One-step electrodeposition method for synthesizing nickel-molybdenum-copper alloy, alloy and application thereof

The synthesis of nickel-molybdenum-copper alloys via a one-step electrodeposition method solves the problems of complexity and high cost in existing nickel-molybdenum-based alloy catalyst synthesis methods. It achieves a tight bond between the catalyst and the electrode, improving catalytic activity and stability, and is suitable for large-scale industrial applications.

CN122406326APending Publication Date: 2026-07-17TAIAN MINGDE NEW MATERIALS CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2026-05-13
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for synthesizing nickel-molybdenum based alloy catalysts suffer from problems such as complex processes, high preparation costs, uneven product performance, low utilization of active sites, and insufficient catalytic efficiency and long-term stability due to powdered catalyst coating methods.

Method used

A one-step electrodeposition method was used to synthesize nickel-molybdenum-copper alloy. Using stainless steel sheets as a substrate, the nickel-molybdenum-copper alloy was directly deposited on the stainless steel sheets by optimizing the composition of the reaction electrodeposition solution and process parameters, forming a catalyst with a rough surface structure. This method avoids the use of binders and achieves a tight bond between the catalyst and the electrode.

Benefits of technology

It improves the utilization rate of active sites of the catalyst, promotes charge transport, reduces preparation costs, enhances the stability of the catalyst and the efficiency of the hydrogen evolution reaction in water electrolysis, and is suitable for large-scale industrial production.

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Abstract

This invention provides a one-step electrodeposition method for synthesizing nickel-molybdenum-copper alloys, mainly comprising the following steps: depositing stainless steel sheets using a reactive electrodeposition solution. The reactive electrodeposition solution includes: nickel sulfate hexahydrate, ammonium molybdate, copper sulfate pentahydrate, sodium citrate, and sodium chloride. The advantages of this invention are that the synthesis method is simple and low-cost, significantly reduces the overpotential of the hydrogen evolution reaction, exhibits good stability, demonstrates excellent catalytic activity in the hydrogen evolution reaction of water electrolysis, and has promising application prospects.
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