Silk quilt capable of preventing silk from getting out and manufacturing process of silk quilt

Abstract

The invention belongs to the technical field of home textiles, and particularly relates to an anti-silk-leakage silk quilt and a manufacturing process thereof, which comprises a silk manufacturing process and a silk quilt manufacturing process, and is characterized in that the silk manufacturing process comprises the following steps: soaking cocoons in warm water, setting the temperature of the water to be 20-55 DEG C, and setting the soaking time to be 2-4 minutes to moisten cocoon layers; peeling off cocoon silks of the cooked cocoons to prepare a silk net; the silk net is placed in a silk softening agent to be soaked, and the soaking time is set to be 25-40 minutes; the silk net soaked for the set time is made into a silk cotton pocket in a silk softener; the silk cotton pocket is placed in the film-forming agent solution to be soaked, and the soaking time is set to be 18-32 minutes; stringing the silk cotton pockets with threads, and airing the silk cotton pockets in a ventilated place for 12-15 hours; compared with the prior art, static electricity is prevented from being generated in the quilt cover in the using process, and silk drilling of the silk quilt is avoided.

Description

Technical Field

[0001] The invention relates to the technical field of home textiles, and more particularly to a silk quilt that is anti-drilling and a manufacturing process thereof. Background Art

[0002] Silk is a high-grade textile raw material, known as the "Queen of Fibers". It is a long fiber among natural fibers, and its length can be directly used for weaving. Silk is strong and elastic, thin and soft, has good moisture absorption and touch, and is especially elegant and beautiful in luster. Silk products have different styles, which can be as thin as gauze or as thick as velvet. The main advantages of silk quilts are that they are soft, breathable and close to the body.

[0003] For example, the application publication number CN117981986A discloses a high-fluff silk quilt production process, in which a ZnONSs@chitosan solution is selected as the impregnation liquid during the impregnation process. The impregnation liquid can improve the fluffiness, resilience, UV resistance and antibacterial properties of the cotton piece.

[0004] Among the above, although the fluffiness, resilience, UV resistance and antibacterial properties of the silk quilt are improved, since silk is thinner than ordinary filling fibers, the silk quilt is easy to be drilled with fluff. The drilled silk not only affects the appearance, but also comes into contact with the human body when covering the quilt, affecting the comfort. Summary of the invention

[0005] In view of the shortcomings of the prior art, the object of the present invention is to provide a silk quilt and a manufacturing process thereof which can prevent thread drilling and improve the comfort of use.

[0006] To achieve the above object, the present invention provides the following technical solutions: A silk quilt that prevents silk from being drilled and a manufacturing process thereof, comprising a silk manufacturing process and a silk quilt manufacturing process, wherein the silk manufacturing process comprises the following steps: S1: Boiling the cocoons, immersing the cocoons in water, heating the water to boiling, and setting the boiling time to 25-45 minutes, then taking out the cocoons and soaking them in warm water, the temperature of the warm water is set to 20-55°C, and the soaking time is set to 2-4 minutes to further soften the cocoon layer; S2: reeling, peeling off the silk from the soaked cocoons to make silk nets; S3: Softening, placing the silk mesh in a silk softener for soaking, and the soaking time is set to 25 to 40 minutes; S4: opening the cotton, and making the silk net soaked for a set time into a silk cotton bag in a silk softener; S5: Film formation, placing the silk cotton bag in the film-forming agent solution for soaking, and the soaking time is set to 18-32 minutes; S6: Drying the cotton: string the silk cotton bags together with thread and place them in a ventilated place to air dry. The air drying time is set to 12-15 hours. S7: Cut the silk cotton pockets, use scissors to cut the silk cotton pockets into cotton pieces; S8: Pulling the cotton sheet into a silk quilt; The manufacturing process of the quilt cover comprises the following steps: S1: Weaving, weaving silk threads into quilt covers; S2: Soaking, soaking the quilt in an antistatic solution; S3: Clean and dry. Place the soaked quilt cover in clean water and wash it. Then dry it. Finally, sew the silk quilt base into the quilt cover.

