Slow-release low-irritation fever composition as well as preparation method and application thereof

Abstract

The invention belongs to the technical field of cosmetics, and discloses a slow-release low-irritation heating composition as well as a preparation method and application thereof. The preparation method comprises the following steps: (1) adding agar, sodium alginate, a humectant, a thickener, a water-soluble preservative and water into an emulsifying pot, heating and stirring until the materials are completely dissolved, then sequentially adding a skin conditioner, vanillyl butyl ether and phenoxyethanol, uniformly stirring, and preserving heat for later use; and (2) dropping the heat-insulating mixed material obtained in the step (1) into cooling oil of 0-5 DEG C through a pill dropping machine, cooling to obtain a spherical object, conveying the spherical object to a cleaning pool, and cleaning oil on the surface of the spherical object to obtain the slow-release low-irritation heating composition. According to the invention, vanillyl butyl ether is adopted as a heating component, and wrapping treatment is carried out through a specific preparation process, so that certain slow release can be achieved, irritation can be reduced, the thermal inductance effect of ginger can be better simulated, and the thermal inductance stability can be improved.

Description

Technical Field

[0001] This invention belongs to the field of cosmetic technology, specifically relating to a sustained-release, low-irritant, and heat-generating composition, its preparation method, and its application. Background Technology

[0002] Currently, some shampoos contain ingredients such as peppermint and ginger, which can dilate scalp capillaries, promote scalp blood circulation, improve hair follicle nutrition supply, and enhance scalp metabolism through physical stimulation or the action of plant active substances, thereby preventing hair loss. For example, patent CN 109730956 B discloses a ginger shampoo, which is prepared from the following raw materials by weight percentage: ginger 20%-50%, sodium lauryl ether sulfate 10%-15%, polyquaternium-10 0.2%-0.5%, acrylate copolymer 2%-6%, polyquaternium-22 1%-4%, polyquaternium-47 1%-4%, cocamide DEA 1%-3%, cocamidopropyl betaine 6%-10%, lauryl ether-23 1%-2%, argan kernel oil 2%-3%, DMDM ​​hydantoin 0.3%-0.5%, fragrance 0.2%-1%, and pure water as the balance.

[0003] However, the stability and sustained-release properties of active heat-sensing components in plants such as ginger (e.g., gingerol) are relatively poor, resulting in poor storage stability and heat-generating stability when applied to products; in addition, the strong odor of plant components such as ginger and the sensitivity of some people to them limit their application. Summary of the Invention

[0004] In view of the shortcomings and deficiencies of the existing technology, the primary objective of the present invention is to provide a method for preparing a sustained-release, low-irritant, exothermic composition.

[0005] Another object of the present invention is to provide a sustained-release, low-irritant, exothermic composition prepared by the above method.

[0006] Another object of the present invention is to provide the use of the above-described sustained-release, low-irritant, heat-generating composition in shampoos.

[0007] The objective of this invention is achieved through the following technical solution:

[0008] A method for preparing a sustained-release, low-irritant, excitatory composition includes the following preparation steps:

[0009] (1) Add agar, sodium alginate, humectant, thickener, water-soluble preservative and water to an emulsifying pot, heat and stir to completely dissolve the materials, then add skin conditioning agent, vanillyl butyl ether and phenoxyethanol in sequence and stir evenly, keep warm for later use.

[0010] (2) The heat-insulating mixture from step (1) is cooled by dripping it into cooling oil at 0-5°C using a pelletizing machine to obtain spherical objects. The spherical objects are then transferred to a cleaning tank to clean the oil off the surface of the spherical objects, thus obtaining a slow-release, low-irritant, exothermic composition.

[0011] Furthermore, the moisturizer mentioned in step (1) includes at least one of sodium hyaluronate and glycerin.

[0012] Further, the thickener mentioned in step (1) includes at least one of hydroxyethyl cellulose and hydroxypropyl methyl cellulose.

[0013] Furthermore, the water-soluble preservative mentioned in step (1) is sodium benzoate.

[0014] Further, the skin conditioning agent mentioned in step (1) is at least one of pearl powder, synthetic fluorophlogopite, jojoba seed oil, keratin, and hydrolyzed keratin.

[0015] Furthermore, the heating and heat preservation temperature in step (1) is 85-90°C.

