Pure traditional Chinese medicine compound toning lipstick and preparation process thereof
By combining cypress extract with Chinese herbal extracts such as Salvia miltiorrhiza and Madhya, a rich and safe Chinese herbal compound lipstick was prepared, which solved the problem of single color of Chinese herbal lipstick and achieved high color saturation and diversified color tone effects.
Patent Information
- Application Number
- CN202510588636.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-05-08
- Publication Date
- 2025-07-04
AI Technical Summary
The color diversity of traditional Chinese medicine lipsticks is insufficient, which is difficult to meet consumers' needs for personalized and diverse makeup. Some people are sensitive to chemical synthetic color powders. The existing Chinese herbal ingredients are not widely used in color tuning.
The main use of purpura extract, combined with other Chinese herbal extracts such as Salvia miltiorrhiza and Madhya extract, Chinese herbal coloring components are prepared by hot extraction, combined with natural beeswax, candle tree wax, lanolin, vaseline and other substrates, and olive oil, glycerin and other ingredients, to prepare a series of Chinese herbal compound lipsticks of different colors.
It has achieved a traditional Chinese medicine color-tuning lipstick that does not use toner, with high color saturation, wide color variation range, high safety, and meets consumers' diverse needs.
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Abstract
Description
Technical Field
[0001] The invention belongs to the field of biotechnology, and in particular relates to a group of pure Chinese herbal compound color-adjusting lipsticks and a preparation process thereof. Background Art
[0002] Lipstick has become an indispensable beauty product in women's daily life. It can effectively modify the lip shape, add color, and make the lips look fuller and more vibrant. Chinese herbal lipstick is favored by consumers because of the health, nourishing, moisturizing, anti-oxidation and anti-inflammatory advantages brought by its natural ingredients. However, color is the core point of lipstick, and its diversity is an important reason restricting the development of Chinese herbal lipstick. The types and color range of natural pigments extracted from Chinese herbal medicines are not as rich as those of synthetic pigments, and it is difficult to mix a variety of fashionable and bright colors. Therefore, the color selection of lipsticks with Chinese herbal ingredients is often relatively single, mostly daily elegant colors, which is difficult to meet consumers' demand for personalized and diversified makeup. Selecting Chinese herbal medicines with high color saturation and a wide range of color variations for color matching is the core of solving this problem.
[0003] Most of the existing lipsticks are toned with chemical color powders, and some people are sensitive to chemical synthetic products, which limits their scope of use. In addition, some lipsticks add Chinese herbal medicine ingredients, but do not use Chinese herbal medicine ingredients as coloring components of multiple shades. According to the relevant regulations of my country's National Medical Products Administration (NMPA), lithospermum extract is currently included in the "Catalogue of Cosmetic Raw Materials". The color of lithospermum root and rhizome usually presents dark purple or dark red. Its main component shikonin and its derivatives have strong dyeing ability and are soluble in animal and vegetable oils. Different concentrations of lithospermum extract can present a series of different colors with red as the main tone. It also has antibacterial and anti-inflammatory effects and is a good lipstick raw material. It has not been studied or reported to prepare a series of different colors of Chinese herbal compound lipsticks using lithospermum extract as the main ingredient and other Chinese herbal extracts as auxiliary ingredients using pure Chinese herbal components. Summary of the invention
[0004] The main problem to be solved by the present invention is how to obtain a traditional Chinese medicine color-adjusting lipstick containing multiple colors without using color powder.
[0005] In order to solve the above problems, the present invention provides a composition containing a traditional Chinese medicine color-adjusting component.
[0006] The composition containing traditional Chinese medicine coloring components provided by the present invention comprises traditional Chinese medicine extracts, a matrix, a lubricant, a moisturizer, and an antioxidant; the traditional Chinese medicine extracts comprise lithospermum officinale extracts and / or other component extracts, the other component extracts comprise one or a combination of salvia miltiorrhiza extracts and madder extracts, and the traditional Chinese medicine extracts are extracted separately and then mixed.
[0007] In the above composition, the preparation method of the lithospermum extract is as follows: By weight, first crush the lithospermum and sieve it through a 60-mesh sieve. Weigh 40.00 g, 20.00 g, and 10.00 g of lithospermum powder and place them in conical flasks. Add 80 mL of olive oil to each flask, and use a glass rod to mix the lithospermum powder and olive oil evenly. After placing the conical flasks in a constant temperature water bath at 90 °C for 60 minutes, cool them to room temperature, and then extract for 2 weeks at 4 °C. After filtration, the lithospermum extract is obtained.