[0007] The present invention is further configured as follows: the S3 softening, the silk softener includes essence, higher fatty acid, emulsifier, dimethyl silicone oil, alkyl amine oxide, antibacterial agent, ethanol, water and polyether hydrophilic silicone.

[0008] The present invention is further configured as follows: 2-5 parts of the essence, 7-10 parts of higher fatty acids, 5-8 parts of emulsifiers, 5-8 parts of dimethyl silicone oils, 12-15 parts of alkyl amine oxides, 1-3 parts of antibacterial agents, 9-12 parts of ethanol and 200-300 parts of water. The present invention is further configured as follows: 250 parts of water are placed in a container, then 10 parts of ethanol are added and the ethanol is fully dissolved, and then 9 parts of higher fatty acids, 7 parts of emulsifiers, 7 parts of dimethyl silicone oils, 13 parts of alkyl amine oxides and 2 parts of antibacterial agents are added in sequence, and 3 parts of flavors are added after they are fully dissolved.

[0009] The present invention is further configured as follows: the S5 film-forming agent solution includes an emulsifier, deionized water, sodium bicarbonate, hydroxyethyl methacrylate, carbonate, vinyl chloride, vinyl acetate, ethylene glycol, polyvinyl alcohol, silicone oil, dodecyl acetate and silicon dioxide.

[0010] The present invention is further configured as follows: 2-5 parts of the emulsifier, 200-300 parts of deionized water, 2-5 parts of sodium bicarbonate, 1-4 parts of hydroxyethyl methacrylate, 2-5 parts of carbonate, 2-5 parts of vinyl chloride, 2-5 parts of vinyl acetate, 2-6 parts of ethylene glycol, 4-8 parts of polyvinyl alcohol, 9-12 parts of silicone oil, 3-6 parts of dodecyl acetate and 2-5 parts of silicon dioxide.

[0011] The present invention is further configured as follows: 3 parts of emulsifier, 250 parts of deionized water, 3 parts of sodium bicarbonate and 2 parts of hydroxyethyl methacrylate are mixed, heated, the heating temperature is set to 50°C, then mixed with 3 parts of carbonate, and 3 parts of vinyl chloride are added dropwise; the temperature is continued to be raised, the temperature is set to 80°C, 3 parts of carbonate and 3 parts of vinyl acetate are added dropwise, and then 5 parts of ethylene glycol, 11 parts of polyvinyl alcohol, 3 parts of silicone oil and 3 parts of carbonate are added dropwise, the temperature is lowered after the reaction, the temperature is set to 25°C, the pH is adjusted to 7, filtered, and then mixed with dodecyl acetate and silicon dioxide.

[0012] The present invention is further configured as follows: the quilt cover comprises an inner layer and an outer layer, the outer layer is blended from flax, jute, ramie, sisal, abaca, bamboo and ramie, and the inner layer is blended from mulberry silk, real silk and mercerized cotton.

[0013] The present invention is further configured as follows: the antistatic solution includes 20 parts of amide phosphate, 27 parts of alkyl alcohol amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water. First, 6 parts of flavor and 300 parts of water are mixed, and the 6 parts of flavor are completely mixed. Then, 20 parts of amide phosphate, 27 parts of alkyl alcohol amide and 6 parts of emulsifier are added in sequence and mixed evenly. Then, the inner layer is placed in the antistatic solution for immersion, and the immersion time is set to 35 minutes.

[0014] Compared with the shortcomings of the prior art, the beneficial effects of the present invention are: By soaking the silk net in silk softener to increase the softness of the silk, the silk can be prevented from drilling into the thread during use, which would affect the use effect. Furthermore, the silk cotton bag is placed in a film-forming agent solution for soaking to form a nanofiber membrane on the surface of the silk. The nanofiber membrane can prevent the sharp end of the silk from contacting the quilt cover, which can effectively prevent the silk quilt from drilling into the thread. Furthermore, the quilt cover adopts a double-layer structure, which can effectively increase the durability of the quilt cover. When the silk is static, the thread ends will open outward and drill out of the quilt cover. Since the outer quilt cover has been soaked in an anti-static solution, the quilt cover can avoid static electricity during use, further preventing the silk from drilling into the thread. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 Schematic diagram of a flow chart of an embodiment of the present invention. DETAILED DESCRIPTION

[0016] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0017] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating the orientation or position relationship are based on the orientation or position relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0018] Embodiment 1: First prepare the materials needed to prepare silk softener: 200 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifiers, 5 parts of dimethyl silicone oil, 12 parts of alkyl amine oxides, 2 parts of antibacterial agents and 3 parts of essences.

