Pressure-adjustable reaction device for producing plant growth regulator paclobutrazol

By introducing a pressure regulating and stirring mechanism into the reactor, the problem of insufficient pressure regulation in paclobutrazol production was solved, enabling precise regulation of the pressure inside the reactor and purification and discharge of gas, thereby improving production safety and efficiency.

CN223931394UActive Publication Date: 2026-02-24XINJI CHENDIAL CHONGGUANG CHEMICAL TECHNOLOGY CO LTD
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Patent Information

Application Number
CN202520300519.5
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-02-25
Publication Date
2026-02-24
Estimated Expiration
2035-02-25

AI Technical Summary

Technical Problem

The existing paclobutrazol production reactors lack effective pressure regulation mechanisms, making it impossible to promptly discharge the gases generated during the reaction, resulting in low production efficiency and potential safety hazards.

Method used

A reaction device including a pressure regulating mechanism and a stirring mechanism was designed. The pressure inside the vessel is detected by a pressure detector, the opening and closing of the exhaust pipe is adjusted by a cylinder and piston system, the gas is purified by a purification unit, and the stirring rod and scraper driven by a motor are used for uniform stirring.

Benefits of technology

It achieves precise regulation of the pressure inside the vessel and timely discharge of gas, avoiding safety hazards, improving production efficiency, and ensuring uniform mixing of materials and cleaning of the vessel wall.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of production of a plant growth regulator paclobutrazol, and discloses a pressure-adjustable reaction device for producing the plant growth regulator paclobutrazol, which comprises a reaction kettle. By means of a pressure adjusting mechanism, when a pressure detector body detects that the pressure of the reaction kettle is too large, a signal of the pressure detector body is transmitted to a controller body, the controller body drives the cylinder, the cylinder drives a baffle and a sliding rod, the sliding rod drives a piston to stretch out and draw back, and a first exhaust pipe is opened; the opened first exhaust pipe enables compressed air to enter the purification box through the conveying pipe, the compressed air is exhausted from the second exhaust pipe after being purified by the purification plate, when the purification plate is blocked, the purification box is opened, the purification plate is pulled to be slidably pulled away from the sliding groove, cleaning is conducted, and the problems that gas is generated in the mixing reaction process of materials in the reaction kettle, the pressure on the inner side of the reaction kettle is increased, and the reaction kettle is damaged are solved. And the problem that human bodies are harmed due to the fact that the materials cannot be purified after being discharged is solved.
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Description

Technical Field

[0001] This utility model relates to the field of paclobutrazol production technology, specifically a reaction device for producing paclobutrazol with adjustable pressure. Background Technology

[0002] Reactors are widely used in petroleum, chemical, rubber, pesticide, dye, pharmaceutical, and food industries to perform processes such as vulcanization, nitration, hydrogenation, hydrocarbonation, polymerization, and condensation. As pressure vessels, reactors play a crucial role in these fields.

[0003] Compared with existing technologies: In the production process of paclobutrazol, the reactor is completely sealed. Specifically, the existing paclobutrazol production reactors lack effective pressure regulation mechanisms, cannot timely discharge the gases generated during the reaction, and cannot accurately adjust the pressure inside the reactor according to production needs. This not only affects production efficiency but may also threaten the safe operation of the reactor. Some harmful gases may have toxic effects on the nervous system, causing workers to experience symptoms such as headaches, dizziness, and memory loss.

[0004] Therefore, a reaction apparatus for the production of paclobutrazol, a plant growth regulator, with adjustable pressure is proposed. Utility Model Content

[0005] The purpose of this invention is to provide a reaction device for the production of paclobutrazol, a plant growth regulator with adjustable pressure, which solves the technical problem of harm caused by the inability to adjust the pressure and achieves the purpose of adjusting the pressure.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a reaction device for producing paclobutrazol, a plant growth regulator with adjustable pressure, comprising a reaction vessel, a feed inlet connected to the top surface of the reaction vessel, a controller body provided on the front end face of the reaction vessel, a pressure detector body penetrating through the top surface of the reaction vessel, a pressure regulating mechanism provided on the right end face of the reaction vessel, and a stirring mechanism provided on the inner side of the reaction vessel;

[0007] The pressure regulating mechanism includes a pressure regulating section and a purification section;

[0008] The purification section is located at the bottom of the pressure regulating section;

[0009] The stirring mechanism includes a drive unit and a stirring unit;

[0010] The stirring section is located on the outer side of the drive section.

