Crystallizing tank for producing veterinary bulk drugs

By introducing a stirring component and a cooling component into the crystallization tank, the problem of high water circulation evaporation in traditional crystallization tanks is solved. The combined use of the stirring component and the cooling component achieves a more uniform cooling effect, higher crystallization efficiency, and less water consumption.

CN223615415UActive Publication Date: 2025-12-02HEBEI ANLIN PHARMA
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Patent Information

Application Number
CN202520266565.8
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-02-19
Publication Date
2025-12-02
Estimated Expiration
2035-02-19

AI Technical Summary

Technical Problem

Traditional crystallizers consume a large amount of water during cooling, and the water consumption is also high during water circulation cooling. In the existing technology, the evaporation rate of water circulation cooling is high, which leads to water waste and increased costs.

Method used

The design employs a combination of stirring and cooling components, including stirring rods and scrapers for stirring, atomizing nozzles for uniform cooling, reducing water consumption, and optimizing the crystallization process through mixing and collecting components.

Benefits of technology

The crystallizer achieves more uniform cooling, reduces water consumption, and improves crystallization efficiency and purity.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of raw material medicines, and provides a crystallizing tank for producing veterinary raw material medicines, which comprises a tank body, a mixing component is mounted at the top of a main support plate, a stirring component is mounted at the bottom of an auxiliary support plate, a cooling component is mounted in the tank body, and a collecting component is mounted at the bottom of the tank body. The driving motor is started to drive the stirring shaft to enable the stirring rod and the scraping rod to rotate, the stirring rod enables the liquid medicine to maintain a rotating state all the time, and meanwhile, the scraping rod can scrape and brush viscous liquid adhered to the inner wall and the bottom of the crystallization bin, so that the viscous liquid continues to participate in stirring and mixing of liquid in the tank; meanwhile, cooling water is atomized and sprayed out through an atomizing nozzle by virtue of a liquid inlet pipe, and the water is released into air in the form of small particles, so that the temperature of the whole space is reduced more uniformly, and the crystallization operation of the crystallization bin is facilitated. By means of the technical scheme, the problem that in the prior art, water consumption is large during cooling is solved.
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Description

Technical Field

[0001] This utility model relates to the field of active pharmaceutical ingredients (APIs), specifically to a crystallization tank for the production of veterinary APIs. Background Technology

[0002] Active pharmaceutical ingredients (APIs) refer to the raw materials used in the production of various formulations. They are the active ingredients in these formulations and are various powders, crystals, extracts, etc., prepared by chemical synthesis, plant extraction, or biotechnology for medicinal use, but which patients cannot directly ingest. After heat processing, APIs need to be placed in crystallization tanks for cooling and crystallization to improve the purity of the finished drug.

[0003] In the process of extracting active pharmaceutical ingredients, in order to enable the active ingredients to exert their effects, it is usually necessary to extract and recrystallize the drugs. Traditional crystallization tanks often use water circulation cooling during crystallization, but water circulation cooling often has a high evaporation rate and uses a large amount of water. Utility Model Content

[0004] This invention proposes a crystallization tank for the production of veterinary raw materials, which solves the problem of excessive water consumption during cooling in related technologies.

[0005] The technical solution of this utility model is as follows: A crystallization tank for the production of veterinary raw materials includes a tank body. A main support plate, a secondary support plate, and a diversion plate are fixedly connected from top to bottom inside the tank body. A mixing component is installed on the top of the main support plate, a stirring component is installed on the bottom of the secondary support plate, a cooling component is installed inside the tank body, and a collecting component is installed at the bottom of the tank body.

[0006] Preferably, the stirring assembly includes a crystallization chamber, which is fixed to the bottom of a secondary support plate. A drive motor is fixedly connected to the top of the secondary support plate. The output end of the drive motor extends into the interior of the crystallization chamber and is fixedly mounted with a stirring shaft. A stirring rod is fixedly connected to the outside of the stirring shaft, and a scraper is fixedly connected to the outside of the stirring rod. The outside of the crystallization chamber is fixedly connected to the inside of a guide plate.

[0007] Preferably, the cooling assembly includes a retaining ring fixed inside the tank, an atomizing nozzle mounted outside the retaining ring, an inlet pipe fixedly connected to the outside of the tank, the end of the inlet pipe extending into the inside of the retaining ring, and a recovery pipe fixedly connected to the bottom of the diversion plate, the end of the recovery pipe extending to the outside of the tank.

