Anti-wrinkle mask essence and preparation method thereof

Abstract

The anti-wrinkle mask essence is prepared from the following raw materials in percentage by mass: 91 to 93 percent of water, 3.5 to 6 percent of 1, 3-propylene glycol, 0.8 to 1.2 percent of glycine betaine, 0.35 to 0.8 percent of sodium hyaluronate, 0.35 to 0.8 percent of p-hydroxyacetophenone, 0.35 to 0.8 percent of 1, 2-hexanediol, 0.08 to 0.125 percent of herba houttuyniae extract, 0.08 to 0.125 percent of golden chamomile, 0.08 to 0.125 percent of herba portulacae extract, 0.08 to 0.125 percent of dipotassium glycyrrhizinate, 0.08 to 0.125 percent of arginine and 0.03 to 0.1 percent of EDTA (Ethylene Diamine Tetraacetic Acid) disodium. The anti-wrinkle mask essence disclosed by the invention has the beneficial effects that the anti-wrinkle mask essence has a remarkable anti-wrinkle effect through a synergistic effect of various active ingredients, moisturizing ingredients such as sodium hyaluronate and the like can keep skin moisture, arginine stimulates collagen synthesis, and various plant extracts resist oxidation and inflammation and jointly act on skin, so that wrinkles are reduced, and the anti-wrinkle effect is achieved. Meanwhile, the product is mild, non-irritant and suitable for various people.

Description

Technical Field

[0001] The invention relates to the technical field of skin care product preparations, and in particular to an anti-wrinkle mask essence and a preparation method thereof. Background Art

[0002] As people age and are affected by environmental factors, skin wrinkles have become a cosmetic problem that people are concerned about. There are many existing anti-wrinkle products, but they still have problems such as insignificant efficacy and highly irritating ingredients. Therefore, it is of great significance to develop an efficient and gentle anti-wrinkle mask essence. Summary of the invention

[0003] The purpose of the present invention is to provide an anti-wrinkle mask essence and a preparation method thereof in order to solve the above problems.

[0004] The present invention achieves the above-mentioned purpose through the following technical solutions:

[0005] An anti-wrinkle facial mask essence is prepared from the following raw materials in percentage by mass: 91-93% of water, 3.5-6% of 1,3-propylene glycol, 0.8-1.2% of betaine, 0.35-0.8% of sodium hyaluronate, 0.35-0.8% of p-hydroxyacetophenone, 0.35-0.8% of 1,2-hexanediol, 0.08-0.125% of houttuynia cordata extract, 0.08-0.125% of golden chamomile, 0.08-0.125% of purslane extract, 0.08-0.125% of dipotassium glycyrrhizinate, 0.08-0.125% of arginine, and 0.03-0.1% of disodium EDTA.

[0006] Furthermore, it is prepared from the following raw materials in percentage by mass: 91.515% water, 6% 1,3-propylene glycol, 0.8% betaine, 0.35% sodium hyaluronate, 0.35% p-hydroxyacetophenone, 0.35% 1,2-hexanediol, 0.121% houttuynia cordata extract, 0.121% golden chamomile, 0.121% purslane extract, 0.121% dipotassium glycyrrhizate, 0.121% arginine, and 0.03% disodium EDTA.

[0007] Furthermore, it is prepared from the following raw materials in percentage by mass: 91.945% water, 5% 1,3-propylene glycol, 1% betaine, 0.5% sodium hyaluronate, 0.5% p-hydroxyacetophenone, 0.5% 1,2-hexanediol, 0.101% houttuynia cordata extract, 0.101% golden chamomile, 0.101% purslane extract, 0.101% dipotassium glycyrrhizinate, 0.101% arginine, and 0.05% disodium EDTA.

[0008] Furthermore, it is prepared from the following raw materials in percentage by mass: 92.37% water, 3.5% 1,3-propylene glycol, 1.2% betaine, 0.8% sodium hyaluronate, 0.8% p-hydroxyacetophenone, 0.8% 1,2-hexanediol, 0.086% houttuynia cordata extract, 0.086% golden chamomile, 0.086% purslane extract, 0.086% dipotassium glycyrrhizinate, 0.086% arginine, and 0.1% disodium EDTA.

