Boron trifluoride acetonitrile complex extraction equipment

Abstract

The invention relates to the technical field of boron trifluoride acetonitrile complex extraction, and discloses boron trifluoride acetonitrile complex extraction equipment which comprises a device tank, a device plate is arranged on one side of the outer surface of the device tank, a cover plate is arranged on one side of the outer surface of the device tank, and a connecting rod is arranged on one side of the outer surface of the cover plate. A connecting box is arranged on one side of the outer surface of the device plate, a device pipe is arranged in the connecting box, a transverse pipe is arranged on one side of the outer surface of the device pipe, an inserting rod is arranged in the transverse pipe, and a movable rod is arranged on one side of the outer surface of the inserting rod. According to the device, when a stirring shaft is connected with a device box and then connected with a supporting frame through a device frame, reactants are placed in a device tank, a cover plate and a threaded rod are covered, a motor and a refrigeration plate are started, after raw materials are mixed, an opening and closing plate is opened, the mixed raw materials enter an extraction tank, and a heating plate is started; and waiting for reaction to obtain the boron trifluoride acetonitrile complex extract.

Description

Technical Field

[0001] The present invention relates to the technical field of boron trifluoride acetonitrile complex extraction, and particularly to an extraction device for boron trifluoride acetonitrile complex. Background Art

[0002] Boron trifluoride acetonitrile complex is a chemical substance. It is a highly active catalyst and has wide applications in multiple fields. It is used in various organic synthesis reactions, especially as a special catalyst for the production of antibiotics in the pharmaceutical industry. In the production of cephalosporin antibiotics, its effect is superior to that of boron trifluoride ethyl ether complex. It is used for the extraction of high-energy fuels and the extraction of isotope B10. Boron trifluoride acetonitrile complex is somewhat dangerous. This substance is flammable and should be kept away from heat sources, sparks, open flames, and hot surfaces. It is corrosive to the skin and eyes, and immediate washing is required after contact.

[0003] With the continuous changes in people's lives, the use of boron trifluoride acetonitrile complex by people has become increasingly common. Therefore, in order to meet the market demand, a new structure is urgently needed to complete the extraction of boron trifluoride acetonitrile complex. Summary of the Invention

[0004] (I) Technical Problems to be Solved

[0005] In view of the deficiencies of the prior art, the present invention provides an extraction device for boron trifluoride acetonitrile complex, which has the advantages of being able to extract boron trifluoride acetonitrile complex, etc., and solves the problem of large market demand mentioned in the above background art.

[0006] (II) Technical Solutions

[0007] To achieve the purpose of extracting boron trifluoride acetonitrile complex mentioned in the above background art, the present invention provides the following technical solution: An extraction device for boron trifluoride acetonitrile complex, including a device tank. One side of the outer surface of the device tank is provided with a device plate, one side of the outer surface of the device tank is provided with a cover plate, one side of the outer surface of the cover plate is provided with a connecting rod, one side of the outer surface of the device plate is provided with a connecting box, a device tube is arranged inside the connecting box, a cross tube is arranged on one side of the outer surface of the device tube, a plug rod is arranged inside the cross tube, a movable rod is arranged on one side of the outer surface of the plug rod, a threaded plate is arranged on one side of the outer surface of the movable rod, a threaded rod is arranged on one side of the outer surface of the threaded plate, and a refrigeration plate is arranged on one side of the inner wall of the device tank;

[0008] Inside the device tank, a support frame is provided. On one side of the outer surface of the support frame, a device rack is provided. On one side of the outer surface of the device rack, a motor is provided. On one side of the outer surface of the motor, a device box is provided. Inside the device box, an auxiliary pipe is provided. One end of the auxiliary pipe is provided with a stirring shaft. On one side of the outer surface of the auxiliary pipe, a branch pipe is provided. Inside the branch pipe, a limiting rod is provided. On one side of the outer surface of the limiting rod, a groove plate is provided. On one side of the outer surface of the groove plate, a turntable is provided. On one side of the outer surface of the turntable, a rotating rod is provided. On one side of the outer surface of the turntable, a movable groove plate is provided. On one side of the outer surface of the movable groove plate, a spring is provided. On one side of the outer surface of the device tank, an extraction tank is provided. Inside the extraction tank, a switch plate is provided. Inside the extraction tank, a heating plate is provided.

