Device and method for rapidly discriminating quality of quartz ore

By using a vacuum chamber and a servo motor-driven turntable device, combined with oxy-acetylene torch heating, the problem of time-consuming quartz ore quality determination in traditional methods has been solved, enabling rapid and accurate determination of quartz sand quality. This method is suitable for high-purity quartz sand requirements in fields such as semiconductors and photovoltaics.

CN121027054APending Publication Date: 2025-11-28SINOMA JIANGSU SOLAR ENERGY NEW MATERIALS
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Patent Information

Application Number
CN202511484594.2
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-10-17
Publication Date
2025-11-28

AI Technical Summary

Technical Problem

Traditional methods for determining the quality of quartz ore are time-consuming and cannot meet the needs of semiconductor and photovoltaic industries for rapid and accurate determination of the quality of high-purity quartz sand.

Method used

A vacuum chamber device is used to establish a vacuum environment of -0.1MPa by a vacuum pump. The quartz sand sample in the test tube is heated to 1600-1800℃ in the vacuum chamber by an oxygen-acetylene torch. The test tube is stabilized by a servo motor-driven turntable and a limiting block, which enables continuous heating and real-time observation of multiple samples.

Benefits of technology

It enables rapid and accurate determination of quartz ore quality, avoids oxidation and contamination during the heating process, improves testing efficiency and consistency, and simplifies the process of determining quartz sand quality.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the technical field of quartz ore, and discloses a device and method for rapidly discriminating the quality of quartz ore, and the device comprises a vacuum box, the front side of the vacuum box is provided with a sliding door, the sliding door is provided with an observation window, one side wall of the vacuum box is provided with a third interface, and the third interface is in pipeline connection with an air pump; a circular rotating disc is further arranged in the inner cavity of the vacuum box, and four circular containing notches distributed in the circumferential direction are formed in the upper portion of the circular rotating disc. According to the invention, the vacuum box and the third interface are connected with the sucking pump, so that a-0.1 MPa vacuum environment can be quickly established, and quartz sand is prevented from being oxidized and polluted during heating; four circular placement notches in the circular turntable are matched with a first limiting block and a second limiting block, so that the test tube body can be stably clamped, and toppling and displacement are prevented; the driving assembly drives the turntable to intermittently rotate, and the oxygen-acetylene spray gun body is automatically lifted and positioned, so that continuous heating of multiple samples is realized, and the detection efficiency and consistency are improved; and the observation window on the sliding door facilitates real-time observation of the melt state.
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Description

TECHNICAL FIELD

[0001] The application belongs to the technical field of quartz ore, and particularly relates to a device and method for rapidly identifying the quality of quartz ore. BACKGROUND

[0002] For the determination of the quality and application potential of quartz ore, a traditional method is to use an industrial experiment method, which often needs hundreds of kilograms of ore, and the ore is purified for a period of ten days or even months, and the purified quartz sand is verified by pipe drawing, ball making or crucible making. The verification time period of the ore is long, and a large amount of experimental sand is required. In the fields of semiconductors, photovoltaics and the like, the quality stability of high-purity quartz sand is required to be high, and the quality of the quartz sand is largely dependent on the quality of the quartz ore, so there is an urgent need for a detection method for rapidly determining the quality of the quartz ore. The detection method rapidly and accurately determines the quality of the quartz sand, and then determines the quality of the quartz ore, and the traditional detection method cannot meet the requirement.

[0003] Therefore, the application is provided. SUMMARY

[0004] To solve the above technical problems, the basic idea of the technical solution of the application is as follows: A device for rapidly identifying the quality of quartz ore, comprising a vacuum box, a sliding door is arranged on the front side of the vacuum box, an observation window is arranged on the sliding door, a third interface is arranged on one side wall of the vacuum box, and a pipeline of the third interface is connected with an air suction pump; a circular turntable is further arranged in the inner cavity of the vacuum box, four circular placing notches arranged in a circumferential distribution are formed in the upper portion of the circular turntable, and a test tube body is arranged in the inner cavity of each of the four circular placing notches; first limiting blocks and second limiting blocks are respectively arranged on the side walls of each of the test tube bodies, the first limiting blocks and the second limiting blocks are mutually symmetrical between each other, and the first limiting blocks and the second limiting blocks are used for limiting the test tube bodies; an oxygen-acetylene torch body and a driving assembly are further arranged in the inner cavity of the vacuum box, the oxygen-acetylene torch body is used for calcining the side walls of the limited test tube bodies, and the driving assembly is used for driving the circular turntable to rotate.