[0009] A method for preparing an anti-wrinkle facial mask essence comprises the following steps:

[0010] Step 1: Place the raw materials of phase B, 1,3-propylene glycol and sodium hyaluronate in a stirring device according to a certain proportion and pre-disperse them until they are uniform and free of particles to obtain a phase B solution, which is then set aside for later use;

[0011] Step 2: Add the raw material water, betaine, p-hydroxyacetophenone, 1,2-hexanediol, dipotassium glycyrrhizinate and disodium EDTA of phase A into the emulsifying pot in proportion, then add the phase B solution into the emulsifying pot, start the stirring function and stir at a speed of 10-30rpm. During the stirring process, heat up to 83-87℃ and keep warm for 15-30 minutes. At the same time, start the homogenization 1-3 times, 3 minutes each time, and the homogenization speed is 1000-2000rpm, until the raw materials are completely dissolved and the material body is transparent;

[0012] Step 3: When the temperature drops to 35-45°C, add the C-phase raw materials, Houttuynia cordata extract, golden chamomile, Portulaca oleracea extract, and arginine, into the emulsifying pot in proportion, stir for 15-30 minutes, at a stirring speed of 10-30rpm, homogenize for 3 minutes, at a homogenizing speed of 1000-2000rpm, so that the materials are evenly dispersed and the material body is uniform and free of particles;

[0013] Step 4: Filling after passing the inspection.

[0014] The effects of each raw material in the present invention are:

[0015] Water: As a solvent, it provides a dispersion medium for other ingredients, helping them to mix evenly and act on the skin.

[0016] 1,3-Propanediol: It has good moisturizing and solubility, which can help other active ingredients penetrate into the skin better.

[0017] Betaine: It has moisturizing, antistatic, and irritation-reducing effects, and can enhance the skin's barrier function and improve skin comfort.

[0018] Sodium hyaluronate: It can effectively moisturize, increase the moisture content of the skin, make the skin plump and firm, and reduce the formation of wrinkles.

[0019] Parahydroxyacetophenone: As a preservative, it can effectively inhibit the growth of microorganisms at lower concentrations and has high safety.

[0020] 1,2-Hexanediol: It works synergistically with p-hydroxyacetophenone to preserve and also has a certain moisturizing and nourishing effect.

[0021] Houttuynia cordata extract: Rich in a variety of active ingredients, it has antioxidant and anti-inflammatory effects, helping to reduce the deepening of wrinkles caused by free radical damage and inflammation.

[0022] Golden Chamomile: Its extract has soothing, antioxidant properties that can relieve skin sensitivity and fight against aging.

[0023] Portulaca Extract: It has multiple functions such as moisturizing, anti-oxidation and anti-inflammatory, which helps maintain the health of the skin and reduce the formation of wrinkles.

[0024] Dipotassium glycyrrhizinate: has good anti-inflammatory, soothing and anti-allergic effects, can reduce the discomfort caused by external stimuli to the skin, and indirectly contributes to the anti-wrinkle effect.

[0025] Arginine: can stimulate collagen production, enhance skin elasticity and effectively reduce wrinkles.

[0026] Disodium EDTA: As a chelating agent, it can stabilize the product system and prevent metal ions from affecting product quality and efficacy.

[0027] The beneficial effects of the present invention are: the anti-wrinkle mask essence of the present invention has a significant anti-wrinkle effect through the synergistic effect of multiple active ingredients. Moisturizing ingredients such as sodium hyaluronate can maintain skin moisture, arginine stimulates collagen synthesis, and multiple plant extracts are antioxidant and anti-inflammatory, acting together on the skin to reduce the formation of wrinkles. At the same time, the product is mild and non-irritating, and is suitable for use by all kinds of people. DETAILED DESCRIPTION

[0028] The technical solution of the present invention will be clearly and completely described below in conjunction with the embodiments. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0029] An anti-wrinkle facial mask essence is prepared from the following raw materials in percentage by mass: 91-93% of water, 3.5-6% of 1,3-propylene glycol, 0.8-1.2% of betaine, 0.35-0.8% of sodium hyaluronate, 0.35-0.8% of p-hydroxyacetophenone, 0.35-0.8% of 1,2-hexanediol, 0.08-0.125% of houttuynia cordata extract, 0.08-0.125% of golden chamomile, 0.08-0.125% of purslane extract, 0.08-0.125% of dipotassium glycyrrhizinate, 0.08-0.125% of arginine, and 0.03-0.1% of disodium EDTA.

