Powerful toner and preparation method thereof

Abstract

The invention discloses a powerful toner, which is prepared from the following raw materials in percentage by weight: 13 to 15 percent of humectant, 1 to 3 percent of methyl glucitol polyether-20, 0.4 to 0.7 percent of p-hydroxyacetophenone, 0.8 to 1 percent of anti-allergy soothing agent, 0.1 to 0.15 percent of EDTA (Ethylene Diamine Tetraacetic Acid) disodium, 0.4 to 0.5 percent of 1, 2-hexanediol, 0.05 to 0.1 percent of additive, 1.6 to 3 percent of nicotinamide and the balance of water. By using the mild additive-free concept preservative, the irritation of the product is greatly reduced, the mildness of the product is greatly improved, the anti-allergy ability of the skin of a user is improved by matching with the plant extract, and meanwhile, the moisturizing effect is further enhanced by adding the low-cost eryngium foetidum extract.

Description

Technical Field

[0001] The present invention belongs to the field of toner, and specifically relates to a powerful toner and a preparation method thereof. Background Art

[0002] Eryngium foetidum, a perennial herb with a special aroma, grows on fertile and moist land such as the edges of forests, roadsides, hillsides, and open fields. It is distributed in Guangdong, Guangxi, Hainan, Yunnan and other places. It has the effects of dispelling wind and removing heat, and promoting digestion with its fragrance. After experiments, adding its enzymolysis product to skin care products can achieve a moisturizing effect.

[0003] At present, the problems existing in toners on the market include: 1. Not suitable for people with sensitive facial skin. People with sensitive skin have relatively weak facial skin and are prone to adverse reactions such as allergies, flushing, and itching; 2. The moisturizing effect is not lasting, the use feeling is sticky, and the experience is poor; 3. Excessive publicity and complicated functions, such as being able to adjust heart rate, blood pressure, anti-aging, etc., which cannot stand verification. Summary of the Invention

[0004] The purpose of the present invention is to provide a toner that can clean facial skin and moisturize facial skin.

[0005] To achieve the above purpose, the present invention adopts the following technical solutions:

[0006] A powerful toner, which comprises the following raw materials in percentage by weight:

[0007] Humectant 13 - 15%, methyl glucitol polyether - 20 1 - 3%, p - hydroxyacetophenone 0.4 - 0.7%, anti - allergy and soothing agent 0.8 - 1%, disodium EDTA 0.1 - 0.15%, 1,2 - hexanediol 0.4 - 0.5%, additive 0.05 - 0.1%, niacinamide 1.6 - 3%, and the balance is water; the additive is Eryngium foetidum extract.

[0008] The humectant is composed of glycerol, propylene glycol, maltool glucoside, and trehalose mixed in a weight ratio of 6 - 7:3 - 4:2 - 3:1 - 2.

[0009] The anti - allergy and soothing agent is composed of gentian root extract, kava root extract, and centella asiatica extract mixed in a weight ratio of 2 - 5:4 - 6:2 - 3.

[0010] The preparation method of the Eryngium foetidum extract is as follows: Take the whole herb of Eryngium foetidum, wash and dry it, add 0.5 - 1 mol / l acetic acid aqueous solution, grind it, add it to the enzymolysis solution, carry out enzymolysis fermentation at 35 - 40 °C for 9 - 10 hours, sterilize and inactivate enzymes at high temperature, filter with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain the extract.

[0011] The dosage of the aqueous acetic acid solution is 5-10% of the weight of the whole Eryngium foetidum L. herb.

[0012] The enzyme in the enzymolysis solution is a mixture of cellulase and callase with a weight ratio of 10:0.8-1.

