A baffle box and reactor

Abstract

The present invention discloses a baffle tube box, wherein a through-hole plate is detachably connected to a baffle plate, a plurality of through-hole plate through-holes are formed on the through-hole plate, a plurality of baffle plate through-holes are formed on the baffle plate, the through-hole plate through-holes correspond to and are connected to the baffle plate through-holes one by one, the two ends of the baffle tube are respectively connected to different baffle plate through-holes, and the baffle tube is detachably connected to the baffle plate. Under the condition of equal tube wall thickness, the minimum bending radius of the hose of the present invention is smaller than that of the hard tube, thereby reducing the bending radius, making the reaction tubes in the reactor denser, and thus reducing the volume of the reactor, solving the problem of a large reactor volume caused by sparse reactor tubes due to the limitation of the bending radius of the elbow or U-shaped tube.

Description

Technical Field

[0001] The invention relates to the technical field of chemical pharmacy, and in particular to a baffle tube box and a reactor. Background Art

[0002] Reactor equipment commonly used in the field of chemical and pharmaceutical technology includes tubular reactors and kettle reactors, among which kettle reactors are often equipped with stirring devices for mixing liquid reactants. The purity of the synthesized product and the reaction conversion rate are low, and the energy consumption and pollution are relatively serious. Since the chemical and pharmaceutical fields have high requirements for product purity, the commonly used reactor equipment is the continuous flow tubular reactor.

[0003] In the continuous flow reactors currently on the market, the pipes are mainly connected in the form of elbows or U-shaped pipes, which have the following problems:

[0004] 1. The traditional connection method is limited by the radius of the elbow or U-shaped pipe, so the pipes must be kept at a long distance, the reactor pipes are relatively sparse, resulting in a larger reactor volume. If the radius of the elbow or U-shaped pipe is small, it is very easy to be damaged during use.

[0005] 2. It is impossible to set up detection, sampling and other instruments in the middle of the pipeline.

[0006] 3. Since the elbow or U-shaped tube is exposed to the outside of the reactor shell and is in direct contact with the air, it absorbs or releases heat in the air, causing the temperature of the reactants in the elbow or U-shaped tube to be different from the temperature of the reactants in the reaction tube in the shell, affecting the reaction rate, the stability and consistency of the reaction process, and ultimately affecting the conversion rate and yield of the reaction products. Summary of the invention

[0007] In view of the above problems, the present application proposes a baffle box and a reactor, which solves the problem of a large reactor volume caused by the sparse space between reactor tubes due to the limitation of the bending radius of the elbow or U-shaped tube; solves the problem that the radius of the elbow or U-shaped tube is small and it is very easy to be damaged during use; solves the problem that it is impossible to set up detection, sampling and other instruments in the middle of the pipeline; and solves the problem that the temperature of the reactants in the elbow or U-shaped tube is different from that of the reactants in the reaction tube.

[0008] A baffle tube box comprises: a through-hole plate, a baffle plate and a baffle tube, wherein the through-hole plate is detachably connected to the baffle plate, the through-hole plate is formed with a plurality of through-hole plate through holes, the baffle plate is formed with a plurality of baffle through holes, the through-hole plate through holes and the baffle through holes correspond to each other and are connected, the two ends of the baffle tube are respectively connected to different baffle through holes, and the baffle tube is detachably connected to the baffle plate.

[0009] Furthermore, it also includes a ferrule-type joint, one end of which is connected to the baffle plate through hole and detachably connected, and the other end of which is connected to the baffle tube and detachably connected;

[0010] The inner wall of the baffle through hole is formed with an internal thread, the ferrule-type joint is formed with an external thread, the ferrule-type joint is inserted into the baffle through hole and is threadedly connected with the baffle through hole; the baffle tube is ferrule-connected with the ferrule-type joint.

[0011] Furthermore, the baffle tube is a hose, and the baffle tube is made of a transparent material; the material of the baffle tube is PFA.

[0012] Furthermore, the baffle tube is located in the inner cavity of the insulation shell, the insulation shell and the baffle are fixed in position, and the insulation shell is provided with an insulation shell side inlet and an insulation shell side outlet communicated with the inner cavity thereof.

[0013] Furthermore, it also includes a fixing plate, the upper part of the baffle plate is detachably connected to the fixing plate, the heat-insulating shell is fixedly connected to the fixing plate, the fixing plate is formed with a connecting hole, and the baffle tube passes through the connecting hole and enters the inner cavity of the heat-insulating shell.

[0014] Furthermore, it also includes a three-way joint, one baffle tube includes two branch baffle tubes, the three-way joint is located between the two branch baffle tubes of one baffle tube, two ends of the three-way joint are respectively fixed to and communicated with the branch baffle tubes; two ends of the three-way joint are respectively detachably connected to the branch baffle tubes; the third end of the three-way joint is detachably connected to and communicated with the outlet pipe, the insulation shell is formed with a through hole, the outlet pipe passes through the through hole and is detachably connected to and communicated with the sensor and / or sampling valve.

[0015] Furthermore, it also includes a three-way joint, one baffle tube includes two branch baffle tubes, the three-way joint is located between the two branch baffle tubes of the baffle tube, two ends of the three-way joint are respectively fixed to and communicated with the branch baffle tubes; two ends of the three-way joint are respectively detachably connected to the branch baffle tubes; the third end of the three-way joint is detachably connected to and communicated with a sensor or a sampling valve through a pipeline.

[0016] Furthermore, the heat-insulating shell is made of transparent material.

