Three-dimensional water locking and moisturizing composition as well as preparation method and application thereof

Abstract

The invention relates to the technical field of daily chemicals, in particular to a three-dimensional water locking and moisturizing composition as well as a preparation method and application thereof. The composition is prepared from the following raw materials: a water phase, an oil phase and an emulsifier, wherein the oil phase is prepared from butyrospermum parkii (BUTYROSPERMUM PARKII) fruit fat, cetostearyl alcohol olivate, sorbitan olivate and polymethylsilsesquioxane, and the oil phase is prepared from the following raw materials of: butyrospermum parkii fruit fat, cetostearyl alcohol olivate, sorbitan olivate and polymethylsilsesquioxane The moisturizing lotion provided by the invention has double effects of moisturizing and locking water, contains the moisture absorbent, can absorb moisture in the environment and convey the moisture to the surface layer of the skin to help the skin keep moist; water locking: a humectant is contained, so that a protective film is formed on the skin surface, and water loss is reduced.

Description

Technical Field

[0001] The present invention relates to the field of daily chemical technology, and in particular to a three-dimensional water-locking and moisturizing composition, a preparation method thereof, and an application thereof. Background Art

[0002] Skin moisturization is an important part of maintaining skin health. Skin water loss may lead to dryness, tightness, sensitivity of the skin, and even accelerate skin aging. When the skin barrier (stratum corneum) is damaged, water is more likely to evaporate. Common causes include over-cleaning, using irritating skin care products, frequent exfoliation, etc.

[0003] Common causes of skin water loss: 1. Skin barrier damage: When the skin barrier (stratum corneum) is damaged, water is more likely to evaporate. Common causes include over-cleaning, using irritating skin care products, frequent exfoliation, etc. Environmental factors: Dry air, cold weather, or staying in an air-conditioned room for a long time will accelerate water evaporation. Ultraviolet radiation can also damage the skin barrier, resulting in water loss. 3. Lifestyle habits: Insufficient water intake, excessive consumption of caffeinated or alcoholic beverages will reduce the water content of the skin. Lack of sleep or high stress may affect the skin's repair ability.

[0004] Effective methods to reduce skin water loss: 1. Repair the skin barrier: Use skin care products containing ceramides, cholesterol, and fatty acids, which can strengthen the skin barrier. Avoid frequent use of acid products (such as fruit acids, AHAs), especially when the skin is sensitive. 2. Increase the moisturizing step: Hydration + water locking: First use a hydrating product (such as a serum containing hyaluronic acid), and then use a occlusive moisturizing product (such as a cream containing petrolatum or mineral oil) to lock in the moisture. After using a spray, remember to gently pat the excess water with a tissue and apply a moisturizer in a timely manner.

[0005] In an extremely dry environment, certain types of moisturizing lotions may indeed cause an exacerbation of skin water loss. This phenomenon is usually related to the ingredients of the moisturizing product, especially its hygroscopic ingredients (such as glycerin, urea, hyaluronic acid, etc.). Hygroscopic ingredients (such as glycerin, hyaluronic acid, propylene glycol) absorb water from the environment and transport it to the skin stratum corneum to help keep the skin moisturized; however, if the humidity of the surrounding environment is extremely low (usually below 30%), the hygroscopic ingredients may instead draw water from the deeper layers of the skin, causing the water to evaporate from the skin into the air and exacerbating dryness. If the skin barrier function is weak and cannot effectively lock in moisture, even if a moisturizing lotion is used, the water will quickly be lost through transepidermal water loss (TEWL).

[0006] In view of this, the present invention provides a three-dimensional water-locking and moisturizing composition, a preparation method thereof, and an application thereof. Summary of the Invention

[0007] To solve the above technical problems, the present invention provides a three-dimensional water-locking composition, and the preparation raw materials of the composition include: an aqueous phase, an oil phase, and an emulsifier;

[0008] Among them, the oil phase includes: shea (BUTYROSPERMUM PARKII) fruit butter, cetearyl olivate, sorbitan olivate, polydimethylsiloxane.

[0009] As an embodiment of the present invention, the viscosity of the polydimethylsiloxane is 1.0 - 3.0 cps at 25 °C.

[0010] As an embodiment of the present invention, the composition further includes citrus (CITRUS RETICULATA) peel extract, which is prepared by a fermentation method.

[0011] As an embodiment of the present invention, the preparation raw materials of the composition further include: cetyl ethylhexanoate, common citron (CITRUS MEDICA VULGARIS) peel oil, tangerine (CITRUS TANGERINA) peel oil.

[0012] The present invention provides a three-dimensional water-locking moisturizing milk, which is prepared from the three-dimensional water-locking composition.

[0013] As an embodiment of the present invention, the preparation raw materials of a three-dimensional water-locking moisturizing milk include:

[0014] Raw materials of phase A: isononyl isononanoate, PEG-100 stearate, glyceryl stearate, cetearyl alcohol, shea (BUTYROSPERMUM PARKII) fruit butter, cetearyl olivate, sorbitan olivate, polydimethylsiloxane;

[0015] Raw materials of phase B: water, glycerol, butanediol, betaine, carbomer, hydrogenated lecithin, disodium EDTA;

[0016] Raw materials of phase C: water, arginine;

[0017] Raw materials of phase D: butanediol, octanoyl hydroxamic acid;

[0018] Raw materials of phase E: water, niacinamide;

[0019] Raw materials of phase F: water, ectoine;

[0020] Raw materials of phase G: water, lauryl polydimethylsiloxane / polyglycerol-3 cross-linked polymer, polymethylsilsesquioxane, caprylyl glycol, phenoxyethanol;

[0021] Phase H raw materials: Cordyceps sinensis extract, 1,3 - propanediol, 1,2 - hexanediol, filtrate of Saccharomyces cerevisiae var. ellipsoideus fermentation product, p - hydroxyacetophenone, ethylhexylglycerin, Cynanchum atratum extract, Sophora angustifolia root extract, Gynostemma pentaphyllum extract, xylitol - based glucoside, dehydrated xylitol, xylitol, Prunus speciosa flower extract, maltooligosaccharide glucoside, hydrogenated starch hydrolysate, bisabolol, isocetane, cetyl alcohol ethylhexanoate, Citrus medica vulgaris peel oil, Citrus tangerina peel oil;

[0022] Phase I raw materials: water, Thermus thermophilus fermentation product fraction, soluble collagen, butanediol, ethylhexylglycerin.