[0008] The lithospermum extract can be lithospermum extract A1 with a solid-to-liquid ratio of 0.5 g / mL (referred to as component A1), lithospermum extract A2 with a solid-to-liquid ratio of 0.25 g / mL (referred to as component A1), or lithospermum extract A3 with a solid-to-liquid ratio of 0.125 g / mL (referred to as component A1).
[0009] The preparation method of the paeonia lactiflora extract is as follows: By weight, first crush the paeonia lactiflora and sieve it through a 60-mesh sieve. Weigh 20 g of paeonia lactiflora powder and place it in a conical flask. Add 80 mL of olive oil to the flask, and use a glass rod to mix the paeonia lactiflora powder and olive oil evenly. After placing the conical flask in a constant temperature water bath at 90 °C for 60 minutes, cool it to room temperature, and then extract for 2 weeks at 4 °C. After filtration, the paeonia lactiflora extract (referred to as component B) is obtained. The solid-to-liquid ratio of the paeonia lactiflora extract is 0.25 g / mL.
[0010] The preparation method of the salvia miltiorrhiza extract is as follows: By weight, first crush the salvia miltiorrhiza and sieve it through a 60-mesh sieve. Weigh 20 g of salvia miltiorrhiza powder and place it in a conical flask. Add 80 mL of olive oil to the flask, and use a glass rod to mix the salvia miltiorrhiza powder and olive oil evenly. After placing the conical flask in a constant temperature water bath at 90 °C for 60 minutes, cool it to room temperature, and then extract for 2 weeks at 4 °C. After filtration, the salvia miltiorrhiza extract (referred to as component C) is obtained. The solid-to-liquid ratio of the salvia miltiorrhiza extract is 0.25 g / mL.
[0011] The combination of the lithospermum extract and other component extracts is as follows: 1) The lithospermum extract, the salvia miltiorrhiza extract, and the rubia cordifolia extract are combined in a weight ratio of 1 - 2:1; 2) The lithospermum extract and the rubia cordifolia extract are combined in a weight ratio of 1 - 2:1; 3) The lithospermum extract, the salvia miltiorrhiza extract, and the rubia cordifolia extract are combined in a weight ratio of 1:1:1.
[0012] In the above composition, the matrix is selected from at least one of natural beeswax, candelilla wax, refined sunflower seed wax, lanolin, petrolatum, and hyaluronic acid; the lubricant includes olive oil and / or sweet almond oil; the moisturizer includes glycerol and / or lubrajel; the flavoring agent is selected from one or more of rose essential oil, angelica dahurica essential oil, rhodiola rosea essential oil, cinnamon essential oil, sandalwood essential oil, magnolia biondii essential oil, osmanthus fragrans essential oil, etc.
[0013] Further, the matrix is composed of natural beeswax, candelilla wax, lanolin, and petrolatum; the lubricant is olive oil; the moisturizer is glycerol; the flavoring agent is rose essential oil; the antioxidant is vitamin E1; In the above composition, the weight ratio of the traditional Chinese medicine extract, natural beeswax, candelilla wax, lanolin, petrolatum, glycerol, rose essential oil, and vitamin E1 is 165:30:30:30:30:3:3:3.
[0014] The application of the composition described above in the preparation of lipsticks also falls within the scope of protection required by the present invention.
[0015] The present invention also provides a method for preparing a traditional Chinese medicine color-adjusted lipstick, and the method includes the following steps: 1) Preparation of the traditional Chinese medicine extract combination: Mix olive oil with traditional Chinese medicine and perform high-temperature hot extraction. After cooling to room temperature, perform extraction at 4°C for 2 weeks, and filter to obtain the traditional Chinese medicine extract; The traditional Chinese medicine is lithospermum erythrorhizon, salvia miltiorrhiza, and / or rubia cordifolia.
[0016] The traditional Chinese medicine extract is lithospermum erythrorhizon extract, or a combination of lithospermum erythrorhizon extract and other component extracts, and the other component extracts include one or two of salvia miltiorrhiza extract and rubia cordifolia extract; 2) Add the matrix and the moisturizer to the traditional Chinese medicine extract combination described in step (1), melt at 80°C, and obtain material M; 3) Add 30 parts of candelilla wax to material M, melt at 90°C, and stir evenly until there are no white particles to obtain material N; 4) Add 3 parts of vitamin E and 3 parts of rose essential oil to material N and stir evenly to obtain material P; 5) Pour material P into a lipstick mold, cool at 4°C, and demold to obtain the traditional Chinese medicine color-adjusted lipstick.