[0016] Furthermore, the cooling oil mentioned in step (2) is liquid paraffin, methyl silicone oil or vegetable oil.

[0017] Furthermore, the cleaning tank in step (2) uses an aqueous solution containing a surfactant.

[0018] In the above preparation method, the mass percentage of each material is as follows: agar 10-15%, sodium alginate 0.2-0.4%, humectant 1-3%, thickener 0.4-0.8%, water-soluble preservative 0.3-0.6%, skin conditioning agent 3-6%, vanillyl butyl ether 3-8%, phenoxyethanol 0.5-1%, and the balance is water.

[0019] More preferably, the mass percentage of each material is as follows: agar 10-15%, sodium alginate 0.2-0.4%, sodium hyaluronate 0.05-0.2%, glycerin 1.5-2.5%, hydroxyethyl cellulose 0.25-0.35%, hydroxypropyl methylcellulose 0.25-0.35%, sodium benzoate 0.4-0.5%, pearl powder 0.3-0.5%, synthetic fluorophlogopite 0.4-0.6%, jojoba seed oil 2-4%, keratin 0.1-0.3%, hydrolyzed keratin 0.4-0.6%, vanillyl butyl ether 4-6%, phenoxyethanol 0.5-1%, and the balance being water.

[0020] A sustained-release, low-irritant, exothermic composition was prepared by the method described above.

[0021] Application of the above-mentioned sustained-release, low-irritant, heat-generating composition in shampoos.

[0022] Compared with the prior art, the beneficial effects of the present invention are:

[0023] (1) The sustained-release, low-irritation heating composition of the present invention uses vanillyl butyl ether as the heating component. Vanillyl butyl ether is an oil-soluble thermosensitive agent. After being applied topically to the skin, it can quickly produce a mild and lasting pyrogenic effect, including accelerating microcirculation, stimulating subcutaneous fat metabolism, and promoting capillary blood circulation. When applied to shampoo, it can generate a warming sensation, giving consumers the feeling of ginger; in anti-hair loss shampoo, it has the effect of promoting scalp blood flow, enhancing hair follicle metabolic activity, and helping to prevent hair loss.

[0024] (2) The heat sensation of vanillyl butyl ether lasts for several hours and can produce a strong heat sensation with very low dosage. When applied to shampoo, the heat sensation is relatively direct and strong, which can easily cause some irritation and is somewhat different from the sensation of real ginger. This invention uses a specific preparation process to encapsulate the ether, which can achieve a certain degree of slow release under the rubbing force during shampooing, reducing irritation and better simulating the heat sensation of ginger and improving the stability of the heat sensation. Detailed Implementation

[0025] The present invention will be further described in detail below with reference to embodiments, but the implementation of the present invention is not limited thereto.

[0026] Example 1

[0027] A sustained-release, low-irritant, exothermic composition is prepared from the following components in weight percentages:

[0028] The composition includes: 12% agar, 0.3% sodium alginate, 0.1% sodium hyaluronate, 2% glycerin, 0.3% hydroxyethyl cellulose, 0.3% hydroxypropyl methylcellulose, 0.45% sodium benzoate, 0.4% pearl powder, 0.5% synthetic fluorophlogopite, 3% jojoba seed oil, 0.2% keratin, 0.5% hydrolyzed keratin, 5% vanillyl butyl ether, 0.8% phenoxyethanol, and 74.15% water.

[0029] The preparation method of the above-mentioned sustained-release, low-irritant, excitatory composition includes the following steps:

[0030] (1) Prepare each raw material according to the above mass percentage content. Add agar, sodium alginate, sodium hyaluronate, glycerin, hydroxyethyl cellulose, hydroxypropyl methylcellulose, sodium benzoate and water to the emulsification pot, heat and stir to 85-90℃ to completely dissolve the materials. Then add pearl powder, synthetic fluorophlogopite, jojoba seed oil, keratin, hydrolyzed keratin, vanillyl butyl ether and phenoxyethanol in sequence and stir evenly. Keep warm for later use.

[0031] (2) The heat-insulating mixture from step (1) is pumped to a pelletizing machine and cooled with cooling oil (liquid paraffin with a viscosity of 40-70 mPa·s (25°C)) at 0-5°C to obtain spherical objects. The spherical objects are then transferred to an aqueous cleaning tank containing surfactants to clean the oil off the surface of the spherical objects, thus obtaining a slow-release, low-irritant, exothermic composition.

