Pressing mechanism for p-nitrophenol hydrolysis
By designing a pressing mechanism that includes a hydrolysis component, a gas storage component, a feeding component, and a display and control component, the problem of inaccurate temperature and pressure control during the hydrolysis of p-nitrophenol was solved, thereby improving the reaction rate and product yield, while also enhancing operational safety.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-02-08
- Publication Date
- 2026-03-13
AI Technical Summary
Existing equipment cannot precisely control the temperature and pressure parameters during the hydrolysis of p-nitrophenol, resulting in low reaction rates and low product yields. At the same time, operators are exposed to harmful chemicals for extended periods, which affects their health.
A pressing mechanism was designed, comprising a hydrolysis component, a gas storage component, a feeding component, a pressurization component, and a display and control component. By detecting and controlling temperature and pressure through sensors, and combining an inert gas environment and automated feeding, the precise hydrolysis of p-nitrophenol is achieved.
This technology enables precise control of the hydrolysis process of nitrophenol, improves the reaction rate and product yield, and reduces safety risks for operators.
Smart Images
Figure CN223988481U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of hydrolysis pressing technology, and more specifically to a pressing mechanism for the hydrolysis of p-nitrophenol. Background Technology
[0002] p-Nitrophenol is an important chemical raw material, widely used in the production of pharmaceuticals, pesticides, dyes and other products. Hydrolysis is a key step in the production of p-nitrophenol. Temperature and pressure are the key parameters of the hydrolysis reaction. Existing equipment may not be able to accurately control these parameters, affecting product quality. Existing hydrolysis presses have a low reaction rate during the hydrolysis process, resulting in low product yield. At the same time, the hydrolysis process requires real-time manual observation of the hydrolysis situation. The operators' long-term exposure to the hydrolysis environment will undoubtedly have an impact on their health. Utility Model Content
[0003] In order to overcome the above-mentioned defects of the prior art, the present invention provides a pressing mechanism for hydrolyzing p-nitrophenol to solve the problems existing in the background art.
[0004] This utility model provides the following technical solution: a pressing mechanism for the hydrolysis of p-nitrophenol, comprising a workbench assembly, a hydrolysis assembly, a gas storage assembly, a feeding assembly, a pressurizing assembly, and a display and control assembly. The hydrolysis assembly is installed on top of the workbench assembly, the gas storage assembly is disposed on one side of the top of the workbench assembly, the feeding assembly is connected to one side of the outer wall of the hydrolysis assembly, the pressurizing assembly is installed on one side of the top of the workbench assembly, and the display and control assembly is installed on the top of the workbench assembly near the pressurizing assembly. The hydrolysis assembly includes a hydrolysis tank, ... The components include a first protective shell, a stirring motor, a connecting body, a stirring rod, a heater, a discharge port, a first pressurization hole, and a feed port. The hydrolysis tank is fixedly installed at the top center of the workbench assembly. The first protective shell is fixedly installed on the top of the hydrolysis tank, and the stirring motor is nested inside the first protective shell. The output shaft of the stirring motor is fixedly connected to the connecting body via a coupling, and a stirring rod is fixedly connected to one side of the connecting body. The heater is installed at the bottom inside the hydrolysis tank. The discharge port is located on the left side of the hydrolysis tank, and the feed port is located on the right side of the hydrolysis tank. The first pressurization hole is located on one side of the hydrolysis tank.
[0005] Preferably, the gas storage assembly includes an inert gas tank, a gas delivery pipe, a second pressurization port, an air inlet, a second protective shell, a gas delivery motor, a stopper, and a gas delivery port. The inert gas tank is fixedly installed on the top left side of the workbench assembly and is connected to the hydrolysis tank through the gas delivery pipe. The second pressurization port is located on one side of the inert gas tank, and the air inlet is located on the top side of the inert gas tank. The second protective shell is located in the middle of the outer wall of the gas delivery pipe, and the gas delivery motor is nested inside the second protective shell. The output shaft of the gas delivery motor is fixedly connected to the stopper through a coupling, and the gas delivery port is located on the stopper.
[0006] Preferably, the feeding assembly includes a feeding pipe, a feeding port, a sealing cap, a fixed column, a fixed shaft, and a clamp. The bottom of the feeding pipe is connected to the inside of the hydrolysis tank through a feeding hole, and the feeding port is fixedly installed on the top of the feeding pipe. The sealing cap is located on the top of the feeding port. The fixed column is fixedly connected to one side of the feeding port, and the fixed column is movably sleeved inside the clamp through the fixed shaft. One end of the clamp is fixedly connected to one side of the sealing cap.
[0007] Preferably, the pressurization assembly includes a pressurizer, a hydrolysis connecting pipe, a gas connecting pipe, a hydrolysis pressurization motor, and a gas pressurization motor. The pressurizer is fixedly installed on one side of the top of the workbench assembly, and the pressurizer is connected to the hydrolysis tank and the inert gas tank through the hydrolysis connecting pipe and the gas connecting pipe, respectively. The hydrolysis pressurization motor and the gas pressurization motor are symmetrically arranged inside the pressurizer.
[0008] Preferably, the display control component includes a bracket, a CNC controller, a gas pressure sensor, a hydrolysis pressure sensor, and a temperature sensor. The bracket is fixedly installed on the top side of the workbench assembly, and the CNC controller is provided on the top of the bracket. The gas pressure sensor is fixedly installed on the top inside the inert gas tank, and the hydrolysis pressure sensor and temperature sensor are symmetrically arranged on the top side inside the hydrolysis tank.