[0030] Embodiment 1:

[0031] An anti-wrinkle facial mask essence is prepared from the following raw materials in mass percentage: 91.515% of water, 6% of 1,3-propylene glycol, 0.8% of betaine, 0.35% of sodium hyaluronate, 0.35% of p-hydroxyacetophenone, 0.35% of 1,2-hexanediol, 0.121% of houttuynia cordata extract, 0.121% of golden chamomile, 0.121% of purslane extract, 0.121% of dipotassium glycyrrhizinate, 0.121% of arginine, and 0.03% of disodium EDTA.

[0032] Embodiment 2:

[0033] An anti-wrinkle facial mask essence is prepared from the following raw materials in percentage by mass: 91.945% of water, 5% of 1,3-propylene glycol, 1% of betaine, 0.5% of sodium hyaluronate, 0.5% of p-hydroxyacetophenone, 0.5% of 1,2-hexanediol, 0.101% of houttuynia cordata extract, 0.101% of golden chamomile, 0.101% of purslane extract, 0.101% of dipotassium glycyrrhizinate, 0.101% of arginine, and 0.05% of disodium EDTA.

[0034] Embodiment three:

[0035] An anti-wrinkle facial mask essence is prepared from the following raw materials in percentage by mass: 92.37% water, 3.5% 1,3-propylene glycol, 1.2% betaine, 0.8% sodium hyaluronate, 0.8% p-hydroxyacetophenone, 0.8% 1,2-hexanediol, 0.086% houttuynia cordata extract, 0.086% golden chamomile, 0.086% purslane extract, 0.086% dipotassium glycyrrhizinate, 0.086% arginine, and 0.1% disodium EDTA.

[0036] A method for preparing an anti-wrinkle facial mask essence comprises the following steps:

[0037] Step 1: Place the raw materials of phase B, 1,3-propylene glycol and sodium hyaluronate in a stirring device according to a certain proportion and pre-disperse them until they are uniform and free of particles to obtain a phase B solution, which is then set aside for later use;

[0038] Step 2: Add the raw material water, betaine, p-hydroxyacetophenone, 1,2-hexanediol, dipotassium glycyrrhizinate and disodium EDTA of phase A into the emulsifying pot in proportion, then add the phase B solution into the emulsifying pot, start the stirring function and stir at a speed of 10-30rpm. During the stirring process, heat up to 83-87℃ and keep warm for 15-30 minutes. At the same time, start the homogenization 1-3 times, 3 minutes each time, and the homogenization speed is 1000-2000rpm, until the raw materials are completely dissolved and the material body is transparent;

[0039] Step 3: When the temperature drops to 35-45°C, add the C-phase raw materials, Houttuynia cordata extract, golden chamomile, Portulaca oleracea extract, and arginine, into the emulsifying pot in proportion, stir for 15-30 minutes, at a stirring speed of 10-30rpm, homogenize for 3 minutes, at a homogenizing speed of 1000-2000rpm, so that the materials are evenly dispersed and the material body is uniform and free of particles;

[0040] Step 4: Filling after passing the inspection.

[0041] Performance Test:

[0042] 1. Moisturizing performance test

[0043] Test method: A skin moisture tester (such as Corneometer CM825) was used to select 90 volunteers aged between 25 and 45 years old with dry to mixed skin types, and they were divided into experimental groups 1 to 3, with 30 people in each group. Experimental groups 1 to 3 used the facial mask liquids of Examples 1 to 3, respectively. After the volunteers cleaned their faces, the skin moisture content was measured before, immediately after, 2 hours after, 4 hours after, and 8 hours after using the facial mask essence in a specific environment (temperature 22±2°C, relative humidity 50±5%). Each time point was measured 3 times, and the average value was taken.

[0044] The test results are shown in the table below:

[0045] From the data, we can see that after using the mask essence, the skin's moisture content increases significantly immediately and remains higher than the level before use within 8 hours, indicating that the essence has a good moisturizing effect and can continuously replenish moisture to the skin and reduce water loss.

[0046] 2. Anti-wrinkle performance test

[0047] Test method: 60 volunteers aged 35-55 years old with obvious crow's feet or nasolabial folds were tested using a three-dimensional skin profiler (such as PRIMOS) and divided into experimental groups 1-3, each with 20 people. Experimental groups 1-3 used the facial mask liquids of Examples 1 to 3 respectively. After the volunteers cleaned their faces, the facial mask essence was applied to one side of the face, and the other side was used as a control, 3 times a week for 4 consecutive weeks. The wrinkle depth, wrinkle area and wrinkle volume were measured before use and after 4 weeks of use.