[0017] In the above method, the traditional Chinese medicine extract combination is composed of the following parts by weight of traditional Chinese medicine: 55 - 165 parts of lithospermum erythrorhizon extract or / and 0 - 55 parts of salvia miltiorrhiza extract, 0 - 55 parts of rubia cordifolia extract are mixed.
[0018] In a specific embodiment, the traditional Chinese medicine extract combination can be mixed according to 165 parts of lithospermum erythrorhizon extract, 0 parts of salvia miltiorrhiza extract, and 0 parts of rubia cordifolia extract.
[0019] In a specific embodiment, the traditional Chinese medicine extract combination can be mixed according to 55 parts of lithospermum extract, 55 parts of salvia miltiorrhiza extract, and 55 parts of rubia cordifolia extract.
[0020] In a specific embodiment, the traditional Chinese medicine extract combination can be mixed according to 110 parts of lithospermum extract and 55 parts of salvia miltiorrhiza extract.
[0021] In a specific embodiment, the traditional Chinese medicine extract combination can be mixed according to 110 parts of lithospermum extract and 55 parts of rubia cordifolia extract.
[0022] The material-liquid ratio (g / mL) of the extract can be 1:2 - 1:8.
[0023] Furthermore, the lithospermum extract can be lithospermum extract A1 with a material-liquid ratio of 0.5 g / mL (abbreviated as component A1), lithospermum extract A2 with a material-liquid ratio of 0.25 g / mL (abbreviated as component A1), or lithospermum extract A3 with a material-liquid ratio of 0.125 g / mL (abbreviated as component A1).
[0024] The material-liquid ratio of the salvia miltiorrhiza extract (abbreviated as component B) can be 0.25 g / mL.
[0025] The material-liquid ratio of the rubia cordifolia extract (abbreviated as component C) can be 0.25 g / mL.
[0026] Furthermore, the high-temperature hot extraction condition in step 1) is hot extraction in a 90°C constant-temperature water bath for 60 minutes.
[0027] Furthermore, the matrix in step 2) is composed of natural beeswax, lanolin, and petrolatum with a weight ratio of 1:1:1; the moisturizer is glycerol.
[0028] The lipstick product prepared by the method described above also belongs to the scope protected by the present invention.
[0029] Furthermore, the lipstick is a lipstick product with the following color numbers: #48282b, #442020, #550E14, #58121A, #5A141C, #6D181F, #6B1019, #8C1A22, #9A1A29, #991626, #961D2C, #AD242B.
[0030] The lipstick of color number #48282b is A1A1A1, where A1A1A1 represents that the proportion of the traditional Chinese medicine components is 165 parts of the A1 component; The lipstick of color number #442020 is A1A1B, where A1A1B represents that the proportion of the traditional Chinese medicine components is 110 parts of the A1 component and 55 parts of the B component; The lipstick numbered #550E14 is A1A1C, where A1A1C indicates that the proportion of the traditional Chinese medicine components is 110 parts of the A1 component and 55 parts of the C component; The lipstick numbered #58121A is A1BC, where A1BC indicates that the proportion of the traditional Chinese medicine components is 55 parts of the A1 component, 55 parts of the B component, and 55 parts of the C component; The lipstick numbered #5A141C is A2A2A2, where A2A2A2 indicates that the proportion of the traditional Chinese medicine components is 165 parts of the A2 component; The lipstick numbered #6D181F is A2A2B, where A2A2B indicates that the proportion of the traditional Chinese medicine components is 110 parts of the A2 component and 55 parts of the B component; The lipstick numbered #6B1019 is A2A2C, where A2A2C indicates that the proportion of the traditional Chinese medicine components is 110 parts of the A2 component and 55 parts of the C component; The lipstick numbered #8C1A22 is A2BC, where A2BC indicates that the proportion of the traditional Chinese medicine components is 55 parts of the A2 component, 55 parts of the B component, and 55 parts of the C component; The lipstick numbered #9A1A29 is A3A3A3, where A3A3A3 indicates that the proportion of the traditional Chinese medicine components is 165 parts of the A3 component; The lipstick numbered #991626 is A3A3B, where A3A3B indicates that the proportion of the traditional Chinese medicine components is 110 parts of the A3 component and 55 parts of the B component; The lipstick numbered #961D2C is A3A3C, where A3A3C indicates that the proportion of the traditional Chinese medicine components is 110 parts of the A3 component and 55 parts of the C component; The lipstick numbered #AD242B is A3BC, where A3BC indicates that the proportion of the traditional Chinese medicine components is 55 parts of the A3 component, 55 parts of the B component, and 55 parts of the C component.