[0008] Preferably, the mixing assembly includes a mixing chamber, which is fixed to the top of the main support plate. A main shaft motor is fixedly connected to the top of the mixing chamber. The output end of the main shaft motor extends into the interior of the mixing chamber and is fixedly mounted with a rotating shaft. A paddle is fixedly connected to the outside of the rotating shaft. A feed pipe is fixedly connected to the top of the mixing chamber, and the end of the feed pipe extends to the outside of the tank. An electric heating rod is fixedly mounted inside the mixing chamber.

[0009] Preferably, the collection assembly includes a support column fixed to the bottom of the tank, a fixing plate fixedly connected to the outside of the support column, a secondary shaft motor fixedly connected to the top of the fixing plate, a fixing block fixedly connected to the top of the fixing plate, and a spiral blade fixedly installed at the output end of the secondary shaft motor.

[0010] Preferably, a base plate is fixedly connected to the bottom of the support column, a collection box is provided on the top of the base plate, a guide tube is fixedly connected to the bottom of the fixing plate, the upper end of the guide tube extends into the interior of the fixing block, and the collection box is located below the guide tube.

[0011] Preferably, a connecting pipe is fixedly connected to the top of the secondary support plate, the upper end of the connecting pipe extends into the interior of the mixing chamber, and the bottom end of the connecting pipe extends into the interior of the crystallization chamber.

[0012] Preferably, a discharge pipe is fixedly connected to the outside of the crystallization chamber, and the lower end of the discharge pipe extends into the interior of the fixed block.

[0013] The working principle and beneficial effects of this utility model are as follows:

[0014] 1. In this utility model, the start-up drive motor drives the stirring shaft, causing the stirring rod and scraper to rotate. The stirring rod keeps the liquid in a rotating state, while the scraper can scrape the viscous liquid adhering to the inner wall and bottom of the crystallization chamber, allowing it to continue to participate in the stirring and mixing of the liquid in the tank. At the same time, cooling water is atomized and sprayed out through the liquid inlet pipe through the atomizing nozzle, releasing water into the air in the form of tiny particles. These particles can be evenly distributed throughout the space, thereby making the temperature of the entire space drop more evenly, thus facilitating the crystallization operation in the crystallization chamber.

[0015] 2. In this utility model, the raw materials are fed into the mixing chamber through the feed pipe. The electric heating rod is started to heat the raw materials to facilitate mixing. The main shaft motor is started to drive the rotating shaft to rotate the blades and accelerate the mixing of the medicine. After the medicine is crystallized, the auxiliary shaft motor is started to make the spiral blades transport the crystallized medicine through the guide pipe to the collection box to prevent crystal precipitation from clogging the discharge pipe. Attached Figure Description

[0016] The present invention will now be described in further detail with reference to the accompanying drawings and specific embodiments.

[0017] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0018] Figure 2 This is a schematic diagram of the main cross-sectional structure of this utility model;

[0019] Figure 3 This is a side view sectional structural diagram of the present invention;

[0020] Figure 4 This is a schematic diagram of the structure of the collection component of this utility model;

[0021] Figure 5 This is a schematic diagram of the hybrid component structure of this utility model;

[0022] In the diagram: 1. Tank body; 2. Main support plate; 3. Secondary support plate; 4. Drain plate; 5. Mixing assembly; 51. Mixing chamber; 52. Main shaft motor; 53. Rotating shaft; 54. Paddle blade; 55. Electric heating rod; 56. Feed pipe; 6. Stirring assembly; 61. Crystallization chamber; 62. Drive motor; 63. Stirring shaft; 64. Stirring rod; 65. Scraper; 7. Cooling assembly; 71. Fixing ring; 72. Liquid inlet pipe; 73. Atomizing nozzle; 74. Recovery pipe; 8. Collection assembly; 81. Fixing plate; 82. Support column; 83. Bottom plate; 84. Secondary shaft motor; 85. Fixing block; 86. Spiral blade; 87. Collection box; 88. Guide pipe; 9. Connecting pipe; 10. Discharge pipe. Detailed Implementation

[0023] The technical solutions of this utility model will be clearly and completely described below with reference to the embodiments of this utility model. Obviously, the described embodiments are only some embodiments of this utility model, and not all embodiments. Based on the embodiments of this utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the scope of protection of this utility model.

[0024] Example 1

[0025] like Figures 1-3 As shown in the figure, this embodiment proposes a crystallization tank for the production of veterinary raw materials, including a tank body 1. Inside the tank body 1, a main support plate 2, a secondary support plate 3 and a diversion plate 4 are fixedly connected from top to bottom. A mixing component 5 is installed on the top of the main support plate 2, a stirring component 6 is installed on the bottom of the secondary support plate 3, a cooling component 7 is installed inside the tank body 1, and a collecting component 8 is installed at the bottom of the tank body 1.