[0011] Preferably, the pressure regulating part includes a support plate, which is fixedly connected to the reactor. A connecting pipe is provided on the top surface of the support plate. A through hole is opened on the right end face of the connecting pipe. A sealing ring is provided on the inner side of the through hole. The connecting pipe is connected to the reactor. An exhaust pipe is provided on the outer end face of the connecting pipe. The exhaust pipe extends through to the bottom of the support plate.

[0012] Preferably, a piston is provided above the exhaust pipe, the piston is slidably connected to the connecting pipe, a slide rod is provided on the right end face of the piston, the slide rod is fixedly connected to the piston, the slide rod extends through to the right side of the connecting pipe, the slide rod is slidably connected to the through hole, and a baffle is provided on the right end face of the slide rod, the baffle is fixedly connected to the slide rod.

[0013] Preferably, the purification unit includes a cylinder, the output end face of the cylinder is fixedly connected to the right end face of the baffle, a fixed seat is provided on the bottom surface of the cylinder, the fixed seat is fixedly connected to the cylinder, the bottom surface of the fixed seat is fixedly connected to the top surface of the support plate, a conveying pipe is provided below the fixed seat, the top end of the conveying pipe is connected to the bottom end face of exhaust pipe one, a purification box is connected to the bottom end face of the conveying pipe, a sealing door is hinged to the front side of the purification box, and an exhaust pipe two is connected to the right end face of the purification box.

[0014] Preferably, a sliding groove is provided on the left side of the exhaust pipe, the sliding groove is located on the inner side of the purification box, the sliding groove is fixedly connected to the purification box, and a purification plate is provided on the inner side of the sliding groove. The purification plate is slidably connected to the sliding groove. Through the pressure regulating part and the purification part in the pressure regulating mechanism, the pressure regulating and purification effects are achieved.

[0015] Preferably, the drive unit includes an L-shaped plate, which is fixedly connected to the reactor. A motor is provided on the inner side of the L-shaped plate and is fixedly connected to the L-shaped plate. A rotating rod is provided on the output end face of the motor and is fixedly connected to the motor. The rotating rod extends through to the inner side of the reactor and is rotatably connected to the inner wall of the reactor through a bearing seat.

[0016] Preferably, the stirring part includes a stirring rod one, which is fixedly connected to a rotating rod. A stirring rod two is provided below the stirring rod one, which is fixedly connected to the rotating rod. A scraper is provided on the outer end face of the stirring rod two, and the scraper is fixedly connected to the outer end face of the stirring rod one. Through the driving part and the stirring part in the stirring mechanism, the stirring and scraping effect is achieved.

[0017] Compared with the prior art, the beneficial effects of this utility model are: a reaction device for the production of paclobutrazol, a plant growth regulator with adjustable pressure.

[0018] 1) Through the pressure regulating mechanism, using the cylinder in the purification section, when the pressure detector detects that the pressure in the reactor is too high, the pressure detector transmits the signal to the controller. The controller drives the cylinder, which in turn drives the baffle and slide rod. The slide rod then drives the piston to extend and retract, thereby opening exhaust pipe one. After the exhaust pipe one is opened, the compressed gas enters the purification box through the delivery pipe, and after being purified by the purification plate, it is discharged from exhaust pipe two. When the purification plate is blocked, the purification box is opened, and the purification plate is pulled away from the slide groove to clean it. This solves the problem that the gas generated during the mixing and reaction of materials in the reactor causes the pressure inside the reactor to increase, making it impossible to discharge the material immediately, and the problem that the discharged material cannot be purified, which may cause harm to the human body.

[0019] 2) The stirring mechanism uses a motor in the drive unit to drive a rotating rod, which in turn drives stirring rod one, stirring rod two, and a scraper to achieve uniform stirring. At the same time, the scraper scrapes the inner wall, thus avoiding problems such as inconvenient cleaning and uneven stirring. Attached Figure Description

[0020] Figure 1 This is a three-dimensional structural schematic diagram of the present utility model;

[0021] Figure 2 This is a three-dimensional cross-sectional view of the overall structure of this utility model;

[0022] Figure 3 This is a three-dimensional cross-sectional view of the pressure regulating structure of this utility model;

[0023] Figure 4 This is a three-dimensional cross-sectional view of the connecting pipe of the pressure regulating structure of this utility model;

[0024] Figure 5 This is a three-dimensional schematic diagram of the stirring structure of this utility model.

