Device for producing ammonium phosphate by utilizing low-grade raffinate acid
By setting up a stirring assembly and scraper in the reactor, the problem of difficult scaling in the inner wall of the reactor is solved, and the effective cleaning and normal operation of the inner wall of the kettle is achieved.
Patent Information
- Application Number
- CN202421727570.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-19
- Publication Date
- 2025-07-08
- Estimated Expiration
- 2034-07-19
AI Technical Summary
The scaling of the inner wall of the reactor is difficult to clean, which affects the normal chemical reaction process.
A stirring assembly and scraper are installed in the reactor. The stirring assembly drives the scraper to rotate to clean up impurities in the inner wall. The scraper can be detached and connected to avoid wear.
It realizes effective cleaning of the inner wall of the reactor to prevent scaling and ensures the normal operation of the reactor.
Smart Images

Figure CN223069507U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the field of producing ammonium phosphate with low-grade raffinate acid, and particularly relates to a device for producing ammonium phosphate by using low-grade raffinate acid. Background Art
[0002] Raffinate acid is a by-product generated when preparing phosphoric acid by the reaction of phosphoric acid monoester and sodium hydroxide. Ammonium phosphate is a colorless and transparent crystal, which is formed by the reaction of ammonia and phosphoric acid and is widely used in fields such as chemical fertilizers, water treatment, and food. Mixing raffinate acid and ammonia water, carrying out a dehydration reaction in a reaction kettle, and then cooperating with subsequent steps such as evaporation and crystallization can produce monoammonium phosphate.
[0003] Generally, scale will adhere to the inner wall of the reaction kettle during the reaction in the reaction kettle. These scales are inside the reaction kettle, so it is not easy for workers to directly clean them. Long-term adhesion will make it more difficult to clean, which will further affect the subsequent normal operation of the reaction kettle, such as polluting the normal chemical reaction process. Summary of the Utility Model
[0004] Based on the above description, the utility model provides a device for producing ammonium phosphate by using low-grade raffinate acid to solve the problem that scale is generated on the inner wall of the existing reaction kettle, making it difficult to clean.
[0005] The technical solution of the utility model to solve the above technical problems is as follows: A device for producing ammonium phosphate by using low-grade raffinate acid includes a device main body. A support frame is arranged at the bottom of the device main body, and a feed inlet and a discharge outlet are respectively arranged at the top and the bottom of the device main body;
[0006] An activity part is arranged at the top of the device main body. The activity part includes a stirring component, a transmission component, a scraper, and a connection component. The transmission component is arranged inside the stirring component, the scraper is arranged on the side wall of the transmission component, and the connection component is used to connect the stirring component and the scraping component.
[0007] Further, the stirring component is composed of a main rod, a first gear, a second gear, a motor, and a stirring rod. The motor is installed at the top of the device main body, the main rod is fixedly installed at the output end of the motor, and the first gear is installed on the surface of the main rod.
[0008] Based on the above technical solution, the utility model can be further improved as follows.
[0009] Further, the top of the main rod is connected to the device main body through a bearing, the second gear is fixedly installed on the main rod, the second gear meshes with the first gear, the stirring rod is fixedly installed on the side wall of the main rod, and an installation groove is opened inside the main rod.
[0010] Further, the transmission assembly consists of a central rod and a convex rod. The convex rod is fixedly installed on the end face of the central rod, and the central rod is movably inserted into the installation groove inside the main rod.
[0011] Further, a rectangular groove is provided on one side of the scraper. The convex rod is movably inserted into the inner cavity of the rectangular groove of the scraper, and the side wall of the scraper is movably attached to the inner wall of the device body.
[0012] Further, the connection assembly includes a connecting plate, a vertical plate, and a sleeve. The vertical plate is fixedly installed at the bottom of the connecting plate, and the sleeve is fixedly installed on the surface of the main rod.
