Chromatography sample loading device for muscone production

Abstract

The utility model belongs to the technical field of chromatographic equipment, and particularly relates to a chromatographic sample loading device for muscone production, which comprises a sample loader and a filter, the bottom of the sample loader is connected with the filter, and a sample inlet is arranged at the top of the side wall of the sample loader; a liquid level sensor is arranged on the side wall of the filter, a sample outlet pipe is arranged at the bottom of the filter, an electromagnetic valve is arranged on the sample outlet pipe, and the liquid level sensor and the electromagnetic valve are respectively connected with a controller. According to the scheme, the situation that a sample is emptied and enters air due to improper operation to cause abnormal atlas can be avoided, and the sample loading efficiency is improved; sample volatilization, pollution or foreign matter falling caused by open operation can be avoided; the flushing opening and the umbrella-shaped dispersing device are arranged, so that the barrel wall flushing efficiency is improved; and the liquid level sensor is linked with the electric control valve, so that manual operation is reduced.

Description

TECHNICAL FIELD

[0001] The utility model belongs to chromatography equipment technical field, concretely relates to a chromatography sample loading device for muscone production. BACKGROUND

[0002] In the muscone production process, muscone in the product is often separated through column chromatography, so that the composition and content of muscone are further analyzed. The sample loading mode of column chromatography directly affects the separation effect of the sample. In the existing muscone column chromatography process, there is no special sample loading device, and the operator often connects one end of the sample inlet pipe to the pressure pump and the other end to the sample barrel to deliver the sample to the chromatography column. This sample loading mode has low sample loading efficiency, and when the sample liquid level in the sample barrel drops to be insufficient to completely cover the sample inlet pipe, air is easily sucked into the sample inlet pipe, thereby causing abnormal chromatogram during sample analysis. At the same time, this sample loading mode is open to operation, which easily causes sample volatilization, pollution or foreign matter falling. SUMMARY

[0003] The utility model aims at providing a chromatography sample loading device for muscone production, which has high sample loading efficiency and can avoid air entering and causing abnormal chromatogram and sample pollution.

[0004] In order to achieve the above-mentioned purpose, the utility model is realized through the following technical scheme:

[0005] The embodiment of the utility model provides a chromatography sample loading device for muscone production, which comprises a sample loader and a filter, the bottom of the sample loader is connected with the filter, and the top of the sidewall of the sample loader is provided with a sample inlet; a liquid level sensor is arranged on the sidewall of the filter, the bottom of the filter is provided with a sample outlet pipe, an electromagnetic valve is arranged on the sample outlet pipe, and the liquid level sensor and the electromagnetic valve are respectively connected with a controller.

[0006] As a further technical scheme, the sample loader has a cylindrical structure, the top of the sample loader is provided with a flushing inlet, and a flushing inlet cover is arranged on the flushing inlet.

[0007] As a further technical scheme, the bottom of the flushing inlet is provided with a distributor.

[0008] As a further technical scheme, the distributor has an umbrella structure, a triangular structure and a circular structure.

[0009] As a further technical scheme, a sample inlet cover is arranged on the sample inlet.

[0010] As a further technical scheme, the filter has a conical structure, and a filter screen is arranged on the top of the filter.

[0011] As a further technical solution, the bracket is arranged on the side wall of the sample loader.

[0012] As a further technical solution, the sample loader is made of glass or stainless steel, and the filter is made of glass or stainless steel.

[0013] As a further technical solution, the side wall of the sample loader or the filter is provided with a scale line.

[0014] As a further technical solution, the sample inlet is connected with the input pump.

[0015] The beneficial effects of the above embodiments of the present application are as follows:

[0016] (1) The sample loading device of the present application can avoid the sample from being emptied due to improper operation, and the abnormal situation of entering air appearing in the spectrum, thereby improving the sample loading efficiency.

[0017] (2) The sample loading device of the present application is all sealed operation, which can avoid the sample from being volatilized, contaminated or foreign matter falling due to open operation.

[0018] (3) The shower inlet and umbrella-shaped dispersion device in the present application improve the barrel wall washing efficiency.

[0019] (4) The liquid level sensor and the electric control valve are linked in the present application, thereby reducing manual operation. BRIEF DESCRIPTION OF DRAWINGS

[0020] The drawings accompanying the specification of the present application form a part thereof and serve to provide further understanding of the present application, and the illustrative embodiments of the present application and their description serve to explain the present application without constituting improper limitations on the present application.

[0021] Figure 1 is a schematic diagram of the overall structure of a chromatography sample loading device for muscone production in the present application;

[0022] The schematic diagram is only used for illustration;

[0023] Among them: sample loader 1, filter 2, shower inlet cover 3, shower inlet 4, distributor 5, sample inlet 6, sample inlet cover 7, filter screen 8, liquid level sensor 9, sample outlet pipe 10, electromagnetic valve 11, bracket 12, controller 13. DETAILED DESCRIPTION

[0024] It should be noted that the following detailed description is exemplary and is intended to provide further explanation of the present application. Unless otherwise specified, all technical and scientific terms used in the present application have the same meaning as generally understood by those skilled in the art to which the present application belongs.