[0017] A reactor using the above-mentioned baffle tube box comprises a shell and a reaction tube, wherein the shell is provided with a shell-side inlet and a shell-side outlet connected to its inner cavity, and a plurality of reaction tubes are arranged in the inner cavity of the shell, and is characterized in that: the upper and lower ends of the shell are respectively connected to the baffle tube box, the through-hole plate of the baffle tube box is fixedly connected to the shell, the two ends of the reaction tube are respectively fixedly connected to the through-hole plates of different baffle tube boxes and are connected to the through holes of the through-hole plates, the baffle tube box is provided with a reactant inlet pipe and a reactant outlet pipe, and the reactant inlet pipe and the reactant outlet pipe are respectively connected to different reaction tubes; and the reaction tubes are connected in series one by one through the baffle tubes.

[0018] Furthermore, the reactant inlet pipe and the reactant outlet pipe are respectively communicated with different baffle through holes and are detachably connected to the baffles, and the reactant inlet pipe and the reactant outlet pipe both pass through the heat-insulating shell.

[0019] The present invention has the following advantages:

[0020] 1. Under the condition of the same tube wall thickness, the minimum bending radius of the hose is smaller than that of the hard tube. The baffle tube uses a hose (the baffle tube of the hose can be bent into an Ω shape, and the bending radius is increased when the distance between the two baffle holes is close), thereby reducing the bending radius, making the reaction tubes in the reactor more dense, thereby reducing the volume of the reactor, and solving the problem of large reactor volume caused by sparse reactor tubes due to the limitation of the bending radius of the elbow or U-shaped tube; the baffle tube using a hose has a small bending radius, and the material is a flexible material that is not easy to be damaged, which solves the problem that the elbow or U-shaped tube has a small radius and is extremely easy to be damaged during use; the baffle tube is translucent or transparent, which is convenient for observing the reactants in the baffle tube; because the baffle tube is a hose, the longer baffle tube bend can be applied to the two baffle holes connected by the shorter baffle tube bend, which improves the versatility of the baffle tube; the ferrule joint and the baffle tube can be disassembled at will, and flexible tube jumping can be realized (that is, the baffle tube is connected to different baffle holes to change the flow path of the reactants).

[0021] 2. By installing a three-way joint on the baffle tube, the sensor and sampling valve can be connected to the baffle tube through the three-way joint, which is convenient for sampling or detection, and solves the problem of not being able to set up detection, sampling and other instruments in the middle of the pipeline.

[0022] 3. By installing an insulation shell on the outside of the elbow or U-shaped tube, a heat exchange medium is introduced into the insulation shell to exchange heat with the elbow or U-shaped tube, so that the temperature of the reactants in the elbow or U-shaped tube is the same as the temperature of the reactants in the reaction tube, the reaction rate is improved, and the problem of different temperatures between the reactants in the elbow or U-shaped tube and the reactants in the reaction tube is solved; the insulation shell can be removed and the baffle tube in the inner cavity of the insulation shell can be replaced; the outlet portion passes through the insulation shell and is detachably connected to the sensor and / or the sampling valve, which ensures that the insulation shell can be freely disassembled and facilitates detection or sampling from the baffle tube. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings required for use in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For those skilled in the art, other drawings can be obtained based on these drawings without creative work.

[0024] Figure 1 : Schematic diagram of the main cross-sectional exploded structure of the baffle box of Example 1;

[0025] Figure 2 : A schematic diagram of the cross-sectional explosion structure of the reactor of Example 2;

[0026] Figure 3 : A schematic diagram of the three-dimensional structure of the reactor of Example 2;

[0027] Figure 4 : The third schematic diagram of the three-dimensional structure of the reactor of Example 2;

[0028] Figure 5 : Schematic diagram of the main cross-sectional exploded structure of the baffle box of embodiment three);

[0029] Figure 6 : Schematic diagram of the main cross-sectional explosion structure of the reactor of Example 4;

[0030] Figure 7 : A schematic diagram of the exploded structure of the left side cross-section of the reactor of Example 4;

[0031] Figure 8 : Schematic diagram of the three-dimensional structure of the reactor of Example 4;

[0032] Fig. 9 : Schematic diagram of the main cross-sectional exploded structure of the baffle box of Embodiment 5;

[0033] Fig.10 : Schematic diagram of the three-dimensional structure of the reactor of Example 6;

[0034] Fig.11 : Schematic diagram of the main cross-sectional exploded structure of the baffle box of embodiment seven;

[0035] Fig.12 : Schematic diagram of the main cross-sectional exploded structure of the baffle box of Example 8;

[0036] Fig.13 : Schematic diagram of the main cross-sectional explosion structure of the reactor of Example 9. DETAILED DESCRIPTION

[0037] The following will be combined with the drawings in the embodiments of the present application to clearly and completely describe the technical solutions in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, not all of the embodiments. Based on the embodiments in the present application, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of this application.

[0038] Embodiment 1:

[0039] like Figure 1 As shown, this embodiment provides a baffle tube box, including: a through-hole plate 3, a baffle plate 4 and a baffle tube 7, wherein the through-hole plate 3 is detachably connected to the baffle plate 4, the through-hole plate 3 is formed with a through-hole plate through-hole 30, the baffle plate 4 is formed with a baffle through-hole 40, the through-hole plate through-hole 30 and the baffle through-hole 40 correspond to each other one by one and are connected, the two ends of the baffle tube 7 are respectively connected to different baffle through-holes 40, and the baffle tube 7 is detachably connected to the baffle plate 4.