[0013] Further, one end of the connecting plate is fixedly connected to the side wall of the central rod, and the outer wall of the central rod is movably attached to the inner wall of the installation groove of the main rod. A plurality of threaded grooves are evenly provided on the side wall of the sleeve. A screw rod is threadedly connected to the inner cavity of the threaded groove on the side close to the vertical plate, and the end of the screw rod away from the threaded groove threadedly penetrates through the vertical plate.
[0014] Compared with the prior art, the technical solution of the present application has the following beneficial technical effects:
[0015] 1. In the present utility model, by arranging a stirring assembly inside the device body, the main rod drives the stirring rod to rotate to achieve the stirring effect. And by arranging a central rod inside the main rod, with the addition of the connection assembly and the scraper, the central rod can drive the scraper to rotate to scrape the inner wall of the device body, achieving the effect of removing impurities on the inner wall of the device body.
[0016] 2. Through the connecting plate and the vertical plate in the connection assembly, the threaded rod passes through the vertical plate and enters the threaded groove of the sleeve, and the connection work between the central rod and the main rod can be completed. And by pulling out the threaded rod from the threaded groove of the sleeve, the central rod and the main rod are separated, switching to a simple stirring state, avoiding the wear phenomenon caused by the scraper scraping the inner wall of the device body all the time. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] Figure 1 is a schematic structural diagram of a device for producing ammonium phosphate using low-grade raffinate acid provided by an embodiment of the present utility model;
[0018] Figure 2 is a schematic perspective sectional structure diagram of the whole in the present utility model;
[0019] Figure 3 is a schematic perspective sectional view of the main rod in the present utility model.
[0020] In the drawings, the list of components represented by each reference numeral is as follows:
[0021] 1. Device main body; 2. Movable part; 201. Stirring assembly; 2011. Main rod; 2012. First gear; 2013. Second gear; 2014. Motor; 2015. Stirring rod; 202. Transmission assembly; 2021. Central rod; 2022. Convex rod; 203. Scraper; 204. Connection assembly; 2041. Connection plate; 2042. Vertical plate; 2043. Sleeve; 3. Support frame. Detailed implementation manner
[0022] To facilitate the understanding of the present application, the present application will be described more comprehensively with reference to the relevant drawings. Embodiments of the present application are shown in the drawings. However, the present application can be implemented in many different forms and is not limited to the embodiments described herein. On the contrary, these embodiments are provided to make the disclosure of the present application more thorough and comprehensive.
[0023] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by those of ordinary skill in the technical field to which this application belongs. The terms used in the description of this application herein are only for the purpose of describing specific embodiments and are not intended to limit this application.
[0024] It should be noted that the orientation or positional relationship indicated by the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc. is based on the orientation or positional relationship shown in the drawings, or the orientation or positional relationship in which the technical product is usually placed during use. It is only for the convenience of describing the present technology and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation to the present technology. In addition, "first" and "second" are only used for descriptive purposes and cannot be understood as indicating or implying relative importance or implicitly indicating the quantity of the indicated technical features. Therefore, the features defined with "first" and "second" may explicitly or implicitly include one or more of such features. Therefore, the terms "first", "second", "third", etc. are only used for distinguishing descriptions and cannot be understood as indicating or implying relative importance. In the description of the present utility model, unless otherwise stated, the meaning of "a plurality" is two or more.
[0025] In addition, terms such as "horizontal", "vertical", "hanging" do not mean that the components are required to be absolutely horizontal or hanging, but can be slightly inclined. For example, "horizontal" only means that its direction is more horizontal relative to "vertical", and does not mean that the structure must be completely horizontal, but can be slightly inclined.
[0026] In the description of the present technology, it should also be noted that unless otherwise clearly specified and defined, the terms "set", "installed", "connected", and "linked" should be understood in a broad sense. For example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be directly connected or indirectly connected through an intermediate medium, and it can be the communication inside two components. For those of ordinary skill in the art, the specific meanings of the above terms in the present technology can be understood according to specific circumstances.
