Gas-liquid separation device

By designing the hydrogen discharge structure and oxygen discharge structure of the gas-liquid separation device, using alkaline solution to adsorb impurities, the problem of decreasing hydrogen purity in electrolytic hydrogen production is solved, and the collection of high-purity hydrogen is achieved.

CN223240177UActive Publication Date: 2025-08-19JIANGSU RONGHYDROGEN NEW ENERGY TECHNOLOGY CO LTD
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Patent Information

Application Number
CN202422813632.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-19
Publication Date
2025-08-19
Estimated Expiration
2034-11-19

AI Technical Summary

Technical Problem

During the electrolytic hydrogen production process, impurities may remain in the hydrogen gas, resulting in a decrease in purity, which is difficult to effectively remove in the prior art.

Method used

A gas-liquid separation device is designed, including a hydrogen discharge structure and an oxygen discharge structure. It uses the alkaline solution in the outer sleeve to absorb impurities and ensure the purity of hydrogen through the combined structure of a conical through hole and an outer conical sleeve.

Benefits of technology

It effectively removes impurities in hydrogen, improves the purity of hydrogen, and ensures the collection quality of hydrogen.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the field of electrolytic hydrogen production, and particularly discloses a gas-liquid separation device which comprises an electrolytic bath and an upper sealing cover, a hydrogen discharging structure is mounted on one side of the upper surface of the upper sealing cover, an oxygen discharging structure is mounted on the other side of the upper surface of the upper sealing cover, the hydrogen discharging structure comprises an outer sleeve and a conical through hole, an outer conical sleeve is arranged above the conical through hole, and an oxygen discharging hole is formed in the outer sleeve. A connecting rod is connected between the outer conical sleeve and the conical through hole, an inner gathering plate is installed on the portion, located on the inner side wall of the outer sleeve, above the outer conical sleeve, an exhaust pipe is arranged above the inner gathering plate, and a flexible sleeve is installed at the end, close to the inner gathering plate, of the exhaust pipe. An inner gathering plate injects an impurity removal solution to the bottom of the outer sleeve, so that the liquid level is integrally lower than the upper end face of a conical through hole, hydrogen carrying possible residual impurities integrally passes through the outer sleeve, then is blocked by an outer conical sleeve, integrally adsorbs and removes the impurities from an alkaline solution in the outer sleeve, and continuously moves upwards; and the purity of the collected hydrogen is ensured.
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Description

Technical Field

[0001] The utility model relates to the field of electrolytic hydrogen production, in particular to a gas-liquid separation device. Background Art

[0002] The important links in water electrolysis hydrogen production include power supply, electrolytic cell, separation, washing and cooling equipment and electrolyte. The electrolyte is very important here. It directly affects the efficiency of electrolysis and the quality of hydrogen produced. If there is a problem with the quality of the electrolyte, no matter how good the production equipment is, it will not be able to produce hydrogen normally and output qualified hydrogen. Selecting qualified electrolytes (such as potassium hydroxide, sodium oxide) as required and ensuring the purity of the water used are the first step to ensure the quality of the electrolyte. Otherwise, the quality of the electrolyte cannot be guaranteed.

[0003] However, since certain impurity gases may remain in the hydrogen produced by electrolysis, the purity of the hydrogen will be affected when it is directly collected. Utility Model Content

[0004] In view of the deficiencies in the prior art, the present invention provides a gas-liquid separation device to solve the problems mentioned in the above background.

[0005] The utility model provides the following technical solutions: a gas-liquid separation device, comprising an electrolytic cell and an upper cover, wherein a hydrogen discharge structure is installed on one side of the upper surface of the upper cover, and an oxygen discharge structure is installed on the other side of the upper surface of the upper cover, the hydrogen discharge structure comprising: an outer sleeve, a conical through hole, an outer conical sleeve is arranged above the conical through hole, a connecting rod is connected between the outer conical sleeve and the conical through hole, an inner converging plate is installed on the inner side wall of the outer sleeve above the outer conical sleeve, an exhaust pipe is arranged above the inner converging plate, and a flexible sleeve is installed on one end of the exhaust pipe located close to the inner converging plate.

[0006] As a further solution of the present invention: a power supply is installed on the upper surface of the upper cover between the hydrogen exhaust structure and the oxygen exhaust structure, a cathode electrolysis wire is installed through the upper cover on the side of the power supply close to the oxygen exhaust structure, and an anode electrolysis wire is installed through the upper cover on the side of the power supply close to the hydrogen exhaust structure.

