An emulsified composition and its preparation method and application

Abstract

The present invention provides an emulsified composition, a preparation method, and an application thereof. The emulsified composition comprises a polyol, a sucrose fatty acid ester, and a polyglycerol fatty acid ester; the sucrose fatty acid ester is a combination of sucrose laurate, sucrose dilaurate, sucrose palmitate, and sucrose stearate. The emulsified composition of the present invention has a smaller emulsified particle size than conventional emulsions after use in cosmetics, and a narrower particle size distribution range, creating a better skin feel and having higher kinetic stability. The smaller particle size helps effectively deliver active ingredients into the skin, making it a potential carrier for cosmetic ingredients, achieving optimal dispersion of active ingredients in specific skin layers, resulting in better efficacy. Furthermore, the smaller particle size allows for rapid penetration into the deep layers of the skin and pores, effectively rinsing away makeup and dirt.

Description

Technical Field

[0001] The present invention belongs to the technical field of cosmetics, and in particular relates to an emulsified composition, a preparation method and an application thereof. Background Art

[0002] Emulsification is the process of uniformly dispersing one liquid in the form of extremely tiny droplets within another immiscible liquid through the creation of an interface. A common emulsification method involves heating the external phase, internal phase, and surfactant (emulsifier) ​​to a certain temperature and, under high-speed stirring, allowing the two phases to form a relatively stable and uniform emulsion. The mixture is then insulated and cooled. Emulsifiers play a crucial role in the emulsification process, significantly reducing the surface tension between the two phases, altering the interfacial state of the system, and forming a monomolecular interfacial film, thereby stabilizing the system. Emulsions typically appear as milky white, opaque liquids. When the diameter of the dispersed phase droplets in an emulsion is less than 0.1 μm, the liquid becomes translucent or transparent, and is called a microemulsion. Creams and creams in cosmetics are often emulsified systems. Emulsification can combine immiscible components, allowing products to combine the physical properties and efficacy of both phases. The formation of emulsions is also more conducive to absorption by the human body.

[0003] CN102415955A discloses an emulsified composition. This invention produces an emulsified composition with a small emulsified particle size, improving emulsion stability and reducing the amount of thickeners used in cosmetics prepared using a D-phase emulsification method gel composition. The emulsified composition contains methoxypolyethylene glycol polymethacrylate, polyglycerol fatty acid ester, glycerin, and an oily component.

[0004] CN117618258A discloses an O / D phase composition and an oil-in-water emulsion composition. The O / D phase composition can be prepared using a general-purpose stirring mixer to form an oil-in-water emulsion composition. Even when diluted, the dispersion state of the fine emulsified particles is stable, resulting in an oil-in-water emulsion composition that is less irritating to the skin. An oily component is added to a surfactant component (cleanser) phase component obtained by dissolving one or more selected from glycyrrhizic acid and its salts in a trivalent or higher polyol to form an O / D phase composition having a pH of 5.0 or less in a 10% by mass aqueous solution. The O / D phase composition is then formed using a stirring mixer such as a homogenizer to form an oil-in-water emulsion composition having a particle size (median particle size) of less than 1.0 μm.

[0005] However, during the emulsification process of the above-mentioned composition, the temperatures of both the oil and water phases must be controlled between 70°C and 85°C. If there are raw materials with higher melting points in the oil phase, a higher temperature is required. After emulsification, it is also necessary to keep the temperature and stir, which consumes a lot of energy. Finally, the emulsion needs to be cooled, and cooling water must be used. This process wastes a lot of energy. Therefore, it is urgent to provide a product with better emulsification effect and lower energy consumption in the emulsification process to meet application needs. Summary of the Invention

[0006] To address the shortcomings of the prior art, the present invention provides an emulsified composition, its preparation method, and its application. This emulsified composition reduces energy consumption by eliminating heating and cooling steps during the emulsification process, selectively applying heat energy to energy-requiring processes. This approach meets the requirements of low energy consumption, simplified processes, and efficient production. Furthermore, when applied to cosmetics, the emulsified composition of the present invention can address the issues of large emulsion droplet diameter and low viscosity, resulting in a product with high transparency, moderate viscosity, small emulsified particle size, and a pleasant skin feel.