[0023] As an embodiment of the present invention, by mass fraction, the raw materials for preparing the moisturizing milk include:

[0024] Phase A raw materials: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of Butyrospermum parkii fruit butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0025] Phase B raw materials: 30 parts of water, 5 parts of glycerin, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0026] Phase C raw materials: 5 parts of water, 0.22 part of arginine;

[0027] Phase D raw materials: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0028] Phase E raw materials: 5 parts of water, 0.11 part of niacinamide;

[0029] Phase F raw materials: 5 parts of water, 0.11 part of ectoine;

[0030] Phase G raw materials: 30.69 parts of water, 0.3 part of lauryl poly(dimethylsiloxane) / polyglycerol - 3 cross - polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of octyldecanol, 0.1 part of phenoxyethanol;

[0031] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of filtrate of fermentation product of galactomyces-like yeast, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitol glucoside, 0.1 part of dehydrated xylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of malt oligosaccharide glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0032] Phase I raw materials: 0.1 part of water, 0.001 part of Thermus thermophilus fermentation product, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0033] As an embodiment of the present invention, the preparation method of the three-dimensional stereoscopic water-locking and moisturizing milk is as follows:

[0034] S1. Do a good job in sanitation and cleaning, and strictly clean and disinfect the equipment and utensils used;

[0035] S2. Put the Phase A raw materials into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside;

[0036] S3. Put the Phase B raw materials into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump the Phase A into the emulsifying pan, homogenize and stir evenly, add the Phase C raw materials, homogenize and stir evenly, and then cool down;

[0037] S4. Cool down to 60 - 65 °C, add the pre-dissolved Phase D raw materials, stir evenly, and continue to cool down;

[0038] S5. Cool down to 40 - 45 °C, add the Phase H, Phase I and the pre-dissolved Phase E, Phase F, Phase G raw materials, stir evenly;

[0039] S6. Send for inspection, after passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling, and that's it.

[0040] As an embodiment of the present invention, the raw materials of phases D, E, F, and G are pre-dissolved before being added to the pot.

[0041] As an embodiment of the present invention, the three-dimensional stereoscopic water-locking and moisturizing milk is applied to the daily chemical field.

[0042] Adopting the above technical solution, the present invention has the following beneficial effects:

[0043] 1. Dual effects: moisturizing + water locking. It contains hygroscopic agents that can absorb moisture in the environment and transport it to the skin surface to help the skin stay moist; water locking: it contains moisturizing agents that form a protective film on the skin surface to reduce water loss.

[0044] 2. Suitable for different skin types: The moisturizing milk of the nourishing type provides deep nourishment. It does not clog pores and balances water and oil at the same time. The formula is mild, without alcohol or fragrance, reducing the risk of irritation.

[0045] 3. The texture of the milk is between that of a cream and a gel, with good ductility. It can be quickly absorbed after application and does not feel heavy or sticky.

[0046] 4. The moisturizing milk can provide water support for the skin for a long time and prevent skin dryness caused by environmental factors (such as wind, cold or air-conditioned rooms). Specific embodiments

[0047] The technical solution of the present invention will be described clearly and completely below. Obviously, the described embodiments are part of the embodiments of the present invention, rather than all of them. All other embodiments obtained by those of ordinary skill in the art based on the embodiments of the present invention without creative efforts shall fall within the protection scope of the present invention.

[0048] The present invention provides a three-dimensional stereoscopic water-locking and moisturizing milk. According to parts by mass, the raw materials for preparing the moisturizing milk include:

[0049] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG-100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0050] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0051] Raw materials of phase C: 5 parts of water, 0.22 part of arginine;

[0052] Raw materials for Phase D: 1 part of butanediol and 0.05 part of octanoyl hydroxamic acid;

[0053] Raw materials for Phase E: 5 parts of water and 0.11 part of niacinamide;

[0054] Raw materials for Phase F: 5 parts of water and 0.11 part of ectoine;

[0055] Raw materials for Phase G: 30.69 parts of water, 0.3 part of lauryl dimethicone / polyglycerin-3 cross-linked polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0056] Raw materials for Phase H: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of galactomyces ferment filtrate, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitol glucoside, 0.1 part of anhydroxylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltodextrin glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0057] Raw materials for Phase I: 0.1 part of water, 0.001 part of Thermus thermophilus fermentation product, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0058] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0059] (1) Wash and dry the Cordyceps sinensis, then crush and sieve it; wash and dry the citrus peel, then cut it into pieces;

[0060] (2) Mix the Cordyceps sinensis powder and the citrus peel pieces, add them to the culture medium and mix evenly. Then continue to inoculate the strain, with an inoculation amount of 10%. After aerobic fermentation at 28°C for 72 hours, filter to remove the residue to obtain the Cordyceps sinensis extract.

[0061] Among them, the strain is Candida rugosa 32586 and Aspergillus niger 40048; the inoculation ratio is 3:2.

[0062] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of plant peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0063] The preparation methods of the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and the pericarp oil of big red tangerine (CITRUS TANGERINA) are as follows:

[0064] (1) Cut the pericarp of common citron (CITRUS MEDICA VULGARIS) and the pericarp of big red tangerine (CITRUS TANGERINA), add them to the culture medium and mix evenly, then continue to inoculate the strain with an inoculation amount of 8%, ferment aerobically at 28°C for 72 h, filter to remove the residue, and then stand to obtain the oil layer to get the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and the pericarp oil of big red tangerine (CITRUS TANGERINA).

[0065] Among them, the strain is Hanseniaspora uvarum 1959 and Aspergillus niger 40048; the inoculation ratio is 2:2.

[0066] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of plant peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 20.2 g of O, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and make up to 1000 mL with distilled water.

[0067] The polydimethylsiloxane described in the present invention is: a mixture of a polydimethylsiloxane with a viscosity of 1.0 - 3.0 cps at 25°C, purchased from Slokchem, model Sicare 2942; and a polydimethylsiloxane with a viscosity of 6 cps at 25°C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, with a mixing ratio of 3:1.

[0068] The polymethylsilsesquioxane described in the present invention is purchased from Slokchem, model Sicare 2115F.

[0069] The moisturizing milk prepared in the present invention will not cause skin dryness even in an extremely dry environment. Glycerol, PEG-100 stearate, etc. added to conventional moisturizing milks can maintain a good moisturizing effect in a relatively moist environment. However, in extremely dry air, they will reverse-adsorb the moisture on the skin surface, thus accelerating skin dryness. The conventional method is to use cream-like skin care products to achieve moisturization of the skin surface; however, cream-like skin care products are relatively greasy for oily or combination skin and can also cause the appearance of clogged pores and acne.

[0070] Therefore, through research on the fermentation process of Cordyceps sinensis, through the selection of the culture medium, the selection of strains, and the research on symbiotic fermentation, it is found that more cordycepic acid in Cordyceps sinensis prepared by the present invention is esterified, thus achieving fat-soluble absorption and not only absorbing on the skin surface, so as to achieve deeper skin moisturization. At the same time, adding citrus peel during the fermentation of Cordyceps sinensis can stimulate the absorption of adenosine in Cordyceps sinensis and further restore the skin barrier; in addition, adding cetyl ethylhexanoate, Citrus medica vulgaris peel oil, Citrus tangerina peel oil and other oily moisturizing components, combined with polydimethylsiloxanes with different molecular weights, achieves good moisturization without producing too much greasiness; and there will be no result of reverse skin dryness in an extremely dry environment.