[0031] The extract of the traditional Chinese medicine Lithospermum erythrorhizon Sieb. et Zucc. is a natural cosmetic raw material. Its main functions in cosmetics and skin care products are as an anti-inflammatory agent and an antioxidant. The extract of Lithospermum erythrorhizon Sieb. et Zucc. can promote the activity of cathepsin, indicating that this extract can enhance the metabolism of skin cells. Combining its antioxidant property, it has an anti-aging effect. The present invention aims to use the extract of Lithospermum erythrorhizon Sieb. et Zucc. as the main component, and at the same time supplement it with other extracts of traditional Chinese medicine for color matching, without using any color powder at all. By using pure traditional Chinese medicine components, a series of traditional Chinese medicine compound lipsticks with different colors are developed, so as to effectively combine aesthetics and practicality while ensuring the safety of the products. This innovative method provides a more ideal choice for consumers. Brief Description of the Drawings
[0032] Figure 1 It is a schematic diagram of different combinations of extracts of traditional Chinese medicine.
[0033] Figure 2 It is a schematic diagram of the experimental results of the heat resistance and cold resistance of the lipstick matrix.
[0034] Figure 3 It is a schematic diagram of 12 formulations of lipsticks.
[0035] Figure 4 It is a schematic diagram of the classification of lipstick color numbers by color system.
[0036] Figure 5 It is a schematic diagram of the results of the color stability of lipsticks. Specific embodiments
[0037] The present invention will be further described in detail below in conjunction with specific embodiments. The provided embodiments are only for clarifying the present invention, rather than limiting the scope of the present invention. The following provided embodiments can be used as a guide for those of ordinary skill in the art to make further improvements, and do not limit the present invention in any way.
[0038] The experimental methods in the following embodiments are all conventional methods unless otherwise specified, and are carried out according to the techniques or conditions described in the literature in this field or according to the product specifications. The materials, reagents, etc. used in the following embodiments can be obtained from commercial sources unless otherwise specified.
[0039] Unless otherwise specified, the quantitative tests in the following embodiments are all set with three repeated experiments, and the results are averaged.
[0040] The lithospermum, red peony root, and salvia miltiorrhiza in the following embodiments were purchased from Bozhou Chinese Herbal Medicine Commodity Trading Center. The public can obtain this biological material from the applicant. This biological material is only used for repeating the experiments of the present invention and cannot be used for other purposes.
[0041] The olive oil in the following embodiments is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 8001-25-0; the water-soluble lanolin is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 8039-09-6; the petrolatum is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 8009-03-8; the glycerol is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 56-81-5; the oil-soluble vitamin E oil is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 7695-91-2; the rose essential oil is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 8007-01-0; the natural beeswax is from Guangzhou Baiyu Biotechnology Co., Ltd., CAS No.: 8012-89-3; the candelilla wax is from Guangzhou Only You Cosmetics Raw Material Store, CAS: 8006-44-8.
[0042] Example 1. Preparation of the raw material composition for lipstick color adjustment Take 200 grams each of the Chinese herbal pieces Lithospermum erythrorhizon, Salvia miltiorrhiza, Rubia cordifolia, Carthamus tinctorius, Paeonia lactiflora, and Rosa rugosa, crush them and pass through a 60-mesh sieve for later use.
[0043] 1. Preparation of Lithospermum erythrorhizon extract First, weigh 40.00 g of Lithospermum erythrorhizon, 20.00 g of Lithospermum erythrorhizon, and 10.00 g of Lithospermum erythrorhizon and place them in a conical flask. Add 80 mL of olive oil to each respectively. Use a glass rod to mix the Lithospermum erythrorhizon powder and olive oil evenly. Place the conical flask in a 90°C constant temperature water bath for heat extraction for 60 minutes. After cooling to room temperature, carry out extraction at 4°C for 2 weeks. After filtration, transfer to a centrifuge tube for later use, and obtain Lithospermum erythrorhizon extract A1 with a solid-liquid ratio of 0.5 g / mL, Lithospermum erythrorhizon extract A2 with a solid-liquid ratio of 0.25 g / mL, and Lithospermum erythrorhizon extract A3 with a solid-liquid ratio of 0.125 g / mL. The solid-liquid ratio (g / mL) of the extract is 1:2 - 1:8.