[0005] As a preferred embodiment of the application, a plurality of connecting pieces are arranged on one side wall of the vacuum box, and supports are arranged in the inner cavities of the connecting pieces, the bottom ends of the supports are provided with mounting bases, and a first interface and a second interface are further arranged above the vacuum box.

[0006] As a preferred embodiment of the present application, the opposite two side walls of the vacuum box cavity are provided with guide sliding grooves, the two guide sliding grooves are mutually symmetrical, the sliding rods are slidably arranged in the cavities of the two guide sliding grooves, the bottom of the sliding rod is provided with a plurality of installation rods which are equidistantly arranged, the bottom of the installation rod is provided with an installation plate, one side wall of the installation plate is provided with a placing plate, the bottom of the placing plate is provided with a plurality of placing rods, and one end of the placing rod away from the placing plate is arranged on the body of the oxygen-acetylene torch.

[0007] As a preferred embodiment of the present application, the moving sliding grooves are arranged above the two sides of the circular placing slot on the circular turntable, each of the moving sliding grooves is mutually symmetrical, each of the moving sliding grooves is slidably provided with a moving slider, each of the moving sliders is mutually symmetrical, each of the moving sliders is provided with a first limiting block and a second limiting block above the two moving sliders, each of the moving sliders is provided with a first reset spring in the moving sliding groove, and one end of each of the first reset springs away from the moving slider is arranged on the inner wall of the moving sliding groove.

[0008] As a preferred embodiment of the present application, the servo motor is arranged in the middle of the bottom of the vacuum box cavity, the driving assembly comprises the servo motor, the output end of the servo motor is provided with a rotating rod, one end of the rotating rod away from the servo motor is arranged on the bottom of the circular turntable, and the opposite two sides of the vacuum box are further provided with positioning blocks, and the opposite ends of the two positioning blocks are rotatably arranged with the circular turntable.

[0009] As a preferred embodiment of the present application, the bottom of the circular turntable is provided with a special-shaped installation plate, the bottom of the special-shaped installation plate is composed of a plurality of arc convex surfaces and arc concave surfaces, and each of the arc convex surfaces and the arc concave surfaces is circumferentially distributed.

[0010] As a preferred embodiment of the present application, the bottom of the vacuum box cavity is further provided with two circular mounting barrels, the two circular mounting barrels are mutually symmetrical, the two circular mounting barrels are provided with rectangular slots, and the rectangular slots are mutually symmetrical, the two circular mounting barrels are movably inserted with circular insertion rods, the two circular insertion rods are mutually symmetrical, and the upper ends of the two circular insertion rods are provided with circular balls.

[0011] As a preferred embodiment of the present application, one end of each of the two circular insertion rods arranged in the cavity of the circular mounting barrel is provided with a circular moving plate, the two circular moving plates are slidably arranged in the cavities of the circular mounting barrels, the bottoms of the two circular moving plates are provided with second reset springs, and one end of each of the second reset springs away from the circular moving plate is arranged on the bottom of the cavity of the circular mounting barrel.

[0012] In a preferred embodiment of the present invention, a connecting rod is provided on the side of each of the two circular movable plates that is far apart from each other. The two connecting rods are symmetrical to each other and each moves through the rectangular slot. A connecting plate is provided on the opposite end of each of the two connecting rods. The two connecting plates are symmetrical to each other. A connecting rod is provided above each of the two connecting plates. The two connecting rods are symmetrical to each other. Each of the two connecting rods moves through the positioning block and each end away from the connecting plate is provided on the sliding rod.

