Multi-stage tubular reaction device for pesticide production

Abstract

The utility model provides a multistage tubular reaction device for pesticide production, which comprises a reaction box, a plurality of groups of reaction components for reaction materials are arranged on the inner side of the reaction box, a mixing component for mixing materials is arranged at one end of each reaction component, and a reaction mechanism for mixing reaction is arranged at one end of each reaction component away from the mixing component. A temperature control assembly is arranged on the outer side of the reaction assembly. The reaction tube is provided with a plurality of groups of spoilers, when materials flow and react in the reaction tube, smooth flowing of the materials in the reaction tube is maintained while the materials move and cut the spoiler materials in the reaction tube according to requirements, meanwhile, the second motor drives the spoilers to rotate, the rotating spoilers can cut the spoiler materials in the process of cutting the spoiler materials, and therefore the materials can flow smoothly. The material pushing effect is achieved, the materials are further dredged, the situation that the materials are deposited and blocked in the reaction pipe is prevented, the possibility that the materials are settled and blocked is reduced, then the materials are subjected to a stable flowing reaction in the reaction assembly, and the mixed reaction effect of the materials is kept.

Description

Technical Field

[0001] This utility model relates to the field of pesticide production equipment technology, specifically to a multi-stage tubular reaction device for pesticide production. Background Technology

[0002] In the production of pesticides, it is usually necessary to mix and react multiple compounds. During the pesticide production process, a reaction device is used to react the required compound materials according to the reaction steps. Currently, the reaction devices used in agricultural production usually include batch reactors, tubular reactors, etc.

[0003] In actual pesticide production using the aforementioned tubular reactor, it was found that due to the continuous flow and reaction of materials in the long tube of the reactor, the inner side of the long tube is prone to blockage over time. These blocked materials are unstable and can easily affect the normal flow and reaction of materials. At the same time, there are sudden flow separations during the pesticide production reaction, which affect the ratio of the mixed materials and are not conducive to ensuring the quality of the pesticide production reaction.

[0004] In summary, there is a need for a tubular reaction apparatus that facilitates the stable reaction of compounds. Utility Model Content

[0005] To address the shortcomings of existing technologies, this invention provides a multi-stage tubular reaction device for pesticide production, which solves the problems mentioned in the background art.

[0006] To achieve the above objectives, this utility model provides the following technical solution:

[0007] A multi-stage tubular reaction device for pesticide production includes a reaction chamber, with multiple reaction components for reacting materials arranged inside the reaction chamber, a mixing component for mixing the materials arranged at one end of the reaction components, a mixing reaction mechanism arranged at the end of the reaction components away from the mixing component, and a temperature control component arranged outside the reaction components.

[0008] The reaction assembly includes a reaction tube, a first reflux tube, and a second reflux tube. The first reflux tube is distributed in opposite directions, and its two ends are connected to the ends of the first reflux tube and the second reflux tube, respectively. The reaction mechanism includes a crossbar and baffles. The crossbar is arranged correspondingly to the reaction tube, and baffles are provided on the outside of the crossbar. Multiple sets of baffles are provided at equal intervals on the inside of the reaction tube.

[0009] Furthermore, the reaction mechanism also includes an electric push rod, a mounting plate, and a second motor. The electric push rod is located on the side of the return pipe, and the end of the electric push rod is provided with a mounting plate. The second motor is located in the middle of the side of the mounting plate away from the electric push rod. The output end of the second motor is connected to the crossbar. The edge of the baffle plate is in close contact with the inside of the reaction pipe, and the baffle plate is engaged and slides with the reaction pipe.

[0010] Furthermore, the temperature control component includes a temperature control sleeve and a liquid guide tube. The temperature control sleeve is correspondingly arranged with the reaction tube and is located outside the reaction tube. The end of the liquid guide tube is connected to the temperature control sleeve, and the end of the liquid guide tube away from the temperature control sleeve extends to the outside of the reaction chamber.

[0011] Furthermore, the top of the reaction chamber is provided with a feed pipe, the bottom end of which is connected to the first reflux pipe. Multiple feeding pipes are provided on the side of the reaction chamber, and the feeding pipes are set in correspondence with the first reflux pipe. A discharge pipe is provided on the bottom side of the second reflux pipe, and a discharge valve is provided in the middle of the discharge pipe. The discharge pipe is connected to the interior of the second reflux pipe below.