[0044] 2. Preparation of extracts of other components Take 20.00 g of Paeonia lactiflora, 20.00 g of Salvia miltiorrhiza, 20.00 g of Rubia cordifolia, 20.00 g of Carthamus tinctorius, and 20.00 g of Rosa rugosa and place them in a conical flask. Add 80 mL of olive oil to each respectively. Use a glass rod to mix the powder and olive oil evenly.
[0045] Place the conical flask in a 90°C constant temperature water bath for heat extraction for 60 minutes. After cooling to room temperature, carry out extraction at 4°C for 2 weeks. After filtration, transfer to a centrifuge tube for later use, and obtain extracts with different solid-liquid ratios of different components as shown in Table 1. The solid-liquid ratio of the extract is 1:4.
[0046] Table 1. Solid-liquid ratio table of other components
[0047] 3. Combination of extracts of different components According to the colors of the Chinese medicine extracts of different components prepared in steps 1 and 2, select component A, component B, and component C as raw materials for the Chinese medicine compound color-adjusting lipstick. Based on the component A extract, add extracts of component B and component C with different ratios for color adjustment to obtain a combination ratio of Chinese medicine extracts with different colors and solid-liquid ratios (2.75 g in 3 mL) (Table 2).
[0048] Table 2. Volume ratio of the oil phase of the Chinese medicine color-adjusting lipstick (unit: mL)
[0049] The color results obtained by blending the oil phase bases of the above different component combinations are shown in Figure 1 .
[0050] Example 2. Screening of lipstick matrix 1. Optimization experiment of different ratios of the base Since the traditional Chinese medicine extract exists in the form of an oil phase, the oil-wax ratio of the lipstick and the ratio of different waxes are the key optimized base conditions.
[0051] Based on the color classification experiment in Example 1, a series of traditional Chinese medicine color-adjusted lipsticks with different formulation ratios and their colors ( Figure 1 ) were obtained. Lipstick matrix optimization experiments were carried out by randomly selecting the intermediate color ratio 5. The specific steps are as follows: 1) Take 22.75 g of Component A (the material-liquid ratio is 0.25 g / ml) and add it to a beaker, then add 0.5 g of lanolin, 0.5 g of vaseline, and 1 drop of glycerol (purity is about 99.7%). Subsequently, add beeswax and candelilla wax according to the ingredient ratio in Table 3 below to obtain Material 1; 2) After melting the Material 1 prepared in step 1) at 90 °C, add 0.05 g of vitamin E (purity is about 97.5%) and 0.05 g of rose essential oil and stir evenly to obtain Material 2; 3) Pour the Material 2 prepared in step 2) into a lipstick mold while it is hot, place it in a 4 °C refrigerator and cool it at low temperature for half an hour, then demold to obtain the traditional Chinese medicine color-adjusted lipsticks numbered 1-9.
[0052] Table 3. Ingredient table of natural beeswax and candelilla wax
[0053] 2. Determination of matrix properties A. Quality inspection Heat resistance and cold resistance experiments: After segmenting the lipsticks prepared in Example 2, place them in a constant temperature box at 50 °C, 4 °C, and -20 °C for 48 h (temperature control accuracy ±1 °C), and observe whether there are any deformation or fracture phenomena in the lipsticks.
[0054] The results show that: The morphology of the lipsticks with Matrix 1 and Matrix 3 changed significantly under the condition of 50 °C. Different degrees of cracking occurred in Matrix 3, Matrix 5, Matrix 6, and Matrix 7 under the experimental conditions. Matrix 2, Matrix 4, Matrix 8, and Matrix 9 showed good performance without deformation and cracking ( Figure 2 )
[0055] Light exposure experiment: Place the prepared lipsticks under direct sunlight and non-direct sunlight, and observe the lipsticks. The surface of the lipsticks is smooth, without pores and foreign impurities. The results show that: The surface of the lipsticks is smooth, without pores and foreign impurities.