[0071] The following further explains the present invention in combination with specific embodiments.

[0072] Example 1

[0073] This example provides a three-dimensional water-locking moisturizing milk. By mass, the raw materials for preparing the moisturizing milk include:

[0074] Phase A Raw Materials: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea butter (BUTYROSPERMUM PARKII) fruit butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0075] Phase B Raw Materials: 30 parts of water, 5 parts of glycerin, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0076] Phase C Raw Materials: 5 parts of water, 0.22 part of arginine;

[0077] Phase D Raw Materials: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0078] Phase E Raw Materials: 5 parts of water, 0.11 part of niacinamide;

[0079] Phase F Raw Materials: 5 parts of water, 0.11 part of ectoine;

[0080] Phase G Raw Materials: 30.69 parts of water, 0.3 part of lauryl dimethicone / polyglycerin - 3 cross - polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0081] Phase H Raw Materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3 - propanediol, 0.15 part of 1,2 - hexanediol, 1 part of filtrate of galactomyces ferment filtrate, 0.05 part of p - hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitylglucoside, 0.1 part of anhydroxylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltodextrin glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0082] Phase I raw materials: 0.1 part of water, 0.001 part of fermentation product of THERMUS THERMOPHILLUS, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0083] Among them, the preparation method of the CORDYCEPS SINENSIS extract is as follows:

[0084] (3) Wash and dry the CORDYCEPS SINENSIS, then crush and sieve it; wash and dry the citrus peel, then cut it into pieces.

[0085] (4) Mix the CORDYCEPS SINENSIS powder and the cut citrus peel, add them to the culture medium and mix evenly. Then continue to inoculate the strain, with an inoculation amount of 10%. After aerobic fermentation at 28°C for 72 hours, filter to remove the residue to obtain the CORDYCEPS SINENSIS extract.

[0086] Among them, the mass ratio of the CORDYCEPS SINENSIS powder to the citrus peel is 4:1.

[0087] Among them, the strain is Candida rugosa 32586 and Aspergillus niger 40048; the inoculation amount ratio is 3:2.

[0088] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of plant peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0089] The preparation methods of the CITRUS MEDICA VULGARIS peel oil and the CITRUS TANGERINA peel oil are as follows:

[0090] (1) Chop the peels of common citron (CITRUS MEDICA VULGARIS) and big red tangerine (CITRUS TANGERINA), add them to the culture medium and mix evenly. Then continue to inoculate with the strains, and the inoculation amount is 8%. After aerobic fermentation at 28 °C for 72 h, filter to remove the residue, and let it stand to obtain the oil layer of the peel of common citron (CITRUS MEDICA VULGARIS) and the oil layer of the peel of big red tangerine (CITRUS TANGERINA).

[0091] Among them, the strain is Hanseniaspora uvarum and Aspergillus niger 1959 and Aspergillus niger 40048; the inoculation amount ratio is 2:2.

[0092] The components of the culture medium include: beef extract powder 3.0 g, peptone 10.0 g, tryptone (BBL) 5.0 g, vegetable peptone 3.0 g, yeast extract powder 5.0 g, glucose 10.0 g, soluble starch 0.5 g, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 5% L-cysteine hydrochloride solution 10.0 mL, Tween 80 1.0 g, and distilled water is added to make up to 1000 mL.

[0093] In this example, the polydimethylsiloxane is: with a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slokker, model Sicare 2942; and with a viscosity of 6 cps at 25 °C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, and the mixing ratio is 3:1.

[0094] In this example, the polymethylsilsesquioxane is purchased from Slokker, model Sicare 2115F.

[0095] The preparation method of the three-dimensional moisture-locking and moisturizing milk is as follows:

[0096] S1. Do a good job in sanitation and cleaning, and strictly clean and disinfect the equipment and utensils used;

[0097] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside;

[0098] S3. Put the raw materials of phase B into the emulsifying pot in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure complete dissolution of the material, pump the raw materials of phase A into the emulsifying pot, homogenize and stir evenly, add the raw materials of phase C, homogenize and stir evenly, and then cool down;

[0099] S4. Cool down to 60 - 65 °C, add the pre - dissolved raw materials of phase D, stir evenly, and continue to cool down;

[0100] S5. Cool down to 40 - 45 °C, add the raw materials of phases H and I and the pre - dissolved raw materials of phases E, F, and G, stir evenly;

[0101] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro - inspection, pour the material into the filling machine for filling, and that's it.

[0102] Example 2

[0103] This example provides a three - dimensional stereoscopic water - locking and moisturizing milk. By mass, the raw materials for preparing the moisturizing milk include:

[0104] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0105] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0106] Raw materials of phase C: 5 parts of water, 0.22 part of arginine;

[0107] Raw materials of phase D: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0108] Raw materials of phase E: 5 parts of water, 0.11 part of niacinamide;

[0109] Raw materials of phase F: 5 parts of water, 0.11 part of ectoine;

[0110] Raw materials of phase G: 30.69 parts of water, 0.3 part of lauryl poly(dimethylsiloxane) / polyglycerol - 3 cross - polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0111] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3 - propanediol, 0.15 part of 1,2 - hexanediol, 1 part of filtrate of fermentation product of galactomyces - like yeast, 0.05 part of p - hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitol - based glucoside, 0.1 part of dehydrated xylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltooligosaccharide glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl alcohol ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0112] Phase I raw materials: 0.1 part of water, 0.001 part of Thermus thermophilus fermentation product, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0113] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0114] (1) Wash and dry the Cordyceps sinensis, then crush and sieve it;

[0115] (2) Add the Cordyceps sinensis powder to the culture medium and mix evenly, then continue to inoculate the strain, the inoculation amount is 10%, ferment aerobically at 28°C for 72 h, and then filter to remove the residue to obtain the Cordyceps sinensis extract.

[0116] Among them, the strain is Candida rugosa 32586 and Aspergillus niger 40048; the inoculation ratio is 3:2.

[0117] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of plant peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 41.0 g, MgSO 4 ·7H 2 O 0.2 g, 5% L-cysteine hydrochloride solution 10.0 mL, Tween 80 1.0 g, made up to 1000 mL with distilled water.

[0118] The preparation methods of the pericarp oil of Citrus medica vulgaris and the pericarp oil of Citrus tangerina are as follows:

[0119] (1) Cut the pericarp of Citrus medica vulgaris and the pericarp of Citrus tangerina, add them to the culture medium and mix evenly. Then continue to inoculate the strains, with an inoculation amount of 8%. After aerobic fermentation at 28 °C for 72 h, filter to remove the residue, and let it stand to obtain the oil layer to get the pericarp oil of Citrus medica vulgaris and the pericarp oil of Citrus tangerina.