[0040] Preferably, it also includes a ferrule-type connector 6, one end of which is connected to the baffle plate through hole 40 and is detachably connected, and the other end of which is connected to the baffle tube 7 and is detachably connected.

[0041] Preferably, the inner wall of the baffle through hole 40 is formed with an internal thread, the ferrule-type joint 6 is formed with an external thread, and the ferrule-type joint 6 is inserted into the baffle through hole 40 and threadedly connected with the baffle through hole 40 .

[0042] Preferably, the baffle tube 7 is connected to the ferrule joint 6 in a ferrule-type connection.

[0043] Preferably, the baffle tube 7 is a hose and is made of a transparent material.

[0044] Preferably, it also includes a sealing gasket 15, one side of which is in contact with the through-hole plate 3 and the other side is in contact with the baffle plate 4; the sealing gasket 15 is formed with a sealing gasket through hole 150, and both ends of the sealing gasket through hole 150 are respectively connected to the through-hole plate through hole 30 and the baffle plate through hole 40.

[0045] Preferably, it further comprises bolts 13 and nuts 14 , wherein the bolts 13 pass through the through-hole plate 3 and the baffle plate 4 and are threadedly connected with the nuts 14 to fix the through-hole plate 3 and the baffle plate 4 .

[0046] Preferably, the baffle tube 7 is made of PFA.

[0047] Working principle: Figure 1 As shown, the reactants enter the baffle box from the through hole 30 of the through-hole plate on the right, and enter the baffle tube 7 upward through the sealing gasket through hole 50 and the baffle through hole 40 on the right in sequence. The reactants change their flow direction after passing through the baffle tube 7, and the reactants flow downward through the baffle through hole 40, the sealing gasket through hole 50 and the through-hole plate through hole 30 on the left in sequence to flow out of the baffle tube box, thereby completing the baffle.

[0048] The ferrule type joint 6 adopts the ferrule type joint of the prior art.

[0049] Embodiment 2:

[0050] like Figures 2 to 4 As shown, this embodiment provides a reactor using the baffle tube box of embodiment one, comprising a shell 1 and a reaction tube 2, the shell 1 being provided with a shell-side inlet 11 and a shell-side outlet 12 connected to its inner cavity, a plurality of reaction tubes 2 being provided in the inner cavity of the shell 1, the upper and lower ends of the shell 1 being respectively connected to the baffle tube box, the through-hole plate 3 of the baffle tube box being fixedly connected to the shell 1, the two ends of the reaction tube 2 being respectively fixedly connected to the through-hole plates 3 of different baffle tube boxes and being connected to the through-holes 30 of the through-hole plates, the baffle tube box being provided with a reactant inlet pipe 21 and a reactant outlet pipe 22, the reactant inlet pipe 21 and the reactant outlet pipe 22 being respectively connected to the reaction tube 2; the reaction tubes 2 are connected in series one by one through the baffle tubes 7.

[0051] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 are respectively connected to different baffle through holes 40 and are detachably connected to the baffle 4 .

[0052] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 can be detachably connected to the baffle plate 4 by using the ferrule type connector 6 used by the baffle plate 4 .

[0053] Working principle:

[0054] like Figures 2 to 4As shown, during operation, the reactants enter the reactor from the reactant inlet pipe 21, and enter the first reaction tube 20 through the through-hole plate through-hole 30, the sealing gasket through-hole 50 and the baffle plate through-hole 40 in sequence. The reactants move upward along the first reaction tube 20 to the first baffle tube 7 located on the upper baffle tube box. After being baffled by the first baffle tube 7, the reactants enter the second reaction tube 20. The reactants move downward in the second reaction tube 20 to the second baffle tube 7 located on the lower baffle tube box. After being baffled by the second baffle tube 7, the reactants enter the third reaction tube 20..., and so on. Finally, the reactants pass through the last reaction tube 20 and then flow through the baffle plate through-hole 40, the sealing gasket through-hole 150 and the through-hole plate through-hole 30 to the reactant outlet pipe 22 and flow out of the reactor from the reactant outlet pipe 22.

[0055] Figure 2 The reaction tube in FIG. 1 is not cut away.

[0056] Embodiment three:

[0057] like Figure 5 As shown, this embodiment provides a baffle tube box, including: a through-hole plate 3, a baffle plate 4 and a baffle tube 7, wherein the through-hole plate 3 is detachably connected to the baffle plate 4, the through-hole plate 3 is formed with a through-hole plate through-hole 30, the baffle plate 4 is formed with a baffle through-hole 40, the through-hole plate through-hole 30 and the baffle through-hole 40 correspond to each other one by one and are connected, the two ends of the baffle tube 7 are respectively connected to different baffle through-holes 40, and the baffle tube 7 is detachably connected to the baffle plate 4.

[0058] Preferably, one baffle tube 7 includes two branch baffle tubes, the three-way joint 8 is located between the two branch baffle tubes of the baffle tube 7, and both ends of the three-way joint 8 are respectively fixed to and connected with the branch baffle tubes.

[0059] Preferably, both ends of the three-way connector 8 are detachably connected to the branching and deflecting flow tubes.

[0060] Preferably, the third end of the three-way connector 8 is detachably connected to and communicates with the sensor 16 or the sampling valve 17 .

[0061] Preferably, it further comprises a through-hole plate 3, wherein the through-hole plate 3 is detachably connected to the baffle plate 4, and the through-hole plate 3 is formed with through-hole plate through holes 30, and the through-hole plate through holes 30 and the baffle plate through holes 40 correspond to each other and are connected.