[0056] B. Determination of lipstick spreadability Weigh 0.1 g of each of the 9 lipstick samples obtained in Step 1, and evenly apply them to the bottom of a weight of 100 g and a diameter of 2.6 cm. Place the weight at the upper end of a glass plate with an inclination angle of 30°, so that the lipstick samples spread on the glass plate under the pressure of the weight until the lipstick at the bottom of the weight is completely wiped clean. Measure the spreading distance of the samples. Under the condition of qualified quality inspection, select the lipstick matrix with the best spreadability as the final lipstick formulation. The spreadability results are shown in Table 4.
[0057] Table 4. Spreading distances of 9 matrix lipsticks
[0058] The above results show that: Matrix No. 2, Matrix No. 4, Matrix No. 8, and Matrix No. 9 have better stability at different temperatures, and there is no deformation or fracture. Combining with the results of the ductility experiment, the extension lengths of Matrix No. 2 and Matrix No. 4 are significantly higher than those of Matrix No. 8 and Matrix No. 9.
[0059] In summary, it can be known that: Matrix No. 2 and Matrix No. 4 are the matrices that meet the conditions selected this time, and Matrix No. 2 is the best matrix. The formulation of Matrix No. 2 is: the weight ratio of natural beeswax, candelilla wax, lanolin, petrolatum, glycerol, rose essential oil, and vitamin E1 is 30:30:30:30:3:3:3.
[0060] Example 3, Lipstick Preparation and Color Evaluation 1. Lipstick Preparation Method 1) Respectively add 2.75 g of the combined traditional Chinese medicine extracts prepared in Example 1 into beakers, numbered 1-12.
[0061] 2) Select the best lipstick matrix (Matrix No. 2) screened in Example 2, and add 0.5 g of natural beeswax, 0.5 g of lanolin, 0.5 g of petrolatum, and 0.05 g of glycerol to each beaker of the 2.75 g combined traditional Chinese medicine extracts. After melting at 80 °C, obtain Material M; 3) Add 0.5 g of candelilla wax to Material M, melt it at 90 °C, and stir evenly until there are no white particles to obtain a uniformly colored Material N; 4) Add 0.05 g of vitamin E and 0.05 g of rose essential oil to Material N, stir evenly, and then pour it into the lipstick mold while it is hot. Place it in a 4 °C refrigerator and cool it at low temperature for half an hour, then demold to obtain the traditional Chinese medicine color-tuned lipsticks numbered 1-12.
[0062] The colors of the prepared lipsticks are as Figure 3 . Each lipstick formula contains 2.75 g of traditional Chinese medicine extracts or their combinations, and the lipstick formulations of different colors are as follows: The lipstick of #48282b is A1A1A1, where A1A1A1 means that the proportion of the traditional Chinese medicine components is 3 ml of Component A1; The lipstick #442020 is A1A1B, where A1A1B indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A1 and 1 ml of component B; The lipstick #550E14 is A1A1C, where A1A1C indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A1 and 1 ml of component C; The lipstick #58121A is A1BC, where A1BC indicates that the ratio of the traditional Chinese medicine components is 1 ml of component A1, 1 ml of component B, and 1 ml of component C; The lipstick #5A141C is A2A2A2, where A2A2A2 indicates that the ratio of the traditional Chinese medicine components is 3 ml of component A2; The lipstick #6D181F is A2A2B, where A2A2B indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A2 and 1 ml of component B; The lipstick #6B1019 is A2A2C, where A2A2C indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A2 and 1 ml of component C; The lipstick #8C1A22 is A2BC, where A2BC indicates that the ratio of the traditional Chinese medicine components is 1 ml of component A2, 1 ml of component B, and 1 ml of component C; The lipstick #9A1A29 is A3A3A3, where A3A3A3 indicates that the ratio of the traditional Chinese medicine components is 3 ml of component A3; The lipstick #991626 is A3A3B, where A3A3B indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A3 and 1 ml of component B; The lipstick #961D2C is A3A3C, where A3A3C indicates that the ratio of the traditional Chinese medicine components is 2 ml of component A3 and 1 ml of component C; The lipstick #AD242B is A3BC, where A3BC indicates that the ratio of the traditional Chinese medicine components is 1 ml of component A3, 1 ml of component B, and 1 ml of component C.
[0063] 2. Color System Classification Use the software ColorHexa to determine the color. According to the RGB color model of the hexadecimal color representation method, classify the range of R to classify the colors of the above lipsticks.
[0064] First, convert each color to an RGB value. In color representation, the red component (R value) of the hexadecimal color value is usually represented in the range of 0 to 255, representing the intensity of red. Then, divide it into 4 groups according to the red component R value < 80, 80 - 120, 120 - 160, > 160.