[0013] A method for quickly identifying the quality of quartz ore, comprising the following steps: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body made of high temperature resistant quartz glass, and then the test tube body is placed in the circular placement slot above the circular turntable inside the vacuum chamber; at this time, the first reset spring in the sliding groove pushes the sliding slider to slide, causing the first limit block and the second limit block to move closer to each other and fit against the side wall of the test tube body, thus completing the stable positioning of the test tube. Step 2: Vacuuming operation of the vacuum chamber; start the air pump connected to the third interface pipe on one side wall of the vacuum chamber, and evacuate the air from the inner cavity of the vacuum chamber through the third interface. At the same time, use the first and second interfaces on the top of the vacuum chamber to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of the vacuum chamber is evacuated to -0.1MPa, so as to eliminate the oxidation effect of the quartz sand sample and external contamination during subsequent heating. Step 3: Turntable rotation and spray gun heating; Start the servo motor at the bottom of the vacuum chamber, its output end drives the circular turntable to rotate through the rotating rod, and the irregularly shaped mounting plate at the bottom of the circular turntable rotates synchronously; When the arc-shaped convex surface presses the circular ball of the circular insertion rod on the circular mounting cylinder, the circular moving plate compresses the second return spring, and drives the sliding rod to move down along the guide groove through the connecting rod, connecting plate, and connecting rod, so that the oxygen-acetylene spray gun body is aligned with the test tube body; After the circular turntable rotates 90°, the servo motor stops, and the oxygen-acetylene spray gun body is heated to 1600-1800℃ and maintained at this temperature for about minutes; Step 4: Stop heating and allow natural cooling; turn off the oxy-acetylene torch and allow the test tube and the molten quartz sand inside to cool naturally in the vacuum chamber. During the cooling process, observe the state of the melt through the observation window on the front sliding door of the vacuum chamber. Step 5: Sample Removal and Quality Assessment; After cooling, open the vacuum chamber door, remove the test tube, analyze the transparency and surface morphology of the melt inside the test tube, and combine with the preset quartz sand quality assessment database to finally determine the quality grade of the quartz sand sample.

[0014] Compared with the prior art, the present invention has the following advantages: This invention, through a vacuum chamber and a third interface connected to a vacuum pump, can quickly establish a -0.1MPa vacuum environment, preventing the quartz sand from being oxidized and contaminated during heating; the four circular placement slots on the circular turntable, in conjunction with the first and second limiting blocks, can stably clamp the test tube body, preventing tipping and displacement; the drive component drives the turntable to rotate intermittently, combined with the automatic lifting and positioning of the oxy-acetylene spray gun body, to achieve continuous heating of multiple samples, improving detection efficiency and consistency; the observation window on the sliding door facilitates real-time observation of the melt state.

[0015] The specific embodiments of the present invention will now be described in further detail with reference to the accompanying drawings. Attached Figure Description

[0016] In the attached diagram: Figure 1 A three-dimensional structural diagram of a device for rapidly identifying the quality of quartz ore; Figure 2 A side view schematic diagram of a device for rapidly identifying the quality of quartz ore; Figure 3 A schematic cross-sectional view of a vacuum chamber used in a device for rapidly identifying the quality of quartz ore. Figure 4 A device for rapidly identifying the quality of quartz ore. Figure 3 Enlarged schematic diagram of the medium vacuum chamber; Figure 5 A schematic cross-sectional view of one side of a vacuum chamber for a device that rapidly identifies the quality of quartz ore; Figure 6 A bottom view of the vacuum chamber structure of a device for rapidly identifying the quality of quartz ore; Figure 7 A schematic diagram of the internal structure of a vacuum chamber for a device to quickly identify the quality of quartz ore; Figure 8 A side view of the inner cavity of a vacuum chamber for a device to quickly identify the quality of quartz ore; Figure 9 A schematic diagram of the inner cavity of a vacuum chamber for a device to quickly identify the quality of quartz ore.

[0017] In the picture: 1. Mounting base; 11. Bracket; 12. Vacuum chamber; 121. Connector; 122. First interface; 123. Second interface; 124. Third interface; 125. Sliding door; 126. Observation window; 2. Circular turntable; 21. Positioning block; 22. Irregularly shaped mounting plate; 221. Arc-shaped convex surface; 222. Arc-shaped concave surface; 23. Servo motor; 231. Rotating rod; 24. Moving slide; 241. Moving slider; 242. First return spring; 243. First limiting block; 244. Second limiting block; 25. Circular placement slot; 251. Test tube body; 3. Circular mounting cylinder; 31. Rectangular slot; 32. Circular plug rod; 321. Ball bearing; 322. Circular moving plate; 323. Second return spring; 33. Connecting rod; 331. Connecting plate; 332. Connecting rod; 34. Guide groove; 341. Sliding rod; 342. Mounting rod; 343. Mounting plate; 344. Placement plate; 345. Placement rod; 346. Oxy-acetylene spray gun body. Detailed Implementation

[0018] To make the objectives, technical solutions, and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments will be clearly and completely described below with reference to the accompanying drawings. The following embodiments are used to illustrate the present invention.