[0120] Among them, the strain is Hanseniaspora uvarum 1959 and Aspergillus niger 40048; the inoculation ratio is 2:2. 1959 and Aspergillus niger 40048; the inoculation ratio is 2:2.

[0121] The components of the culture medium include: beef extract powder 3.0 g, peptone 10.0 g, tryptone (BBL) 5.0 g, vegetable peptone 3.0 g, yeast extract powder 5.0 g, glucose 10.0 g, soluble starch 0.5 g, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 5% L-cysteine hydrochloride solution 10.0 mL, Tween 80 1.0 g, made up to 1000 mL with distilled water.

[0122] In this example, the polydimethylsiloxane is: with a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slok, model Sicare 2942; and with a viscosity of 6 cps at 25 °C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, and the mixing ratio is 3:1.

[0123] In this example, the polymethylsilsesquioxane is purchased from Slok, model Sicare 2115F.

[0124] The preparation method of the described three-dimensional water-locking moisturizing milk is as follows:

[0125] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used;

[0126] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside;

[0127] S3. Put the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, homogenize and stir evenly, and then cool down;

[0128] S4. Cool down to 60 - 65 °C, add the pre-dissolved raw materials of phase D, stir evenly, and continue to cool down;

[0129] S5. Cool down to 40 - 45 °C, add phases H and I and the pre-dissolved raw materials of phases E, F, and G, and stir evenly;

[0130] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling, and that's it.

[0131] Example 3

[0132] This example provides a three-dimensional water-locking moisturizing milk. By mass, the raw materials for preparing the moisturizing milk include:

[0133] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) fruit butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0134] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0135] Raw materials of phase C: 5 parts of water, 0.22 part of arginine;

[0136] Raw materials of phase D: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0137] Raw materials of phase E: 5 parts of water, 0.11 part of niacinamide;

[0138] Raw materials of phase F: 5 parts of water, 0.11 part of ectoine;

[0139] Phase G raw materials: 30.69 parts of water, 0.3 part of lauryl dimethicone / polyglycerol-3 cross-linked polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of octyldecanol, 0.1 part of phenoxyethanol;

[0140] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of filtrate of Saccharomyces cerevisiae fermentation product, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitol glucoside, 0.1 part of dehydrated xylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltodextrin glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isododecane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0141] Phase I raw materials: 0.1 part of water, 0.001 part of Thermus thermophilus fermentation product, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0142] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0143] (1) Wash and dry the Cordyceps sinensis, then crush and sieve it; wash and dry the citrus peel, then cut it into pieces;

[0144] (2) Mix the Cordyceps sinensis powder and the citrus peel pieces, add them to the culture medium and mix evenly, then continue to inoculate the strain, the inoculation amount is 10%, ferment aerobically at 28°C for 72 hours, filter to remove the residue, and obtain the Cordyceps sinensis extract.

[0145] Among them, the mass ratio of the Cordyceps sinensis powder to the citrus peel is 4:1.

[0146] Among them, the strain is Candida rugosa 32586.

[0147] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0148] The preparation methods of the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA) are as follows:

[0149] (1) Chop the pericarp of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA), add them to the culture medium and mix evenly. Then continue to inoculate the strain, with an inoculation amount of 8%. After aerobic fermentation at 28°C for 72 h, filter to remove the residue, and then let it stand to obtain the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA) by taking the oil layer.

[0150] Among them, the strain is Hanseniaspora 1959 and Aspergillus 40048; the inoculation amount ratio is 2:2.

[0151] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0152] In this example, the polydimethylsiloxane is as follows: with a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slokchem, model Sicare 2942; and with a viscosity of 6 cps at 25 °C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, and they are mixed in a ratio of 3:1.

[0153] In this example, the polymethylsilsesquioxane is purchased from Slokchem, model Sicare 2115F.

[0154] The preparation method of the three-dimensional stereoscopic water-locking and moisturizing milk is as follows:

[0155] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used.

[0156] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside.

[0157] S3. Put the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, and homogenize and stir evenly before cooling down.

[0158] S4. Cool down to 60 - 65 °C, add the pre-dissolved raw materials of phase D, stir evenly, and continue to cool down.

[0159] S5. Cool down to 40 - 45 °C, add phases H and I and the pre-dissolved raw materials of phases E, F, and G, and stir evenly.

[0160] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling.

[0161] Example 4

[0162] This example provides a three-dimensional stereoscopic water-locking and moisturizing milk. According to mass parts, the raw materials for preparing the moisturizing milk include:

[0163] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG-100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0164] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0165] Phase C raw materials: 5 parts of water, 0.22 parts of arginine;

[0166] Phase D raw materials: 1 part of butanediol, 0.05 parts of octanoyl hydroxamic acid;

[0167] Phase E raw materials: 5 parts of water, 0.11 parts of niacinamide;

[0168] Phase F raw materials: 5 parts of water, 0.11 parts of ectoine;

[0169] Phase G raw materials: 30.69 parts of water, 0.3 parts of lauryl dimethicone / polyglycerin-3 cross-linked polymer, 0.3 parts of polymethylsilsesquioxane, 0.1 parts of caprylyl glycol, 0.1 parts of phenoxyethanol;

[0170] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 parts of 1,2-hexanediol, 1 part of galactomyces ferment filtrate, 0.05 parts of p-hydroxyacetophenone, 0.1 parts of ethylhexylglycerin, 0.05 parts of Cynanchum atratum extract, 0.1 parts of Sophora angustifolia root extract, 0.1 parts of Gynostemma pentaphyllum extract, 0.1 parts of xylitylglucoside, 0.1 parts of anhydroxylitol, 0.1 parts of xylitol, 0.4 parts of Prunus speciosa flower extract, 0.1 parts of maltodextrin glucoside, 0.1 parts of hydrogenated starch hydrolysate, 0.11 parts of bisabolol, 0.05 parts of isocetane, 0.1 parts of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0171] Phase I raw materials: 0.1 part of water, 0.001 parts of Thermus thermophilus fermentation product, 0.001 parts of soluble collagen, 0.001 parts of butanediol, 0.001 parts of ethylhexylglycerin.

[0172] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0173] (1) After washing and drying the Cordyceps sinensis, crush it and sieve it; after washing and drying the citrus peel, cut it into pieces;

[0174] (2) Mix the cordyceps sinensis powder and the citrus peel shreds (wherein, the mass ratio of the cordyceps sinensis powder to the citrus peel is 4:1), and obtain an extract by water extraction method. The solid-liquid ratio is 1:10, the solvent is distilled water, the extraction temperature is 80 °C, and the extraction time is 2 h; after extraction, filter and concentrate the filtrate to the same volume as that in Example 1.

