Graphdiyne material preparation device
By introducing a motor-driven stirring rod and scraper structure into the reactor, the problems of insufficient mixing and adhesion to the inner wall of graphylene materials are solved, achieving uniform mixing and convenient cleaning, thus improving the performance of the reactor.
Patent Information
- Application Number
- CN202422565170.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-23
- Publication Date
- 2025-12-19
- Estimated Expiration
- 2034-10-23
AI Technical Summary
In existing technologies, the graphylene material is not sufficiently stirred in the reactor, causing the material to stick to the inner wall, affecting subsequent use and making cleaning difficult.
The system uses a motor-driven rotating shaft to drive the stirring rod and scraper structure, achieving uniform stirring of the graphylene material and scraping of the inner wall. Combined with a temperature monitoring and control system, it ensures uniform mixing and cleanliness within the reactor.
This method achieves thorough mixing and cleaning of the graphylene material's inner wall, preventing material adhesion and improving the efficiency and ease of cleaning of the reactor.
Smart Images
Figure CN223683524U_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The utility model relates to the technical field of graphite diyne preparation, and specifically relates to a graphite diyne material preparation device. BACKGROUND
[0002] Graphite diyne is a new carbon material, which has higher electrical conductivity and thermal conductivity. When preparing graphite diyne, a reaction kettle is needed to uniformly mix and react raw materials. However, when the reaction kettle is used, the materials will adhere to the inner wall of the reaction kettle and cannot be fully stirred and reacted. In addition, if the raw materials adhere to the inner wall of the reaction kettle, it is not convenient to clean, which will also affect the next use of the reaction kettle.
[0003] Therefore, the technical personnel in the art provide a graphite diyne material preparation device to solve the problems in the background art. CONTENT OF THE UTILITY MODEL
[0004] The technical problem to be solved by the utility model is that in the prior art, when the reaction kettle is used, the materials will adhere to the inner wall of the reaction kettle and cannot be fully stirred and reacted. In addition, if the raw materials adhere to the inner wall of the reaction kettle, it is not convenient to clean, which will also affect the next use of the reaction kettle. Therefore, the utility model provides a graphite diyne material preparation device.
[0005] To achieve the above-mentioned purpose, the utility model provides the following technical scheme:
[0006] A graphite diyne material preparation device, comprising a reaction kettle, the upper surface of the reaction kettle is fixedly connected with a motor in the middle, the output end of the motor is fixedly connected with a rotating shaft, the outer wall of the rotating shaft is fixedly connected with a stirring rod on both sides, the lower surface of the stirring rod is fixedly connected with a fixed frame on one side, the inside of the fixed frame is fixedly connected with a connecting rod, the outer wall of the connecting rod is rotatably connected with a connecting ring on the upper and lower parts, the outer wall of the connecting ring is fixedly connected with a rotating plate on both sides, the inside of the shell of the reaction kettle is provided with a heating element, the outer wall of the rotating shaft is provided with a scraping device on the other side, and the upper surface of the reaction kettle is provided with a monitoring device.
[0007] As a further embodiment of the utility model: the scraping device comprises a fixed frame, the two ends of the fixed frame are fixedly connected to the outer wall of the rotating shaft on the other side, the outer wall of the fixed frame is fixedly connected with a scraper on one side, and the scraper is in close contact with the inner wall of the reaction kettle on one side.
[0008] As a further embodiment of the utility model: the monitoring device comprises a temperature sensor, a temperature monitor and a controller, one end of the temperature sensor is fixedly connected to the inside of the reaction kettle on one side of the upper surface, one end of the temperature monitor is fixedly connected to the upper surface of the reaction kettle on one side, and one side of the controller is fixedly connected to the outer wall of the reaction kettle on one side.
[0009] As a further place of the utility model: temperature sensor and temperature monitor are electrically connected, temperature monitor and controller are electrically connected.
[0010] As a further place of the utility model: the outer wall upper portion of the rotating shaft is fixedly connected with a flow guide disc, the upper surface of the flow guide disc is arc-shaped, and a plurality of flow guide holes are formed in the upper surface of the flow guide disc.
[0011] As a further place of the utility model: the upper surface of the reaction kettle is provided with a hose, the upper surface of the reaction kettle is provided with a hose, the outer wall of the reaction kettle is fixedly connected with a feeding port, and the upper surface of the feeding port is provided with a sealing cover.