[0062] Preferably, it also includes a ferrule-type joint 6, one end of which is connected to the baffle plate through hole 40 and is detachably connected, and the other end is connected to the baffle tube 7 and is detachably connected; the inner wall of the baffle plate through hole 40 is formed with an internal thread, and the ferrule-type joint 6 is formed with an external thread, the ferrule-type joint 6 is inserted into the baffle plate through hole 40 and is threadably connected to the baffle plate through hole 40; the baffle tube 7 is ferrule-connected to the ferrule-type joint 6.

[0063] Preferably, both ends of the baffle tube 7 are fixedly connected to the baffle plate 4 respectively.

[0064] Preferably, the baffle tube 7 is a hose or a hard tube. When the baffle tube 70 is a hose, the baffle tube 7 is made of a transparent material, and the material of the baffle tube 7 is PFA.

[0065] Preferably, it also includes a sealing gasket 15, one side of which is in contact with the through-hole plate 3 and the other side is in contact with the baffle plate 4; the sealing gasket 15 is formed with a sealing gasket through hole 150, and both ends of the sealing gasket through hole 150 are respectively connected to the through-hole plate through hole 30 and the baffle plate through hole 40.

[0066] Preferably, it further comprises bolts 13 and nuts 14 , wherein the bolts 13 pass through the through-hole plate 3 and the baffle plate 4 and are threadedly connected with the nuts 14 to fix the through-hole plate 3 and the baffle plate 4 .

[0067] Figure 5 The sensor 16 is not shown in cross-section.

[0068] Working principle:

[0069] Figure 5 The baffle tube 7 is a hose. Figure 5 As shown, the reactants enter the baffle box from the through hole 30 of the through-hole plate on the right, and enter the baffle tube 7 upward through the sealing gasket through hole 50 and the baffle through hole 40 on the right in sequence. The reactants change their flow direction after passing through the baffle tube 7, and the reactants flow downward through the baffle through hole 40, the sealing gasket through hole 50 and the through-hole plate through hole 30 on the left in sequence to flow out of the baffle tube box, thereby completing the baffle.

[0070] The three-way joint 8 is connected to the sensor 16, and the reactants in the three-way joint 8 can reach the sensor 16. The sensor 16 can be a temperature sensor or a pressure sensor. The three-way joint 8 is connected to the sampling valve 17, and the reactants in the three-way joint 8 can reach the sampling valve 17. The staff can control the opening and closing of the sampling valve 17 to sample the reactants in the reaction tube 2.

[0071] The three-way connector 8 and the ferrule connector 6 are both made of equipment of the prior art.

[0072] Embodiment 4:

[0073] like Figures 6 to 8 As shown, this embodiment provides a reactor using the baffle tube box of embodiment three, comprising a shell 1 and a reaction tube 2, wherein the shell 1 is provided with a shell-side inlet 11 and a shell-side outlet 12 connected to its inner cavity, and a plurality of reaction tubes 2 are arranged in the inner cavity of the shell 1, characterized in that: the upper and lower ends of the shell 1 are respectively connected to the baffle tube box, the through-hole plate 3 of the baffle tube box is fixedly connected to the shell 1, the two ends of the reaction tube 2 are respectively fixedly connected to the through-hole plates 3 of different baffle tube boxes and are connected to the through-holes 30 of the through-hole plates, the baffle tube box is provided with a reactant inlet pipe 21 and a reactant outlet pipe 22, and the reactant inlet pipe 21 and the reactant outlet pipe 22 are respectively connected to different reaction tubes 2.

[0074] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 are respectively connected to different baffle through holes 40 and are detachably connected to the baffle 4 .

[0075] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 can be detachably connected to the baffle plate 4 by using the ferrule type connector 6 used by the baffle plate 4 .

[0076] Figure 7 The reaction tube in the figure is not cut away. The reaction tube 2 can be an existing reaction tube, such as a straight tube or a spirally wound tube.

[0077] Figures 6 to 8 The sensor 16 or the sampling valve 17 are not shown.

[0078] Working principle:

[0079] During operation, the reactants enter the reactor from the reactant inlet pipe 21, and enter the first reaction tube 20 through the through-hole plate through-hole 30, the sealing gasket through-hole 50 and the baffle plate through-hole 40 in sequence. The reactants move upward along the first reaction tube 20 to the first baffle tube 7 located on the upper baffle tube box. After being baffled by the first baffle tube 7, the reactants enter the second reaction tube 20. The reactants move downward in the second reaction tube 20 to the second baffle tube 7 located on the lower baffle tube box. After being baffled by the second baffle tube 7, the reactants enter the third reaction tube 20... and so on. Finally, the reactants pass through the last reaction tube 20 and then flow through the baffle plate through-hole 40, the sealing gasket through-hole 150 and the through-hole plate through-hole 30 to the reactant outlet pipe 22 and flow out of the reactor from the reactant outlet pipe 22.

[0080] Embodiment five:

[0081] like Fig. 9As shown, this embodiment provides a baffle box, including: a baffle 4, a baffle tube 7 and an insulation shell 9, the baffle 4 is formed with a baffle through hole 40, and the two ends of the baffle tube 7 are respectively connected to different baffle through holes 40 and fixed in position; the baffle tube 7 is located in the inner cavity of the insulation shell 9, the insulation shell 9 and the baffle 4 are fixed in position, and the insulation shell 9 is provided with an insulation shell side inlet 91 and an insulation shell side outlet 92 connected with its inner cavity.