[0019] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0020] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 200 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 2 parts of carbonate, 3 parts of vinyl chloride, 2 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0021] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0022] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0023] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0024] like Figure 1 As shown, first pour clean water into the special pot for boiling cocoons, then light the stove, and while waiting for the water to boil, put the selected cocoons into the cloth bag and tie the bag tightly. Then put the bagged cocoons into the pot. Depending on the size of the pot, put 12 bags at a time, so that each bag of cocoons is completely immersed in water, cover the pot, and continue heating. When boiling cocoons, the water is always kept boiling. Boil for about half an hour, take out the cocoons, rinse with clean water, and then soak the cocoons in warm water at 50℃ for about half an hour.

[0025] After cooking, peel the cocoons and remove the impurities. Find a container and pour clean water into it. Take a cooked cocoon, make a notch on either end of the cocoon, turn the cocoon over, inside out, and put it on your hand to make a silk net the size of your palm. Then, peel off the silkworm pupae, silkworm sand and other impurities in the net. After peeling the first one, take another cocoon and put it on the peeled silk net, and use the same method to remove the impurities. Peel 5 cocoons in a row. Then, turn the silk net back and stretch it out to make a silk net.

[0026] Then, water, ethanol, higher fatty acid, emulsifier, dimethyl silicone oil, alkyl amine oxide, antibacterial agent and fragrance are evenly mixed to prepare silk softener.

[0027] Then soak the silk net in silk softener for 30 minutes, find a container, and fix a 30 cm wide bamboo bow on one side of the container. Stretch the silk net with force and put it on the bamboo bow to make it a silk cotton bag. After stretching the first silk cotton bag, take another silk net, stretch it in the same way, and put it on the silk cotton bag just stretched. In this way, put 5 silk nets in a row, because the thickness of the 5 silk nets is just suitable for the subsequent wire drawing work. Then, take the stretched silk cotton bag from the bamboo bow and twist it into a ball. The twisted silk cotton bag still contains a certain amount of moisture, and the silk cotton bag is dried.

[0028] Then, the film solution is prepared, and the emulsifier, deionized water, sodium bicarbonate and hydroxyethyl methacrylate are mixed, heated to 50°C, mixed with carbonate, and vinyl chloride is added; the temperature is continued to rise to 80°C, carbonate and vinyl acetate are added, and then ethylene glycol, polyvinyl alcohol, silicone oil and carbonate are added, and after the reaction, the temperature is lowered to 25°C, the pH is adjusted to 7, filtered, and then mixed with dodecyl acetate and silicon dioxide. Since sodium bicarbonate is alkaline, the alkali can soften sericin, dissolve impurities, and improve the whiteness of the silk.

[0029] Finally, place the dried silk cotton bags in the film-forming agent solution and soak them for 28 minutes. After soaking, wring the silk cotton bags dry, flatten the silk cotton bags, string them together with thread, hang them on bamboo poles, and place them in a ventilated place to dry for 12 hours.

[0030] After drying, use scissors to cut the silk cotton bag open, cut the silk cotton bag into cotton sheets, and then pull the cotton sheets into a silk quilt frame, and then prepare the quilt cover.

[0031] The quilt cover includes an inner layer and an outer layer. The outer layer is blended from flax, jute, ramie, sisal, abaca, bamboo and ramie, and the inner layer is blended from mulberry silk, real silk and mercerized cotton.

[0032] First, mix the essence and water completely, then add amide phosphate, alkyl alcohol amide and emulsifier in turn and mix evenly, then place the inner layer in the antistatic solution and soak for 30 minutes.