[0025] Example 1

[0026] In a typical embodiment of this utility model, such as Figure 1 As shown, a chromatographic sample loading device for the production of muscone is provided, including a sample container 1, a filter 2, and a support 12. The bottom of the sample container 1 is connected to the filter 2, and the support 12 is disposed on the side wall of the sample container 1. The support 12 is used to increase the overall structural stability of the sample loading device. The chromatographic sample loading device is directly connected to the chromatographic column and is used to add samples to the chromatographic column.

[0027] The sample container 1 has a cylindrical structure and is located on top of the filter 2. It is used for adding samples. A rinsing port 4 is located at the top of the sample container 1, and a rinsing port cover 3 is provided on the rinsing port 4. The rinsing port 4 is used to add rinsing liquid into the sample container 1. A distributor 5 with an umbrella-shaped structure is located at the bottom of the rinsing port 4. The umbrella head of the distributor 5 is connected to the bottom of the rinsing port 4, and it is used for uniform distribution of liquid, thereby achieving thorough rinsing of the sample remaining on the side wall of the sample container 1. An inlet 6 is located at the top of the side wall of the sample container 1, and an inlet cover 7 is provided on the inlet 6. The inlet 6 is connected to a delivery pump. The inlet 6 uses an input pump to add the sample from the sample container into the sample container 1. One end of the input pump is connected to the inlet 6, and the other end is connected to the sample container.

[0028] The filter 2 has a conical structure, and a filter screen 8 is provided at the top of the filter 2. The filter screen 8 is used to filter solid impurities in the sample or rinsing liquid. A liquid level sensor 9 is provided on the side wall of the filter 2. The liquid level sensor 9 is used to measure the liquid level in the filter 2. A sample outlet tube 10 is provided at the bottom of the filter 2. The sample outlet tube 10 is connected to the chromatography column via a delivery pump. A solenoid valve 11 is provided on the sample outlet tube 10. The liquid level sensor 9 and the solenoid valve 11 are respectively connected to the controller 13, thereby realizing the timely closure of the sample outlet tube 10 to prevent air from entering the chromatography column. The controller 13 can be a commercially available product.

[0029] In some other embodiments, the sample container 1 or filter 2 is made of glass or stainless steel. The side wall of the sample container 1 or filter 2 is provided with graduation lines to facilitate observation of the liquid level in the sample loading device.

[0030] The sample loading process of the chromatographic sample loading device for muscone production in this utility model is as follows:

[0031] (1) Close the shower cover 3 on the shower inlet 4, and add the sample into the sample loader 1 through the sample inlet 6 by the delivery pump, and close the sample inlet cover 7. The sample passes through the filter screen 7 in the filter 2 to remove the solid impurities in the sample, and when the liquid level sensor 8 in the filter 2 detects that the liquid surface is higher than the specified height, the controller 13 is linked to open the electromagnetic valve 11, and the sample enters the chromatographic column through the sample outlet pipe 10.

[0032] (2) When the liquid level sensor 8 in the filter 2 detects that the liquid surface is lowered to the specified height, the controller 13 is linked to close the electromagnetic valve 11, and the liquid remains in the cavity of the filter 2 to avoid the air entering the sample outlet pipe 10.

[0033] (3) Open the shower cover 3 on the shower inlet 4 again, add the residual sample in the sample barrel into the shower liquid, and add the sample into the sample loader 1 through the shower inlet 4, and the shower liquid is uniformly distributed through the distributor 5 to sufficiently wash the residual sample on the side wall of the sample loader 1. At the same time, according to the detection of the liquid level sensor 8 in the filter 2, the controller 13 is linked to control the electromagnetic valve 11 to control the sample into the chromatographic column.

[0034] The above only describes the preferred embodiments of the present application and is not used to limit the present application. For those skilled in the art, the present application can be variously changed and modified. Any modification, equivalent replacement, improvement, etc. within the spirit and principle of the present application shall be included in the protection scope of the present application.

Claims

1. A chromatography sample loading device for muscone production, characterized by, The device comprises a sample loader and a filter, the bottom of the sample loader is connected with the filter, the top of the side wall of the sample loader is provided with a sample inlet, the side wall of the filter is provided with a liquid level sensor, the bottom of the filter is provided with a sample outlet pipe, the sample outlet pipe is provided with an electromagnetic valve, and the liquid level sensor and the electromagnetic valve are connected with a controller respectively.

2. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, The sample loader has a cylindrical structure, the top of the sample loader is provided with a flushing inlet, and the flushing inlet is provided with a flushing inlet cover.

3. The chromatographic sample loading device for musk ketone production according to claim 2, characterized by, The bottom of the flushing inlet is provided with a distributor.

4. The chromatographic sample application device for musk ketone production according to claim 3, characterized by The distributor has an umbrella structure, a triangular structure or a circular structure.

5. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, The sample inlet is provided with a sample inlet cover.

6. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, The filter has a conical structure, and the top of the filter is provided with a filter screen.

7. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, A support is further included, and the support is arranged on the side wall of the sample loader.

8. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, The material of the sample loader is glass or stainless steel, and the material of the filter is glass or stainless steel.

9. The chromatographic sample loading device for musk ketone production according to claim 1, characterized by, The side wall of the sample loader or the filter is provided with a scale line.

10. The chromatographic sample loading device for musk ketone production according to claim 5, characterized by, The sample inlet is connected with an input pump.

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