[0012] Furthermore, the mixing assembly includes a motor, a drive rod, a support plate, and mixing rods. The motor is located at both ends of the return pipe, the output end of the motor is provided with a drive rod, the outside of the drive rod is provided with a support plate, and the middle of the support plate is provided with multiple sets of mixing rods.

[0013] Furthermore, a flow divider is provided on the inner side of the return pipe, and the flow divider is distributed in a ring.

[0014] This invention provides a multi-stage tubular reaction device for pesticide production. Compared with the prior art, it has the following advantages:

[0015] Multiple baffles are installed in the reaction tube. When the material flows and reacts in the reaction tube, they move within the tube as needed, cutting and disrupting the material flow while maintaining smooth material flow. Simultaneously, motor 2 drives the baffles to rotate. The rotating baffles can push the material during the cutting and disrupting process, further clearing the material and preventing material from settling and clogging in the reaction tube. This reduces the possibility of material settling and clogging, thus facilitating stable flow and reaction of the material in the reaction assembly and maintaining the mixing effect of the material. Attached Figure Description

[0016] To more clearly illustrate the technical solutions in the embodiments of this utility model or the prior art, the drawings used in the description of the embodiments or the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of this utility model. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort.

[0017] Figure 1 This invention provides a schematic diagram of the structure of a multi-stage tubular reaction device for pesticide production.

[0018] Figure 2 A schematic diagram showing the distribution of the reaction components of this invention is provided.

[0019] Figure 3 A schematic diagram of the reaction mechanism of this utility model is shown;

[0020] Figure 4 A schematic diagram of the mixing assembly of this utility model is shown;

[0021] The diagram shows: 1. Reaction chamber; 11. Feed pipe; 12. Feeding pipe; 2. Reaction assembly; 21. Reaction tube; 22. Reflux pipe one; 23. Reflux pipe two; 24. Feeding pipe; 25. Feeding valve; 3. Mixing assembly; 31. Motor one; 32. Drive rod; 33. Support plate; 34. Mixing rod; 35. Diverting rod; 4. Reaction mechanism; 41. Crossbar; 42. Baffle plate; 43. Electric actuator; 44. Mounting plate; 45. Motor two; 5. Temperature control assembly; 51. Temperature control sleeve; 52. Liquid guide pipe. Detailed Implementation

[0022] To make the objectives, technical solutions, and advantages of the embodiments of this utility model clearer, the technical solutions in the embodiments of this utility model are described clearly and completely. Obviously, the described embodiments are only some embodiments of this utility model, not all embodiments. Based on the embodiments of this utility model, all other embodiments obtained by those skilled in the art without creative effort are within the protection scope of this utility model.

[0023] To address the technical problems in the background section, the following multi-stage tubular reaction apparatus for pesticide production is provided:

[0024] Combination Figures 1-4 As shown, this utility model provides a multi-stage tubular reaction device for pesticide production, including a reaction chamber 1. Multiple reaction components 2 containing reactants are arranged inside the reaction chamber 1. A mixing component 3 for mixing the reactants is located at one end of each reaction component 2. A reaction mechanism 4 for mixing the reactants is located at the end of the reaction component 2 opposite to the mixing component 3. A temperature control component 5 for stabilizing the reaction is located outside the reaction component 2. The reaction component 2 includes a reaction tube 21, a first reflux tube 22, and a second reflux tube 23. The first reflux tube 22 is relatively distributed, and the reflux... The two ends of the first tube 22 are connected to the ends of the first return tube 22 and the second return tube 23, respectively. The arrangement of the reaction tube 21, the first return tube 22 and the second return tube 23 enables the material to flow and mix during the reaction. The reaction mechanism 4 includes a crossbar 41 and a baffle 42. The crossbar 41 is correspondingly arranged with the reaction tube 21. The baffle 42 is provided on the outside of the crossbar 41. Multiple sets of baffles 42 are equally spaced on the inside of the reaction tube 21. The multiple sets of baffles 42 can turbulent and cut the material during the material flow reaction, thereby improving the uniformity of material mixing.