[0027] Please refer to Figure 1 and Figure 2 , a device for producing ammonium phosphate using low-grade raffinate acid, including a device main body 1. A support frame 3 is provided at the bottom of the device main body 1, and a feed inlet and a discharge outlet are respectively provided at the top and the bottom of the device main body 1;
[0028] An active part 2 is provided at the top of the device main body 1. The active part 2 includes a stirring assembly 201, a transmission assembly 202, a scraper 203, and a connection assembly 204. The transmission assembly 202 is arranged inside the stirring assembly 201, the scraper 203 is arranged on the side wall of the transmission assembly 202, and the connection assembly 204 is used to connect the stirring assembly 201 and the scraping assembly.
[0029] A scraper 203 is added to the active part 2, so that the scraper 203 rotates with the stirring assembly 201 in cooperation with the connection assembly 204 and the transmission assembly 202, so that the scraper 203 can scrape and clean the inner wall of the device main body 1 to remove the impurities adsorbed on the inner wall of the device main body 1.
[0030] Please refer to Figure 1 and Figure 2 , the stirring assembly 201 of this embodiment is composed of a main rod 2011, a first gear 2012, a second gear 2013, a motor 2014, and a stirring rod 2015. The motor 2014 is installed at the top of the device main body 1, the main rod 2011 is fixedly installed on the output end of the motor 2014, and the first gear 2012 is installed on the surface of the main rod 2011.
[0031] Please refer to Figure 1 and Figure 2 , the top of the main rod 2011 of this embodiment is connected to the device main body 1 through a bearing, and the second gear 2013 is fixedly installed on the main rod 2011, and the second gear 2013 meshes with the first gear 2012. The stirring rod 2015 is fixedly installed on the side wall of the main rod 2011, and an installation groove is provided inside the main rod 2011.
[0032] Starting the motor 2014 allows the motor 2014 to drive the first gear 2012 to rotate. The first gear 2012 will then drive the second gear 2013 to rotate. Since the second gear 2013 is fixed to the main rod 2011, the main rod 2011 rotates, and together with the stirring rod 2015 on the main rod 2011, it performs a stirring operation inside the device main body 1.
[0033] Please refer to Figure 2 and Figure 3 , the transmission component 202 of this embodiment consists of a central rod 2021 and a convex rod 2022. The convex rod 2022 is fixedly installed on the end face of the central rod 2021, and the central rod 2021 is movably inserted into the installation groove inside the main rod 2011.
[0034] Please refer to Figure 2 and Figure 3 , one side of the scraper 203 of this embodiment is provided with a rectangular groove. The convex rod 2022 is movably inserted into the inner cavity of the rectangular groove of the scraper 203, and the side wall of the scraper 203 is movably attached to the inner wall of the device main body 1.
[0035] The cross-section of the convex rod 2022 is rectangular. Inserting the convex rod 2022 into the inner cavity of the rectangular groove facilitates the central rod 2021 to drive the scraper 203 to rotate.
[0036] Please refer to Figure 2 and Figure 3 , the connection component 204 of this embodiment includes a connecting plate 2041, a vertical plate 2042, and a sleeve 2043. The vertical plate 2042 is fixedly installed at the bottom of the connecting plate 2041, and the sleeve 2043 is fixedly installed on the surface of the main rod 2011.
[0037] Please refer to Figure 2 and Figure 3 , one end of the connecting plate 2041 of this embodiment is fixedly connected to the side wall of the central rod 2021, and the outer wall of the central rod 2021 is movably attached to the inner wall of the installation groove of the main rod 2011. A plurality of threaded grooves are evenly opened on the side wall of the sleeve 2043. A screw is threadedly connected to the inner cavity of the threaded groove on the side close to the vertical plate 2042, and the end of the screw away from the threaded groove threadedly penetrates through the vertical plate 2042.