[0175] The preparation methods of the pericarp oil of the common citron (CITRUS MEDICA VULGARIS) and the pericarp oil of the big red tangerine (CITRUS TANGERINA) are as follows:

[0176] (1) Chop the pericarp of the common citron (CITRUS MEDICA VULGARIS) and the pericarp of the big red tangerine (CITRUS TANGERINA), add them to the culture medium and mix evenly. Then continue to inoculate the strain, and the inoculation amount is 8%. After aerobic fermentation at 28 °C for 72 h, filter to remove the residue, and then let it stand to obtain the oil layer of the pericarp oil of the common citron (CITRUS MEDICA VULGARIS) and the pericarp oil of the big red tangerine (CITRUS TANGERINA).

[0177] Among them, the strain is Hanseniaspora uvarum 1959 and Aspergillus niger 40048; the inoculation amount ratio is 2:2. 1959 and Aspergillus niger 40048; the inoculation amount ratio is 2:2.

[0178] The components of the culture medium include: beef extract powder 3.0 g, peptone 10.0 g, tryptone (BBL) 5.0 g, plant peptone 3.0 g, yeast extract powder 5.0 g, glucose 10.0 g, soluble starch 0.5 g, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 5% L-cysteine hydrochloride solution 10.0 mL, Tween 80 1.0 g, and distilled water is added to make up to 1000 mL.

[0179] The polydimethylsiloxane in this example is: a mixture of a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slokor, model Sicare 2942; and a viscosity of 6 cps at 25 °C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, and the mixing ratio is 3:1.

[0180] The polymethylsilsesquioxane in this example is purchased from Slokor, model Sicare 2115F.

[0181] The preparation method of the described three-dimensional water-locking and moisturizing milk is as follows:

[0182] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used;

[0183] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside;

[0184] S3. Put the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, and homogenize and stir evenly before cooling;

[0185] S4. Cool down to 60 - 65 °C, add the pre-dissolved raw materials of phase D, stir evenly, and continue to cool down;

[0186] S5. Cool down to 40 - 45 °C, add phases H and I and the pre-dissolved raw materials of phases E, F, and G, and stir evenly;

[0187] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling, and that's it.

[0188] Example 5

[0189] This example provides a three-dimensional water-locking and moisturizing milk. By mass, the raw materials for preparing the moisturizing milk include:

[0190] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0191] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0192] Raw materials of phase C: 5 parts of water, 0.22 part of arginine;

[0193] Raw materials of phase D: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0194] Raw materials of phase E: 5 parts of water, 0.11 part of niacinamide;

[0195] Raw materials of phase F: 5 parts of water, 0.11 part of ectoine;

[0196] Phase G raw materials: 30.69 parts of water, 0.3 part of lauryl dimethicone / polyglycerol-3 cross-linked polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0197] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of filtrate of Saccharomycopsis ferment, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitol glucoside, 0.1 part of dehydrated xylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltooligosaccharide glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0198] Phase I raw materials: 0.1 part of water, 0.001 part of Thermus thermophilus ferment, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0199] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0200] (5) Wash and dry Cordyceps sinensis, then crush and sieve it; wash and dry citrus peel, then cut it into pieces;

[0201] (6) Mix the Cordyceps sinensis powder and citrus peel pieces, add them to the culture medium and mix evenly. Then continue to inoculate the strain, with an inoculation amount of 10%. After aerobic fermentation at 28°C for 72 hours, filter to remove the residue to obtain the Cordyceps sinensis extract.

[0202] Among them, the strain is Candida rugosa 32586 and Aspergillus niger 40048; the inoculation amount ratio is 3:2.

[0203] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0204] The preparation methods of the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA) are as follows:

[0205] (1) Chop the pericarp of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA), add them to the culture medium and mix evenly. Then continue to inoculate the strain, with an inoculation amount of 8%. After aerobic fermentation at 28 °C for 72 h, filter to remove the residue, and then let it stand to obtain the oil layer, which is the pericarp oil of common citron (CITRUS MEDICA VULGARIS) and red tangerine (CITRUS TANGERINA).

[0206] Among them, the strain is Hanseniaspora 1959 and Aspergillus 40048; the inoculation amount ratio is 2:2.

[0207] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0208] The polydimethylsiloxane in the present invention is: with a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slok, model Sicare 2942.

[0209] In the present invention, the polymethylsilsesquioxane is purchased from Slokchem, with the model Sicare 2113.

[0210] The preparation method of the three-dimensional water-locking and moisturizing milk is as follows:

[0211] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used.

[0212] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside.

[0213] S3. Put the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, and homogenize and stir evenly before cooling down.

[0214] S4. Cool down to 60 - 65 °C, add the pre-dissolved raw materials of phase D, stir evenly, and continue to cool down.

[0215] S5. Cool down to 40 - 45 °C, add phases H and I and the pre-dissolved raw materials of phases E, F, and G, and stir evenly.

[0216] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling.

[0217] Example 6

[0218] This example provides a three-dimensional water-locking and moisturizing milk. According to mass parts, the preparation raw materials of the moisturizing milk include:

[0219] Raw materials of phase A: 5 parts of isononyl isononanoate, 0.5 part of PEG - 100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0220] Raw materials of phase B: 30 parts of water, 5 parts of glycerol, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0221] Raw materials of phase C: 5 parts of water, 0.22 part of arginine;

[0222] Raw materials of phase D: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0223] Raw materials of phase E: 5 parts of water, 0.11 part of niacinamide;

[0224] Phase F raw materials: 5 parts of water, 0.11 part of ectoine;

[0225] Phase G raw materials: 30.69 parts of water, 0.3 part of lauryl dimethicone / polyglycerin-3 cross-linked polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0226] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of filtrate of galactomyces ferment, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylityl glucoside, 0.1 part of anhydroxylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltodextrin glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isododecane, 2.6 parts of cetyl ethylhexanoate;

[0227] Phase I raw materials: 0.1 part of water, 0.001 part of Thermus thermophilus fermentation product, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0228] Among them, the preparation method of the Cordyceps sinensis extract is as follows:

[0229] (7) Wash and dry Cordyceps sinensis, then crush and sieve it; wash and dry citrus peel, then cut it into pieces;

[0230] (8) Mix the Cordyceps sinensis powder and citrus peel pieces (mass ratio 4:1), add them to the culture medium and mix evenly, then continue to inoculate the strain, the inoculation amount is 10%, ferment aerobically at 28°C for 72h, filter to remove the residue, and obtain the Cordyceps sinensis extract.

[0231] Among them, the strain is Candida rugosa 32586 and Aspergillus niger 40048; the inoculation amount ratio is 3:2.

[0232] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0233] In this example, the polydimethylsiloxane is: a mixture of one with a viscosity of 1.0 - 3.0 cps at 25 °C, purchased from Slokor, model Sicare 2942; and one with a viscosity of 6 cps at 25 °C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, with a mixing ratio of 3:1.

[0234] In this example, the polymethylsilsesquioxane is purchased from Slokor, model Sicare 2115F.