[0009] Preferably, the number of the device plates is two, and the two device plates are evenly arranged on the left and right sides of the outer surface of the device tank and are fixedly connected to the device tank.

[0010] Preferably, the number of the connection boxes is two, and the two connection boxes are evenly arranged on one side of the outer surfaces of the left and right device plates and are fixedly connected to the device plates. And device pipes are arranged in both the left and right connection boxes.

[0011] Preferably, one end of the device pipe is fixedly connected to one side of the inner wall of the connection box, and the other end of the device pipe contacts the other side of the inner wall of the connection box and penetrates through one side of the inner wall of the connection box to the outer surface of the connection box and is fixedly connected to the connection box.

[0012] Preferably, the number of the horizontal pipes is two, and the two horizontal pipes are evenly arranged in the left and right connection boxes. One end of the horizontal pipe is fixedly connected to one side of the inner wall of the connection box, and the other end contacts one side of the outer surface of the device pipe and penetrates through one side of the outer surface of the device pipe to the inner side of the device pipe and is fixedly connected to the device pipe.

[0013] Preferably, the number of the auxiliary pipes is two, and the two auxiliary pipes are evenly arranged in the device box.

[0014] Preferably, one end of the auxiliary pipe is fixedly connected to one side of the inner wall of the device box, and the other end contacts one side of the inner wall of the device box and penetrates through one side of the inner wall of the device box to the outer surface of the device box and is fixedly connected to the device box.

[0015] Preferably, the number of the rotating rods is multiple, and every two of the multiple rotating rods are in a group and are evenly arranged on one side of the outer surfaces of the left and right turntables and are fixedly connected to the turntables.

[0016] Chutes are provided on the upper and lower sides of the inner wall of the horizontal pipe. One side of the outer surface of the chute is in contact with one side of the inner wall of the horizontal pipe and penetrates through one side of the inner wall of the horizontal pipe to one side of the outer surface of the horizontal pipe. A plug rod is arranged inside the horizontal pipe. A sliding rod is arranged on one side of the outer surface of the plug rod. One end of the sliding rod is fixedly connected to one side of the outer surface of the plug rod, and the other end of the sliding rod is slidably connected to the chute. This makes the plug rod more stable when moving left and right. One end of the movable rod is fixedly connected to one side of the outer surface of the plug rod, and the threaded plate is fixedly connected to the movable rod. This makes the threaded plate drive the movable rod to drive the plug rod to move left and right when moving left and right.

[0017] There are multiple rotating rods. Every two of the multiple rotating rods form a group and are evenly arranged on one side of the outer surface of the left and right turntables and are fixedly connected to the outer surface of the turntable. One rotating rod on one side of each group of rotating rods is slidably connected to the inner wall of the movable groove plate, and the other rotating rod is slidably connected to the inner wall of the groove plate. This makes the movable groove plate drive the turntable to rotate when moving up and down, and makes the other rotating rod drive the limiting rod to move left and right.

[0018] A device rod is arranged inside the device box. The upper and lower ends of the device rod are respectively fixedly connected to the upper side of the inner wall of the device box and the upper side of the outer surface of the branch pipe. The device rod penetrates through the movable groove plate. The upper and lower ends of the spring are respectively fixedly connected to one side of the inner wall of the device box and the upper side of the outer surface of the movable groove plate. This makes the movable groove plate move under the thrust of the spring when not affected by external forces, and makes the limiting rod in an inserted state with the stirring shaft.

[0019] Compared with the prior art, the present invention provides a boron trifluoride acetonitrile complex extraction device, which has the following beneficial effects:

[0020] 1. In the present invention, through the stirring shaft arranged in the device, when the stirring shaft is connected to the device box, then connected to the support frame through the device frame, and the reactants are placed in the device tank and the cover plate is covered, the threaded rod is rotated, and the motor and the refrigerating plate are started. When the raw materials are mixed, the opening and closing plate is opened, so that the mixed raw materials enter the extraction tank, and the heating plate is started to wait for the reaction to obtain the boron trifluoride acetonitrile complex extract.