[0032] The application of the sustained-release, low-irritant, effervescent composition obtained in this embodiment in shampoo. The basic shampoo formulation is as follows:

[0033] The composition includes 8% ammonium lauryl ether sulfate, 5% ammonium lauryl sulfate, 4% sustained-release low-irritant effervescent composition, 3% cocamidopropyl betaine, 1% cocamidopropyl DEA, 0.5% ethylene glycol stearate, 0.4% fragrance, 0.3% polyquaternium-10, 0.2% citric acid, and 0.1% disodium EDTA.

[0034] The shampoo obtained in this embodiment was evaluated for its thermal effect and tested for thermal stability (40±2℃, 75%±5%RH, 180-day accelerated test). A shampoo with the same amount of ginger extract instead of the heating composition was used as a control group. The test results are shown in Table 1 below.

[0035] Table 1 Results of thermal effect and thermal stability tests

[0036] Test group odor Thermal effect Thermal stability Heating composition Mild scent The heating effect is noticeable, and it is gentle and non-irritating. The thermal effect is obvious, and the difference in thermal sensation before and after the acceleration test is not significant. ginger extract The smell is rather pungent The heating effect is noticeable, and it is gentle and non-irritating. The heating effect was not obvious, and the heating effect was significantly reduced after accelerated testing.

[0037] The results above show that the heating composition of the present invention can avoid the pungent smell of ginger, has a good heating effect, and has better heating stability than ginger extract.

[0038] Example 2

[0039] A sustained-release, low-irritant, exothermic composition is prepared from the following components in weight percentages:

[0040] The composition includes: 10% agar, 0.4% sodium alginate, 0.2% sodium hyaluronate, 1.5% glycerin, 0.35% hydroxyethyl cellulose, 0.35% hydroxypropyl methylcellulose, 0.4% sodium benzoate, 0.3% pearl powder, 0.6% synthetic fluorophlogopite, 4% jojoba seed oil, 0.1% keratin, 0.6% hydrolyzed keratin, 4% vanillyl butyl ether, 0.5% phenoxyethanol, and 76.7% water.

[0041] The preparation method of the above-mentioned sustained-release, low-irritant, excitatory composition includes the following steps:

[0042] (1) Prepare each raw material according to the above mass percentage content. Add agar, sodium alginate, sodium hyaluronate, glycerin, hydroxyethyl cellulose, hydroxypropyl methylcellulose, sodium benzoate and water to the emulsification pot, heat and stir to 85-90℃ to completely dissolve the materials. Then add pearl powder, synthetic fluorophlogopite, jojoba seed oil, keratin, hydrolyzed keratin, vanillyl butyl ether and phenoxyethanol in sequence and stir evenly. Keep warm for later use.

[0043] (2) The heat-insulating mixture from step (1) is pumped to a pelletizing machine and cooled with cooling oil (methyl silicone oil with a viscosity of 30-50 mPa·s (25°C)) at 0-5°C to obtain spherical objects. The spherical objects are then transferred to an aqueous cleaning tank containing surfactants to clean the oil off the surface of the spherical objects, thus obtaining a slow-release, low-irritant, exothermic composition.

[0044] The application of the sustained-release, low-irritant heating composition obtained in this embodiment in shampoo is the same as in Example 1. The results of the heating effect and heating stability tests show that the heating effect is significant, mild, and non-irritating; the difference in heating sensation before and after the accelerated heating test is not significant.

[0045] Example 3

[0046] A sustained-release, low-irritant, exothermic composition is prepared from the following components in weight percentages:

[0047] The composition includes: 15% agar, 0.2% sodium alginate, 0.05% sodium hyaluronate, 2.5% glycerin, 0.25% hydroxyethyl cellulose, 0.25% hydroxypropyl methylcellulose, 0.5% sodium benzoate, 0.5% pearl powder, 0.4% synthetic fluorophlogopite, 2% jojoba seed oil, 0.3% keratin, 0.4% hydrolyzed keratin, 6% vanillyl butyl ether, 1% phenoxyethanol, and 70.65% water.