[0025] In the diagram: 1. Reactor; 2. Controller body; 3. Pressure detector body; 4. Pressure regulating mechanism; 41. Pressure regulating section; 42. Purification section; 411. Support plate; 412. Connecting pipe; 413. Exhaust pipe one; 414. Piston; 415. Slide rod; 416. Baffle; 421. Cylinder; 422. Fixing seat; 423. Conveying pipe; 424. Purification box; 425. Exhaust pipe two; 426. Slide groove; 427. Purification plate; 5. Stirring mechanism; 51. Drive section; 52. Stirring section; 511. L-shaped plate; 512. Motor; 513. Rotating rod; 521. Stirring rod one; 522. Stirring rod two; 523. Scraper. Detailed Implementation

[0026] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0027] Example 1:

[0028] Based on the existing problem of harm caused by the inability to regulate pressure, please refer to Figures 1-4 This utility model provides a technical solution: a reaction device for producing paclobutrazol, a plant growth regulator with adjustable pressure, including a reaction vessel 1, a feed inlet connected to the top surface of the reaction vessel 1, a controller body 2 provided on the front surface of the reaction vessel 1, a pressure detector body 3 penetrating through the top surface of the reaction vessel 1, a pressure regulating mechanism 4 provided on the right end surface of the reaction vessel 1, and a stirring mechanism 5 provided on the inner side of the reaction vessel 1.

[0029] The pressure regulating mechanism 4 includes a pressure regulating section 41 and a purification section 42;

[0030] Purification section 42 is located on the bottom surface of pressure regulating section 41;

[0031] The stirring mechanism 5 includes a drive unit 51 and a stirring unit 52;

[0032] The stirring part 52 is located on the outer side of the drive part 51.

[0033] The pressure regulating unit 41 includes a support plate 411, which is fixedly connected to the reactor 1. A connecting pipe 412 is provided on the top surface of the support plate 411. A through hole is opened on the right end face of the connecting pipe 412. A sealing ring is provided on the inner side of the through hole. The connecting pipe 412 is connected to the reactor 1. An exhaust pipe 413 is provided on the outer end face of the connecting pipe 412. The exhaust pipe 413 extends through to the bottom of the support plate 411.

[0034] A piston 414 is installed above the exhaust pipe 413. The piston 414 is slidably connected to the connecting pipe 412. A slide rod 415 is installed on the right end face of the piston 414. The slide rod 415 is fixedly connected to the piston 414. The slide rod 415 extends through to the right side of the connecting pipe 412. The slide rod 415 is slidably connected to the through hole. A baffle 416 is installed on the right end face of the slide rod 415. The baffle 416 is fixedly connected to the slide rod 415.

[0035] The purification unit 42 includes a cylinder 421. The output end face of the cylinder 421 is fixedly connected to the right end face of the baffle 416. A fixed seat 422 is provided on the bottom surface of the cylinder 421. The fixed seat 422 is fixedly connected to the cylinder 421. The bottom surface of the fixed seat 422 is fixedly connected to the top surface of the support plate 411. A conveying pipe 423 is provided below the fixed seat 422. The top end of the conveying pipe 423 is connected to the bottom end face of the first exhaust pipe 413. A purification box 424 is connected to the bottom end face of the conveying pipe 423. A sealing door is hinged to the front side of the purification box 424. An exhaust pipe 425 is connected to the right end face of the purification box 424.

[0036] A sliding groove 426 is provided on the left side of the exhaust pipe 425. The sliding groove 426 is located on the inner side of the purification box 424 and is fixedly connected to the purification box 424. A purification plate 427 is provided on the inner side of the sliding groove 426 and is slidably connected to the sliding groove 426.

[0037] Furthermore, in this embodiment, through the pressure regulating mechanism 4 and the cylinder 421 in the purification unit 42, when the pressure inside the reactor 1 is too high, the pressure detector body 3 will promptly detect this abnormality. After detecting the abnormality, the pressure detector body 3 will immediately transmit this signal to the controller body 2. Upon receiving the signal, the controller body 2 will quickly respond and drive the cylinder 421 in the purification unit 42 to operate. After the cylinder 421 is driven, it will drive the baffle 416 and the slide rod 415 to move. The movement of the slide rod 415 further drives... The piston 414 extends and retracts, causing the exhaust pipe 413 to open, thus releasing the compressed gas in the reactor 1. The released compressed gas enters the purification box 424 through the delivery pipe 423. In the purification box 424, the compressed gas is purified by the purification plate 427. The purified gas is finally discharged from the exhaust pipe 425. When the purification plate 427 becomes blocked due to long-term use, the purification box 424 can be opened, and the purification plate 427 can be pulled out by sliding it in the slide groove 426, which facilitates cleaning and maintenance.