[0026] Furthermore, the stirring assembly 6 includes a crystallization chamber 61, which is fixed to the bottom of the auxiliary support plate 3. A drive motor 62 is fixedly connected to the top of the auxiliary support plate 3. The output end of the drive motor 62 extends into the interior of the crystallization chamber 61 and is fixedly mounted with a stirring shaft 63. A stirring rod 64 is fixedly connected to the outside of the stirring shaft 63, and a scraper 65 is fixedly connected to the outside of the stirring rod 64. The outside of the crystallization chamber 61 is fixedly connected to the inside of the diversion plate 4. A connecting pipe 9 is fixedly connected to the top of the auxiliary support plate 3. The upper end of the connecting pipe 9 extends into the interior of the mixing chamber 51, and the bottom end of the connecting pipe 9 extends into the interior of the crystallization chamber 61. A discharge pipe 10 is fixedly connected to the outside of the crystallization chamber 61, and the lower end of the discharge pipe 10 extends into the interior of the fixing block 85. When the drive motor 62 is started, it drives the stirring shaft 63 to rotate the stirring rod 64 and the scraper 65. The stirring rod 64 keeps the liquid rotating, while the scraper 65 scrapes the viscous liquid adhering to the inner wall and bottom of the crystallization chamber 61, allowing it to continue to participate in the stirring and mixing of the liquid in the tank.

[0027] Furthermore, the cooling assembly 7 includes a fixing ring 71, which is fixed inside the tank 1. An atomizing nozzle 73 is installed outside the fixing ring 71. An inlet pipe 72 is fixedly connected to the outside of the tank 1, and the end of the inlet pipe 72 extends into the inside of the fixing ring 71. A recovery pipe 74 is fixedly connected to the bottom of the guide plate 4, and the end of the recovery pipe 74 extends to the outside of the tank 1. The cooling water is atomized and sprayed out through the atomizing nozzle 73 via the inlet pipe 72, releasing the water into the air in the form of tiny particles. These particles can be evenly distributed throughout the space, thereby making the temperature of the entire space drop more evenly, which facilitates the crystallization operation of the crystallization chamber 61.

[0028] In this embodiment, the drive motor 62 is started to drive the stirring shaft 63, causing the stirring rod 64 and scraper 65 to rotate. The stirring rod 64 keeps the liquid in a rotating state, while the scraper 65 can scrape the viscous liquid adhering to the inner wall and bottom of the crystallization chamber 61, so that it can continue to participate in the stirring and mixing of the liquid in the tank. At the same time, the cooling water is atomized and sprayed out through the liquid inlet pipe 72 through the atomizing nozzle 73, releasing the water into the air in the form of tiny particles. These particles can be evenly distributed throughout the space, thereby making the temperature of the entire space drop more evenly, thus facilitating the crystallization operation of the crystallization chamber 61.

[0029] Example 2

[0030] like Figures 1-5As shown, based on the same concept as Embodiment 1 above, this embodiment also proposes a mixing component 5 including a mixing chamber 51. The mixing chamber 51 is fixed to the top of the main support plate 2. A main shaft motor 52 is fixedly connected to the top of the mixing chamber 51. The output end of the main shaft motor 52 extends into the interior of the mixing chamber 51 and a rotating shaft 53 is fixedly installed thereon. A paddle 54 is fixedly connected to the outside of the rotating shaft 53. A feed pipe 56 is fixedly connected to the top of the mixing chamber 51. The end of the feed pipe 56 extends to the outside of the tank body 1. An electric heating rod 55 is fixedly installed inside the mixing chamber 51. The raw materials are allowed to enter the mixing chamber 51 through the feed pipe 56. The electric heating rod 55 is activated to heat the raw materials to facilitate mixing. The main shaft motor 52 is activated to drive the rotating shaft 53 to rotate the paddle 54 and accelerate the mixing of the liquid medicine.

[0031] Furthermore, the collection component 8 includes a support column 82, which is fixed to the bottom of the tank 1. A fixing plate 81 is fixedly connected to the outside of the support column 82. A secondary shaft motor 84 is fixedly connected to the top of the fixing plate 81, and a fixing block 85 is fixedly connected to the top of the fixing plate 81. A spiral blade 86 is fixedly installed at the output end of the secondary shaft motor 84. A base plate 83 is fixedly connected to the bottom of the support column 82. A collection box 87 is provided on the top of the base plate 83. A guide pipe 88 is fixedly connected to the bottom of the fixing plate 81. The upper end of the guide pipe 88 extends into the interior of the fixing block 85. The collection box 87 is located below the guide pipe 88. After the liquid crystallizes, the secondary shaft motor 84 is started so that the spiral blade 86 transports the crystallized liquid through the guide pipe 88 into the collection box 87 to prevent crystallization and precipitation from clogging the discharge pipe 10.