[0025] As an improvement to the above scheme, the reaction mechanism 4 also includes an electric push rod 43, a mounting plate 44, and a second motor 45. The electric push rod 43 is located on the side of the second return pipe 23. The electric push rod 43 can move the crossbar 41 and the baffle 42 repeatedly in the reaction pipe 21. The end of the electric push rod 43 is provided with a mounting plate 44. The second motor 45 is located in the middle of the side of the mounting plate 44 away from the electric push rod 43. The output end of the second motor 45 is connected to the crossbar 41. The edge of the baffle 42 is in close contact with the inner side of the reaction pipe 21. The baffle 42 engages and slides with the reaction pipe 21. The baffle plate 42, which is attached to the reaction tube 21, can move inside the reaction tube 21. While cutting the baffle material, it keeps the material flow in the reaction tube 21 smoothly and prevents the material from settling and blocking in the reaction tube 21. At the same time, the motor 45 drives the baffle plate 42 to rotate. At this time, the baffle plate 42 can push the material during the cutting of the baffle material, further reducing the possibility of material settling and blocking. This is conducive to the stable flow reaction of the material in the reaction component 2 and maintains the mixing reaction effect of the material.

[0026] In this embodiment, the temperature control component 5 includes a temperature control sleeve 51 and a liquid guide tube 52. The temperature control sleeve 51 is correspondingly arranged with the reaction tube 21 and is located outside the reaction tube 21. The end of the liquid guide tube 52 is connected to the temperature control sleeve 51, and the end of the liquid guide tube 52 away from the temperature control sleeve 51 extends to the outside of the reaction chamber 1. The liquid guide tube 52 can send media of different temperatures into the temperature control sleeve 51 to adjust the reaction environment in the reaction tubes 21 at different levels, which is beneficial to adapting to the reaction conditions of different steps of pesticides.

[0027] In this embodiment, a feed pipe 11 is provided at the top of the reaction chamber 1, and the bottom end of the feed pipe 11 is connected to the first return pipe 22. Multiple feeding pipes 12 are provided on the side of the reaction chamber 1, and the feeding pipes 12 are correspondingly arranged with the first return pipe 22. The feeding pipes 12 are used to deliver the additives required for different steps of the pesticide reaction into the reaction components 2 at different levels. A discharge pipe 24 is provided at the bottom of the second return pipe 23, and a discharge valve 25 for controlling the flow of materials is provided in the middle of the discharge pipe 24. The discharge pipe 24 is connected to the interior of the second return pipe 23 below.

[0028] To ensure that the added materials can be mixed and reacted quickly and promptly within the reaction apparatus, this embodiment presents the following design:

[0029] The mixing assembly 3 includes a motor 31, a drive rod 32, a support plate 33, and mixing rods 34. The motor 31 is located at the end of the return pipe 23. The output end of the motor 31 is equipped with a drive rod 32. The support plate 33 is located on the outside of the drive rod 32. Multiple sets of mixing rods 34 are located in the middle of the support plate 33. A flow divider 35 is located on the inside of the return pipe 23. The flow divider 35 is arranged in a ring. When the added material enters the return pipe 22 from the addition pipe, the support plate 33 and the mixing rods 34 driven by the motor 31 can work with the multiple flow dividers 35 to quickly divide and disperse the reactants and the added material, so that the reactants and the added material are quickly mixed and then enter the reaction pipe 21 for mixing and flow reaction.

[0030] Working principle and usage process of this utility model:

[0031] When using:

[0032] First, the materials for pesticide production are sequentially fed into the return pipe 22 of the reaction assembly 2 located at the top inside the reaction chamber 1 through the feed pipe 11. Next, the liquid guide pipe 52 in the temperature control assembly 5 introduces external hot and cold media into the temperature control sleeve 51, changing the reaction environment in the reaction tube 21. At this time, the materials flow and react in the return pipe 22. When the flowing materials pass through multiple sets of baffles 42, the baffles 42 can turbulently cut the materials, improving the uniformity of material mixing. After the materials have mixed and reacted, they flow into the next stage of the reaction assembly 2 through the discharge pipe 24 for further reaction. Then, the secondary reaction component 2 is fed into the return pipe 22 through the feeding pipe 12 with the materials required for different steps and mixed with the materials. During this process, the motor 31 in the mixing component 3 drives the drive rod 32 to rotate. The support plate 33 on the outside of the drive rod 32 can drive the mixing rod 34 to rotate. With the help of multiple diversion rods 35, the added materials and the flowing reaction materials are quickly and fully mixed together to ensure that the materials can react stably and fully according to the steps of pesticide production. The products after multiple reactions are discharged from the reaction box 1 and made into pesticides by distillation or recrystallization as needed.