[0021] 2. In the present invention, through the movable groove plate arranged in the device, when the movable groove plate moves up and down, the turntable rotates. When the turntable rotates, the groove plate drives the limiting rod to move left and right. When the limiting rod is disengaged from the stirring shaft, the stirring shaft can be removed, thus achieving the effect of replacing the stirring shaft. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] Figure 1 is a schematic structural diagram of the present invention;

[0023] Figure 2 is a front sectional view of the structure of the present invention;

[0024] Figure 3 is the first partial enlarged front sectional view of the structure of the present invention;

[0025] Figure 4 is the second partial enlarged front sectional view of the structure of the present invention.

[0026] Wherein: 1. device tank; 2. device plate; 3. cover plate; 4. connecting rod; 5. connecting box; 6. device pipe; 7. horizontal pipe; 8. insertion rod; 9. movable rod; 10. threaded plate; 11. threaded rod; 12. support frame; 13. device frame; 14. motor; 15. device box; 16. auxiliary pipe; 17. stirring shaft; 18. branch pipe; 19. limiting rod; 20. groove plate; 21. turntable; 22. rotating rod; 23. movable groove plate; 24. spring; 25. refrigeration plate; 26. extraction tank; 27. opening and closing plate; 28. heating plate. Specific embodiments

[0027] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

[0028] Please refer to Figures 1-4 , a boron trifluoride acetonitrile complex extraction device, including a device tank 1;

[0029] As Figures 1-4 shown, on one side of the outer surface of the device tank 1, there is a device plate 2, on one side of the outer surface of the device tank 1, there is a cover plate 3, on one side of the outer surface of the cover plate 3, there is a connecting rod 4, on one side of the outer surface of the device plate 2, there is a connecting box 5, inside the connecting box 5, there is a device pipe 6, on one side of the outer surface of the device pipe 6, there is a horizontal pipe 7, inside the horizontal pipe 7, there is an insertion rod 8, on one side of the outer surface of the insertion rod 8, there is a movable rod 9, on one side of the outer surface of the movable rod 9, there is a threaded plate 10, on one side of the outer surface of the threaded plate 10, there is a threaded rod 11, and on one side of the inner wall of the device tank 1, there is a refrigeration plate 25;

[0030] Inside the device tank 1, there is a support frame 12. On one side of the outer surface of the support frame 12, there is a device rack 13. On one side of the outer surface of the device rack 13, there is a motor 14. On one side of the outer surface of the motor 14, there is a device box 15. Inside the device box 15, there is an auxiliary pipe 16. One end of the auxiliary pipe 16 is provided with a stirring shaft 17. On one side of the outer surface of the auxiliary pipe 16, there is a branch pipe 18. Inside the branch pipe 18, there is a limiting rod 19. On one side of the outer surface of the limiting rod 19, there is a groove plate 20. On one side of the outer surface of the groove plate 20, there is a turntable 21. On one side of the outer surface of the turntable 21, there is a rotating rod 22. On one side of the outer surface of the turntable 21, there is a movable groove plate 23. On one side of the outer surface of the movable groove plate 23, there is a spring 24. On one side of the outer surface of the device tank 1, there is an extraction tank 26. Inside the extraction tank 26, there is a switching plate 27. Inside the extraction tank 26, there is a heating plate 28.

[0031] Specifically, as Figures 1-4 shown, the number of device plates 2 is two, and the two device plates 2 are evenly arranged on the left and right sides of the outer surface of the device tank 1 and are fixedly connected to the device tank 1.

[0032] Specifically, as Figures 1-4 shown, the number of connection boxes 5 is two, and the two connection boxes 5 are evenly arranged on one side of the outer surfaces of the device plates 2 on the left and right sides and are fixedly connected to the device plates 2, and device pipes 6 are arranged in both the left and right connection boxes 5.

[0033] Specifically, as Figures 1-4 shown, one end of the device pipe 6 is fixedly connected to one side of the inner wall of the connection box 5, and the other end of the device pipe 6 contacts the other side of the inner wall of the connection box 5 and penetrates one side of the inner wall of the connection box 5 to the outer surface side of the connection box 5 and is fixedly connected to the connection box 5.

