Device for preventing asphaltene in esterified acid water from being separated out and aggregated
By introducing a high-flow circulation pump and a conveying pump into the esterification device, the problem of asphaltene aggregation in the esterified acid water is solved, ensuring the stable operation and safety of the system, and reducing production costs and operation difficulty.
Patent Information
- Application Number
- CN202422379522.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-27
- Publication Date
- 2025-07-18
- Estimated Expiration
- 2034-09-27
AI Technical Summary
The precipitation and aggregation of asphaltene in esterified acid water affects the stable operation of the esterification system, increases the workload and labor intensity of operators, leads to damage to the storage tank equipment, increases the difficulty of solid waste disposal and production costs, and poses safety risks.
Using a device including a first esterification kettle and a second esterification kettle, combined with a high-flow material circulation pump and a material delivery pump, the esterified acid water is forced to circulate the asphaltene completely dissolves in the acid water, avoids aggregation and condensation, and treats the asphaltene through an incinerator.
The stable operation of the esterification system has been achieved, the demand for solid waste treatment and equipment cleaning has been reduced, the labor intensity and safety risks of operators have been reduced, and the production costs have been reduced.
Smart Images
Figure CN223113040U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of esterification protection, in particular to a device for preventing the precipitation and aggregation of asphaltene in esterification acid water. Background Art
[0002] During the production process of MMA, the esterification acid water enters the acid water storage tank. After staying for a period of time, the asphaltene in the acid water will precipitate, aggregate and coagulate, which will affect the transportation and storage of acid water in the long run, and it is necessary to regularly switch the acid water storage tank for cleaning.
[0003] The inventor found the following problems in the prior art during the implementation of the present utility model: 1. It affects the stable operation of the esterification system. 2. It increases the workload and labor intensity of operators. 3. It is easy to cause damage to storage tank equipment. 4. It increases the difficulty of solid waste treatment. 5. It increases the production cost. 6. There are personnel safety risks in regular switching and cleaning. Content of the Utility Model
[0004] In view of the deficiencies of the prior art, the present utility model provides a device for preventing the precipitation and aggregation of asphaltene in esterification acid water, which solves the following problems existing in the existing device: 1. It affects the stable operation of the esterification system. 2. It increases the workload and labor intensity of operators. 3. It is easy to cause damage to storage tank equipment. 4. It increases the difficulty of solid waste treatment. 5. It increases the production cost. 6. There are personnel safety risks in regular switching and cleaning.
[0005] To achieve the above object, the present utility model is realized through the following technical solutions: A device for preventing the precipitation and aggregation of asphaltene in esterification acid water, including a first esterification kettle, the first esterification kettle is connected with a second esterification kettle, the lower end of the second esterification kettle is connected with a first filter and a second filter, the first filter is connected with the input end of a material circulation pump, the output end of the material circulation pump is connected to the inside of the second esterification kettle, the second filter is connected with the input end of a material delivery pump, and the output end of the material delivery pump is connected to a waste acid device incinerator.
[0006] Preferably, both the first esterification kettle and the second esterification kettle can carry out esterification gas phase.
[0007] Preferably, both the material circulation pump and the material delivery pump are large flow pumps.
[0008] Beneficial Effects
[0009] The utility model provides a device for preventing the precipitation and aggregation of asphaltene in esterification acid water. The utility model designs a structure for promoting the complete dissolution of asphaltene in acid water. The first esterification kettle and the second esterification kettle can carry out esterification gas phase. During the esterification operation process, in the second esterification kettle, a large-flow material circulation pump is added to force the acid water in the second esterification kettle to circulate in a large flow, so that all the asphaltene in the acid water is dissolved in the acid water and will not be sucked out, aggregated and condensed. Through the forced circulation of the large-flow pump, all the asphaltene in the acid water is dissolved in the acid water, and will not be sucked out, aggregated and condensed. There is no need to switch and clean, no need to treat solid waste, and the stable operation of the device can be ensured. BRIEF DESCRIPTION OF THE DRAWINGS
[0010] Figure 1 It is a schematic diagram of the overall structure of the present utility model.
[0011] In the figure: 1. The first esterification kettle; 2. The second esterification kettle; 3. The waste acid device incinerator; 4. The material circulation pump; 5. The first filter; 6. The material delivery pump; 7. The second filter. DETAILED DESCRIPTION OF THE EMBODIMENTS
[0012] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present utility model.
[0013] Please refer to Figure 1 , the present utility model provides a technical solution: a device for preventing the precipitation and aggregation of asphaltene in esterification acid water, including a first esterification kettle 1, the first esterification kettle 1 is connected with a second esterification kettle 2, the lower end of the second esterification kettle 2 is connected with a first filter 5 and a second filter 7, the first filter 5 is connected with the input end of a material circulation pump 4, the output end of the material circulation pump 4 is connected to the inside of the second esterification kettle 2, the second filter 7 is connected with the input end of a material delivery pump 6, and the output end of the material delivery pump 6 is connected to a waste acid device incinerator 3.
[0014] In this embodiment, it is further set that both the first esterification kettle 1 and the second esterification kettle 2 can carry out esterification gas phase.
[0015] In this embodiment, it is further set that both the material circulation pump 4 and the material delivery pump 6 are large-flow pumps.
[0016] The detailed connection means are well-known techniques in the art. The following mainly introduces the working principle and process, and the specific work is as follows.
[0017] Example: The first esterification kettle 1 and the second esterification kettle 2 can carry out esterification in the gas phase. During the esterification operation process, a large-flow material circulation pump 4 is added in the last esterification kettle, that is, the second esterification kettle 2, to force the large-flow circulation of the acid water in the second esterification kettle 2, so that all the asphaltenes in the acid water are dissolved in the acid water, and will not be sucked out, aggregated and condensed. All are dissolved in the acid water and are directly transported to the incinerator 3 of the waste acid device through the material transfer pump 6 for incineration treatment, without the need to switch and clean for solid waste treatment anymore. The first filter 5 and the second filter 7 filter the small pieces of asphaltenes that have condensed.
[0018] It should be noted that in this article, relational terms such as first and second are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any actual relationship or order between these entities or operations.
Claims
1. An apparatus for preventing precipitation and aggregation of asphaltene in esterification acid water, comprising a first esterification kettle (1), characterized in that, The first esterification kettle (1) is connected to a second esterification kettle (2). The lower end of the second esterification kettle (2) is connected to a first filter (5) and a second filter (7). The first filter (5) is connected to the input end of a material circulation pump (4). The output end of the material circulation pump (4) is connected to the inside of the second esterification kettle (2). The second filter (7) is connected to the input end of a material delivery pump (6). The output end of the material delivery pump (6) is connected to a waste acid device incinerator (3).
2. The device for preventing precipitation and aggregation of asphaltene in esterification acid water according to claim 1, characterized in that, Both the first esterification kettle (1) and the second esterification kettle (2) can carry out esterification gas phase.
3. The device for preventing precipitation and aggregation of asphaltene in esterification acid water according to claim 1, characterized in that, Both the material circulation pump (4) and the material delivery pump (6) are high-flow pumps.