[0019] Example 1:

[0020] like Figures 1 to 9 As shown, a device for rapidly identifying the quality of quartz ore includes a vacuum chamber 12. A sliding door 125 is provided on the front of the vacuum chamber 12, and an observation window 126 is provided on the sliding door 125. A third interface 124 is provided on one side wall of the vacuum chamber 12, and the third interface 124 is connected to a vacuum pump via a pipe. A circular turntable 2 is also provided inside the vacuum chamber 12. Four circular placement slots 25 are provided above the circular turntable 2, arranged in a circular pattern. Each of the four circular placement slots 25 contains a test tube body 251. The sidewalls of the test tube body 251 are respectively provided with a first limiting block 243 and a second limiting block 244. Each first limiting block 243 and the second limiting block 244 are symmetrical to each other, and the first limiting block 243 and the second limiting block 244 are used to limit the placement of the test tube body 251. The inner cavity of the vacuum chamber 12 is also provided with an oxygen-acetylene spray gun body 346 and a driving assembly. The oxygen-acetylene spray gun body 346 is used to calcine the sidewalls of the test tube body 251 after it is limited, and the driving assembly is used to drive the circular turntable 2 to rotate. A vacuum pump connected to the vacuum chamber 12 and the third interface 124 can quickly establish a -0.1MPa vacuum environment, preventing the quartz sand from being oxidized and contaminated during heating. The four circular placement slots 25 on the circular turntable 2, together with the first limiting block 243 and the second limiting block 244, can firmly clamp the test tube body 251, preventing it from tipping over or shifting. The drive component drives the turntable to rotate intermittently, which, combined with the automatic lifting and positioning of the oxy-acetylene spray gun body 346, enables continuous heating of multiple samples, improving detection efficiency and consistency. The observation window 126 on the sliding door 125 facilitates real-time observation of the melt state.

[0021] like Figures 1 to 6 As shown, in a specific embodiment, a plurality of connectors 121 are provided on one side wall of the vacuum chamber 12, and a bracket 11 is provided through the inner cavity of each connector 121. A mounting base 1 is provided at the bottom end of the bracket 11, and a first interface 122 and a second interface 123 are also provided on the top of the vacuum chamber 12. In this configuration, the specific installation position of the vacuum chamber 12 is determined.

[0022] like Figures 4 to 9 As shown, furthermore, guide grooves 34 are provided on both opposite side walls of the inner cavity of the vacuum chamber 12. The two guide grooves 34 are symmetrical to each other. Sliding rods 341 are slidably arranged inside the inner cavities of the two guide grooves 34. Multiple mounting rods 342 are provided at equal intervals at the bottom of the sliding rods 341, and mounting plates 343 are provided at the bottom of the mounting rods 342. A placement plate 344 is provided on one side wall of the mounting plate 343. Multiple placement rods 345 are provided at the bottom of the placement plate 344, and the end of the placement rod 345 away from the placement plate 344 is attached to the oxygen-acetylene spray gun body 346. In this configuration, the specific installation position of the oxygen-acetylene spray gun body 346 is determined.

[0023] like Figures 4 to 9 As shown, further, movable slides 24 are respectively provided on both sides of the circular placement slot 25 above the circular turntable 2. Each movable slide 24 is symmetrical to the others. A movable slider 241 is slidably disposed in the inner cavity of each movable slide 24. Each movable slider 241 is symmetrical to the others. A first limiting block 243 and a second limiting block 244 are respectively provided above each pair of movable sliders 241. A first return spring 242 is provided in the movable slide 24 of each movable slider 241. The end of each first return spring 242 away from the movable slider 241 is disposed on the inner wall of the movable slide 24. In this configuration, the specific installation positions of the first limiting block 243 and the second limiting block 244 are determined.

[0024] like Figures 4 to 9 As shown, the drive assembly further includes a servo motor 23, which is located at the bottom center of the vacuum chamber 12. A rotating rod 231 is located at the output end of the servo motor 23, with one end of the rotating rod 231 away from the servo motor 23 positioned at the bottom of the circular turntable 2. Positioning blocks 21 are also provided on opposite sides of the vacuum chamber 12, with one end of each positioning block 21 rotatably mounted to the circular turntable 2. This configuration defines the installation position of the drive assembly.

[0025] Example 2:

[0026] The difference between the above embodiments and this embodiment is that: Figures 4 to 9As shown, a device for rapidly identifying the quality of quartz ore includes a circular turntable 2 with an irregularly shaped mounting plate 22 at its bottom. The bottom of the irregularly shaped mounting plate 22 consists of multiple arc-shaped convex surfaces 221 and arc-shaped concave surfaces 222, with each arc-shaped convex surface 221 and arc-shaped concave surface 222 arranged circumferentially. In this configuration, the components of the bottom of the irregularly shaped mounting plate 22 are defined.