[0038] Furthermore, in this embodiment, through the pressure regulating mechanism 4, the cylinder 421 in the purification unit 42 is used. When the pressure detector body 3 detects that the pressure in the reactor 1 is too high, the pressure detector body 3 transmits the signal to the controller body 2. The controller body 2 drives the cylinder 421, which drives the baffle 416 and the slide rod 415. As a result, the slide rod 415 drives the piston 414 to extend and retract, thereby opening the exhaust pipe 1 413. After the exhaust pipe 1 413 is opened, the compressed gas enters the purification box 424 through the conveying pipe 423. After being purified by the purification plate 427, it is discharged from the exhaust pipe 2 425. When the purification plate 427 is blocked, the purification box 424 is opened, and the purification plate 427 is pulled to slide away from the slide groove 426, thereby cleaning. This solves the problem that the gas generated during the mixing and reaction of materials in the reactor 1 causes the pressure inside the reactor 1 to increase, making it impossible to discharge the material immediately, and the problem that the discharged material cannot be purified, which may cause harm to the human body.

[0039] Example 2:

[0040] Please see Figure 1 , Figure 2 , Figure 5 Furthermore, based on Embodiment 1, the following is obtained: the drive unit 51 includes an L-shaped plate 511, which is fixedly connected to the reactor 1. A motor 512 is provided on the inner side of the L-shaped plate 511, which is fixedly connected to the L-shaped plate 511. A rotating rod 513 is provided on the output end face of the motor 512, which is fixedly connected to the motor 512. The rotating rod 513 extends through to the inner side of the reactor 1 and is rotatably connected to the inner wall of the reactor 1 through a bearing seat.

[0041] The stirring unit 52 includes a stirring rod 521, which is fixedly connected to the rotating rod 513. A stirring rod 522 is provided below the stirring rod 521 and is fixedly connected to the rotating rod 513. A scraper 523 is provided on the outer end face of the stirring rod 522 and is fixedly connected to the outer end face of the stirring rod 521.

[0042] Furthermore, in this embodiment, the stirring mechanism 5 utilizes the motor 512 in the drive unit 51. When it is necessary to stir the material in the reactor, the motor 512 is started. After the motor 512 is started, its rotational power is transmitted to the rotating rod 513. After receiving the power, the rotating rod 513 starts to rotate. The rotating rod 513 further drives the stirring rod 1 521 and the stirring rod 2 522 to perform stirring action. At the same time, the rotating rod 513 also drives the scraper 523 to perform scraping action along the inner wall of the reactor. The design of the scraper 523 ensures that it can closely fit the inner wall of the reactor 1 and effectively scrape off the material attached to the wall.

[0043] Furthermore, in this embodiment, the stirring mechanism 5 utilizes the motor 512 in the drive unit 51 to drive the rotating rod 513, which in turn drives the stirring rod 521, the stirring rod 522, and the scraper 523, thereby achieving uniform stirring while scraping the inner wall with the scraper 523, thus avoiding the problems of inconvenient cleaning and uneven stirring.

[0044] In use, the raw materials are fed into the reactor through the inlet. The stirring mechanism 5, driven by the motor 512 in the drive unit 51, activates the motor 512 when stirring is required. The motor 512 transmits its rotational power to the rotating rod 513, which then rotates. This rotation further drives the stirring rods 521 and 522 to perform stirring. Simultaneously, the rotating rod 513 drives the scraper 523 to scrape along the inner wall of the reactor. The scraper 523 is designed to fit tightly against the inner wall of the reactor 1, effectively removing material adhering to the wall. The pressure regulating mechanism 4, using the cylinder 421 in the purification unit 42, detects excessive pressure inside the reactor 1 when the pressure is too high. The pressure detector 3 then detects this abnormality. Afterwards, this signal will be immediately transmitted to the controller body 2. Upon receiving the signal, the controller body 2 will respond quickly and drive the cylinder 421 in the purification unit 42 to operate. After the cylinder 421 is driven, it will drive the baffle 416 and the slide rod 415 to move. The movement of the slide rod 415 will further drive the piston 414 to extend and retract. The extension and retraction of the piston 414 will cause the exhaust pipe 1 413 to be opened, thereby releasing the compressed gas in the reactor 1. The released compressed gas enters the purification box 424 through the delivery pipe 423. In the purification box 424, the compressed gas is purified by the purification plate 427. The purified gas is finally discharged from the exhaust pipe 2 425. When the purification plate 427 is blocked due to long-term use, the purification box 424 can be opened, and the purification plate 427 can be pulled out by sliding in the slide groove 426, thereby facilitating cleaning and maintenance.