[0007] In order to achieve the purpose of the invention, the present invention adopts the following technical solutions:

[0008] In a first aspect, the present invention provides an emulsified composition comprising a polyol, a sucrose fatty acid ester, and a polyglycerol fatty acid ester;

[0009] The sucrose fatty acid ester is a combination of sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate.

[0010] Preferably, the emulsified composition comprises, by weight, 60-90 parts of a polyol (for example, 62 parts, 65 parts, 68 parts, 70 parts, 72 parts, 75 parts, 78 parts, 80 parts, 82 parts, 85 parts or 88 parts, etc.), 10-30 parts of a sucrose fatty acid ester (for example, 11 parts, 13 parts, 15 parts, 17 parts, 19 parts, 20 parts, 23 parts, 25 parts, 27 parts or 29 parts, etc.), and 1-10 parts of a polyglycerol fatty acid ester (for example, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts or 9 parts, etc.).

[0011] Preferably, the emulsified composition comprises 64-83 parts of polyol, 12-26 parts of sucrose fatty acid ester and 5-10 parts of polyglycerol fatty acid ester in parts by weight.

[0012] Preferably, the emulsified composition comprises 70-80 parts of polyol, 15-22 parts of sucrose fatty acid ester and 5-8 parts of polyglycerol fatty acid ester in parts by weight.

[0013] Preferably, the mass ratio of sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate is (3-9): (0.1-2): (0.5-3): (0.5-3).

[0014] Among them, "3-9" can be 3.5, 4, 4.5, 5, 5.5, 6, 6.5, 7, 7.5, 8 or 8.5, etc.

[0015] “0.1-2” can be 0.3, 0.5, 0.7, 1, 1.3, 1.5, 1.7, or 1.9, etc.

[0016] The first "0.5-3" can be 0.7, 0.9, 1, 1.1, 1.3, 1.5, 1.7, 1.9, 2, 2.1, 2.3, 2.5, 2.7 or 2.9, etc.

[0017] The second "0.5-3" can be 0.7, 0.9, 1, 1.1, 1.3, 1.5, 1.7, 1.9, 2, 2.1, 2.3, 2.5, 2.7 or 2.9, etc.

[0018] Preferably, the polyol is any one of glycerol, butanediol or 1,3-propylene glycol, or a combination of at least two thereof.

[0019] Preferably, the polyglyceryl fatty acid ester includes any one of polyglyceryl-6 laurate, polyglyceryl-6 stearate, polyglyceryl-8 stearate, polyglyceryl-10 laurate, polyglyceryl-10 palmitate or polyglyceryl-10 stearate, or a combination of at least two thereof.

[0020] Preferably, the polyglycerol fatty acid ester is polyglyceryl-10 laurate.

[0021] Any specific point value within the above numerical range can be selected and will not be described in detail here.

[0022] In a second aspect, the present invention provides a method for preparing the emulsified composition as described in the first aspect, the preparation method comprising homogenizing polyol, sucrose fatty acid ester and polyglycerol fatty acid ester to obtain the emulsified composition.

[0023] Preferably, the mixing and homogenizing temperature is 80-100°C, for example, it can be 82°C, 85°C, 88°C, 90°C, 92°C, 95°C or 98°C, etc. Specific point values ​​within the above numerical range can be selected and will not be described here one by one.

[0024] In a third aspect, the present invention provides a use of the emulsified composition as described in the first aspect in preparing cosmetics.

[0025] Preferably, the cosmetics include essence, essence cream, facial cleanser or gel, etc.

[0026] Preferably, the mass percentage of the emulsified composition in the cosmetic is 1-15%, for example, it can be 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%, 13% or 14%.

[0027] Any specific point value within the above numerical range can be selected and will not be described in detail here.

[0028] In a fourth aspect, the present invention provides a makeup remover gel, wherein the components of the makeup remover gel include, by weight, 5-15 parts of the emulsified composition described in the first aspect, 3-7 parts of an auxiliary emulsifier, 5-20 parts of a polyol, 50-80 parts of oil, and 1-15 parts of water.

[0029] In the makeup remover gel of the present invention, the added amount of the emulsified composition can be 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts or 14 parts.