[0027] like Figures 4 to 9 As shown in the specific embodiment, two circular mounting cylinders 3 are also provided at the bottom of the inner cavity of the vacuum box 12. The two circular mounting cylinders 3 are symmetrical to each other, and each of the two circular mounting cylinders 3 has a rectangular slot 31, which is symmetrical to each other. Circular insertion rods 32 are movably inserted into the top of each of the two circular mounting cylinders 3. The two circular insertion rods 32 are symmetrical to each other, and a circular ball bearing 321 is provided at the upper end of each of the two circular insertion rods 32. Circular movable plates 322 are provided at one end of each of the two circular insertion rods 32 in the inner cavity of the circular mounting cylinder 3. The two circular movable plates 322 are slidably disposed with respect to the inner cavity of the circular mounting cylinder 3. A second return spring 323 is provided at the bottom of each of the two circular movable plates 322, and the end of the second return spring 323 away from the circular movable plate 322 is located at the bottom of the inner cavity of the circular mounting cylinder 3. Two circular movable plates 322 are provided with connecting rods 33 on opposite sides. The two connecting rods 33 are symmetrical and each moves through a rectangular slot 31. Connecting plates 331 are provided at opposite ends of the two connecting rods 33. The two connecting plates 331 are symmetrical. Connecting rods 332 are provided above the two connecting plates 331. The two connecting rods 332 are symmetrical. Each of the two connecting rods 332 moves through a positioning block 21, and each end away from the connecting plate 331 is provided on a sliding rod 341. In this configuration, when the arc-shaped concave surface 222 of the irregular mounting plate 22 rotates to the circular ball bearing 321, the second return spring 323 is no longer compressed and releases its elastic force, pushing the circular moving plate 322 to slide vertically upward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 drives the circular insertion rod 32 and the circular ball bearing 321 to return upward, so that the circular ball bearing 321 fits tightly against the arc-shaped concave surface 222. At the same time, the circular moving plate 322 drives the sliding rod 341 to slide upward along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, thereby driving the oxygen-acetylene spray gun body 346 to move upward, thus ensuring that the oxygen-acetylene spray gun body 346 leaves the test tube body 251.

[0028] Example 3:

[0029] This invention also discloses a method for rapidly identifying the quality of quartz ore, the steps of which are as follows: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body 251 made of high temperature resistant quartz glass, and then the test tube body 251 is placed in the circular placement slot 25 above the circular turntable 2 inside the vacuum chamber 12; at this time, the first reset spring 242 in the movable slide 24 pushes the movable slider 241 to slide, causing the first limiting block 243 and the second limiting block 244 to move closer to each other and fit against the side wall of the test tube body 251, thus completing the stable positioning of the test tube; Step 2: Vacuuming operation of the vacuum chamber; start the vacuum pump connected to the third interface 124 on one side wall of the vacuum chamber 12, and evacuate the inner cavity of the vacuum chamber 12 through the third interface 124. At the same time, use the first interface 122 and the second interface 123 on the top of the vacuum chamber 12 to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of the vacuum chamber 12 is evacuated to -0.1MPa, so as to eliminate the oxidation effect of the quartz sand sample and external contamination during subsequent heating. Step 3: Turntable rotation and spray gun heating; Start the servo motor 23 at the bottom of the vacuum chamber 12, and its output end drives the circular turntable 2 to rotate through the rotating rod 231. The irregularly shaped mounting plate 22 at the bottom of the circular turntable 2 rotates synchronously; When the arc-shaped convex surface 221 presses the circular ball 321 of the circular insertion rod 32 on the circular mounting cylinder 3, the circular moving plate 322 compresses the second return spring 323, and drives the sliding rod 341 to move down along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, so that the oxygen-acetylene spray gun body 346 is aligned with the test tube body 251; After the circular turntable 2 rotates 90°, the servo motor 23 stops, and the oxygen-acetylene spray gun body 346 is heated to 1600-1800℃ and maintained at this temperature for about 3 minutes; Step 4: Stop heating and allow natural cooling; close the oxygen-acetylene torch body 346 and allow the test tube body 251 and the internal quartz sand melt to cool naturally in the vacuum chamber 12. During the cooling process, observe the state of the melt through the observation window 126 on the front sliding door 125 of the vacuum chamber 12. Step 5: Sample Removal and Quality Assessment; After cooling, open the sliding door 125 of the vacuum chamber 12, remove the test tube body 251, analyze the transparency and surface morphology of the melt inside the test tube body 251, and combine it with the preset quartz sand quality assessment database to finally determine the quality grade of the quartz sand sample.