[0013] A preparation method of a powerful toner, comprising the following steps:

[0014] (1) Mix water, a moisturizer, methyl gluceth-20, and hydroxyacetophenone, add them to an emulsifying pan, stir and heat to raise the temperature to 80-90 °C, and keep warm for 25-40 minutes;

[0015] (2) When the temperature is lowered to 40-50 °C, add an anti-allergic and soothing agent, disodium EDTA, and an additive in sequence, stir for 5-10 minutes, add niacinamide and 1,2-hexanediol in sequence, and stir for 10-20 minutes;

[0016] (3) When the temperature is lowered to 30-35 °C, filter and discharge the material, let it stand, fill it, package it, and store the finished product in the warehouse.

[0017] Advantages of the present invention:

[0018] The toner of the present invention can cover most skin types of people, has strong applicability, good experience, and excellent moisturizing effect. By using mild concept preservatives without addition, the irritation of the product is greatly reduced, and the mildness of the product is greatly improved. By combining with plant extracts (Piper methysticum root extract, Gentiana root extract, Centella asiatica extract), the anti-allergic ability of the user's own skin is enhanced. By compounding and using a variety of moisturizers such as glycerin, propylene glycol, trehalose, and maltooligosyl glucoside, the effect of long-term moisturization is achieved. At the same time, the extract of Eryngium foetidum L. with low cost is added to further enhance the moisturizing effect.

[0019] Description of the drawings

[0020] Figures 1 - 2 It is the test record of the moisturizing efficacy of the product in Example 1 of the present invention;

[0021] Figures 3 - 4 It is the test record of the basic performance of the product in Example 1 of the present invention. Detailed implementation manners

[0022] Example 1

[0023] A powerful toner, which comprises the following raw materials in the following weight percentages:

[0024] Moisturizer 13%, methyl gluceth-20 1%, hydroxyacetophenone 0.4%, anti-allergic and soothing agent 0.8%, disodium EDTA 0.1%, 1,2-hexanediol 0.4%, additive 0.05%, niacinamide 1.6%, and the rest is water.

[0025] The moisturizer is composed of glycerol, propylene glycol, malt oligosaccharide glucoside, and trehalose mixed in a weight ratio of 6:3:2:1.

[0026] The anti-allergic and soothing agent is composed of gentian root extract, kava kava root extract, and centella asiatica extract mixed in a weight ratio of 3:5:2.

[0027] The additive is eryngium foetidum extract.

[0028] The preparation method of the eryngium foetidum extract is as follows: Take the whole herb of eryngium foetidum, wash and dry it in the sun, add 0.5 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 35 °C for 9 hours, sterilize and inactivate the enzyme at high temperature, filter with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain the eryngium foetidum extract.

[0029] The dosage of the acetic acid aqueous solution is 5% of the weight of the whole herb of eryngium foetidum.

[0030] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and callose enzyme in a weight ratio of 10:0.8.

[0031] A preparation method of a powerful toner, comprising the following steps:

[0032] (1) Mix water, moisturizer, methyl gluceth-20, and p-hydroxyacetophenone, add them to an emulsifying pot, stir and heat to 80 °C, and keep warm for 25 minutes;

[0033] (2) When the temperature is lowered to 40 °C, add the anti-allergic and soothing agent, disodium EDTA, and additive in sequence, stir for 5 minutes, add niacinamide and 1,2-hexanediol in sequence, and stir for 10 minutes;

[0034] (3) When the temperature is lowered to 30 °C, filter and discharge the material, let it stand, fill it, package it, and store the finished product in the warehouse.

[0035] Example 2

[0036] A powerful toner, which comprises the following raw materials in the following weight percentages:

[0037] Moisturizer 15%, methyl gluceth-20 3%, p-hydroxyacetophenone 0.7%, anti-allergic and soothing agent 1%, disodium EDTA 0.15%, 1,2-hexanediol 0.5%, additive 0.1%, niacinamide 3%, and the rest is water.

[0038] The moisturizer is composed of glycerol, propylene glycol, malt oligosaccharide glucoside, and trehalose mixed in a weight ratio of 7:4:3:2.