[0045] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to the embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A reaction apparatus for producing paclobutrazol, a plant growth regulator with adjustable pressure, comprising a reaction vessel (1), characterized in that: The top surface of the reactor (1) is connected to the feed inlet, the front end of the reactor (1) is provided with the controller body (2), the top surface of the reactor (1) is provided with the pressure detector body (3), the right end of the reactor (1) is provided with the pressure regulating mechanism (4), and the inner side of the reactor (1) is provided with the stirring mechanism (5). The pressure regulating mechanism (4) includes a pressure regulating section (41) and a purification section (42). The purification section (42) is located on the bottom surface of the pressure regulating section (41); The stirring mechanism (5) includes a drive unit (51) and a stirring unit (52). The stirring part (52) is located on the outer side of the driving part (51); The pressure regulating unit (41) includes a support plate (411), which is fixedly connected to the reactor (1). A connecting pipe (412) is provided on the top surface of the support plate (411). A through hole is opened on the right end face of the connecting pipe (412). A sealing ring is provided on the inner side of the through hole. The connecting pipe (412) is connected to the reactor (1). An exhaust pipe (413) is provided on the outer end face of the connecting pipe (412). The exhaust pipe (413) extends through to the bottom of the support plate (411). A piston (414) is provided above the exhaust pipe (413). The piston (414) is slidably connected to the connecting pipe (412). A slide rod (415) is provided on the right end face of the piston (414). The slide rod (415) is fixedly connected to the piston (414). The slide rod (415) extends through to the right side of the connecting pipe (412). The slide rod (415) is slidably connected to the through hole. A baffle (416) is provided on the right end face of the slide rod (415). The baffle (416) is fixedly connected to the slide rod (415). The purification unit (42) includes a cylinder (421). The output end face of the cylinder (421) is fixedly connected to the right end face of the baffle (416). A fixed seat (422) is provided on the bottom surface of the cylinder (421). The fixed seat (422) is fixedly connected to the cylinder (421). The bottom surface of the fixed seat (422) is fixedly connected to the top surface of the support plate (411). A conveying pipe (423) is provided below the fixed seat (422). The top end of the conveying pipe (423) is connected to the bottom end face of the first exhaust pipe (413). A purification box (424) is connected to the bottom end face of the conveying pipe (423). A sealing door is hinged to the front side of the purification box (424). A second exhaust pipe (425) is connected to the right end face of the purification box (424).

2. The reaction apparatus for producing paclobutrazol, a plant growth regulator with adjustable pressure, according to claim 1, is characterized in that: The exhaust pipe 2 (425) is provided with a sliding groove (426) on the left side. The sliding groove (426) is located on the inner side of the purification box (424). The sliding groove (426) is fixedly connected to the purification box (424). The inner side of the sliding groove (426) is provided with a purification plate (427). The purification plate (427) is slidably connected to the sliding groove (426).

3. The reaction apparatus for producing paclobutrazol, a plant growth regulator with adjustable pressure, according to claim 1, is characterized in that: The drive unit (51) includes an L-shaped plate (511), which is fixedly connected to the reactor (1). A motor (512) is provided on the inner side of the L-shaped plate (511), which is fixedly connected to the L-shaped plate (511). A rotating rod (513) is provided on the output end face of the motor (512), which is fixedly connected to the motor (512). The rotating rod (513) extends through to the inner side of the reactor (1), and the rotating rod (513) is rotatably connected to the inner wall of the reactor (1) through a bearing seat.

4. The reaction apparatus for producing paclobutrazol, a plant growth regulator with adjustable pressure, according to claim 3, is characterized in that: The stirring part (52) includes a stirring rod one (521), which is fixedly connected to a rotating rod (513). A stirring rod two (522) is provided below the stirring rod one (521), which is fixedly connected to the rotating rod (513). A scraper (523) is provided on the outer end face of the stirring rod two (522), which is fixedly connected to the outer end face of the stirring rod one (521).