[0030] The implementation principle of the device for rapidly identifying the quality of quartz ore in this embodiment is as follows: First, sample preparation and fixation are carried out before testing. Approximately 7g of quartz sand sample is placed into a test tube body 251 made of high-temperature resistant quartz glass. Then, the test tube body 251 containing the sample is placed in the circular placement slot 25 above the circular turntable 2 inside the vacuum chamber 12. At this time, the movable slider 241 in the movable sliding grooves 24 on both sides of the circular placement slot 25 slides under the elastic force of the first return spring 242, which drives the first limiting block 243 and the second limiting block 244 respectively set above the movable slider 241 to move closer to each other until they are tightly attached to the side wall of the test tube body 251, thus achieving stable positioning of the test tube body 251. Next, the vacuuming process begins. The vacuum pump connected to the third interface 124 on one side wall of the vacuum chamber 12 is started. The vacuum pump pumps the air inside the vacuum chamber 12 through the third interface 124. During the process, the first interface 122 and the second interface 123 set on the top of the vacuum chamber 12 can be used to help adjust the air pressure inside the chamber until the vacuum degree inside the vacuum chamber 12 is reduced to -0.1MPa. This eliminates the oxidation effect and external contamination that the quartz sand sample may be affected by during subsequent heating, and provides a clean vacuum environment for testing. The heating process is then initiated. First, the servo motor 23, located in the middle of the bottom of the vacuum chamber 12, is turned on. The output of the servo motor 23 drives the rotating rod 231 to rotate, which in turn drives the circular turntable 2 connected to the top to rotate. When the circular turntable 2 rotates, the irregularly shaped mounting plate 22 at its bottom rotates synchronously. The bottom of the irregularly shaped mounting plate 22 consists of multiple circumferentially distributed arc-shaped convex surfaces 221 and arc-shaped concave surfaces 222. When the arc-shaped convex surfaces 221 of the irregularly shaped mounting plate 22 rotate to above the two mutually symmetrical circular mounting cylinders 3 at the bottom of the vacuum chamber 12, the arc-shaped convex surfaces 221 will squeeze the circular ball bearing 321 at the top of the circular insertion rod 32 above the circular mounting cylinder 3, causing the circular insertion rod 32 to move vertically downward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 connected to one end of the circular insertion rod 32 in the inner cavity of the circular mounting cylinder 3 slides downward synchronously, compressing the second return spring 323 connected to the bottom of the circular moving plate 322 and the bottom of the inner cavity of the circular mounting cylinder 3. The connecting rod 33, located on the opposite side of the movable plate 322, moves downward along the rectangular slot 31 on the circular mounting cylinder 3. The connecting plate 331 connected to the opposite end of the connecting rod 33 and the connecting rod 332 connected above the connecting plate 331 move downward synchronously. The end of the connecting rod 332 away from the connecting plate 331 passes through the positioning blocks 21 on both sides of the vacuum chamber 12 and connects to the sliding rod 341. Therefore, the connecting rod 332 will drive the sliding rod 341 to slide downward in the guide grooves 34 opened on the opposite side walls of the inner cavity of the vacuum chamber 12. The multiple equally spaced mounting rods 342 at the bottom of the sliding rod 341, the mounting plate 343 at the bottom of the mounting rod 342, and the placement rod 345 at the bottom of the placement plate 344 on one side wall of the mounting plate 343 move downward synchronously. Finally, the oxygen-acetylene spray gun body 346 connected to the end of the placement rod 345 away from the placement plate 344 moves downward until the oxygen-acetylene spray gun body 346 moves to the position corresponding to the quartz sand sample in the test tube body 251. When the arc-shaped concave surface 222 of the irregular mounting plate 22 rotates to the circular ball bearing 321, the second return spring 323 is no longer compressed and releases its elastic force, pushing the circular moving plate 322 to slide vertically upward along the inner cavity of the circular mounting cylinder 3. The circular moving plate 322 drives the circular insertion rod 32 and the circular ball bearing 321 to return upward, so that the circular ball bearing 321 tightly fits the arc-shaped concave surface 222. At the same time, the circular moving plate 322 drives the sliding rod 341 to slide upward along the guide groove 34 through the connecting rod 33, connecting plate 331, and connecting rod 332, thereby driving the oxygen-acetylene spray gun body 346 to move upward, thus ensuring The oxy-acetylene spray gun body 346 leaves the test tube body 251; during the rotation of the circular turntable 2, the positioning blocks 21 on both sides of the vacuum chamber 12 play an auxiliary positioning role for the circular turntable 2. When the circular turntable 2 rotates 90 degrees, the servo motor 23 stops running, realizing the switching of the test tube body 251. At this time, the oxy-acetylene spray gun body 346 is exactly located on the outer wall of the switched test tube body 251. Then the oxy-acetylene spray gun body 346 is started, its heating temperature is adjusted to 1600-1800℃, and this temperature is maintained for about 3 minutes to heat the quartz sand sample in the test tube body 251. Finally, the cooling analysis is performed. After the heating maintenance time is over, the oxy-acetylene torch body 346 is turned off, and the test tube body 251 and the quartz sand melt inside are allowed to cool naturally in the vacuum chamber 12. During the cooling process, the state of the melt can be observed through the observation window 126 set on the sliding door 125. After cooling is completed, the sliding door 125 is opened, the test tube body 251 is taken out, and the transparency and surface morphology of the melt inside the test tube body 251 are analyzed. Combined with the preset quartz sand quality judgment database, the quality grade of the quartz sand sample is finally determined.