[0034] Specifically, as Figures 1-4 shown, the number of horizontal pipes 7 is two, and the two horizontal pipes 7 are evenly arranged in the left and right connection boxes 5. One end of the horizontal pipe 7 is fixedly connected to one side of the inner wall of the connection box 5, and the other end contacts one side of the outer surface of the device pipe 6 and penetrates one side of the outer surface of the device pipe 6 to the inner wall side of the device pipe 6 and is fixedly connected to the device pipe 6.

[0035] Specifically, as Figures 1-4 shown, the number of auxiliary pipes 16 is two, and the two auxiliary pipes 16 are evenly arranged in the device box 15.

[0036] Specifically, as Figures 1-4 shown, one end of the auxiliary pipe 16 is fixedly connected to one side of the inner wall of the device box 15, and the other end contacts one side of the inner wall of the device box 15 and penetrates one side of the inner wall of the device box 15 to the outer surface side of the device box 15 and is fixedly connected to the device box 15.

[0037] Specifically, asFigures 1-4 As shown, the number of the rotating rods 22 is multiple, and every two of the multiple rotating rods 22 form a group, which are evenly arranged on one side of the outer surface of the left and right turntables 21 and fixedly connected to the turntables 21.

[0038] Through the above technical solution, sliding grooves are arranged on the upper and lower sides of the inner wall of the horizontal pipe 7, one side of the outer surface of the sliding groove is in contact with one side of the inner wall of the horizontal pipe 7 and penetrates through one side of the inner wall of the horizontal pipe 7 to the outer surface side of the horizontal pipe 7. The inserting rod 8 is arranged in the horizontal pipe 7, a sliding rod is arranged on one side of the outer surface of the inserting rod 8, one end of the sliding rod is fixedly connected to one side of the outer surface of the inserting rod 8, and the other end of the sliding rod is slidably connected to the sliding groove, so that the inserting rod 8 is more stable when moving left and right. One end of the movable rod 9 is fixedly connected to one side of the outer surface of the inserting rod 8, and the threaded plate 10 is fixedly connected to the movable rod 9, so that when the threaded plate 10 moves left and right, the movable rod 9 drives the inserting rod 8 to move left and right;

[0039] The number of the rotating rods 22 is multiple, and every two of the multiple rotating rods 22 form a group, which are evenly arranged on one side of the outer surface of the left and right turntables 21 and fixedly connected to one side of the outer surface of the turntables 21. One side of each group of rotating rods 22 is slidably connected to the inner wall of the movable groove plate 23, and the other side of the rotating rod 22 is slidably connected to the inner wall of the groove plate 20, so that when the movable groove plate 23 moves up and down, the rotating rod 22 drives the turntable 21 to rotate, and the other rotating rod 22 drives the limiting rod 19 to move left and right;

[0040] A device rod is arranged inside the device box 15, the upper and lower ends of the device rod are respectively fixedly connected to the upper side of the inner wall of the device box 15 and the upper side of the outer surface of the branch pipe 18, the device rod penetrates through the movable groove plate 23, and the upper and lower ends of the spring 24 are respectively fixedly connected to one side of the inner wall of the device box 15 and the upper side of the outer surface of the movable groove plate 23, so that when the movable groove plate 23 is not affected by external forces, it moves under the thrust of the spring 24, and the limiting rod 19 is in an inserted state with the stirring shaft 17.

[0041] During use, connect the device tank 1 to the extraction tank 26, then insert the device rack 13 into the support frame 12, so that the stirring shaft 17 is arranged in the device tank 1, add raw materials, cover the cover plate 3, start the refrigeration plate 25, stir for a period of time, then open the opening and closing plate 27, so that the mixed raw materials enter the extraction tank 26, close the opening and closing plate 27, start the heating plate 28, and wait for the preparation to be completed.