[0033] Finally, sew the silk quilt base onto the quilt cover.

[0034] Embodiment 2: First prepare the materials needed to prepare silk softener: 200 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifiers, 5 parts of dimethyl silicone oil, 12 parts of alkyl amine oxides, 2 parts of antibacterial agents and 3 parts of essences.

[0035] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0036] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 250 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 3 parts of carbonate, 3 parts of vinyl chloride, 3 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0037] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0038] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0039] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0040] Then, the processing is carried out according to the working process of Example 1.

[0041] Embodiment three: First prepare the materials needed to prepare silk softener: 200 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifiers, 5 parts of dimethyl silicone oil, 12 parts of alkyl amine oxides, 2 parts of antibacterial agents and 3 parts of essences.

[0042] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0043] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 300 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 5 parts of carbonate, 3 parts of vinyl chloride, 5 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 6 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0044] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0045] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0046] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0047] Then, the processing is carried out according to the working process of Example 1.

[0048] Embodiment 4: First prepare the materials needed to prepare silk softener: 250 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 7 parts of dimethyl silicone oil, 13 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0049] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0050] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 200 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 2 parts of carbonic acid, 3 parts of vinyl chloride, 2 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0051] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0052] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0053] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0054] Then, the processing is carried out according to the working process of Example 1.

[0055] Embodiment five: First prepare the materials needed to prepare silk softener: 250 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 7 parts of dimethyl silicone oil, 13 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0056] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0057] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 250 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 3 parts of carbonate, 3 parts of vinyl chloride, 3 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0058] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0059] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0060] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0061] Then, the processing is carried out according to the working process of Example 1.

[0062] Embodiment six: First prepare the materials needed to prepare silk softener: 250 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 7 parts of dimethyl silicone oil, 13 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0063] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0064] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 300 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 5 parts of carbonate, 3 parts of vinyl chloride, 5 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 6 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0065] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0066] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0067] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0068] Then, the processing is carried out according to the working process of Example 1.

[0069] Embodiment seven: First prepare the materials needed to prepare silk softener: 300 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 8 parts of dimethyl silicone oil, 15 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0070] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0071] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 200 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 2 parts of carbonate, 3 parts of vinyl chloride, 2 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0072] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0073] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0074] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0075] Then, the processing is carried out according to the working process of Example 1.

[0076] Embodiment eight: First prepare the materials needed to prepare silk softener: 300 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 8 parts of dimethyl silicone oil, 15 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0077] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0078] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 250 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 3 parts of carbonate, 3 parts of vinyl chloride, 3 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 3 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0079] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reducing the friction between the fabrics, thereby improving the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer, etc. Hydroxyethyl methacrylate is then fully contacted with silk and undergoes a polymerization reaction at high temperature to form a film.

[0080] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0081] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0082] Then, the processing is carried out according to the working process of Example 1.

[0083] Embodiment nine: First prepare the materials needed to prepare silk softener: 300 parts of water, 10 parts of ethanol, 9 parts of higher fatty acids, 7 parts of emulsifier, 8 parts of dimethyl silicone oil, 15 parts of alkyl amine oxide, 2 parts of antibacterial agent and 3 parts of essence.

[0084] Dimethicone and alkylamine oxide can enhance the effect of higher fatty acids as emulsifiers, making silk softer and smoother.

[0085] Then prepare the materials needed to prepare the membrane solution: 3 parts of emulsifier, 300 parts of deionized water, 3 parts of sodium bicarbonate, 2 parts of hydroxyethyl methacrylate, 5 parts of carbonate, 3 parts of vinyl chloride, 5 parts of vinyl acetate, 3 parts of ethylene glycol, 5 parts of polyvinyl alcohol, 11 parts of silicone oil, 6 parts of dodecyl acetate and 3 parts of silicon dioxide.

[0086] Dodecyl alcohol can form a lubricating film on the surface of the fabric, reduce the friction between the fabrics, and thus improve the softness and comfort of the fabric. Hydroxyethyl methacrylate can be used as an adhesive for synthetic textiles and a medical polymer monomer. Then hydroxyethyl methacrylate is in full contact with silk, and a polymerization reaction occurs at a high temperature to form a film. Then hydroxyethyl methacrylate is in full contact with silk, and a polymerization reaction occurs at a high temperature to form a film.