Claims

1. A device for rapidly identifying the quality of quartz ore, comprising a vacuum chamber (12), characterized in that: The vacuum chamber (12) is provided with a sliding door (125) on the front side, and an observation window (126) is provided on the sliding door (125). A third interface (124) is provided on one side wall of the vacuum chamber (12), and the third interface (124) is connected to a vacuum pump. The vacuum chamber (12) is also provided with a circular turntable (2). Four circular placement slots (25) are provided above the circular turntable (2) and are arranged in a circular pattern. Test tube bodies (251) are placed in the inner cavity of each of the four circular placement slots (25). A first limiting block (243) and a second limiting block (244) are respectively provided on the side wall of each test tube body (251). Each first limiting block (243) and second limiting block (244) are symmetrical to each other and are used to limit the placement of the test tube body (251). The vacuum chamber (12) is also equipped with an oxygen-acetylene spray gun body (346) and a drive assembly. The oxygen-acetylene spray gun body (346) is used to calcine the side wall of the test tube body (251) after it is limited. The drive assembly is used to drive the circular turntable (2) to rotate.

2. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The vacuum chamber (12) has multiple connectors (121) on one side wall, and each connector (121) has a bracket (11) running through its inner cavity. The bracket (11) has a mounting base (1) at its bottom end, and the vacuum chamber (12) also has a first interface (122) and a second interface (123) on its top.

3. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The vacuum chamber (12) has guide grooves (34) on both sides of its inner cavity. The two guide grooves (34) are symmetrical to each other. A sliding rod (341) is slidably arranged in the inner cavity of the two guide grooves (34). Multiple mounting rods (342) are arranged at equal intervals at the bottom of the sliding rods (341). A mounting plate (343) is arranged at the bottom of the mounting rods (342). A placement plate (344) is arranged on one side wall of the mounting plate (343). Multiple placement rods (345) are arranged at the bottom of the placement plate (344). The end of the placement rod (345) away from the placement plate (344) is arranged on the oxygen-acetylene spray gun body (346).

4. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The circular turntable (2) is provided with movable slides (24) on both sides of the circular placement slot (25) above it. Each movable slide (24) is symmetrical to each other. Each movable slide (24) is slidably provided with a movable slider (241) in its inner cavity. Each movable slider (241) is symmetrical to each other. Each movable slider (241) is provided with a first limiting block (243) and a second limiting block (244) above each pair of movable sliders (241). Each movable slider (241) is provided with a first return spring (242) in the movable slide (24). The end of each first return spring (242) away from the movable slider (241) is provided on the inner wall of the movable slide (24).

5. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The drive assembly includes a servo motor (23), which is located at the bottom center of the vacuum chamber (12). A rotating rod (231) is provided at the output end of the servo motor (23). The end of the rotating rod (231) away from the servo motor (23) is located at the bottom of the circular turntable (2). Positioning blocks (21) are also provided on opposite sides of the vacuum chamber (12). The opposite ends of the two positioning blocks (21) are respectively rotatably set with the circular turntable (2).

6. The device for rapidly identifying the quality of quartz ore according to claim 5, characterized in that, The bottom of the circular turntable (2) is provided with an irregularly shaped mounting plate (22). The bottom of the irregularly shaped mounting plate (22) is composed of multiple arc-shaped convex surfaces (221) and arc-shaped concave surfaces (222), and each arc-shaped convex surface (221) and arc-shaped concave surface (222) is circumferentially distributed.