[0039] The anti-allergic and soothing agent is composed of a mixture of gentian root extract, kava root extract, and centella asiatica extract with a weight ratio of 3:5:3.

[0040] The additive is false coriander extract.

[0041] The preparation method of the false coriander extract is as follows: Take the whole plant of false coriander, wash it, dry it in the sun, add 1 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 40 °C for 10 hours, sterilize and inactivate the enzyme at high temperature, filter it with a microporous filter membrane, concentrate the filtrate, dry it, and pulverize it to obtain the product.

[0042] The dosage of the acetic acid aqueous solution is 10% of the weight of the whole plant of false coriander.

[0043] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and callose enzyme with a weight ratio of 10:1.

[0044] A preparation method of a powerful toner, comprising the following steps:

[0045] (1) Mix water, a moisturizer, methyl gluceth-20, and p-hydroxyacetophenone, add them to an emulsifying pot, stir and heat to 90 °C, and keep warm for 40 minutes;

[0046] (2) When the temperature is lowered to 40 - 50 °C, add the anti-allergic and soothing agent, disodium EDTA, and the additive in sequence, stir for 10 minutes, add niacinamide and 1,2-hexanediol in sequence, and stir for 20 minutes;

[0047] (3) When the temperature is lowered to 35 °C, filter and discharge the material, let it stand, fill it, package it, and store the finished product in the warehouse.

[0048] Example 3

[0049] A powerful toner, which comprises the following raw materials in the following weight percentages:

[0050] Moisturizer 14%, methyl gluceth-20 2%, p-hydroxyacetophenone 0.5%, anti-allergic and soothing agent 0.9%, disodium EDTA 0.12%, 1,2-hexanediol 0.45%, additive 0.06%, niacinamide 2%, and the rest is water.

[0051] The moisturizer is composed of a mixture of glycerin, propylene glycol, maltooligosaccharide glucoside, and trehalose with a weight ratio of 6:4:3:1.

[0052] The anti-allergic and soothing agent is composed of a mixture of gentian root extract, kava root extract, and centella asiatica extract with a weight ratio of 3:5:3.

[0053] The additive is false coriander extract.

[0054] The preparation method of the Eryngium foetidum extract is as follows: Take the whole herb of Eryngium foetidum, wash it and dry it in the sun, add 1 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 38 °C for 9 hours, sterilize and inactivate the enzyme at high temperature, filter it with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain the product.

[0055] The dosage of the acetic acid aqueous solution is 8% of the weight of the whole herb of Eryngium foetidum.

[0056] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and callose enzyme with a weight ratio of 10:1.

[0057] A preparation method of a powerful toner, comprising the following steps:

[0058] (1) Mix water, a moisturizer, methyl glucitol polyether-20, and p-hydroxyacetophenone, add them to an emulsifying pot, stir and heat to raise the temperature to 85 °C, and keep warm for 30 minutes;

[0059] (2) When the temperature is lowered to 46 °C, add an anti-allergy and soothing agent, disodium EDTA, and an additive in sequence, stir for 6 minutes, add niacinamide and 1,2-hexanediol in sequence, and stir for 13 minutes;

[0060] (3) When the temperature is lowered to 35 °C, filter and discharge the material, let it stand, fill it, package it, and store the finished product in the warehouse.

[0061] Control Example 1 (without additive);

[0062] A powerful toner, which comprises the following raw materials in the following weight percentages:

[0063] Moisturizer 14%, methyl glucitol polyether-20 2%, p-hydroxyacetophenone 0.5%, anti-allergy and soothing agent 0.9%, disodium EDTA 0.12%, 1,2-hexanediol 0.45%, niacinamide 2%, and the rest is water.

[0064] The moisturizer is composed of a mixture of glycerol, propylene glycol, maltool glucoside, and trehalose with a weight ratio of 6:4:3:1.