[0065] The color system classification results of lipsticks with different components are as Figure 4 shown in Table 5.
[0066] Table 5. Color Grading of Lipsticks with Different Components
[0067] 3. Color Stability Test Take the lipsticks with different formulation ratios after color classification in Step 2 and divide them evenly into three parts, labeled as X-1, X-2, and X-3. Place the three parts of lipsticks under different formulation ratios in constant temperature incubators at 4°C, 25°C, and 50°C respectively, and take them out after 48 hours to detect whether their colors have changed.
[0068] The results are as Figure 5 shown: Under the three different temperature treatment conditions, there are no obvious differences in the colors of the 12 lipsticks under different temperature conditions. It can be seen that the colors of the lipsticks with traditional Chinese medicine compound color matching in this group are stable. Through different component ratios of traditional Chinese medicine, a total of 12 lipsticks with different colors are formulated, and the colors are #48282b, #442020, #550E14, #58121A, #5A141C, #6D181F, #6B1019, #8C1A22, #9A1A29, #991626, #961D2C, #AD242B respectively. According to the RGB color model of the hexadecimal color representation method, the range of the red component R value is 68 - 173. It can be seen that the lipsticks with traditional Chinese medicine compound color matching in this group have high color saturation and a wide range of color variation.
[0069] Example 4. Test of Microbial Index and Heavy Metal Index of Lipstick Detect the total number of colonies, the total number of molds and yeasts, thermotolerant coliforms, Staphylococcus aureus, Pseudomonas aeruginosa and other five microorganisms of the prepared lipsticks, and the operation method is carried out in accordance with the "Technical Specifications for Cosmetics Safety" (2015 edition) of the country.
[0070] The results show that all the microbial index items of this sample meet the requirements of the "Technical Specifications for Cosmetics Safety" (2015 edition). The test results are shown in Table 6 below.
[0071] Table 6. Five-item Test Results of Lipstick Microorganisms
[0072] Detect the four heavy metals of mercury, lead, arsenic, and cadmium in the prepared lipsticks, and the operation method is carried out in accordance with the inductively coupled plasma mass spectrometry method in Chapter 4, Section 1.6 of the "Technical Specifications for Cosmetics Safety" (2015 edition) of the country.
[0073] The results show that all the heavy metal index items of this sample meet the requirements of the "Technical Specifications for Cosmetics Safety" (2015 edition). The test results are shown in Table 7 below.
[0074] Table 7. Four-item Test Results of Lipstick Heavy Metals
[0075] The present invention has been described in detail above. For those skilled in the art, without departing from the spirit and scope of the present invention and without the need for unnecessary experiments, the present invention can be implemented within a relatively wide range under equivalent parameters, liquid material ratios and conditions. Although specific embodiments of the present invention are given, it should be understood that the present invention can be further improved. In short, according to the principle of the present invention, this application is intended to cover any modifications, uses or improvements of the present invention, including those that depart from the scope disclosed in this application and are made by conventional techniques known in the art.
Claims
1. A composition containing traditional Chinese medicine color - adjusting components, characterized in that, The composition comprises a traditional Chinese medicine extract, a matrix, a lubricant, a humectant, and an antioxidant; the traditional Chinese medicine extract comprises a lithospermum extract, or a combination of a lithospermum extract and extracts of other components, and the extracts of other components include one or a combination of two of a salvia miltiorrhiza extract and a rubia cordifolia extract. The traditional Chinese medicine extracts are prepared separately and then mixed.