7. The device for rapidly identifying the quality of quartz ore according to claim 1, characterized in that, The vacuum chamber (12) is also provided with two circular mounting cylinders (3) at the bottom of the inner cavity. The two circular mounting cylinders (3) are symmetrical to each other. Each of the two circular mounting cylinders (3) has a rectangular slot (31) and the rectangular slots (31) are symmetrical to each other. A circular plug rod (32) is movably inserted above each of the two circular mounting cylinders (3). The two circular plug rods (32) are symmetrical to each other. A circular ball bearing (321) is provided at the upper end of each of the two circular plug rods (32).

8. The device for rapidly identifying the quality of quartz ore according to claim 7, characterized in that, Two circular plug rods (32) are respectively provided with circular moving plates (322) at one end of the inner cavity of the circular mounting cylinder (3). The two circular moving plates (322) are respectively slidably provided with the inner cavity of the circular mounting cylinder (3). A second reset spring (323) is provided at the bottom of each of the two circular moving plates (322), and the end of the second reset spring (323) away from the circular moving plate (322) is provided at the bottom of the inner cavity of the circular mounting cylinder (3).

9. The device for rapidly identifying the quality of quartz ore according to claim 8, characterized in that, Each of the two circular movable plates (322) is provided with a connecting rod (33) on the side away from each other. The two connecting rods (33) are symmetrical to each other and are respectively movably inserted through the rectangular slot (31). The opposite ends of the two connecting rods (33) are respectively provided with a connecting plate (331). The two connecting plates (331) are symmetrical to each other. A connecting rod (332) is provided above the two connecting plates (331). The two connecting rods (332) are symmetrical to each other. The two connecting rods (332) are respectively movably inserted through the positioning block (21), and the ends of the two connecting rods (332) away from the connecting plate (331) are respectively provided on the sliding rod (341).

10. A method for rapidly identifying the quality of quartz ore, characterized in that, The apparatus for rapidly identifying the quality of quartz ore, as described in any one of claims 1 to 9, and the method for rapidly identifying the quality of quartz ore, comprises the following steps: Step 1: Sample preparation and test tube fixation; about 7g of quartz sand sample is loaded into the test tube body (251) made of high temperature resistant quartz glass, and then the test tube body (251) is placed in the circular placement slot (25) above the circular turntable (2) inside the vacuum chamber (12); at this time, the first reset spring (242) in the sliding groove (24) pushes the sliding slider (241) to slide, causing the first limiting block (243) and the second limiting block (244) to approach each other and fit against the side wall of the test tube body (251), thus completing the stable positioning of the test tube; Step 2: Vacuuming operation of vacuum chamber; start the pump connected to the third interface (124) pipe on one side wall of vacuum chamber (12), and pump air into the inner cavity of vacuum chamber (12) through the third interface (124). At the same time, use the first interface (122) and the second interface (123) on the top of vacuum chamber (12) to help adjust the air pressure in the inner cavity until the vacuum degree of the inner cavity of vacuum chamber (12) is pumped down to -0.1MPa to eliminate the oxidation effect of quartz sand sample and external contamination during subsequent heating; Step 3: Rotating the turntable and heating the spray gun; Start the servo motor (23) at the bottom of the vacuum chamber (12), and its output end drives the circular turntable (2) to rotate through the rotating rod (231). The irregular mounting plate (22) at the bottom of the circular turntable (2) rotates synchronously; When the arc-shaped convex surface (221) squeezes the circular ball (321) of the circular insertion rod (32) on the circular mounting cylinder (3), the circular moving plate (322) compresses the second reset spring (323), and drives the sliding rod (341) to move down along the guide groove (34) through the connecting rod (33), connecting plate (331), and connecting rod (332), so that the oxygen-acetylene spray gun body (346) is aligned with the test tube body (251); After the circular turntable (2) rotates 90°, the servo motor (23) stops, and the oxygen-acetylene spray gun body (346) is heated to 1600-1800℃ and maintained at this temperature for about 3 minutes; Step 4: Stop heating and allow natural cooling; close the oxygen-acetylene torch body (346) and allow the test tube body (251) and the internal quartz sand melt to cool naturally in the vacuum chamber (12). During the cooling process, observe the state of the melt through the observation window (126) on the front sliding door (125) of the vacuum chamber (12). Step 5: Sample removal and quality assessment; After cooling, open the sliding door (125) of the vacuum chamber (12), remove the test tube body (251), analyze the transparency and surface morphology of the melt inside the test tube body (251), and finally determine the quality grade of the quartz sand sample by combining the preset quartz sand quality assessment database.

Citation Information

Patent Citations

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    CN109765088A

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  • Gene detector and detection method

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  • Quartz tube vacuum sealing method and quartz tube vacuum sealing equipment

    CN118702399A

  • Quartz sand pickling device and method

    CN119565987A