[0038] Let the threaded rod pass through the vertical plate 2042 and enter the threaded groove of the sleeve 2043 to fix the central rod 2021 to the main rod 2011. At this time, when the main rod 2011 rotates, it will drive the central rod 2021 to rotate together. Since the central rod 2021 is inserted into the rectangular groove of the scraper 203 and the convex rod 2022 is in contact with the rectangular groove, it drives the scraper 203 to rotate, so that the scraper 203 scrapes and cleans the inner wall of the device main body 1.
[0039] An additional connecting component 204 is provided. By loosening the threaded rod, the central rod 2021 is separated from the main rod 2011, so that the scraper 203 will not rotate, and the working state can be switched, preventing the scraper 203 from continuously scraping the inner wall of the device main body 1 and causing wear.
[0040] The above are only the preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention shall be included within the protection scope of the present invention.
Claims
1. An apparatus for producing ammonium phosphate using low-grade raffinate acid, comprising a main body of the apparatus (1), a support frame (3) is provided at the bottom of the main body of the apparatus (1), and a feed inlet and a discharge outlet are respectively provided at the top and the bottom of the main body of the apparatus (1), and it is characterized in that: A movable part (2) is provided at the top of the main body of the apparatus (1), the movable part (2) includes a stirring assembly (201), a transmission assembly (202), a scraper (203) and a connecting assembly (204), the transmission assembly (202) is arranged inside the stirring assembly (201), the scraper (203) is arranged on the side wall of the transmission assembly (202), and the connecting assembly (204) is used to connect the stirring assembly (201) and the scraping assembly.
2. The device for producing ammonium phosphate by using low-grade raffinate acid according to claim 1, characterized in that, The stirring assembly (201) is composed of a main rod (2011), a first gear (2012), a second gear (2013), a motor (2014) and stirring rods (2015), the motor (2014) is installed at the top of the main body of the apparatus (1), the main rod (2011) is fixedly installed on the output end of the motor (2014), and the first gear (2012) is installed on the surface of the main rod (2011).
3. The device for producing ammonium phosphate by using low-grade raffinate acid according to claim 2, characterized in that, The top of the main rod (2011) is connected to the main body of the apparatus (1) through a bearing, and the second gear (2013) is fixedly installed on the main rod (2011), and the second gear (2013) meshes with the first gear (2012), the stirring rods (2015) are fixedly installed on the side wall of the main rod (2011), and an installation groove is opened inside the main rod (2011).
4. The device for producing ammonium phosphate by using low-grade raffinate acid according to claim 1, characterized in that, The transmission assembly (202) is composed of a central rod (2021) and a convex rod (2022), the convex rod (2022) is fixedly installed on the end face of the central rod (2021), and the central rod (2021) is movably inserted into the installation groove inside the main rod (2011).
5. The device for producing ammonium phosphate by using low-grade raffinate acid according to claim 1, characterized in that, A rectangular groove is opened on one side of the scraper (203), the convex rod (2022) is movably inserted into the inner cavity of the rectangular groove of the scraper (203), and the side wall of the scraper (203) is movably attached to the inner wall of the main body of the apparatus (1).
6. The device for producing ammonium phosphate by using low-grade raffinate acid according to claim 1, characterized in that, The connecting assembly (204) includes a connecting plate (2041), a vertical plate (2042) and a sleeve (2043), the vertical plate (2042) is fixedly installed at the bottom of the connecting plate (2041), and the sleeve (2043) is fixedly installed on the surface of the main rod (2011).
7. An apparatus for producing ammonium phosphate using low-grade raffinate acid according to claim 6, characterized in that, One end of the connecting plate (2041) is fixedly connected to the side wall of the central rod (2021), and the outer wall of the central rod (2021) is movably attached to the inner wall of the installation groove of the main rod (2011), and a plurality of threaded grooves are uniformly opened on the side wall of the sleeve (2043), and a screw rod is threadedly connected to the inner cavity of the threaded groove on one side close to the vertical plate (2042), and the end of the screw rod away from the threaded groove threadedly penetrates through the vertical plate (2042).