[0048] The preparation method of the above-mentioned sustained-release, low-irritant, excitatory composition includes the following steps:

[0049] (1) Prepare each raw material according to the above mass percentage content. Add agar, sodium alginate, sodium hyaluronate, glycerin, hydroxyethyl cellulose, hydroxypropyl methylcellulose, sodium benzoate and water to the emulsification pot, heat and stir to 85-90℃ to completely dissolve the materials. Then add pearl powder, synthetic fluorophlogopite, jojoba seed oil, keratin, hydrolyzed keratin, vanillyl butyl ether and phenoxyethanol in sequence and stir evenly. Keep warm for later use.

[0050] (2) The heat-insulating mixture from step (1) is pumped to a pelletizing machine and cooled with cooling oil (vegetable oil with a viscosity of 20-50 mPa·s (25°C)) at 0-5°C to obtain spherical objects. The spherical objects are then transferred to an aqueous cleaning tank containing surfactants to clean the oil off the surface of the spherical objects, thus obtaining a slow-release, low-irritant, exothermic composition.

[0051] The application of the sustained-release, low-irritant heating composition obtained in this embodiment in shampoo is the same as in Example 1. The results of the heating effect and heating stability tests show that the heating effect is significant, mild, and non-irritating; the difference in heating sensation before and after the accelerated heating test is not significant.

[0052] The above embodiments are preferred embodiments of the present invention, but the embodiments of the present invention are not limited to the above embodiments. Any changes, modifications, substitutions, combinations, or simplifications made without departing from the spirit and principle of the present invention shall be considered equivalent substitutions and shall be included within the protection scope of the present invention.

Claims

1. A method for preparing a sustained-release, low-irritant, exothermic composition, characterized in that, The preparation steps include the following: (1) Add agar, sodium alginate, humectant, thickener, water-soluble preservative and water to an emulsifying pot, heat and stir to completely dissolve the materials, then add skin conditioning agent, vanillyl butyl ether and phenoxyethanol in sequence and stir evenly, keep warm for later use. (2) The heat-insulating mixture from step (1) is cooled by dripping it into cooling oil at 0-5°C using a pelletizing machine to obtain spherical objects. The spherical objects are then transferred to a cleaning tank to clean the oil off the surface of the spherical objects, thus obtaining a slow-release, low-irritant, exothermic composition.

2. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 1, characterized in that, The moisturizer in step (1) includes at least one of sodium hyaluronate and glycerin; the thickener includes at least one of hydroxyethyl cellulose and hydroxypropyl methylcellulose.

3. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 2, characterized in that, The water-soluble preservative mentioned in step (1) is sodium benzoate.

4. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 3, characterized in that, The skin conditioning agent mentioned in step (1) is at least one of pearl powder, synthetic fluorophlogopite, jojoba seed oil, keratin, and hydrolyzed keratin.

5. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 1, characterized in that, The heating and heat preservation temperature in step (1) is 85-90℃.

6. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 1, characterized in that, The cooling oil mentioned in step (2) is liquid paraffin, methyl silicone oil or vegetable oil; the cleaning tank uses an aqueous solution containing surfactants.

7. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 1, characterized in that, The mass percentage ratio of each material is as follows: agar 10-15%, sodium alginate 0.2-0.4%, humectant 1-3%, thickener 0.4-0.8%, water-soluble preservative 0.3-0.6%, skin conditioner 3-6%, vanillyl butyl ether 3-8%, phenoxyethanol 0.5-1%, and the balance is water.

8. The method for preparing a sustained-release, low-irritant, exothermic composition according to claim 4, characterized in that, The mass percentage ratio of each material is as follows: agar 10-15%, sodium alginate 0.2-0.4%, sodium hyaluronate 0.05-0.2%, glycerin 1.5-2.5%, hydroxyethyl cellulose 0.25-0.35%, hydroxypropyl methylcellulose 0.25-0.35%, sodium benzoate 0.4-0.5%, pearl powder 0.3-0.5%, synthetic fluorophlogopite 0.4-0.6%, jojoba seed oil 2-4%, keratin 0.1-0.3%, hydrolyzed keratin 0.4-0.6%, vanillyl butyl ether 4-6%, phenoxyethanol 0.5-1%, and the balance is water.

9. A sustained-release, low-irritant, exothermic composition, characterized in that, It is prepared by the method described in any one of claims 1 to 8.

10. The use of the sustained-release, low-irritant, heat-generating composition according to claim 9 in shampoo.