Oral care solution containing natural components and preparation method of oral care solution

Abstract

The invention discloses an oral care solution based on natural raw materials and a preparation method thereof, and belongs to the technical field of oral care. The oral care solution is prepared from the following raw materials: mint leaves, halite, gypsum, divaricate saposhnikovia roots, Chinese prickly ash and cloves. The preparation method comprises the following steps: mixing the raw materials, and distilling through water boiling type distillation equipment to extract the active ingredients. Through the synergistic effect of multiple components, the oral care solution disclosed by the invention can effectively refresh breath and purify bad breath, and has remarkable insecticidal and mothproof effects. The used raw materials are all natural components, are safe and non-irritant, and are suitable for daily oral care of various people.

Description

Technical Field

[0001] The present invention relates to the technical field of oral care, and particularly relates to an oral care liquid mainly composed of natural plant components and a water-boiling distillation preparation process thereof. This care liquid has the effects of refreshing the breath, purifying oral odor, and killing insects and preventing tooth decay. Background Art

[0002] With the increasing attention of people to oral health, there are a wide variety of oral care products on the market. However, most products rely on chemically synthesized components (such as bactericides, artificial fragrances, etc.), which may cause irritation to the oral mucosa and easily lead to an imbalance in the oral microecology after long-term use. Due to the characteristics of natural plant components being mild, low-irritation, and having multiple effects, they have become a research hotspot in the field of oral care. Currently, the technology for extracting effective plant components by distillation process has gradually matured, but the natural formulations for oral odor and tooth decay problems still need to be optimized.

[0003] In the prior art, components such as mint leaves and blue salt have been applied in oral care, but there are few studies on combining them in specific proportions and using the distillation process to enhance the synergistic effect. The present invention aims to provide a safe and efficient oral care liquid by screening the ratio of natural raw materials and adopting a water-boiling distillation process to solve the deficiencies of existing products. Summary of the Invention

[0004] Provide an oral care liquid based on natural raw materials, which realizes multiple effects of refreshing the breath, purifying odor, and killing insects and preventing tooth decay through specific component ratios and distillation processes, while avoiding the side effects of chemical additives.

[0005] Fixed ratio formula (parts by weight): 10 parts of mint leaves, 10 parts of blue salt, 10 parts of gypsum, 10 parts of ledebouriella root, 4 parts of Chinese prickly ash, 4 parts of cloves.

[0006] Ratio range formula (parts by weight): 8 - 12 parts of mint leaves, 8 - 12 parts of blue salt, 8 - 12 parts of gypsum, 8 - 12 parts of ledebouriella root, 3 - 6 parts of Chinese prickly ash, 3 - 6 parts of cloves.

[0007] 1. Pretreatment of raw materials: Wash, dry, and crush mint leaves, ledebouriella root, Chinese prickly ash, and cloves to a particle size of 0.5 mm - 2 mm; Crush blue salt and gypsum to a particle size ≤ 0.2 mm and set aside.

[0008] 2. Water-boiling distillation: Put the pretreated raw materials into a water-boiling distillation device and add distilled water 6 - 10 times the total weight of the raw materials; Heat to 100 - 105 °C, maintain a slightly boiling state and distill for 2 - 3 hours, and collect the distillate.

[0009] 3. Filtration and aging: Filter the distillate through a filter cloth, and age the filtrate in a cool place for 12 - 24 hours to obtain the finished product.

[0010] Use it directly as a mouthwash. Take 10 - 15 ml each time, gargle for 30 seconds, 2 - 3 times a day; Refresh the breath and prevent dental caries.

[0011] Natural and safe: Made from all - plant - source raw materials, without chemical preservatives and artificial fragrances, mild and non - irritating, suitable for long - term use.

[0012] Multiple effects: Peppermint leaves: Contain menthol and menthone, quickly refresh the breath and inhibit the reproduction of oral bacteria; Qing salt: Sterilize and reduce inflammation, regulate the oral osmotic pressure, and improve gum health; Gypsum: Astringe to stop bleeding and promote the repair of oral mucosa; Ledebouriella root + Chinese prickly ash + Clove: Contain volatile oil components (such as eugenol), have broad - spectrum antibacterial and insecticidal effects, and effectively prevent dental caries and periodontal problems.

[0013] Process advantages: The water - boiling and distillation process fully extracts the volatile active ingredients (such as menthol and clove oil) in the raw materials, while retaining minerals and water - soluble active ingredients, ensuring the integrity and synergistic effect of the active ingredients.