[0082] Preferably, it also includes a fixing plate 5, the baffle plate 4 is detachably connected to the fixing plate 5, the insulation shell 8 is fixedly connected to the fixing plate 5, the fixing plate 5 is formed with a connecting hole 50, and the baffle tube 7 passes through the connecting hole 50 to enter the inner cavity of the insulation shell 9.

[0083] Preferably, a through-hole plate 3 is further included, and the baffle plate 4 is detachably connected to the through-hole plate 3 at the bottom, and the through-hole plate 3 is formed with through-hole plate through holes 30, and the through-hole plate through holes 30 and the baffle plate through holes 40 correspond to each other one by one and are connected.

[0084] Preferably, the baffle tube 7 is detachably connected to the baffle plate 4.

[0085] Preferably, it also includes a ferrule-type joint 6, the inner wall of the baffle through hole 40 is formed with an internal thread, the ferrule-type joint 6 is formed with an external thread, one end of the ferrule-type joint 6 is inserted into the baffle through hole 40 and is threadedly connected to the baffle through hole 40, and the other end is clamped with the baffle tube 7; the two ends of the ferrule-type joint 6 are respectively connected to the baffle through hole 40 and the baffle tube 7.

[0086] Preferably, it also includes bolts 13 and nuts 14. The bolts 13 pass through the fixing plate 5, the baffle plate 4 and the through-hole plate 3 and are threadedly connected with the nuts 14 to fix the fixing plate 5, the baffle plate 4 and the through-hole plate 3.

[0087] Preferably, it also includes a sealing gasket 15, one side of which is in contact with the through-hole plate 3 and the other side is in contact with the baffle plate 4; the sealing gasket 15 is formed with a sealing gasket through hole 150, and both ends of the sealing gasket through hole 150 are respectively connected to the through-hole plate through hole 30 and the baffle plate through hole 40.

[0088] Working principle: Fig. 9 As shown, the reactants enter the baffle box from the through hole 30 of the through hole plate on the right, and enter the baffle tube 7 upward through the sealing gasket through hole 90 and the baffle through hole 40 on the right in sequence. The reactants change their flow direction after passing through the baffle tube 7, and the reactants flow out of the baffle box downward through the baffle through hole 40, the sealing gasket through hole 150 and the through hole plate through hole 30 on the left in sequence, thereby completing the baffle.

[0089] During this process, the heat exchange medium enters the insulation shell 9 from the insulation shell side inlet 91 to perform heat exchange with the baffle tube 7 , and then leaves the insulation shell 9 from the insulation shell side outlet 92 .

[0090] The ferrule type joint 6 adopts the ferrule type joint of the prior art. The reaction tube 2 adopts the reaction tube of the prior art, such as a straight tube or a spirally wound tube.

[0091] It should be noted that this embodiment does not include Fig. 9 and Fig.10 The three-way joint 8 and the outlet pipe 10 are formed in the heat-insulating shell 9, and the through hole 90 is not formed.

[0092] Embodiment six:

[0093] like Fig.10 As shown, this embodiment provides a reactor using the baffle tube box of embodiment five, comprising a shell 1 and a reaction tube 2, the shell 1 being provided with a shell-side inlet 11 and a shell-side outlet 12 connected to its inner cavity, a plurality of reaction tubes 2 being arranged in the inner cavity of the shell 1, the upper and lower ends of the shell 1 being respectively connected to the baffle tube box, the through-hole plate 3 of the baffle tube box being fixedly connected to the shell 1, the two ends of the reaction tube 2 being respectively fixedly connected to the through-hole plates 3 of different baffle tube boxes and being connected to the through-holes 30 of the through-hole plates, the baffle tube box being provided with a reactant inlet pipe 21 and a reactant outlet pipe 22, the reactant inlet pipe 21 and the reactant outlet pipe 22 being both connected to different reaction tubes 2.

[0094] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 are respectively connected to different baffle through holes 40 and are detachably connected to the baffle 4 .

[0095] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 can be detachably connected to the baffle plate 4 by using the ferrule type connector 6 used by the baffle plate 4 .

[0096] Working principle:

[0097] like Fig.10As shown, during operation, the reactants enter the reactor from the reactant inlet pipe 21, and enter the first reaction tube 20 through the through-hole plate through-hole 30, the sealing gasket through-hole 150 and the baffle plate through-hole 40 in sequence. The reactants move upward along the first reaction tube 20 to the first baffle tube 7 located on the upper baffle tube box. After being baffled by the first baffle tube 7, the reactants enter the second reaction tube 20. The reactants move downward in the second reaction tube 20 to the second baffle tube 7 located on the lower baffle tube box. After being baffled by the second baffle tube 7, the reactants enter the third reaction tube 20..., and so on. Finally, the reactants pass through the last reaction tube 20 and then flow through the baffle plate through-hole 40, the sealing gasket through-hole 150 and the through-hole plate through-hole 30 to the reactant outlet pipe 22 and flow out of the reactor from the reactant outlet pipe 22.

[0098] In this process, the heat exchange medium enters the inner cavity of the shell 1 from the shell side inlet 11 to exchange heat with the reaction tube 20, and then leaves the shell 1 from the shell side outlet 12. At the same time, the heat exchange medium enters the inner cavity of the insulation shell 9 from the insulation shell side inlet 91 to exchange heat with the baffle tube 7, and then leaves the insulation shell 9 from the insulation shell side outlet 92. The heat exchange medium temperature of the shell 1 and the insulation shell 9 is the same.