[0007] As a further solution of the present invention: a diaphragm is installed on the lower surface of the upper cover between the cathode electrolysis wire and the anode electrolysis wire.

[0008] As a further solution of the present invention: the tapered through hole is connected to the upper cover, and the outer tapered sleeve is fixedly connected to the tapered through hole via the connecting rod.

[0009] As a further solution of the present invention: the diaphragm is fixedly connected to the upper cover.

[0010] As a further solution of the present invention: the cathode electrolysis wire and the anode electrolysis wire are both electrically connected to the power supply.

[0011] As a further solution of the present invention: the outer sleeve is a transparent material component, and the outer sleeve and the upper cover are fixedly formed as one piece.

[0012] As a further solution of the present invention: a pipe clamp is installed at the connection between the outer side of the flexible sleeve and the inner converging plate.

[0013] Compared with the prior art, the beneficial effects of the present invention are:

[0014] 1. Use a pipe to insert from the inside of the inner converging plate to the bottom position of the outer sleeve and then inject the impurity removal solution so that the overall liquid level is lower than the upper end surface of the tapered through-hole. The hydrogen carrying any remaining impurities will pass through the outer sleeve as a whole. Under the blockage of the outer conical sleeve, the hydrogen will be adsorbed from the alkaline solution inside the outer sleeve to remove impurities. The hydrogen will then continue to move upward to ensure the purity of the collected hydrogen. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 Schematic diagram of the structure of a gas-liquid separation device;

[0016] Figure 2 It is a structural schematic diagram of a hydrogen discharge structure in a gas-liquid separation device;

[0017] Figure 3 This is a schematic diagram of the internal structure of a hydrogen discharge structure in a gas-liquid separation device;

[0018] Figure 4 It is a front view of an electrolytic cell in a gas-liquid separation device;

[0019] Figure 5 A cross-sectional view of an electrolytic cell in a gas-liquid separation device.

[0020] In the figure: 1. electrolytic cell; 2. upper cover; 3. hydrogen exhaust structure; 4. oxygen exhaust structure; 5. diaphragm; 6. power supply; 301. outer sleeve; 302. conical through hole; 303. outer conical sleeve; 304. connecting rod; 305. inner converging plate; 306. exhaust pipe; 307. flexible sleeve; 601. cathode electrolysis wire; 602. anode electrolysis wire. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0022] like Figure 1-5 As shown, this embodiment provides a gas-liquid separation device, including an electrolytic cell 1 and an upper cover 2, a hydrogen discharge structure 3 is installed on one side of the upper surface of the upper cover 2, and an oxygen discharge structure 4 is installed on the other side of the upper surface of the upper cover 2, the hydrogen discharge structure 3 includes: an outer sleeve 301, a tapered through hole 302, the outer sleeve 301 is a transparent material component, the outer sleeve 301 and the upper cover 2 are fixedly formed as a whole, the tapered through hole 302 is connected to the upper cover 2, an outer tapered sleeve 303 is provided above the tapered through hole 302, and an outer tapered sleeve 303 is provided above the tapered through hole 302. A connecting rod 304 is connected between the conical sleeve 303 and the conical through hole 302. The outer conical sleeve 303 is fixedly connected to the conical through hole 302 through the connecting rod 304. An inner converging plate 305 is installed above the outer conical sleeve 303 on the inner side wall of the outer sleeve 301. An exhaust pipe 306 is provided above the inner converging plate 305. A flexible sleeve 307 is installed at one end of the exhaust pipe 306 close to the inner converging plate 305. A pipe clamp is installed at the connection between the outer side of the flexible sleeve 307 and the inner converging plate 305.

[0023] like Figure 2-3 As shown, in this embodiment, a power supply 6 is installed on the upper surface of the upper cover 2 between the hydrogen exhaust structure 3 and the oxygen exhaust structure 4, a cathode electrolysis wire 601 is installed on the side of the power supply 6 close to the oxygen exhaust structure 4 and passes through the upper cover 2, and an anode electrolysis wire 602 is installed on the side of the power supply 6 close to the hydrogen exhaust structure 3 and passes through the upper cover 2, both the cathode electrolysis wire 601 and the anode electrolysis wire 602 are electrically connected to the power supply 6, and a diaphragm 5 is installed on the lower surface of the upper cover 2 between the cathode electrolysis wire 601 and the anode electrolysis wire 602, and the diaphragm 5 is fixedly connected to the upper cover 2.