[0032] In this embodiment, the raw materials are fed into the mixing chamber 51 through the feed pipe 56. The electric heating rod 55 is started to heat the raw materials to facilitate mixing. The main shaft motor 52 is started to drive the rotating shaft 53 to make the paddle 54 rotate, which accelerates the mixing of the medicine liquid. After the medicine liquid crystallizes, the secondary shaft motor 84 is started to make the spiral blade 86 transport the crystallized medicine liquid through the guide pipe 88 to the collection box 87 to prevent crystal precipitation from clogging the discharge pipe 10.

[0033] The above are merely preferred embodiments of the present utility model and are not intended to limit the present utility model. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model shall be included within the protection scope of the present utility model.

Claims

1. A crystallization tank for the production of veterinary raw materials, characterized in that, The tank (1) includes a main support plate (2), a secondary support plate (3) and a diversion plate (4) which are fixedly connected from top to bottom inside the tank (1). A mixing component (5) is installed on the top of the main support plate (2), a stirring component (6) is installed on the bottom of the secondary support plate (3), a cooling component (7) is installed inside the tank (1), and a collecting component (8) is installed at the bottom of the tank (1).

2. A crystallization tank for the production of veterinary raw materials according to claim 1, characterized in that, The stirring assembly (6) includes a crystallization chamber (61), which is fixed to the bottom of a secondary support plate (3). A drive motor (62) is fixedly connected to the top of the secondary support plate (3). The output end of the drive motor (62) extends into the interior of the crystallization chamber (61) and is fixedly installed with a stirring shaft (63). A stirring rod (64) is fixedly connected to the outside of the stirring shaft (63). A scraper (65) is fixedly connected to the outside of the stirring rod (64). The outside of the crystallization chamber (61) is fixedly connected to the inside of the diversion plate (4).

3. A crystallization tank for the production of veterinary raw materials according to claim 1, characterized in that, The cooling assembly (7) includes a retaining ring (71) fixed inside the tank (1), an atomizing nozzle (73) installed outside the retaining ring (71), an inlet pipe (72) fixedly connected to the outside of the tank (1), the end of the inlet pipe (72) extending into the inside of the retaining ring (71), and a recovery pipe (74) fixedly connected to the bottom of the diversion plate (4), the end of the recovery pipe (74) extending to the outside of the tank (1).

4. A crystallization tank for the production of veterinary raw materials according to claim 2, characterized in that, The mixing assembly (5) includes a mixing chamber (51), which is fixed to the top of the main support plate (2). A main shaft motor (52) is fixedly connected to the top of the mixing chamber (51). The output end of the main shaft motor (52) extends into the interior of the mixing chamber (51) and is fixedly installed with a rotating shaft (53). A paddle (54) is fixedly connected to the outside of the rotating shaft (53). A feed pipe (56) is fixedly connected to the top of the mixing chamber (51). The end of the feed pipe (56) extends to the outside of the tank (1). An electric heating rod (55) is fixedly installed inside the mixing chamber (51).

5. A crystallization tank for the production of veterinary raw materials according to claim 2, characterized in that, The collection component (8) includes a support column (82), which is fixed to the bottom of the tank (1). A fixing plate (81) is fixedly connected to the outside of the support column (82). A secondary shaft motor (84) is fixedly connected to the top of the fixing plate (81). A fixing block (85) is fixedly connected to the top of the fixing plate (81). A spiral blade (86) is fixedly installed at the output end of the secondary shaft motor (84).

6. A crystallization tank for the production of veterinary raw materials according to claim 5, characterized in that, The bottom of the support column (82) is fixedly connected to a base plate (83), and a collection box (87) is provided on the top of the base plate (83). The bottom of the fixing plate (81) is fixedly connected to a guide tube (88), the upper end of the guide tube (88) extends into the interior of the fixing block (85), and the collection box (87) is located below the guide tube (88).

7. A crystallization tank for the production of veterinary raw materials according to claim 4, characterized in that, The top of the secondary support plate (3) is fixedly connected to a connecting pipe (9), the upper end of the connecting pipe (9) extends into the interior of the mixing chamber (51), and the bottom of the connecting pipe (9) extends into the interior of the crystallization chamber (61).

8. A crystallization tank for the production of veterinary raw materials according to claim 5, characterized in that, The crystallization chamber (61) is fixedly connected to the outside of the discharge pipe (10), and the lower end of the discharge pipe (10) extends into the interior of the fixed block (85).