[0030] The amount of the auxiliary emulsifier added can be 3.2 parts, 3.5 parts, 3.8 parts, 4 parts, 4.2 parts, 4.5 parts, 4.8 parts, 5 parts, 5.2 parts, 5.5 parts, 5.8 parts, 6 parts, 6.2 parts, 6.5 parts or 6.8 parts, etc.

[0031] The amount of the polyol added can be 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts or 19 parts, etc.

[0032] The added amount of the oil can be 52 parts, 55 parts, 58 parts, 60 parts, 62 parts, 65 parts, 68 parts, 70 parts, 72 parts, 75 parts or 78 parts, etc.

[0033] The amount of water added can be 2 parts, 4 parts, 5 parts, 7 parts, 9 parts, 10 parts, 12 parts or 14 parts, etc.

[0034] Preferably, the oil comprises any one or a combination of at least two of ethylhexyl stearate, cetyl ethylhexanoate, triethylhexanoin, propylene glycol dicaprylate / dicaprate, butylene glycol dicaprylate / dicaprate, sunflower seed oil, olive oil, dicaprylyl carbonate, caprylic / capric triglyceride or C9-19 alkanes.

[0035] Preferably, the oil comprises C9-19 alkanes, butylene glycol dicaprylate / dicaprate and cetyl ethylhexanoate.

[0036] Preferably, the mass percentage of the C9-19 alkane in the makeup remover gel is 10-40%, for example, 12%, 15%, 18%, 20%, 22%, 25%, 28%, 30%, 32%, 35% or 38%.

[0037] Preferably, the mass percentage of butylene glycol dicaprylate / dicaprate in the makeup remover gel is 15-35%, for example, it can be 16%, 18%, 20%, 22%, 25%, 28%, 30%, 32% or 34%.

[0038] Preferably, the polyol includes any one or a combination of at least two of glycerol, butylene glycol, 1,3-propylene glycol, isoprene glycol or ethylhexylglycerin.

[0039] Preferably, the auxiliary emulsifier includes any one of laureth-3, polysorbate-20, polysorbate-60 or polysorbate-85, or a combination of at least two thereof.

[0040] Preferably, the auxiliary emulsifier is a combination of polysorbate-20 and laureth-3.

[0041] Preferably, the mass ratio of polysorbate 20 to laureth-3 may be 1:(1-4), for example, 1:1.1, 1:1.3, 1:1.5, 1:1.8, 1:2, 1:2.2, 1:2.5, 1:2.8, 1:3, 1:3.2, 1:3.5 or 1:3.8, etc.

[0042] Preferably, the makeup remover gel further comprises 0.1-2 parts of a skin conditioner by weight, for example, 0.2 parts, 0.5 parts, 0.7 parts, 1 part, 1.2 parts, 1.5 parts, 1.7 parts or 1.9 parts.

[0043] Preferably, the skin conditioning agent comprises any one of purslane extract, purslane extract, hydrolyzed ginsenosides or Centella asiatica extract, or a combination of at least two thereof.

[0044] Preferably, the skin conditioning agent is Centella asiatica extract and hydrolyzed ginsenosides.

[0045] Preferably, the mass ratio of the Centella asiatica extract to the hydrolyzed ginsenosides can be 1:(0.01-5), for example, it can be 1:0.02, 1:0.05, 1:0.08, 1:0.1, 1:0.3, 1:0.5, 1:0.8, 1:1, 1:1.2, 1:1.5, 1:1.8, 1:2, 1:2.2, 1:2.5, 1:2.8, 1:3, 1:3.2, 1:3.5, 1:3.8, 1:4, 1:4.2, 1:4.5 or 1:4.8, etc.

[0046] Preferably, the makeup remover gel further comprises any one or a combination of at least two of a preservative, a pH adjuster or a fragrance.

[0047] Any specific point value within the above numerical range can be selected and will not be described in detail here.

[0048] In a fifth aspect, the present invention provides a method for preparing the makeup remover gel according to the fourth aspect, the method comprising: first, mixing and homogenizing a polyol, an emulsifying composition, and an auxiliary emulsifier, then adding oil and mixing and homogenizing, and finally adding water and homogenizing to obtain the makeup remover gel;

[0049] Preferably, the step of adding oil and mixing homogenously further includes adding any one of a skin conditioner, a preservative, a pH regulator or a fragrance, or a combination of at least two of them.