[0235] The preparation method of the three-dimensional moisture-locking and moisturizing lotion is as follows:

[0236] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used;

[0237] S2. Add the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85 °C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside;

[0238] S3. Add the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90 °C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, and homogenize and stir evenly before cooling;

[0239] S4. Cool down to 60 - 65 °C, add the pre-dissolved raw materials of phase D, stir well, and continue to cool down;

[0240] S5. Cool down to 40 - 45 °C, add phases H, I and the pre-dissolved raw materials of phases E, F, G, and stir well;

[0241] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling.

[0242] Example 7

[0243] This embodiment provides a three-dimensional stereoscopic water-locking moisturizing milk. By mass, the raw materials for preparing the moisturizing milk include:

[0244] Phase A raw materials: 5 parts of isononyl isononanoate, 0.5 part of PEG-100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of shea (BUTYROSPERMUM PARKII) butter, 0.5 part of cetearyl olivate, 0.5 part of sorbitan olivate, 0.5 part of polydimethylsiloxane, 0.5 part of squalane, 0.2 part of tocopheryl acetate;

[0245] Phase B raw materials: 30 parts of water, 5 parts of glycerin, 1 part of butanediol, 0.5 part of betaine, 0.2 part of carbomer, 0.11 part of hydrogenated lecithin, 0.11 part of disodium EDTA;

[0246] Phase C raw materials: 5 parts of water, 0.22 part of arginine;

[0247] Phase D raw materials: 1 part of butanediol, 0.05 part of octanoyl hydroxamic acid;

[0248] Phase E raw materials: 5 parts of water, 0.11 part of niacinamide;

[0249] Phase F raw materials: 5 parts of water, 0.11 part of ectoine;

[0250] Phase G raw materials: 30.69 parts of water, 0.3 part of lauryl poly(dimethylsiloxane) / polyglycerol-3 cross-linked polymer, 0.3 part of polymethylsilsesquioxane, 0.1 part of caprylyl glycol, 0.1 part of phenoxyethanol;

[0251] Phase H raw materials: 1 part of Cordyceps sinensis extract, 0.25 part of citrus peel extract, 0.1 part of 1,3-propanediol, 0.15 part of 1,2-hexanediol, 1 part of filtrate of galactomyces ferment, 0.05 part of p-hydroxyacetophenone, 0.1 part of ethylhexylglycerin, 0.05 part of Cynanchum atratum extract, 0.1 part of Sophora angustifolia root extract, 0.1 part of Gynostemma pentaphyllum extract, 0.1 part of xylitylglucoside, 0.1 part of anhydroxylitol, 0.1 part of xylitol, 0.4 part of Prunus speciosa flower extract, 0.1 part of maltodextrin glucoside, 0.1 part of hydrogenated starch hydrolysate, 0.11 part of bisabolol, 0.05 part of isocetane, 0.1 part of cetyl ethylhexanoate, 1.5 parts of Citrus medica vulgaris peel oil, 1 part of Citrus tangerina peel oil;

[0252] Phase I raw materials: 0.1 part of water, 0.001 part of fermentation product of THERMUS THERMOPHILLUS, 0.001 part of soluble collagen, 0.001 part of butanediol, 0.001 part of ethylhexylglycerin.

[0253] Among them, the preparation method of the CORDYCEPS SINENSIS extract is as follows:

[0254] (1) Wash and dry the CORDYCEPS SINENSIS, then crush and sieve it; (2) Add the CORDYCEPS SINENSIS powder to the culture medium and mix evenly, then continue to inoculate the strain, with an inoculation amount of 8%, and ferment aerobically at 28°C for 72h. After filtering to remove the residue, the CORDYCEPS SINENSIS extract is obtained.

[0255] Among them, the strain is Candida 32586 and Aspergillus 40048; the inoculation amount ratio is 3:2.

[0256] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of plant peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water are added to make up to 1000 mL.

[0257] The preparation method of the citrus peel extract is as follows:

[0258] (1) Wash and dry the citrus peel, then cut it into pieces;

[0259] (2) Add the chopped citrus peel to the culture medium and mix evenly, then continue to inoculate the strain, with an inoculation amount of 2%, and ferment aerobically at 28°C for 72h. After filtering to remove the residue, the citrus peel extract is obtained.

[0260] Among them, the strain is Candida 32586 and Aspergillus 40048; the inoculation amount ratio is 3:2.

[0261] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0262] The preparation methods of the pericarp oil of Citrus medica vulgaris and the pericarp oil of Citrus tangerina are as follows:

[0263] (1) Cut the pericarps of Citrus medica vulgaris and Citrus tangerina, add them to the culture medium and mix evenly. Then continue to inoculate the strains, with an inoculation amount of 8%. After aerobic fermentation at 28 °C for 72 h, filter to remove the residue, and then let it stand to obtain the oil layer, which is the pericarp oil of Citrus medica vulgaris and the pericarp oil of Citrus tangerina.

[0264] Among them, the strains are Hanseniaspora uvarum 1959 and Aspergillus niger 40048; the inoculation amount ratio is 2:2.

[0265] The components of the culture medium include: 3.0 g of beef extract powder, 10.0 g of peptone, 5.0 g of tryptone (BBL), 3.0 g of vegetable peptone, 5.0 g of yeast extract powder, 10.0 g of glucose, 0.5 g of soluble starch, K 2 HPO 4 1.0 g, KH 2 PO 4 1.0 g, MgSO 4 ·7H 2 O 0.2 g, 10.0 mL of 5% L-cysteine hydrochloride solution, 1.0 g of Tween 80, and distilled water is added to make up to 1000 mL.

[0266] In this embodiment, the polydimethylsiloxane is as follows: with a viscosity of 1.0 - 3.0 cps at 25°C, purchased from Slokchem, model Sicare 2942; and with a viscosity of 6 cps at 25°C, purchased from Shin-Etsu Silicone International Trade (Shanghai) Co., Ltd., model KF-96A-6T, and they are mixed in a mixing ratio of 3:1.

[0267] In this embodiment, the polymethylsilsesquioxane is purchased from Slokchem, model Sicare 2115F.

[0268] The preparation method of the three-dimensional moisture-locking and moisturizing lotion is as follows:

[0269] S1. Do a good job in sanitation cleaning, and strictly clean and disinfect the equipment and utensils used.

[0270] S2. Put the raw materials of phase A into the oil pan in sequence, stir and heat up to 80 - 85°C, keep warm for a period of time to ensure that the material is completely dissolved, and set aside.

[0271] S3. Put the raw materials of phase B into the emulsifying pan in sequence, stir and heat up to 85 - 90°C, keep warm for a period of time to ensure that the material is completely dissolved, pump phase A into the emulsifying pan, homogenize and stir evenly, add the raw materials of phase C, and homogenize and stir evenly before cooling down.

[0272] S4. Cool down to 60 - 65°C, add the pre-dissolved raw materials of phase D, stir evenly, and continue to cool down.

[0273] S5. Cool down to 40 - 45°C, add phases H and I and the pre-dissolved raw materials of phases E, F, and G, and stir evenly.