[0024] The working principle of the present invention is as follows: when in use, after pouring the electrolyte into the interior of the electrolytic cell 1 as a whole, the upper cover 2 is sealed as a whole at the upper end position of the electrolytic cell 1, and different adsorption solutions are selected to be poured into the interior of the outer sleeve 301 according to the type of electrolyte. When the impurities in the hydrogen are acidic impurities, a high-concentration alkaline solution is injected from the interior of the inner convergence plate 305 to the bottom position of the outer sleeve 301, so that the liquid level is lower than the upper end surface of the tapered through hole 302. The flexible sleeve 307 at the lower end of the exhaust pipe 306 is completely covered on the upper end of the inner convergence plate 305 and then fastened with a clamp. 6 The cathode electrolysis wire 601 and the anode electrolysis wire 602 are powered respectively to energize the electrolyte inside the electrolytic cell 1. Hydrogen will be generated at the position of the cathode electrolysis wire 601, and oxygen will be generated at the position of the anode electrolysis wire 602. The hydrogen will be transmitted to the inside of the outer sleeve 301 through the tapered through hole 302. The hydrogen will pass through the outer sleeve 301 as a whole, carrying any remaining impurities. After the hydrogen is blocked by the outer conical sleeve 303, the hydrogen will be removed from the alkaline solution inside the outer sleeve 301 by adsorption. After that, the hydrogen will continue to move upward, and under the interception effect of the inner converging plate 305, the hydrogen will be transferred and collected from the position of the exhaust pipe 306.

[0025] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variations thereof are intended to cover non-exclusive inclusion, so that a process, method, article or apparatus that includes a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or apparatus.

[0026] Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations may be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A gas-liquid separation device, comprising an electrolytic cell (1) and an upper cover (2), characterized in that: A hydrogen discharge structure (3) is installed on one side of the upper surface of the upper cover (2), and an oxygen discharge structure (4) is installed on the other side of the upper surface of the upper cover (2). The hydrogen discharge structure (3) comprises: an outer sleeve (301), a conical through hole (302), an outer conical sleeve (303) is provided above the conical through hole (302), a connecting rod (304) is connected between the outer conical sleeve (303) and the conical through hole (302), an inner converging plate (305) is installed above the outer conical sleeve (303) and located on the inner side wall of the outer sleeve (301), an exhaust pipe (306) is provided above the inner converging plate (305), and a flexible sleeve (307) is installed at one end of the exhaust pipe (306) located near the inner converging plate (305).

2. A gas-liquid separation device according to claim 1, characterized in that: A power supply (6) is installed on the upper surface of the upper cover (2) between the hydrogen discharge structure (3) and the oxygen discharge structure (4); a cathode electrolysis wire (601) is installed on the side of the power supply (6) close to the oxygen discharge structure (4) and passing through the upper cover (2); and an anode electrolysis wire (602) is installed on the side of the power supply (6) close to the hydrogen discharge structure (3) and passing through the upper cover (2).

3. A gas-liquid separation device according to claim 2, characterized in that: A diaphragm (5) is installed on the lower surface of the upper cover (2) between the cathode electrolysis wire (601) and the anode electrolysis wire (602).

4. The gas-liquid separation device according to claim 1, characterized in that: The conical through hole (302) is connected to the upper cover (2), and the outer conical sleeve (303) is fixedly connected to the conical through hole (302) via the connecting rod (304).

5. The gas-liquid separation device according to claim 3, characterized in that: The diaphragm (5) is fixedly connected to the upper cover (2).

6. A gas-liquid separation device according to claim 2, characterized in that: The cathode electrolysis wire (601) and the anode electrolysis wire (602) are both electrically connected to the power supply (6).

7. The gas-liquid separation device according to claim 1, characterized in that: The outer sleeve (301) is a transparent material component, and the outer sleeve (301) and the upper cover (2) are fixedly formed as one piece.

8. The gas-liquid separation device according to claim 1, characterized in that: A pipe clamp is installed at the connection between the outer side of the flexible sleeve (307) and the inner converging plate (305).