[0065] The anti-allergy and soothing agent is composed of a mixture of gentian root extract, kava kava root extract, and centella asiatica extract with a weight ratio of 3:5:3.

[0066] A preparation method of a powerful toner, comprising the following steps:

[0067] (1) Mix water, a moisturizer, methyl glucitol polyether-20, and p-hydroxyacetophenone, add them to an emulsifying pot, stir and heat to raise the temperature to 85 °C, and keep warm for 30 minutes;

[0068] (2) When the temperature is lowered to 46 °C, add the anti-allergy and soothing agent and disodium EDTA in sequence, stir for 6 minutes, then add niacinamide and 1,2-hexanediol in sequence, and stir for 13 minutes;

[0069] (3) When the temperature is lowered to 35 °C, filter and discharge the material, let it stand, fill, package, and store the finished product in the warehouse for performance testing:

[0070] Detection basis: QTC-C-LAB-TOP-042 "In Vitro Test Method for Moisturizing Efficacy of Cosmetics (Weighing Method)";

[0071] Detection method:

[0072] Use a weighing bottle as a carrier to weigh 1 g of the sample of Example 3 of the present invention and the sample of Comparative Example 1 (accurate to 0.0001 g). Place the above two samples in an environment of (22 ± 2) °C and humidity of (50 ± 10)%, weigh and record the data at regular intervals, and calculate the moisturizing rate;

[0073]

[0074] Send the sample of Example 1 of the present invention for inspection: The test results are as shown in the accompanying drawings of the specification.

Claims

1. A strong toner, characterized in that: It includes the following raw materials in weight percentage: Moisturizer 13-15%, methyl gluceth-20 1-3%, parahydroxyacetophenone 0.4-0.7%, anti-allergic soothing agent 0.8-1%, disodium EDTA 0.1-0.15%, 1,2-hexanediol 0.4-0.5%, additive 0.05-0.1%, niacinamide 1.6-3%, the rest is water; The additive is a pseudo-parsley extract.

2. A strong toner according to claim 1, characterized in that: The moisturizing agent is a mixture of glycerol, propylene glycol, maltooligosaccharide glucoside and trehalose in a weight ratio of 6-7:3-4:2-3:1-2.

3. A strong toner according to claim 1, characterized in that: The anti-allergic soothing agent is a mixture of gentian root extract, kava root extract and centella asiatica extract in a weight ratio of 2-5:4-6:2-3.

4. A strong toner according to claim 1, characterized in that: The preparation method of the pseudocaraway extract is as follows: washing the whole plant of the pseudocaraway, drying it in the sun, adding 0.5-1 mol / l acetic acid aqueous solution, grinding it, adding it to an enzymatic hydrolysis solution, performing enzymatic hydrolysis and fermentation at 35-40° C. for 9-10 hours, sterilizing it at high temperature to inactivate the enzyme, filtering it with a microporous filter membrane, concentrating the filtrate, drying it, and crushing it to obtain the extract.

5. A strong toner according to claim 4, characterized in that: The amount of the acetic acid aqueous solution used is 5-10% of the weight of the whole plant of Pseudo-Centella odorata.

6. A strong toner according to claim 4, characterized in that: The enzyme in the enzymolysis solution has a weight ratio of 10: 0.8-1 mixture of cellulase and callose.

7. A method for preparing the strong toner as claimed in claim 1, characterized in that: The following steps are involved: (1) Mix water, moisturizer, methyl gluceth-20 and p-hydroxyacetophenone, add to an emulsifier, stir and heat to 80-90°C, and keep warm for 25-40 minutes; (2) When the temperature drops to 40-50°C, add the anti-allergic soothing agent, disodium EDTA, and additives in sequence, stir for 5-10 minutes, add niacinamide and 1,2-hexanediol in sequence, and stir for 10-20 minutes; (3) When the temperature drops to 30-35℃, filter the material, let it stand, fill, package, and store the finished product.

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