[0042] Although the embodiments of the present invention have been shown and described, those of ordinary skill in the art can understand that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principles and spirit of the present invention. The scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A boron trifluoride acetonitrile complex extraction device, comprising a device tank (1), characterized in that: On one side of the outer surface of the device tank (1), a device plate (2) is provided. On one side of the outer surface of the device tank (1), a cover plate (3) is provided. On one side of the outer surface of the cover plate (3), a connecting rod (4) is provided. On one side of the outer surface of the device plate (2), a connecting box (5) is provided. Inside the connecting box (5), a device pipe (6) is provided. On one side of the outer surface of the device pipe (6), a horizontal pipe (7) is provided. Inside the horizontal pipe (7), a plug rod (8) is provided. On one side of the outer surface of the plug rod (8), a movable rod (9) is provided. On one side of the outer surface of the movable rod (9), a threaded plate (10) is provided. On one side of the outer surface of the threaded plate (10), a threaded rod (11) is provided. On one side of the inner wall of the device tank (1), a refrigeration plate (25) is provided; Inside the device tank (1), a support frame (12) is provided. On one side of the outer surface of the support frame (12), a device rack (13) is provided. On one side of the outer surface of the device rack (13), a motor (14) is provided. On one side of the outer surface of the motor (14), a device box (15) is provided. Inside the device box (15), an auxiliary pipe (16) is provided. One end of the auxiliary pipe (16) is provided with a stirring shaft (17). On one side of the outer surface of the auxiliary pipe (16), a branch pipe (18) is provided. Inside the branch pipe (18), a limiting rod (19) is provided. On one side of the outer surface of the limiting rod (19), a groove plate (20) is provided. On one side of the outer surface of the groove plate (20), a turntable (21) is provided. On one side of the outer surface of the turntable (21), a rotating rod (22) is provided. On one side of the outer surface of the turntable (21), a movable groove plate (23) is provided. On one side of the outer surface of the movable groove plate (23), a spring (24) is provided. On one side of the outer surface of the device tank (1), an extraction tank (26) is provided. Inside the extraction tank (26), a switching plate (27) is provided. Inside the extraction tank (26), a heating plate (28) is provided.

2. The extraction device for boron trifluoride acetonitrile complex according to claim 1, wherein: The number of the device plates (2) is two, and the two device plates (2) are evenly arranged on the left and right sides of the outer surface of the device tank (1) and are fixedly connected to the device tank (1).

3. The extraction device for boron trifluoride acetonitrile complex according to claim 1, characterized in that: The number of the connecting boxes (5) is two, and the two connecting boxes (5) are evenly arranged on one side of the outer surfaces of the left and right device plates (2) and are fixedly connected to the device plates (2). And device pipes (6) are arranged in both the left and right connecting boxes (5).

4. A boron trifluoride acetonitrile complex extraction device according to claim 1, characterized in that: One end of the device pipe (6) is fixedly connected to one side of the inner wall of the connecting box (5), and the other end of the device pipe (6) contacts the other side of the inner wall of the connecting box (5), penetrates through one side of the inner wall of the connecting box (5) to the outer surface side of the connecting box (5), and is fixedly connected to the connecting box (5).

5. The extraction device for boron trifluoride acetonitrile complex according to claim 1, characterized in that: The number of the horizontal pipes (7) is two, and the two horizontal pipes (7) are evenly arranged in the left and right connecting boxes (5). One end of the horizontal pipe (7) is fixedly connected to one side of the inner wall of the connecting box (5), and the other end contacts the outer surface side of the device pipe (6), penetrates through the outer surface side of the device pipe (6) to the inner wall side of the device pipe (6), and is fixedly connected to the device pipe (6).

6. The extraction device for boron trifluoride acetonitrile complex according to claim 1, characterized in that: The number of the auxiliary pipes (16) is two, and the two auxiliary pipes (16) are evenly arranged in the device box (15).

7. The extraction device for boron trifluoride acetonitrile complex according to claim 1, wherein: One end of the auxiliary pipe (16) is fixedly connected to one side of the inner wall of the device box (15), and the other end contacts one side of the inner wall of the device box (15), penetrates through one side of the inner wall of the device box (15) to one side of the outer surface of the device box (15), and is fixedly connected to the device box (15).

8. The extraction device for boron trifluoride acetonitrile complex according to claim 1, wherein: The number of the rotating rods (22) is multiple, and every two of the multiple rotating rods (22) are in a group, which are evenly arranged on one side of the outer surfaces of the left and right turntables (21) and are fixedly connected to the turntables (21).

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