.

[0045] Although the embodiments of the present invention have been shown and described, for those of ordinary skill in the art, it can be understood that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principle and spirit of the present invention. The scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A traditional nine-square polymer of deer horn glue, characterized in that, The invention comprises the following raw materials in parts by weight: 30-40 parts of water, 15-25 parts of antler glue, 5-10 parts of Chuanxiong rhizome, 5-10 parts of asparagus cochinchinensis, 5-10 parts of ophiopogon japonicus, 3-7 parts of bamboo shavings, 3-7 parts of angelica dahurica, 3-7 parts of astragalus membranaceus, 3-7 parts of white atractylodes macrocephala, and 3-7 parts of apricot kernel.

2. A preparation method of an old - fashioned nine - palace polymer of deer horn glue, characterized in that: The method for preparing the deer antler glue ancient method nine-palace polymer according to claim 1 comprises the following steps: S1. Pretreatment: Low-temperature drying of antler glue and subsequent coarse grinding and ultrafine grinding are performed by weight to obtain antler glue ultrafine powder; Chuanxiong, asparagus cochinchinensis, ophiopogon japonicus, bamboo shavings, angelica dahurica, astragalus root, atractylodes macrocephala, and apricot kernel are selected, cleaned, vacuum-dried, and ultrafine ground to obtain Chinese medicinal material ultrafine powder; S2. Water extraction: Add water by weight to a multifunctional extraction tank, heat, and stir, then add deer antler glue ultrafine powder and stir until dissolved, add Chinese herbal medicine ultrafine powder, open a condensation reflux device for extraction, and obtain an extract; S3, solid-liquid separation: the extract is sequentially subjected to coarse filtration, centrifugal separation, and membrane fine filtration to obtain a clarified extract; S4, concentration: the clarified extract is transported to a vacuum concentration tank for concentration. When the relative density reaches 1.15-1.2 at 60°C, the concentration is stopped to obtain a concentrated solution. S5. Drying and molding: When preparing a solid powder product, the concentrate is spray-dried and then sieved to obtain a solid powder polymer. When preparing a paste product, the concentrate is concentrated under reduced pressure until the relative density reaches 1.3-1.35 at 60°C, and then homogenized to obtain a paste polymer. S6. Packaging and storage: Use aluminum foil bags to seal the solid powdered polymer and use glass bottles to package the paste polymer and store them in the warehouse.

3. The preparation method of an ancient nine - palace polymer of deer horn glue according to claim 2, characterized in that: The low-temperature drying temperature of the antler glue in S1 is 40°C, and the drying time is 2 hours. The vacuum drying conditions are 60°C, -0.08MPa, and the drying time is 6 hours. The particle size of the antler glue ultrafine powder and the Chinese medicinal material ultrafine powder are both 300 mesh.

4. The preparation method of an ancient nine-square polymer of deer horn glue according to claim 2, characterized in that: The water in S2 is deionized water, and its conductivity does not exceed 2 μS / cm at 25° C., the heating temperature is 90° C., the stirring addition rate is 150 r / min, and the extraction is performed at 80° C. and 120 r / min for 8 hours. During this period, the content of the active ingredient is detected every 2 hours, and the extraction is stopped when a stable value is reached.

5. The preparation method of a traditional nine-square polymer of deer horn glue according to claim 2, characterized in that: The coarse filtration in S3 adopts a plate and frame filter press, the centrifugal separation rate is 4000 r / min, the time is 20 minutes, and the micropore diameter of the filter membrane is 0.45 μm.

6. The preparation method of an ancient nine - palace polymer of deer - horn glue according to claim 2, characterized in that: The concentration in S4 is performed under the conditions of -0.09 MPa and 50°C.

7. The preparation method of an ancient nine - palace polymer of deer horn glue according to claim 2, characterized in that: The inlet air temperature of the spray drying in S5 is 180-200°C, the outlet air temperature is 80-90°C, the atomization pressure is 0.2-0.3 MPa, the sieving and granulation is performed using an 80-mesh screen, and the pressure of the homogenization treatment is 20-30 MPa.

8. The preparation method of a traditional nine-square polymer of deer horn glue according to claim 2, characterized in that: The temperature of the warehouse in S6 is 10-20°C and the relative humidity is 40%-60%.

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