[0033] During the reaction process of pesticide production:

[0034] During operation of the reaction device, monitoring equipment such as pressure sensors and flow sensors can be installed to monitor the pressure and flow changes in the reaction tube 21 in real time. When the reaction effect of materials at different levels is not good, motor 2 45 can drive the crossbar 41 and the baffle 42 to rotate. Then, the electric push rod 43 drives the crossbar 41 and the baffle 42 to move back and forth in the reaction tube 21 to ensure that there is no material deposition or blockage in the reaction tube 21 that affects the flow and mixing reaction of materials. This allows the materials to flow stably in the reaction tube 21, the first return tube 22 and the second return tube 23. The materials can continuously mix and react during the flow, achieving the purpose of stable mixing reaction of materials in the reaction component 2, thereby ensuring that the materials reach the expected mixing reaction state.

[0035] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such a process, method, article, or apparatus. Without further limitations, an element defined by the phrase "comprising one..." does not exclude the presence of other identical elements in the process, method, article, or apparatus that includes said element.

[0036] The above embodiments are only used to illustrate the technical solutions of this utility model, and are not intended to limit it. Although this utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that modifications can still be made to the technical solutions described in the foregoing embodiments, or equivalent substitutions can be made to some of the technical features. Such modifications or substitutions do not cause the essence of the corresponding technical solutions to deviate from the spirit and scope of the technical solutions of the embodiments of this utility model.

Claims

1. A multi-stage tubular reaction apparatus for pesticide production, characterized in that: The reaction chamber (1) includes a reaction assembly (2) with multiple sets of reactants inside the reaction chamber (1), a mixing assembly (3) for mixing the reactants at one end of the reaction assembly (2), a mixing reaction mechanism (4) for mixing the reactants at the end of the reaction assembly (2) away from the mixing assembly (3), and a temperature control assembly (5) on the outside of the reaction assembly (2). The reaction assembly (2) includes a reaction tube (21), a first reflux tube (22) and a second reflux tube (23). The first reflux tube (22) is distributed in opposite directions. The two ends of the first reflux tube (22) are connected to the ends of the first reflux tube (22) and the ends of the second reflux tube (23) respectively. The reaction mechanism (4) includes a crossbar (41) and a baffle (42). The crossbar (41) is correspondingly arranged with the reaction tube (21). The baffle (42) is provided on the outside of the crossbar (41). Multiple sets of baffles (42) are provided at equal intervals on the inside of the reaction tube (21).

2. The multi-stage tubular reaction device for pesticide production according to claim 1, characterized in that: The reaction mechanism (4) also includes an electric push rod (43), a mounting plate (44), and a second motor (45). The electric push rod (43) is located on the side of the second return pipe (23). The end of the electric push rod (43) is provided with a mounting plate (44). The second motor (45) is located in the middle of the side of the mounting plate (44) away from the electric push rod (43). The output end of the second motor (45) is connected to the crossbar (41). The edge of the baffle plate (42) is in contact with the inner side of the reaction tube (21). The baffle plate (42) and the reaction tube (21) are engaged and slide together.

3. A multi-stage tubular reaction device for pesticide production according to claim 1, characterized in that: The temperature control component (5) includes a temperature control sleeve (51) and a liquid guide tube (52). The temperature control sleeve (51) is correspondingly arranged with the reaction tube (21). The temperature control sleeve (51) is located outside the reaction tube (21). The end of the liquid guide tube (52) is connected to the temperature control sleeve (51). The end of the liquid guide tube (52) away from the temperature control sleeve (51) extends to the outside of the reaction chamber (1).

4. A multi-stage tubular reaction device for pesticide production according to claim 1, characterized in that: The top of the reaction chamber (1) is provided with a feed pipe (11), the bottom end of which is connected to the first reflux pipe (22). The side of the reaction chamber (1) is provided with multiple feeding pipes (12), which are correspondingly set with the first reflux pipe (22). The bottom of the second reflux pipe (23) is provided with a discharge pipe (24), and the middle of the discharge pipe (24) is provided with a discharge valve (25). The discharge pipe (24) is connected to the interior of the second reflux pipe (23) below.

5. A multi-stage tubular reaction device for pesticide production according to claim 1, characterized in that: The mixing assembly (3) includes a motor (31), a drive rod (32), a support plate (33), and mixing rods (34). The motor (31) is located at the end of the return pipe (23). The output end of the motor (31) is provided with a drive rod (32). The outside of the drive rod (32) is provided with a support plate (33). The middle part of the support plate (33) is provided with multiple sets of mixing rods (34).

6. A multi-stage tubular reaction apparatus for pesticide production according to claim 5, characterized in that: The inner side of the return pipe (23) is provided with a diverter rod (35), which is distributed in a ring.

Images