[0050] Preferably, the homogenization temperature is independently 30-40°C, for example, 31°C, 33°C, 35°C, 37°C or 39°C.

[0051] Any specific point value within the above numerical range can be selected and will not be described in detail here.

[0052] Compared with the prior art, the present invention has the following beneficial effects:

[0053] (1) When the emulsified composition of the present invention is used for cosmetics prepared by the D-phase emulsification method, the heating process and the cooling process can be greatly reduced, the use of cooling water can be reduced, energy can be saved, a lot of energy can be saved, the process can be simplified, the process time can be shortened, the production efficiency of the product can be improved, and the production cost can be greatly reduced.

[0054] (2) The emulsified particle size of the emulsified composition of the present invention is smaller than that of ordinary emulsions after being used in cosmetics, and the particle size distribution range is narrower, creating a better skin feel and having higher kinetic stability. The smaller particle size helps to effectively deliver active ingredients to the skin, and can be used as a potential carrier of cosmetic ingredients, so that the active ingredients can be optimally dispersed in specific skin layers, with better efficacy. In addition, the smaller particle size can quickly penetrate deep into the skin and pores, better washing away makeup and dirt.

[0055] (3) The makeup remover gel provided by the present invention is mixed with components such as polyols and oils through a specific emulsifying composition, which can improve the emulsification effect of the product. A small amount of water can form a bicontinuous phase structure, thereby making the makeup remover more effective. DETAILED DESCRIPTION

[0056] The technical solution of the present invention is further described below by way of specific embodiments. It should be understood by those skilled in the art that the embodiments are merely to help understand the present invention and should not be regarded as specific limitations of the present invention.

[0057] Some of the materials and brand information involved in the following examples and comparative examples are shown in Table 1:

[0058] Table 1

[0059]

[0060] The rest of the raw materials can be used as long as they are purchased from regular dealers.

[0061] Example 1

[0062] This embodiment provides an emulsified composition comprising 75 parts of glycerol, 20 parts of sucrose fatty acid ester and 5 parts of polyglyceryl-10 laurate;

[0063] The sucrose fatty acid esters are sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate in a mass ratio of 3:0.5:1:1;

[0064] The preparation method of the emulsified composition is:

[0065] The polyol, sucrose fatty acid ester and polyglycerol fatty acid ester are mixed and homogenized at 90° C. to obtain the emulsified composition.

[0066] Example 2

[0067] This embodiment provides an emulsified composition comprising 82 parts of a polyol (41 parts each of glycerol and butylene glycol), 10 parts of a sucrose fatty acid ester, and 8 parts of polyglyceryl-10 laurate;

[0068] The sucrose fatty acid esters are sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate in a mass ratio of 5:0.8:2:3;

[0069] The preparation method of the emulsified composition is as described in Example 1.

[0070] Example 3

[0071] This embodiment provides an emulsified composition comprising 70 parts of glycerol, 26 parts of sucrose fatty acid ester and 4 parts of polyglyceryl-10 laurate;

[0072] The sucrose fatty acid esters are sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate in a mass ratio of 8:0.15:3:1;

[0073] The preparation method of the emulsified composition is as described in Example 1.

[0074] Example 4

[0075] This embodiment provides an emulsified composition, which differs from Example 1 only in that sucrose fatty acid ester does not include sucrose laurate, and its reduced amount is distributed among sucrose dilaurate, sucrose palmitate and sucrose stearate in proportion. The remaining components are consistent with those in Example 1, and the preparation method refers to Example 1.

[0076] Example 5

[0077] This embodiment provides an emulsified composition, which differs from Example 1 only in that sucrose dilaurate is not included in the sucrose fatty acid ester, and its reduced amount is distributed among sucrose laurate, sucrose palmitate and sucrose stearate in proportion. The remaining components are consistent with those in Example 1, and the preparation method refers to Example 1.

[0078] Example 6

[0079] This embodiment provides an emulsified composition, which differs from Example 1 only in that sucrose fatty acid esters do not include sucrose palmitate, and the reduced amount thereof is distributed among sucrose laurate, sucrose dilaurate and sucrose stearate in proportion. The remaining components are consistent with those in Example 1, and the preparation method refers to Example 1.