[0274] S6. Send for inspection. After passing the inspection, discharge the material. After passing the micro-inspection, pour the material into the filling machine for filling.

[0275] Performance test

[0276] Test 1: Place lotions 1 - 7 at 5°C, 25°C, and 40°C respectively, and let them stand for 90 days to check the properties. Conduct a thermal cycling experiment (Thermal cycling stability: One cycle of thermal cycling is 2 days. On the first day, place it in a -18°C constant temperature oven, and on the second day, place it in a 48°C constant temperature oven. After restoring to room temperature, observe whether the appearance of the solution changes, whether there are phenomena such as stratification, precipitation, emulsification, and turbidity. Test for 8 cycles, and the test results are shown in Table 1.

[0277] Table 1 Test results of Test 1

[0278] Example 5℃ 25℃ 40℃ Example 1 The properties remain unchanged The properties remain unchanged The properties remain unchanged Example 2 Slight delamination The properties remain unchanged Slight delamination Example 3 The properties remain unchanged The properties remain unchanged The properties remain unchanged Example 4 Slight delamination The properties remain unchanged Slight delamination Example 5 The properties remain unchanged The properties remain unchanged The properties remain unchanged Example 6 The properties remain unchanged The properties remain unchanged The properties remain unchanged Example 7 Slight delamination The properties remain unchanged Slight delamination

[0279] Test 2: Moisture retention test

[0280] There were 34 participants, and 32 were actually included, including 7 males and 25 females, aged 30 to 50 years old, with an average age of 32.50 ± 1.45 years. The test area was the face; the test environment was a temperature of 21 ± 1°C and a relative humidity of 50 ± 10% RH.

[0281] One week before the start of the test, the subjects stopped using facial cosmetics or topical medications. The night before the test, after washing their faces at home, the subjects did not apply any skin care products to their faces. On the morning of the test day, after washing their faces with clean water at home, the subjects did not apply any skin care products to their faces; the eligible subjects filled out the informed consent form; after cleaning their faces with clean water, the subjects rested in a constant temperature and humidity chamber (temperature 21 ± 1°C, relative humidity 50 ± 10% RH) for 30 minutes. No other products were used during the test (the products related to the examples were used morning and evening, and relevant tests were carried out after 18h and 7d of use).

[0282] Stratum corneum water content:

[0283] Test site: Cheek skin

[0284] Test instrument: Courage+Khazaka skin moisture tester Corneometer CM825

[0285] Table 2 Stratum corneum water content test

[0286]

[0287] Average improvement rate = (mean after use - mean before use) / (mean before use) * 100%

[0288] Test 3: Difference in transepidermal water loss rate

[0289] Healthy subjects aged 25 - 60 years old (all subjects already had characteristics of sensitive skin, such as being prone to allergies, having red blood streaks, etc.), including 6 males and 23 females, with an average age of 40.13 ± 3.42 years.

[0290] Application site: Forearm

[0291] Application method: When applied to the forearm, the test sample was applied at a dosage of (2.0 ± 0.1) mg / cm 2 and spread evenly in the test area using a latex finger cot.

[0292] Test steps

[0293] Before the subjects visited, the inner part of their arms did not come into contact with water

[0294] Before the experiment, the subjects needed to clean their arms with dry paper towels uniformly;

[0295] Mark 2 measurement areas on the inner side of the left or right arm of the subject, each area having an area of 3 cm * 3 cm, and the distance between the areas being at least 1 cm;

[0296] The sample area and the negative control area are randomly distributed in the calibrated area to ensure that the position of each area is statistically balanced: The subject exposes the arm and rests in an environment with a temperature of 21 ± 1 °C and a relative humidity of 40 ± 10% RH for 30 minutes; Apply the inducer (0.1% histamine solution) to the sample area and the negative area for 10 min. After the application and before using the sample (Timm), measure the trans-epidermal water loss rate of the calibrated area with a Tewameter and measure the heme of the calibrated area with a Mexamter.

[0297] After using the sample, the subject exposes the arm and rests in an environment with a temperature of 21 ± 1 °C and a relative humidity of 40 ± 10% RH; After 1 h (T1), measure the trans-epidermal water loss rate of the calibrated area with a Tewameter; After 1 h (T1), measure the heme of the calibrated area with a Mexamter.

[0298] The Courage+Khazaka trans-epidermal water loss and water evaporation heat loss test probe Tewameter TM300 is used to detect the trans-epidermal water loss rate of the skin.

[0299] Table 3 Comparison of trans-epidermal water loss rate before and after

[0300]

[0301]

[0302] The Courage+Khazaka skin melanin and heme tester Mexamter MX18 is used to detect the heme of the skin.

[0303] Table 4 Comparison of heme before and after

[0304] Example Same as before (mean ± standard deviation) After using the sample for 1 h (mean ± standard deviation) Example 1 352.64±43.28 191.32±38.31 Example 2 352.32±25.31 205.21±32.18 Example 3 352.75±15.28 207.56±28.57 Example 4 352.19±32.38 208.49±32.93 Example 5 352.52±26.56 201.26±42.28 Example 6 353.02±30.21 200.16±41.31 Example 7 352.61±31.43 202.52±32.18 Negative region 353.12±27.12 331.24±32.32

[0305] Test 4: Human trial comprehensive evaluation experiment: The candidates for this test are the same as those for Test 3. After using the sample, the subject exposes the arm and rests in an environment with a temperature of 21 ± 1 °C and a relative humidity of 15 ± 5% RH, and scores are given during the experience period.

[0306] Table 5 Use feeling scoring form

[0307] Serial number Problem Score 1 Using this sample is mild and non-irritating; □5□4□3□2□1 2 After use, it is felt that this sample can improve dryness and moisturize the skin; □5□4□3□2□1 3 After use, it is felt that this sample has a moisturizing effect after use; □5□4□3□2□1 4 After use, it is felt that this sample can repair the skin; □5□4□3□2□1 5 Generally, I am satisfied with this sample. □5□4□3□2□1

[0308] 5 points means fully agree, 4 points means relatively agree, 3 points means neither agree nor disagree, 2 points means relatively disagree, and 1 point means fully disagree. There are 29 people in total, and the total number is recorded in Table 6.

[0309] Test results of Test 4 in Table 6

[0310] Example Example 1 Example 2 Example 3 Example 4 Example 5 Example 6 Example 7 Problem 1 145 144 145 144 145 145 145 Problem 2 143 136 140 133 130 129 138 Problem 3 142 134 139 132 128 128 137 Problem 4 140 122 121 118 130 132 127 Problem 5 141 136 138 132 131 129 137

[0311] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention, rather than to limit them; although the present invention has been described in detail with reference to the foregoing embodiments, those of ordinary skill in the art should understand that they can still modify the technical solutions recorded in the foregoing embodiments, or perform equivalent replacements for some or all of the technical features; and these modifications or replacements do not cause the essence of the corresponding technical solutions to deviate from the scope of the technical solutions of the embodiments of the present invention.