[0012] Beneficial effects
[0013] The utility model discloses the beneficial effect is:
[0014] The utility model discloses a motor, rotating shaft, stirring rod, connecting rod, connecting ring and the setting of rotary plate can be mixed evenly with the carbon source and catalyst, when rotating shaft rotates, can drive fixed frame to rotate simultaneously, can make the material that scraping blade is adhered to the inner wall of reaction kettle to scrape off, thereby avoid the problem that material can be adhered to the inner wall of reaction kettle and cannot be fully stirred and reacted, and the inner wall of reaction kettle has raw material adhered and is inconvenient to clean, also can lead to the problem of influence reaction kettle's next use. BRIEF DESCRIPTION OF DRAWINGS
[0015] Figure 1 It is a kind of stereogram of graphite alkyne material preparation device:
[0016] Figure 2 It is a kind of sectional view of graphite alkyne material preparation device:
[0017] Figure 3 It is a kind of stirring structure schematic diagram in graphite alkyne material preparation device:
[0018] Figure 4 It is a kind of graphite alkyne material preparation device structure schematic diagram.
[0019] In the drawing: 1, reaction kettle;2, motor: 3, rotating shaft;4, stirring rod;5, fixed frame: 6, connecting rod: 7, connecting ring;8, rotary plate;9, fixed frame;10, scraping blade;11, flow guide disc;12, temperature monitor;13, temperature sensor;14, controller;15, hose one: 16, hose two;17, feeding port;18, sealing cover;19, heating element. DETAILED DESCRIPTION
[0020] The technical solutions in the embodiments of the present application will be clearly and completely described with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments of the present application, all other embodiments obtained by those skilled in the art without creative efforts fall within the scope of the present application.
[0021] Please refer to Figures 1-4 The graphite material preparation device comprises a reaction kettle 1, a motor 2 fixedly connected to the middle part of the upper surface of the reaction kettle 1, an output end of the motor 2 fixedly connected with a rotating shaft 3, both sides of the outer wall of the rotating shaft 3 fixedly connected with stirring rods 4, one side of the lower surface of the stirring rods 4 fixedly connected with fixed frames 5, the inside of the fixed frames 5 fixedly connected with connecting rods 6, the upper and lower parts of the outer wall of the connecting rods 6 rotatably connected with connecting rings 7, both sides of the outer wall of the connecting rings 7 fixedly connected with rotating plates 8, a heating element 19 arranged in the inside of the shell of the reaction kettle 1, the other side of the outer wall of the rotating shaft 3 provided with a scraping device, and the upper surface of the reaction kettle 1 provided with a monitoring device.
[0022] Through the above technical solution, the motor 2 drives the rotating shaft 3 to rotate, which in turn drives the stirring rods 4 to rotate, and at the same time, the stirring rods 4 drive the fixed frames 5 and the rotating plates 8 to rotate on the connecting rods 6 through the connecting rings 7, so that the carbon source and the catalyst can be stirred and mixed; when the rotating shaft 3 rotates, the fixed frame 9 rotates simultaneously, so that the scraper 10 can scrape the materials adhered to the inner wall of the reaction kettle 1, thereby avoiding the problem that the materials adhere to the inner wall of the reaction kettle 1 and cannot be fully stirred and reacted, and the problem that the inner wall of the reaction kettle 1 is adhered with raw materials and is not convenient to clean, which also affects the next use of the reaction kettle 1.
[0023] Specifically, the scraping device comprises a fixed frame 9, both ends of the fixed frame 9 fixedly connected to the other side of the outer wall of the rotating shaft 3, and one side of the outer wall of the fixed frame 9 fixedly connected with a scraper 10, and one side of the scraper 10 abuts against the inner wall of the reaction kettle 1.
[0024] Through the above technical solution, when the motor 2 drives the rotating shaft 3 to rotate, the rotating shaft 3 rotates with the fixed frame 9, so that the scraper 10 can scrape the materials adhered to the inner wall of the reaction kettle 1.
[0025] Specifically, the monitoring device comprises a temperature monitor 12, a temperature sensor 13 and a controller 14, one end of the temperature monitor 12 fixedly connected to one side of the upper surface in the inside of the reaction kettle 1, one end of the temperature sensor 13 fixedly connected to one side of the upper surface of the reaction kettle 1, and one side of the controller 14 fixedly connected to one side of the outer wall of the reaction kettle 1.
[0026] Through the technical scheme, the temperature in the reaction kettle 1 can be monitored in real time through the temperature monitor 12, the temperature can be observed in real time through the temperature sensor 13, and the temperature can be controlled through the controller 14.