[0099] Embodiment seven:

[0100] like Fig.11 As shown, this embodiment provides a baffle tube box, characterized in that it includes: a baffle plate 4, a baffle tube 7 and an insulation shell 9, the baffle plate 4 is formed with a baffle plate through hole 40, the baffle tube 7 includes two baffle tube parts, a three-way part and a pass-through part, the two ends of the three-way part are respectively connected with the baffle tube part, the third end of the three-way part is connected with the pass-through part, the pass-through part passes through the insulation shell 9 and is connected with the sensor 16 and / or the sampling valve 17; the baffle tube part and the three-way part are located in the inner cavity of the insulation shell 9, and the insulation shell 8 is provided with an insulation shell side inlet 91 and an insulation shell side outlet 92 connected with its inner cavity.

[0101] Preferably, the three-way portion is a three-way joint 8, the outlet portion is an outlet pipe 10, both ends of the three-way joint 8 are detachably connected to the baffle pipe portion, the third end of the three-way joint 8 is detachably connected to the outlet pipe 10, the heat-insulating shell 9 is formed with a through hole 90, the outlet pipe 10 passes through the through hole 90 and is detachably connected to the sensor 16 and / or the sampling valve 17. A sealing ring or other sealing measures are adopted between the outlet pipe 10 and the through hole 90.

[0102] Preferably, it also includes a fixing plate 5, the baffle plate 4 is detachably connected to the fixing plate 5, the insulation shell 8 is fixedly connected to the fixing plate 5, the fixing plate 5 is formed with a connecting hole 50, and the baffle tube 7 passes through the connecting hole 50 to enter the inner cavity of the insulation shell 9.

[0103] Preferably, a through-hole plate 3 is further included, and the baffle plate 4 is detachably connected to the through-hole plate 3 at the bottom, and the through-hole plate 3 is formed with through-hole plate through holes 30, and the through-hole plate through holes 30 and the baffle plate through holes 40 correspond to each other one by one and are connected.

[0104] Preferably, the baffle tube 7 is detachably connected to the baffle plate 4; it also includes a ferrule-type joint 6, the inner wall of the baffle plate through hole 40 is formed with an internal thread, the ferrule-type joint 6 is formed with an external thread, one end of the ferrule-type joint 6 is inserted into the baffle plate through hole 40 and is threadedly connected to the baffle plate through hole 40, and the other end is clamped with the baffle tube 7; the two ends of the ferrule-type joint 6 are respectively connected to the baffle plate through hole 40 and the baffle tube 7.

[0105] Preferably, it also includes a sealing gasket 15, one side of which is in contact with the through-hole plate 3 and the other side is in contact with the baffle plate 4; the sealing gasket 15 is formed with a sealing gasket through hole 150, and both ends of the sealing gasket through hole 150 are respectively connected with the through-hole plate through hole 30 and the baffle plate through hole 40.

[0106] Preferably, it also includes bolts 13 and nuts 14. The bolts 13 pass through the fixing plate 5, the baffle plate 4 and the through-hole plate 3 and are threadedly connected with the nuts 14 to fix the fixing plate 5, the baffle plate 4 and the through-hole plate 3.

[0107] Preferably, the baffle tube 7 is a hose, and the baffle tube 7 is made of a transparent material; the material of the baffle tube 7 is PFA.

[0108] Preferably, the heat-insulating shell 9 is made of transparent material.

[0109] Working principle: Fig.11 As shown, the reactants enter the baffle box from the through hole 30 of the through-hole plate on the right, and enter the baffle tube 7 upward through the sealing gasket through hole 150 and the baffle through hole 40 on the right in sequence. The reactants change their flow direction after passing through the baffle tube 7, and the reactants flow out of the baffle box downward through the baffle through hole 40, the sealing gasket through hole 150 and the through-hole plate through hole 30 on the left in sequence, thereby completing the baffle.

[0110] When the reactants flow in the deflector tube 7, part of the reactants will flow from the three-way joint 8 to the outlet tube 10, then leave the insulation shell 9 through the outlet tube 10 and flow into the sensor 16 and / or the sampling valve 17, so as to detect the temperature, pressure or take samples.

[0111] During this process, the heat exchange medium enters the insulation shell 9 from the insulation shell side inlet 91 to perform heat exchange with the baffle tube 7 , and then leaves the insulation shell 9 from the insulation shell side outlet 92 .

[0112] The outlet tube 10 is connected to the sensor 16 and / or the sampling valve 17 through an external ferrule, and the outlet tube 10 is not provided with a connection structure such as a thread, so that when the heat-insulating shell 8 is disassembled, the through hole 90 will not be blocked by the outlet tube 10. A sealing treatment is adopted between the through hole 90 and the outlet tube 10, such as a sealing ring.

[0113] The ferrule type joint 6 adopts the ferrule type joint of the prior art.

[0114] The transparent baffle tube 7 and the heat-insulating shell 9 facilitate observation of the conditions of the reactants in the baffle tube 7 and the conditions of the heat exchange medium in the heat-insulating shell 9 .

[0115] Embodiment eight:

[0116] like Fig.12 As shown, this embodiment provides a baffle tube box, characterized in that it includes: a baffle plate 4, a baffle tube 7 and an insulation shell 9, the baffle plate 4 is formed with a baffle plate through hole 40, the baffle tube 7 includes two baffle tube parts, a three-way part and a through-out part, the two ends of the three-way part are respectively connected with the baffle tube part, the third end of the three-way part is connected with the through-out part, the through-out part passes through the insulation shell 9 and is connected with the sensor 16 and / or the sampling valve 17; the baffle tube part and the three-way part are located in the inner cavity of the insulation shell 9, and the insulation shell 9 is provided with an insulation shell side inlet 91 and an insulation shell side outlet 92 connected with its inner cavity.