[0087] Finally, prepare the materials needed to prepare the antistatic solution: 20 parts of amide phosphate, 27 parts of alkane amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water.

[0088] After being mixed with alkanolamide, alkanolamide and emulsifier, it has good antistatic, softening, bactericidal and lubricating effects.

[0089] Then, the processing is carried out according to the working process of Example 1.

[0090] Effect test, the silk softener formula and film-forming agent solution formula prepared according to Examples 1-9 of the present invention are respectively recorded as Experimental Examples 1-9, and the authorization number CN117981986A is recorded as the comparison group, and then the appearance and touch of the silk are judged by sensory organs, and then the silk is taken for performance test, Elongation test: According to GB / T 24252-2009, the sample is cut at a distance of more than 20cm from the edge of the quilt, excluding the quilt cover, and should be representative and without defects that affect the test results. Each sample has an area of ​​20cm×20cm.

[0091] The silk of the control group was produced according to the scheme presented by the control group, and the same experiment was carried out. The test results are as follows:

[0092] Then, the silks of Examples 1-9 were assembled into corresponding quilt covers, and the silks of the comparison group were assembled into ordinary quilt covers. Air permeability test: According to GB / T5453-1997 test: test area 20cm, test pressure difference 200Pa, place a textile air permeability tester under the silk quilt for measurement; Warmth retention test: According to GB / T11048-1989 test: select a water bottle with 250ml, 100℃ water, put it into a corner of the silk quilt, wait for 30 minutes and then take it out, measure the water temperature in the bottle, and compare the rise and fall of the water temperature to test the warmth retention of the girl's silk quilt. Antistatic test: According to GB50944-2013 test, the test area is 20cm, and the test pressure difference is 200Pa; the warp and weft resistance of the quilt cover is measured with a surface resistance tester. According to the surface electrostatic voltage and charge surface density of the textile under specified conditions, the antistatic level of the textile can be divided into four standards, namely: 1. Grade A: ≤1.0S, half-life performance requirement: Grade A ≤1.0S.

[0093] 2. Grade B: ≤5.0S, half-life performance requirement: Grade B ≤5.0S.

[0094] 3. Grade C: ≤15.0S, half-life performance requirement: Grade C ≤15.0S.

[0095] 4. Grade D: ≤60.0S, half-life performance requirement: Grade D ≤60.0S; The test results are as follows:

[0096] As shown in Table 1 and Table 2, compared with the control group, the appearance, touch, resilience, air permeability, warmth retention and antistatic evaluation scores of the example group are better than those of the control group, while the differences between the experimental groups are not obvious; among them, the best performance is Example 5. This result shows that the manufacturing process of the silk quilt provided by the present invention can effectively improve the performance of the silk quilt.

[0097] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Common changes and substitutions made by those skilled in the art within the scope of the technical solution of the present invention should be included in the protection scope of the present invention.

Claims

1. A silk quilt with anti-drilling function and a manufacturing process thereof, including a silk manufacturing process and a quilt cover manufacturing process, characterized in that: The production process of the silk comprises the following steps: S1: Boiling the cocoons, immersing the cocoons in water, heating the water to boiling, and setting the boiling time to 25-45 minutes, then taking out the cocoons and soaking them in warm water, the temperature of the warm water is set to 20-55°C, and the soaking time is set to 2-4 minutes to further soften the cocoon layer; S2: reeling, peeling off the silk from the soaked cocoons to make silk nets; S3: Softening, placing the silk mesh in a silk softener for soaking, and the soaking time is set to 25 to 40 minutes; S4: opening the cotton, and making the silk net soaked for a set time into a silk softener to form a silk cotton bag; S5: Film formation, placing the silk cotton bag in the film-forming agent solution for soaking, and the soaking time is set to 18-32 minutes; S6: Drying the cotton: string the silk cotton bags together with thread and place them in a ventilated place to air dry. The air drying time is set to 12-15 hours. S7: Cut the silk cotton pockets, use scissors to cut the silk cotton pockets into cotton pieces; S8: Pulling the cotton sheet into a silk quilt; The manufacturing process of the quilt cover comprises the following steps: S1: Weaving, weaving silk threads into quilt covers; S2: Soaking, soaking the quilt in an antistatic solution; S3: Clean and dry. Place the soaked quilt cover in clean water and wash it. Then dry it. Finally, sew the silk quilt base into the quilt cover.