[0048] The results showed that after 4 weeks of use, the depth and area of ​​facial wrinkles on the side using the mask essence were significantly reduced, while there was no obvious change on the control side, indicating that the essence can improve skin wrinkle conditions to a certain extent and has anti-wrinkle effects.

[0049] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited to the above embodiments, and the above embodiments and descriptions are only for explaining the principles of the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, and these changes and improvements all fall within the scope of the present invention to be protected.

Claims

1. An anti-wrinkle facial mask essence, characterized in that: The invention is prepared from the following raw materials in percentage by mass: 91-93% water, 3.5-6% 1,3-propylene glycol, 0.8-1.2% betaine, 0.35-0.8% sodium hyaluronate, 0.35-0.8% p-hydroxyacetophenone, 0.35-0.8% 1,2-hexanediol, 0.08-0.125% houttuynia cordata extract, 0.08-0.125% golden chamomile, 0.08-0.125% purslane extract, 0.08-0.125% dipotassium glycyrrhizinate, 0.08-0.125% arginine and 0.03-0.1% disodium EDTA.

2. The anti-wrinkle facial mask essence according to claim 1, characterized in that: The invention is prepared from the following raw materials in percentage by mass: 91.515% water, 6% 1,3-propylene glycol, 0.8% betaine, 0.35% sodium hyaluronate, 0.35% p-hydroxyacetophenone, 0.35% 1,2-hexanediol, 0.121% houttuynia cordata extract, 0.121% golden chamomile, 0.121% purslane extract, 0.121% dipotassium glycyrrhizinate, 0.121% arginine, and 0.03% disodium EDTA.

3. The anti-wrinkle facial mask essence according to claim 1, characterized in that: The invention is prepared from the following raw materials in percentage by mass: 91.945% water, 5% 1,3-propylene glycol, 1% betaine, 0.5% sodium hyaluronate, 0.5% p-hydroxyacetophenone, 0.5% 1,2-hexanediol, 0.101% houttuynia cordata extract, 0.101% golden chamomile, 0.101% purslane extract, 0.101% dipotassium glycyrrhizinate, 0.101% arginine, and 0.05% disodium EDTA.

4. The anti-wrinkle facial mask essence according to claim 1, characterized in that: The invention is prepared from the following raw materials in percentage by mass: 92.37% water, 3.5% 1,3-propylene glycol, 1.2% betaine, 0.8% sodium hyaluronate, 0.8% p-hydroxyacetophenone, 0.8% 1,2-hexanediol, 0.086% houttuynia cordata extract, 0.086% golden chamomile, 0.086% purslane extract, 0.086% dipotassium glycyrrhizinate, 0.086% arginine, and 0.1% disodium EDTA.

5. A method for preparing the anti-wrinkle facial mask essence according to any one of claims 1 to 4, characterized in that: The following steps are involved: Step 1: Place the raw materials of phase B, 1,3-propylene glycol and sodium hyaluronate in a stirring device according to a certain proportion and pre-disperse them until they are uniform and free of particles to obtain a phase B solution, which is then set aside for later use; Step 2: Add the raw material water, betaine, p-hydroxyacetophenone, 1,2-hexanediol, dipotassium glycyrrhizinate and disodium EDTA of phase A into the emulsifying pot in proportion, then add the phase B solution into the emulsifying pot, start the stirring function and stir at a speed of 10-30rpm. During the stirring process, heat up to 83-87℃ and keep warm for 15-30 minutes. At the same time, start the homogenization 1-3 times, each time for 3 minutes, and the homogenization speed is 1000-2000rpm, until the raw materials are completely dissolved and the material body is transparent; Step 3: When the temperature drops to 35-45°C, add the C-phase raw materials, Houttuynia cordata extract, golden chamomile, Portulaca oleracea extract, and arginine, into the emulsifying pot in proportion, stir for 15-30 minutes, at a stirring speed of 10-30rpm, homogenize for 3 minutes, at a homogenizing speed of 1000-2000rpm, so that the materials are evenly dispersed and the material body is uniform and free of particles; Step 4: Filling after passing the inspection.

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