[0027] Specifically, the temperature monitor 12 is electrically connected with the temperature sensor 13, and the temperature sensor 13 is electrically connected with the controller 14.
[0028] Through the technical scheme, the temperature in the reaction kettle 1 can be monitored in real time through the temperature monitor 12, the temperature can be observed in real time through the temperature sensor 13, and the temperature can be controlled through the controller 14.
[0029] Specifically, the outer wall of the rotating shaft 3 is fixedly connected with the flow guide disc 11, the upper surface of the flow guide disc 11 is arc-shaped, and a plurality of flow guide holes are formed in the upper surface of the flow guide disc 11.
[0030] Through the technical scheme, when the motor 2 drives the rotating shaft 3 to rotate, the rotating shaft 3 rotates with the flow guide disc 11, so that the carbon source and the catalyst can be dispersed and enter the reaction kettle 1 from the flow guide holes, thereby ensuring that the carbon source and the metal catalyst are uniformly distributed in the reaction kettle 1.
[0031] Specifically, the upper surface of the reaction kettle 1 is provided with a first hose 15, the upper surface of the reaction kettle 1 is provided with a second hose 16, the outer wall of the reaction kettle 1 is fixedly connected with a feeding port 17, and the upper surface of the feeding port 17 is provided with a sealing cover 18.
[0032] Through the technical scheme, the carbon source and the metal catalyst with high purity and specific structure are poured into the reaction kettle 1 from the feeding port 17.
[0033] Finally, it should be noted that: the above only for the preferred embodiments of the present application, and not for limiting the present application, although the present application has been described in detail with reference to the foregoing embodiments, for those skilled in the art, it still can be modified to the technical scheme recorded in the foregoing embodiments, or equivalent replacement of part of the technical features. Any modification, equivalent replacement, improvement, etc. made within the spirit and principles of the present application shall be included in the protection scope of the present application.
Claims
1. A device for preparing graphyne material, comprising a reaction kettle (1), characterized in that The upper surface middle part of the reaction kettle (1) is fixedly connected with a motor (2), the output end of the motor (2) is fixedly connected with a rotating shaft (3), the outer wall of the rotating shaft (3) is fixedly connected with a stirring rod (4) on both sides, the lower surface of the stirring rod (4) is fixedly connected with a fixed frame (5) on one side, the inside of the fixed frame (5) is fixedly connected with a connecting rod (6), the outer wall of the connecting rod (6) is rotatably connected with a connecting ring (7) on the upper and lower parts, the outer wall of the connecting ring (7) is fixedly connected with a rotating plate (8) on both sides, the inside of the shell of the reaction kettle (1) is provided with a heating element (19), the outer wall of the rotating shaft (3) is provided with a scraping device on the other side, and the upper surface of the reaction kettle (1) is provided with a monitoring device.
2. The preparation device of graphyne material according to claim 1, characterized in that The scraping device comprises a fixed frame (9), the both ends of the fixed frame (9) are fixedly connected on the outer wall of the rotating shaft (3) on the other side, and the outer wall of the fixed frame (9) is fixedly connected with a scraper (10) on one side.
3. The preparation device of graphyne material according to claim 1, characterized in that The monitoring device comprises a temperature monitor (12), a temperature sensor (13) and a controller (14), one end of the temperature monitor (12) is fixedly connected on the inside upper surface of the reaction kettle (1) on one side, one end of the temperature sensor (13) is fixedly connected on the upper surface of the reaction kettle (1) on one side, and one side of the controller (14) is fixedly connected on the outer wall of the reaction kettle (1) on one side.
4. The device for preparing graphyne material according to claim 3, characterized in that The temperature monitor (12) and the temperature sensor (13) are electrically connected, and the temperature sensor (13) and the controller (14) are electrically connected.
5. The preparation device of graphyne material according to claim 1, characterized in that The outer wall of the rotating shaft (3) is fixedly connected with a flow guide disc (11) on the upper part, the upper surface of the flow guide disc (11) is arc-shaped, and a plurality of flow guide holes are formed in the upper surface of the flow guide disc (11).
6. The preparation device of graphyne material according to claim 1, characterized in that One side of the upper surface of the reaction kettle (1) is provided with a hose (15), the other side of the upper surface of the reaction kettle (1) is provided with a hose (16), one side of the outer wall of the reaction kettle (1) is fixedly connected with a feeding port (17), and the upper surface of the feeding port (17) is provided with a sealing cover (18).