2. The silk production process according to claim 1, characterized in that: The S3 softening, silk softener includes essence, higher fatty acid, emulsifier, dimethyl silicone oil, alkyl amine oxide, antibacterial agent, ethanol, water and polyether type hydrophilic silicone.

3. The silk production process according to claim 2, characterized in that: The essence comprises 2 to 5 parts, higher fatty acids 7 to 10 parts, emulsifiers 5 to 8 parts, dimethyl silicone oils 5 to 8 parts, alkyl amine oxides 12 to 15 parts, antibacterial agents 1 to 3 parts, ethanol 9 to 12 parts and water 200 to 300 parts.

4. The silk production process according to claim 2, characterized in that: Put 250 parts of water in a container, then add 10 parts of ethanol and dissolve it fully, then add 9 parts of higher fatty acids, 7 parts of emulsifiers, 7 parts of dimethyl silicone oils, 13 parts of alkyl amine oxides and 2 parts of antibacterial agents in sequence, and add 3 parts of flavor after it is fully dissolved.

5. The silk production process according to claim 2, characterized in that: The S5 film-forming agent solution includes an emulsifier, deionized water, sodium bicarbonate, hydroxyethyl methacrylate, carbonate, vinyl chloride, vinyl acetate, ethylene glycol, polyvinyl alcohol, silicone oil, dodecyl acetate and silicon dioxide.

6. The silk production process according to claim 4, characterized in that: The emulsifier comprises 2 to 5 parts, deionized water 200 to 300 parts, sodium bicarbonate 2 to 5 parts, hydroxyethyl methacrylate 1 to 4 parts, carbonate 2 to 5 parts, vinyl chloride 2 to 5 parts, vinyl acetate 2 to 5 parts, ethylene glycol 2 to 6 parts, polyvinyl alcohol 4 to 8 parts, silicone oil 9 to 12 parts, dodecyl acetate 3 to 6 parts and silicon dioxide 2 to 5 parts.

7. The process for making a silk quilt according to claim 6, characterized in that: Mix 3 parts of emulsifier, 250 parts of deionized water, 3 parts of sodium bicarbonate and 2 parts of hydroxyethyl methacrylate, heat, set the heating temperature to 50°C, mix with 3 parts of carbonate, and add 3 parts of vinyl chloride; continue to heat, set the temperature to 80°C, add 3 parts of carbonate and 3 parts of vinyl acetate, and then add 5 parts of ethylene glycol, 11 parts of polyvinyl alcohol, 3 parts of silicone oil and 3 parts of carbonate, cool after reaction, set the temperature to 25°C, adjust pH7, filter, and then mix with dodecyl acetate and silicon dioxide.

8. The process for making a silk quilt according to claim 1, characterized in that: The quilt cover comprises an inner layer and an outer layer, the outer layer is blended from flax, jute, ramie, sisal, abaca, bamboo and ramie, and the inner layer is blended from mulberry silk, real silk and mercerized cotton.

9. The process for making a silk quilt according to claim 1, characterized in that: The antistatic solution includes 20 parts of amidophosphate, 27 parts of alkyl alcohol amide, 6 parts of emulsifier, 6 parts of flavor and 300 parts of water. First, 6 parts of flavor and 300 parts of water are mixed, and the 6 parts of flavor are completely mixed. Then, 20 parts of amidophosphate, 27 parts of alkyl alcohol amide and 6 parts of emulsifier are added in sequence and mixed evenly. Then, the inner layer is placed in the antistatic solution for immersion, and the immersion time is set to 35 minutes.

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