Claims

1. A three-dimensional water-locking composition, characterized in that: The raw materials for preparing the composition include: water phase, oil phase and emulsifier; The oil phase includes: avocado tree (BUTYROSPERMUM PARKII) fruit butter, cetearyl olivate, sorbitan olivate, and polydimethylsiloxane.

2. A three-dimensional water-locking composition according to claim 1, characterized in that: The viscosity of the polydimethylsiloxane is 1.0-3.0 cps at 25°C.

3. A three-dimensional water-locking composition according to claim 1, characterized in that: The composition also contains citrus (CITRUS RETICULATA) peel extract, which is prepared by fermentation.

4. A three-dimensional water-locking composition according to claim 1, characterized in that: The raw materials for preparing the composition also include: cetyl ethylhexanoate, common citron (CITRUS MEDICA VULGARIS) peel oil, and tangerine (CITRUS TANGERINA) peel oil.

5. A three-dimensional water-locking moisturizing lotion, characterized in that: The three-dimensional water-locking composition is prepared from any one of claims 1 to 4.

6. A three-dimensional water-locking moisturizing lotion according to claim 5, characterized in that: The raw materials for preparing the moisturizing lotion include: Phase A ingredients: isononyl isononanoate, PEG-100 stearate, glyceryl stearate, cetearyl alcohol, shea butter (BUTYROSPERMUM PARKII) fruit butter, cetearyl olive oil ester, sorbitan olive oil ester, dimethicone; Phase B ingredients: water, glycerin, butylene glycol, betaine, carbomer, hydrogenated lecithin, disodium EDTA; Phase C materials: water, arginine; Phase D raw materials: butanediol, caprylhydroxamic acid; Phase E materials: water, niacinamide; Phase F materials: water, tetrahydromethylpyrimidine carboxylic acid; Phase G ingredients: water, lauryl dimethicone / polyglyceryl-3 crosspolymer, polymethylsilsesquioxane, caprylyl glycol, phenoxyethanol; Phase H ingredients: Cordyceps sinensis extract, 1,3-propylene glycol, 1,2-hexanediol, galactose yeast fermentation product filtrate, p-hydroxyacetophenone, ethylhexylglycerin, CYNANCHUM ATRATUM extract, SOPHORA ANGUSTIFOLIA root extract, Gynostemma PENTAPHYLLUM extract, xylitol glucoside, dehydrated xylitol, xylitol, PRUNUS SPECIOSA flower extract, maltooligosaccharide glucoside, hydrogenated starch hydrolyzate, bisabolol, isohexadecane, cetyl ethylhexanoate, Citrus medicavulgaris peel oil, Citrus tangerina peel oil; Phase I ingredients: water, fermentation product of Thermus thermophilus, soluble collagen, butylene glycol, ethylhexylglycerin.

7. The three-dimensional water-locking moisturizing lotion according to claim 5, characterized in that: The raw materials for preparing the moisturizing lotion include: Phase A ingredients: 5 parts of isononyl isononanoate, 0.5 parts of PEG-100 stearate, 1 part of glyceryl stearate, 1.2 parts of cetearyl alcohol, 1 part of avocado tree (BUTYROSPERMUM PARKII) fruit butter, 0.5 parts of cetearyl olive oil, 0.5 parts of sorbitan olive oil, 0.5 parts of polydimethylsiloxane, 0.5 parts of squalane, and 0.2 parts of tocopheryl acetate; Phase B materials: 30 parts of water, 5 parts of glycerin, 1 part of butylene glycol, 0.5 parts of betaine, 0.2 parts of carbomer, 0.11 parts of hydrogenated lecithin, and 0.11 parts of disodium EDTA; Phase C materials: 5 parts of water, 0.22 parts of arginine; Phase D raw materials: 1 part of butanediol, 0.05 parts of octanoylhydroxamic acid; Phase E materials: 5 parts of water, 0.11 parts of niacinamide; Phase F materials: 5 parts of water, 0.11 parts of tetrahydromethylpyrimidine carboxylic acid; Phase G materials: 30.69 parts of water, 0.3 parts of lauryl dimethicone / polyglyceryl-3 crosspolymer, 0.3 parts of polymethylsilsesquioxane, 0.1 parts of caprylyl glycol, and 0.1 parts of phenoxyethanol; Phase H ingredients: 1 part of Cordyceps sinensis extract, 0.1 part of 1,3-propylene glycol, 0.15 parts of 1,2-hexanediol, 1 part of galactosyl yeast fermentation product filtrate, 0.05 parts of p-hydroxyacetophenone, 0.1 parts of ethylhexylglycerin, 0.05 parts of CYNANCHUM ATRATUM extract, 0.1 parts of Sophora angustifolia root extract, 0.1 parts of Gynostemma pentaphyllum extract, 0.1 parts of xylitol glucoside, 0.1 parts of dehydrated xylitol, 0.1 parts of xylitol, 0.1 parts of PRUNUS SPECIOSA) flower extract 0.4 parts, maltooligosaccharide glucoside 0.1 parts, hydrogenated starch hydrolyzate 0.1 parts, bisabolol 0.11 parts, isohexadecane 0.05 parts, cetyl ethylhexanoate 0.1 parts, Citrus vulgaris peel oil 1.5 parts, Citrus tangerina peel oil 1 part; Phase I raw materials: 0.1 parts of water, 0.001 parts of Thermus thermophilus fermentation product, 0.001 parts of soluble collagen, 0.001 parts of butylene glycol, and 0.001 parts of ethylhexylglycerin.

8. The method for preparing a three-dimensional water-locking moisturizing lotion according to claim 7, characterized in that: Here are the steps: S1. Do a good job of sanitation and cleaning, and strictly clean and disinfect the equipment and utensils; S2. Put the raw materials of phase A into the oil pan in turn, stir and heat to 80-85°C, keep warm for a while to ensure that the material is completely dissolved, and set aside; S3. Add the raw materials of phase B into the emulsification pot in turn, stir and heat to 85-90℃, keep warm for a while to ensure that the material is completely dissolved, draw phase A into the emulsification pot, homogenize and stir evenly, add the raw materials of phase C, homogenize and stir evenly, and then cool down; S4. Cool down to 60-65°C, add phase D raw materials, stir well, and continue to cool; S5. Cool down to 40-45°C, add H, I phase and E, F, G phase raw materials, and stir well; S6. After the materials are sent for inspection and qualified, they are discharged. After the materials are qualified for micro-inspection, they are poured into the filling machine for filling.

9. The method for preparing a three-dimensional water-locking moisturizing lotion according to claim 8, characterized in that: The raw materials of phases D, E, F and G are dissolved in advance before being added into the pot.

10. The three-dimensional water-locking moisturizing lotion according to claim 7, characterized in that: Used in daily chemical field.

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