[0117] Preferably, the baffle tube portion, the tee portion and the outlet portion are connected as one piece, which means that the baffle tube portion, the tee portion and the outlet portion form one pipe.

[0118] Preferably, it also includes a fixing plate 5, the baffle plate 4 is detachably connected to the fixing plate 5, the insulation shell 9 is fixedly connected to the fixing plate 5, the fixing plate 5 is formed with a connecting hole 50, and the baffle tube 7 passes through the connecting hole 50 to enter the inner cavity of the insulation shell 9.

[0119] Preferably, a through-hole plate 3 is further included, and the baffle plate 4 is detachably connected to the through-hole plate 3 at the bottom, and the through-hole plate 3 is formed with through-hole plate through holes 30, and the through-hole plate through holes 30 and the baffle plate through holes 40 correspond to each other one by one and are connected.

[0120] Preferably, the baffle tube 7 is detachably connected to the baffle plate 4; it also includes a ferrule-type joint 6, the inner wall of the baffle plate through hole 40 is formed with an internal thread, the ferrule-type joint 6 is formed with an external thread, one end of the ferrule-type joint 6 is inserted into the baffle plate through hole 40 and is threadedly connected to the baffle plate through hole 40, and the other end is clamped with the baffle tube 7; the two ends of the ferrule-type joint 6 are respectively connected to the baffle plate through hole 40 and the baffle tube 7.

[0121] Preferably, it also includes a sealing gasket 15, one side of which is in contact with the through-hole plate 3 and the other side is in contact with the baffle plate 4; the sealing gasket 15 is formed with a sealing gasket through hole 150, and both ends of the sealing gasket through hole 150 are respectively connected with the through-hole plate through hole 30 and the baffle plate through hole 40.

[0122] Preferably, it also includes bolts 13 and nuts 14. The bolts 13 pass through the fixing plate 5, the baffle plate 4 and the through-hole plate 3 and are threadedly connected with the nuts 14 to fix the fixing plate 5, the baffle plate 4 and the through-hole plate 3.

[0123] Preferably, the baffle tube 7 is a hose, and the baffle tube 7 is made of a transparent material; the material of the baffle tube 7 is PFA.

[0124] Preferably, the heat-insulating shell 9 is made of transparent material.

[0125] Working principle: Fig.12 As shown, the reactants enter the baffle tube box with heat preservation function from the through-hole 30 of the through-hole plate on the right side, and enter the baffle tube 7 upward through the sealing gasket through-hole 150 and the baffle through-hole 40 on the right side in sequence. The reactants change their flow direction after passing through the baffle tube 7, and the reactants flow downward through the baffle through-hole 40, the sealing gasket through-hole 150 and the through-hole plate through-hole 30 on the left side in sequence, and flow out of the baffle tube box with heat preservation function, thereby completing the baffle.

[0126] When the reactants flow in the baffle tube 7, part of the reactants will flow from the three-way portion to the outlet portion, then leave the insulation shell 9 through the outlet portion and flow into the sensor 16 and / or the sampling valve 17, so as to detect the temperature, pressure or take samples.

[0127] During this process, the heat exchange medium enters the insulation shell 9 from the insulation shell side inlet 91 to perform heat exchange with the baffle tube 7 , and then leaves the insulation shell 9 from the insulation shell side outlet 92 .

[0128] The outlet is connected to the sensor 16 and / or the sampling valve 17 through an external ferrule, and the outlet is not provided with a connection structure such as a thread, so that the through hole 90 will not be blocked by the outlet when the heat-insulating shell 9 is disassembled. A sealing treatment is adopted between the through hole 90 and the outlet, such as a sealing ring. The ferrule-type joint 6 adopts the ferrule-type joint of the prior art.

[0129] Embodiment nine:

[0130] like Fig.13As shown, this embodiment provides a reactor using the baffle tube box of embodiment seven or embodiment eight, comprising a shell 1 and a reaction tube 2, wherein the shell 1 is provided with a shell-side inlet 11 and a shell-side outlet 12 connected to its inner cavity, and a plurality of reaction tubes 2 are arranged in the inner cavity of the shell 1, characterized in that: the upper and lower ends of the shell 1 are respectively connected to the baffle tube box, the through-hole plate 3 of the baffle tube box is fixedly connected to the shell 1, the two ends of the reaction tube 2 are respectively fixedly connected to the through-hole plates 3 of different baffle tube boxes and are connected to the through-holes 30 of the through-hole plates, the baffle tube box is provided with a reactant inlet pipe 21 and a reactant outlet pipe 22, and the reactant inlet pipe 21 and the reactant outlet pipe 22 are both connected to different reaction tubes 2.

[0131] Preferably, the reactant inlet pipe 21 and the reactant outlet pipe 22 are respectively connected to different baffle through holes 40 and are detachably connected to the baffle 4 , and both the reactant inlet pipe 21 and the reactant outlet pipe 22 pass through the heat-insulating shell 9 .

[0132] Working principle:

[0133] like Fig.13 As shown, during operation, the reactants enter the reactor from the reactant inlet pipe 21, and enter the first reaction tube 2 through the through hole 30 of the through-hole plate, the through hole 150 of the sealing gasket and the through hole 40 of the baffle plate in sequence. The reactants move upward along the first reaction tube 2 to the first baffle tube 7 located on the upper baffle tube box. After being baffled by the first baffle tube 7, the reactants enter the second reaction tube 2. The reactants move downward in the second reaction tube 2 to the second baffle tube 7 located on the lower baffle tube box. After being baffled by the second baffle tube 7, the reactants enter the third reaction tube 2... and so on. Finally, the reactants pass through the last reaction tube 2 and then through the baffle through hole 40, the sealing gasket through hole 150 and the through hole 30 of the through-hole plate to the reactant outlet pipe 22 and flow out of the reactor from the reactant outlet pipe 22.