[0080] Example 7

[0081] This embodiment provides an emulsified composition, which differs from Example 1 only in that sucrose fatty acid ester does not include sucrose stearate, and its reduced amount is distributed among sucrose laurate, sucrose dilaurate and sucrose palmitate in proportion. The remaining components are consistent with those in Example 1, and the preparation method refers to Example 1.

[0082] Comparative Example 1

[0083] This comparative example provides an emulsified composition, which differs from Example 1 only in that the emulsified composition does not contain polyols and the ratio of sucrose fatty acid ester to polyglycerol-10 laurate remains unchanged. The preparation method is similar to that of Example 1.

[0084] Comparative Example 2

[0085] This comparative example provides an emulsified composition, which differs from Example 1 only in that the emulsified composition does not contain sucrose fatty acid ester and the ratio of polyol to polyglycerol-10 laurate remains unchanged. The preparation method is similar to that of Example 1.

[0086] Comparative Example 3

[0087] This comparative example provides an emulsified composition, which differs from Example 1 only in that the emulsified composition does not contain polyglycerol-10 laurate and the ratio of polyol to sucrose fatty acid ester remains unchanged. The preparation method is similar to that of Example 1.

[0088] Application Examples 1-3

[0089] This application example provides three types of makeup remover gels. The components of the makeup remover gels are shown in Table 2 below. The amounts of each component in the table are in parts:

[0090] Table 2

[0091]

[0092] The preparation method of the makeup remover gel comprises:

[0093] First, the polyol, the emulsified composition and the auxiliary emulsifier are mixed and homogenized at 35° C., then the oil and the skin conditioner are added and mixed and homogenized at 35° C., and finally water is added and homogenized at 35° C. to obtain the makeup remover gel.

[0094] Application Examples 4-7

[0095] Application Examples 4-7 provide four makeup remover gels, which differ from Application Example 1 only in that the emulsified composition of Example 1 is replaced with the emulsified composition of Examples 4-7 in equal amounts, and the remaining components and amounts remain unchanged. The preparation method refers to Application Example 1.

[0096] Application Example 8

[0097] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the oil does not include C9-19 alkanes, and the reduced amount is supplemented by butylene glycol dicaprylate / dicaprate. The remaining components and added amounts are consistent with Application Example 1. The preparation method refers to Application Example 1.

[0098] Application Example 9

[0099] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the oil does not include butylene glycol dicaprylate / dicaprate, and the reduced amount is supplemented by C9-19 alkanes. The remaining components and addition amounts are consistent with Application Example 1. The preparation method refers to Application Example 1.

[0100] Application Example 10

[0101] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the auxiliary emulsifier does not include laureth-3, and its reduced amount is supplemented by polysorbate 20. The remaining components and added amounts are consistent with those in Application Example 1. The preparation method refers to Application Example 1.

[0102] Application Example 11

[0103] This application example provides a makeup remover gel, which differs from Application Example 1 only in that polysorbate 20 is not included in the auxiliary emulsifier, and its reduced amount is supplemented by laureth-3. The remaining components and addition amounts are consistent with those in Application Example 1. The preparation method refers to Application Example 1.

[0104] Application Example 12

[0105] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the components do not include a skin conditioner, and the reduced amount is supplemented by cetyl ethylhexanoate. The remaining components and added amounts are consistent with Application Example 1. The preparation method refers to Application Example 1.

[0106] Application Example 13

[0107] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the skin conditioner does not include hydrolyzed ginsenosides, and the reduced amount is supplemented by Centella asiatica extract. The remaining components and added amounts are consistent with Application Example 1. The preparation method refers to Application Example 1.

[0108] Application Example 14

[0109] This application example provides a makeup remover gel, which differs from Application Example 1 only in that the skin conditioner does not include Centella asiatica extract, and the reduced amount is supplemented by hydrolyzed ginsenosides. The remaining components and added amounts are consistent with Application Example 1. The preparation method refers to Application Example 1.

[0110] Comparative Application Examples 1-3

[0111] The comparative application examples 1-3 provide three makeup remover gels, which differ from application example 1 only in that the emulsified composition of Example 1 is replaced by the emulsified compositions of comparative examples 1-3 in equal amounts, and the remaining components and amounts remain unchanged. The preparation method refers to application example 1.