2. The composition according to claim 1, wherein the preparation method of the lithospermum extract is as follows: By weight, first crush the lithospermum powder and pass it through a 60-mesh sieve. Weigh 10.00 - 40.00 g or 10.00 g of the lithospermum powder and place it in a conical flask. Add 80 mL of olive oil, and mix the lithospermum powder and olive oil evenly with a glass rod; place the conical flask in a 90°C constant temperature water bath for heat extraction for 60 minutes, then cool it to room temperature, and extract it at 4°C for 2 weeks. After filtration, the lithospermum extract is obtained; the material-liquid ratio of the lithospermum extract is 0.125 - 0.5 g / mL; the preparation method of the paeonia lactiflora extract is as follows: By weight, first crush the paeonia lactiflora powder and pass it through a 60-mesh sieve. Weigh 20 g of the paeonia lactiflora powder and place it in a conical flask. Add 80 mL of olive oil respectively, and mix the paeonia lactiflora powder and olive oil evenly with a glass rod; place the conical flask in a 90°C constant temperature water bath for heat extraction for 60 minutes, then cool it to room temperature, and extract it at 4°C for 2 weeks. After filtration, the paeonia lactiflora extract is obtained, and the material-liquid ratio of the paeonia lactiflora extract is 0.25 g / mL; the preparation method of the salvia miltiorrhiza extract is as follows: By weight, first crush the salvia miltiorrhiza powder and pass it through a 60-mesh sieve. Weigh 20 g of the salvia miltiorrhiza powder and place it in a conical flask. Add 80 mL of olive oil respectively, and mix the salvia miltiorrhiza powder and olive oil evenly with a glass rod; place the conical flask in a 90°C constant temperature water bath for heat extraction for 60 minutes, then cool it to room temperature, and extract it at 4°C for 2 weeks. After filtration, the salvia miltiorrhiza extract is obtained, and the material-liquid ratio of the salvia miltiorrhiza extract is 0.25 g / mL; the combination of the lithospermum extract and extracts of other components is as follows: 1) The lithospermum extract and the salvia miltiorrhiza extract are combined in a weight ratio of 1 - 2:1; 2) The lithospermum extract and the rubia cordifolia extract are combined in a weight ratio of 1 - 2:1; 3) The lithospermum extract, the salvia miltiorrhiza extract, and the rubia cordifolia extract are combined in a weight ratio of 1:1:
1.
3. The composition according to claim 1 or 2, characterized in that, The matrix is selected from at least one of natural beeswax, candelilla wax, lanolin, and petrolatum; the lubricant includes olive oil and / or sweet almond oil; the humectant includes glycerol; the flavoring agent is selected from one or more of rose essential oil, angelica dahurica essential oil, rhodiola rosea essential oil, cinnamon essential oil, sandalwood essential oil, magnolia liliflora essential oil, osmanthus essential oil, etc.
4. The composition according to claim 3, characterized in that, The matrix consists of natural beeswax, candelilla wax, lanolin, and petrolatum; the lubricant is olive oil; the humectant is glycerol; the flavoring agent is rose essential oil; the antioxidant is vitamin E1; The weight ratio of the traditional Chinese medicine extract, natural beeswax, candelilla wax, lanolin, petrolatum, glycerol, rose essential oil, and vitamin E1 is 165:30:30:30:30:3:3:
3.
5. Use of the composition according to any one of claims 1-4 in the preparation of a lipstick.
6. Preparation method of traditional Chinese medicine color-adjusting lipstick, characterized in that, The method comprises the following steps: 1) Preparation of the traditional Chinese medicine extract combination: Olive oil is mixed with traditional Chinese medicine, and high-temperature hot extraction is carried out. After cooling to room temperature, extraction is carried out at 4 °C for 2 weeks, and the traditional Chinese medicine extract is obtained after filtration; The traditional Chinese medicine extract is a lithospermum erythrorhizon extract, or a combination of a lithospermum erythrorhizon extract and extracts of other components, and the extracts of other components include one or two of a salvia miltiorrhiza extract and a rubia cordifolia extract; 2) Add the matrix and the moisturizer to the traditional Chinese medicine extract combination described in step (1), and melt at 80 °C to obtain material M; 3) Add 30 parts of candelilla wax to material M, melt at 90 °C and stir evenly until there are no white particles to obtain material N; 4) Add 3 parts of vitamin E and 3 parts of rose essential oil to material N and stir evenly to obtain material P; 5) Pour material P into a lipstick mold, cool at a low temperature of 4 °C, and demold to obtain a traditional Chinese medicine color-adjusted lipstick.
7. The method according to claim 6, wherein The traditional Chinese medicine extract combination consists of the following traditional Chinese medicines in parts by weight: 55-165 parts of lithospermum erythrorhizon extract, 0-55 parts of salvia miltiorrhiza extract, and 0-55 parts of rubia cordifolia extract.
8. The method according to claim 6 or 7, characterized in that, The high-temperature hot extraction condition in step 1) is hot extraction in a 90 °C constant temperature water bath for 60 minutes.
9. The method according to claim 6 or 7, characterized in that, The matrix in step 2) consists of natural beeswax, lanolin, and petrolatum with a weight ratio of 30:30:30; the moisturizer is glycerol.
10. A lipstick product prepared by the method according to any one of claims 6-9.
Citation Information
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