[0134] In this process, the heat exchange medium enters the inner cavity of the shell 1 from the shell side inlet 11 to exchange heat with the reaction tube 2, and then the heat exchange medium leaves the shell 1 from the shell side outlet 12. At the same time, the heat exchange medium enters the inner cavity of the insulation shell 9 from the insulation shell side inlet 91 to exchange heat with the baffle tube 7, and then the heat exchange medium leaves the insulation shell 9 from the insulation shell side outlet 92. The heat exchange medium temperature of the shell 1 and the insulation shell 9 is the same.

[0135] The reactant inlet pipe 21 and the reactant outlet pipe 22 respectively pass through different through holes 90 and are sealed with the through holes 90. The reactant first enters the reactant inlet pipe 21 and then enters the reaction tube 2, and heat is exchanged in the insulation shell 9 below, which can play a role in preheating the reactant.

[0136] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present application, rather than to limit it. Although the present application has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that they can still modify the technical solutions described in the aforementioned embodiments, or make equivalent replacements for some of the technical features therein. However, these modifications or replacements do not cause the essence of the corresponding technical solutions to deviate from the spirit and scope of the technical solutions of the embodiments of the present application.

Claims

1. A baffle tube box, characterized in that: include: A through-hole plate (3), a baffle plate (4), a baffle tube (7) and a heat-insulating shell (9), wherein the through-hole plate (3) and the baffle plate (4) are detachably connected, the through-hole plate (3) is formed with a plurality of through-hole plate through holes (30), the baffle plate (4) is formed with a plurality of baffle plate through holes (40), the through-hole plate through holes (30) and the baffle plate through holes (40) correspond to each other one by one and are connected, the two ends of the baffle tube (7) are respectively connected with different baffle plate through holes (40), and the baffle tube (7) and the baffle plate (4) are detachably connected; It also comprises a ferrule-type joint (6), one end of which is connected to the baffle plate through hole (40) and is detachably connected, and the other end of which is connected to the baffle tube (7) and is detachably connected; The inner wall of the baffle through hole (40) is formed with an internal thread, the ferrule-type joint (6) is formed with an external thread, the ferrule-type joint (6) is inserted into the baffle through hole (40) and is threadedly connected to the baffle through hole (40); the baffle tube (7) is ferrule-connected to the ferrule-type joint (6); The baffle tube (7) is a hose, and the baffle tube (7) is made of a transparent material; the material of the baffle tube (7) is PFA; The baffle tube (7) is located in the inner cavity of the heat-insulating shell (9); the heat-insulating shell (9) and the baffle plate (4) are fixed in position; the heat-insulating shell (9) is provided with a heat-insulating shell-side inlet (91) and a heat-insulating shell-side outlet (92) which are connected to the inner cavity thereof; It also comprises a three-way joint (8), wherein one baffle tube (7) comprises two branch baffle tubes, the three-way joint (8) is located between the two branch baffle tubes of the baffle tube (7), and the two ends of the three-way joint (8) are respectively fixed to and communicated with the branch baffle tubes; the two ends of the three-way joint (8) are respectively detachably connected to the branch baffle tubes; the third end of the three-way joint (8) is detachably connected to and communicated with a through-hole (10), the heat-insulating shell (9) is formed with a through hole (90), and the through-hole (90) is detachably connected to and communicated with a sensor (16) and / or a sampling valve (17).

2. A baffle tube box according to claim 1, characterized in that: It also comprises a fixing plate (5), the upper part of the baffle plate (4) is detachably connected to the fixing plate (5), the heat-insulating shell (9) is fixedly connected to the fixing plate (5), the fixing plate (5) is formed with a connecting hole (50), and the baffle tube (7) passes through the connecting hole (50) and enters the inner cavity of the heat-insulating shell (9).

3. The baffle tube box according to claim 1, characterized in that: The heat-insulating shell (9) is made of a transparent material.

4. A reactor using the baffle box according to any one of claims 1 to 3, comprising a shell (1) and a reaction tube (2), wherein the shell (1) is provided with a shell-side inlet (11) and a shell-side outlet (12) connected to its inner cavity, and a plurality of reaction tubes (2) are arranged in the inner cavity of the shell (1), characterized in that: The upper and lower ends of the shell (1) are respectively connected to the baffle tube box, the through-hole plate (3) of the baffle tube box is fixedly connected to the shell (1), the two ends of the reaction tube (2) are respectively fixedly connected to the through-hole plates (3) of different baffle tube boxes and are connected to the through holes (30) of the through-hole plates, the baffle tube box is provided with a reactant inlet pipe (21) and a reactant outlet pipe (22), the reactant inlet pipe (21) and the reactant outlet pipe (22) are respectively connected to different reaction tubes (2); the reaction tubes (2) are connected in series one by one through the baffle tubes (7).

5. A reactor according to claim 4, characterized in that: The reactant inlet pipe (21) and the reactant outlet pipe (22) are respectively connected to different baffle through holes (40) and are detachably connected to the baffle (4). The reactant inlet pipe (21) and the reactant outlet pipe (22) both pass through the heat-insulating shell (9).

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