[0112] Test Example 1

[0113] Stability testing included high and low temperature, as well as thermal cycling tests. Samples from Application Examples 1-14 and Comparative Application Examples 1-3 were stored at -16°C, 25°C, and 45°C for three months, and the products were regularly observed for abnormalities such as turbidity, delamination, and color change. The test results are shown in Table 3.

[0114] Table 3

[0115]

[0116] It can be seen from the data in Table 3 that the makeup remover gel prepared using the emulsified composition of the present invention has good stability. If any component of the emulsified composition is missing, the makeup remover gel cannot be formed.

[0117] Test Example 2

[0118] Cleansing test for makeup (liquid foundation, lipstick, eyeliner):

[0119] Test subjects: 102 volunteers were divided into 17 groups, with 6 people in each group. The 17 groups of volunteers used the makeup remover gel prepared in Application Examples 1-14 and Comparative Application Examples 1-3 for cleansing.

[0120] The test method is as follows: apply liquid foundation, lipstick, and eyeliner on the inside of the subject's dry and clean arm. After the makeup is naturally dried, apply the makeup remover gel prepared in Application Examples 1-14 and Comparative Application Examples 1-3 to the corresponding makeup area (dosage: 0.8 g-1 g), apply evenly, massage in circles to dissolve the makeup, massage with a small amount of water to emulsify, and then rinse with water. Use a dermatoscope to photograph the test area before and after makeup application and after makeup removal, and use IPP software to analyze the images to obtain the lightness L, red / green value a, and blue / yellow value b of each area. Then calculate the color difference △E ( ), and calculate the cleaning rate C value ( ).

[0121] The results are shown in Table 4:

[0122] Table 4

[0123]

[0124] The data in Table 4 show that the makeup remover gel of the present invention has a very good makeup removal ability by adding the emulsified composition, and the makeup remover gel prepared using the phase D emulsified composition of the present invention has a more excellent makeup removal ability.

[0125] As can be seen from Application Examples 4-7, the formula of sucrose fatty acid ester also has a significant impact on the makeup removal effect of the makeup removal gel;

[0126] As can be seen from Application Examples 8-9, the lack of any one of the components, C9-19 alkane or butanediol dicaprylate / dicaprate, will lead to a significant decrease in the makeup removal ability of the system;

[0127] As shown in Application Examples 10-11, auxiliary emulsifiers can improve the makeup removal effect of the product, and laureth-3 and polysorbate 20 have a synergistic effect in improving the makeup removal effect;

[0128] It can be seen from comparative application examples 1-3 that the absence of any component in the emulsified composition cannot form a makeup remover gel, thereby affecting the makeup remover effect.

[0129] Test Example 3 Consumer Sensory Effect Evaluation

[0130] The test subjects were the same volunteers as in Test Example 2. Test Method: The test subjects used the makeup remover gels prepared in Application Examples 1-14 and Comparative Application Examples 1-3, respectively. The test subjects used their daily skincare products normally during the day. Every night, they applied an appropriate amount of gel to their hands, dried their hands and face, and massaged the gel in circular motions to dissolve the makeup. They then massaged the gel with a small amount of water to emulsify the makeup, and then rinsed it off with water. The products were then rated for mildness, skin feel, cleansing properties, and makeup removal. The average score was taken, and the evaluation results are shown in the table below. The 5-point scale is as follows: 4.5 points and above indicate excellent (very satisfactory); 4-4.5 points indicate good; 3-4 points indicate acceptable; and 3 points or less indicate poor (unacceptable). The scores for each group are the average of 10 participants, as shown in Table 5.

[0131] Table 5

[0132]

[0133] As shown in Table 5, the human body trial results of Application Examples 1-3 show that the makeup remover gel prepared using the emulsified composition of the present invention has a good user experience.

[0134] As can be seen from Application Examples 4-7, the formula of sucrose fatty acid ester also has a significant impact on the experience of makeup remover gel;

[0135] As shown in Application Examples 8-9, C9-19 alkanes and butylene glycol dicaprylate / dicaprate can improve the makeup removal ability and skin feel of the system;

[0136] As shown in Application Examples 10-11, the combination of auxiliary surfactants laureth-3 and polysorbate-20 can provide better cleaning and skin feel, but excessive addition of laureth-3 may affect mildness.