[0014] 3.4.1 Example 1: Preparation with standard formula Raw material formula (parts by weight): 10 g of peppermint leaves, 10 g of Qing salt, 10 g of gypsum, 10 g of ledebouriella root, 4 g of Chinese prickly ash, 4 g of clove Preparation steps: 1. Raw material pretreatment: Wash the peppermint leaves, ledebouriella root, Chinese prickly ash, and clove, dry them at 60 °C and then crush them to 20 mesh; crush the Qing salt and gypsum to 100 mesh.

[0015] 2. Water - boiling and distillation: Put the raw materials into the distillation kettle, add 480 g of distilled water (8 times the total weight of the raw materials), heat to boiling and then keep slightly boiling for 2 hours, and collect about 320 ml of distillate.

[0016] 3. Filtration and aging: Filter the distillate through a 100 - mesh filter cloth, and age the filtrate in a sealed container at 25 °C for 24 hours to obtain a light - yellow clear liquid.

[0017] 3.4.2 Example 2: High - peppermint formula Raw material formula (parts by weight): 12 g of peppermint leaves, 10 g of Qing salt, 8 g of gypsum, 9 g of ledebouriella root, 5 g of Chinese prickly ash, 4 g of clove Preparation steps: The same as in Example 1, the distillation time was adjusted to 2.5 hours, and the water addition was 9 times the total weight of the raw materials, obtaining a light green clear liquid with a strong mint odor.

[0018] 3.4.3 Example 3: High bactericidal formula Raw material formula (parts by weight): 8 g of mint leaves, 12 g of blue salt, 10 g of gypsum, 8 g of ledebouriella root, 6 g of Chinese prickly ash, 6 g of cloves Preparation steps: The same as in Example 1, the distillation time was 3 hours, and the water addition was 10 times the total weight of the raw materials, obtaining a light yellowish-green clear liquid with an obvious clove odor.

[0019] 3.4.4 Comparative Example 1: Single component control (mint group) Raw material formula: 48 g of mint leaves (the total weight is the same as in Example 1) Preparation steps: The same as in Example 1, after obtaining the distillate, filter and age.

[0020] 3.4.5 Comparative Example 2: Missing component control (no clove group) Raw material formula: 10 g of mint leaves, 10 g of blue salt, 10 g of gypsum, 10 g of ledebouriella root, 4 g of Chinese prickly ash, 0 g of cloves (substituted with an equal amount of gypsum) Preparation steps: The same as in Example 1.

[0021] 3.4.6 Comparative Example 3: Traditional process control (soaking method) Raw material formula: The same as in Example 1 Preparation steps: Crush the raw materials and add 480 g of distilled water, soak at room temperature for 24 hours, and use directly after filtration.

[0022] 3.4.7 Trial feedback results Recruit 60 volunteers with bad breath and divide them into 6 groups, with 10 people in each group using the above 6 cases 3 times a day for 14 consecutive days, and record the average usage experience: Sensory evaluation of breath freshness (1 - 5 points, 5 points being the best) Conclusion: In the present invention, each component is indispensable. The whole formula uses natural raw materials without any chemical additives, can effectively clean the oral cavity, freshen the breath, and protect the oral cavity environment.

Claims

1. An oral care liquid, characterized in that, It consists of the following raw materials: Peppermint leaves, rock salt, gypsum, ledebouriella root, Chinese prickly ash, cloves.

2. The oral care liquid according to claim 1, wherein The weight proportion range of the said raw materials is: Peppermint leaves 8 - 12 parts, rock salt 8 - 12 parts, gypsum 8 - 12 parts, ledebouriella root 8 - 12 parts, Chinese prickly ash 3 - 6 parts, cloves 3 - 6 parts.

3. An oral care liquid, characterized in that, It consists of the following raw materials by weight: Peppermint leaves 10 parts, rock salt 10 parts, gypsum 10 parts, ledebouriella root 10 parts, Chinese prickly ash 4 parts, cloves 4 parts.

4. The oral care liquid according to claim 1, 2, or 3, characterized in that, The said raw materials are prepared by a water-boiling distillation process, and the specific steps include: After crushing the raw materials, add distilled water 6 - 10 times the total weight of the raw materials; Distill at 100 - 105 °C for 2 - 3 hours; Collect the distillate, filter it and age for 12 - 24 hours.