[0137] As shown in Application Examples 12-14, the addition of skin conditioners can increase the mildness and skin feel of the system, and the hydrolyzed ginsenosides and Centella asiatica extract have a synergistic effect;

[0138] It can be seen from comparative application examples 1-3 that the absence of any component in the emulsified composition cannot form a makeup remover gel, thereby affecting the experience.

[0139] Test Example 4 Safety Evaluation:

[0140] The specific method is as follows: 35 male and female subjects aged 18-55 years with no history of allergies were selected. Each subject was tested with the products prepared in Examples 1-14. Using a qualified patch tester, approximately 0.020ml to 0.025ml of the sample was added to the patch tester. The patch was then applied to the subject's flexed forearm using specialized adhesive tape. After 24 hours, the test substance was removed. Skin reactions were observed 30 minutes, 24 hours, and 48 hours after removal. Results were recorded according to the skin reaction grading standards (Table 6) in the "Safety Technical Specifications for Cosmetics" (2015 edition).

[0141] The grading standards for adverse skin reactions are shown in Table 6:

[0142] Table 6

[0143]

[0144] The results are shown in Table 7:

[0145] Table 7

[0146]

[0147] The data in Table 7 show that no adverse skin reactions were observed 30 minutes, 24 hours, and 48 hours after the spot tester was removed. This indicates that the makeup remover gel of the present invention has no adverse reactions on the human body and is highly safe.

[0148] The applicant declares that the present invention uses the above-mentioned embodiments to illustrate an emulsified composition, its preparation method, and its use. However, the present invention is not limited to the above-mentioned embodiments, and it does not mean that the present invention must rely on the above-mentioned embodiments in order to be implemented. Those skilled in the art should understand that any improvements to the present invention, equivalent replacements for the raw materials of the present invention, addition of auxiliary ingredients, and selection of specific methods, etc., are all within the scope of protection and disclosure of the present invention.

[0149] The preferred embodiments of the present invention are described in detail above. However, the present invention is not limited to the specific details in the above embodiments. Within the technical concept of the present invention, various simple modifications can be made to the technical solution of the present invention, and these simple modifications all fall within the scope of protection of the present invention.

[0150] It should also be noted that the various specific technical features described in the above specific embodiments can be combined in any appropriate manner without contradiction. In order to avoid unnecessary repetition, the present invention will not further describe various possible combinations.

Claims

1. An emulsified composition, characterized in that The emulsified composition comprises polyol, sucrose fatty acid ester and polyglycerol fatty acid ester; The sucrose fatty acid ester is a combination of sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate; The polyol includes glycerol and / or butylene glycol; The mass ratio of sucrose laurate, sucrose dilaurate, sucrose palmitate and sucrose stearate is (3-9): (0.1-2): (0.5-3): (0.5-3); The polyglycerol fatty acid ester is polyglyceryl-10 laurate.

2. The emulsified composition according to claim 1, characterized in that The emulsified composition comprises 60-90 parts of polyol, 10-30 parts of sucrose fatty acid ester and 1-10 parts of polyglycerol fatty acid ester in parts by weight.

3. A method for preparing an emulsion composition according to any one of claims 1 to 2, characterized in that: The preparation method comprises the steps of homogenizing polyol, sucrose fatty acid ester and polyglycerol fatty acid ester to obtain the emulsified composition.

4. Use of the emulsified composition according to any one of claims 1 to 2 in the preparation of cosmetics; The cosmetics include any one of essence, essence cream, facial cleanser or gel; The mass percentage of the emulsified composition in the cosmetic is 1-15%.

5. A makeup remover gel, characterized in that: The makeup remover gel comprises, by weight, 5-15 parts of the emulsified composition according to any one of claims 1 to 2, 3-7 parts of an auxiliary emulsifier, 5-20 parts of a polyol, 50-80 parts of oil, and 1-15 parts of water.

6. The makeup remover gel according to claim 5, characterized in that The oils include C9-19 alkanes, butylene glycol dicaprylate / dicaprate, and cetyl ethylhexanoate; The auxiliary emulsifier is a combination of laureth-3 and polysorbate-20.

7. The makeup remover gel according to claim 5, characterized in that The makeup remover gel further comprises 0.1-2 parts of a skin conditioner by weight; The skin conditioning agent comprises any one of purslane extract, hydrolyzed ginsenosides or Centella asiatica extract, or a combination of at least two thereof.

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