[0009] The technical effects and advantages of this utility model are as follows:
[0010] 1. This utility model, by incorporating a pressurization component and a display and control component, facilitates the detection and control of the temperature and pressure inside the hydrolysis tank and the inert gas tank, accurately controls temperature and pressure parameters, and improves the reaction rate and product yield.
[0011] 2. By incorporating a hydrolysis component and a gas storage component, this utility model helps reduce the operator's contact with harmful chemicals and improves the operator's safety. Attached Figure Description
[0012] Figure 1 This is a schematic diagram of the overall structure of this utility model.
[0013] Figure 2 This is a schematic diagram of the overall structure and some cross-sectional views of the present invention.
[0014] Figure 3 For the present utility model Figure 2 Schematic diagram of structure A in the middle.
[0015] Figure 4 For the present utility model Figure 2 Schematic diagram of structure B in the middle.
[0016] The attached figures are labeled as follows: 1. Workbench assembly; 2. Hydrolysis assembly; 201. Hydrolysis tank; 202. First protective shell; 203. Stirring motor; 204. Connector; 205. Stirring rod; 206. Heater; 207. Discharge port; 208. First pressurization port; 209. Feed port; 3. Gas storage assembly; 301. Inert gas tank; 302. Gas delivery pipe; 303. Second pressurization port; 304. Air inlet; 305. Second protective shell; 306. Gas delivery motor; 307. Blocker; 308. 4. Feeding assembly; 401. Feeding pipe; 402. Feed inlet; 403. Sealing cover; 404. Fixed column; 405. Fixed shaft; 406. Snap-fit connector; 5. Pressurization assembly; 501. Pressurizer; 502. Hydrolysis connecting pipe; 503. Gas connecting pipe; 504. Hydrolysis pressurization motor; 505. Gas pressurization motor; 6. Display and control assembly; 601. Bracket; 602. CNC controller; 603. Gas pressure sensor; 604. Hydrolysis pressure sensor; 605. Temperature sensor. Detailed Implementation
[0017] The technical solution of this utility model will be clearly and completely described below with reference to the accompanying drawings. In addition, the forms of the various structures described in the following embodiments are merely illustrative. The pressing mechanism for hydrolyzing p-nitrophenol involved in this utility model is not limited to the structures described in the following embodiments. All other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this utility model.
[0018] Reference Figure 1-4 This utility model provides a pressing mechanism for the hydrolysis of p-nitrophenol, including a workbench assembly 1, a hydrolysis assembly 2, a gas storage assembly 3, a feeding assembly 4, a pressurizing assembly 5, and a display and control assembly 6. The hydrolysis assembly 2 is installed on the top of the workbench assembly 1, the gas storage assembly 3 is located on one side of the top of the workbench assembly 1, the feeding assembly 4 is connected to one side of the outer wall of the hydrolysis assembly 2, the pressurizing assembly 5 is installed on one side of the top of the workbench assembly 1, and the display and control assembly 6 is installed on the top of the workbench assembly 1 near the pressurizing assembly 5.
[0019] The hydrolysis assembly 2 includes a hydrolysis tank 201, a first protective shell 202, a stirring motor 203, a connector 204, a stirring rod 205, a heater 206, a discharge port 207, a first pressurization hole 208, and a feed hole 209. The hydrolysis tank 201 is fixedly installed at the top center of the workbench assembly 1. The first protective shell 202 is fixedly installed on the top of the hydrolysis tank 201, and the stirring motor 203 is nested inside the first protective shell 202. The output shaft of the stirring motor 203 is fixedly sleeved by a coupling. A connecting body 204 is connected, and a stirring rod 205 is fixedly connected to one side of the connecting body 204. A heater 206 is installed at the bottom inside the hydrolysis tank 201. A discharge port 207 is opened on the left side of the hydrolysis tank 201, and a feed hole 209 is opened on the right side of the hydrolysis tank 201. A first pressurization hole 208 is opened on one side of the hydrolysis tank 201. This facilitates the starting of the stirring motor 203, which drives the transmission shaft to rotate and drives the stirring rod 205 and the heater 206 to rotate, so that the reactants are evenly mixed together in the pressing cylinder.
[0020] The gas storage assembly 3 includes an inert gas tank 301, a gas delivery pipe 302, a second pressurization port 303, an air inlet 304, a second protective housing 305, a gas delivery motor 306, a stopper 307, and a gas delivery port 308. The inert gas tank 301 is fixedly installed on the top left side of the workbench assembly 1, and is connected to the hydrolysis tank 201 via the gas delivery pipe 302. The second pressurization port 303 is located on one side of the inert gas tank 301, and the air inlet 304 is located on the inert gas delivery port 308. On one side of the top of the body tank 301, the second protective shell 305 is located in the middle of the outer wall of the gas supply pipe 302, and the gas supply motor 306 is nested inside the second protective shell 305. The output shaft of the gas supply motor 306 is fixedly connected to the blocking device 307 through a coupling. The gas supply hole 308 is opened on the blocking device 307, which is conducive to starting the gas supply motor 306, driving the transmission shaft to rotate and driving the gas supply hole 308 to rotate, so that the inert gas in the inert gas tank 301 is sent into the hydrolysis tank 201.
[0021] The feeding assembly 4 includes a feeding pipe 401, a feeding port 402, a sealing cover 403, a fixed column 404, a fixed shaft 405, and a clamping device 406. The bottom of the feeding pipe 401 is connected to the inside of the hydrolysis tank 201 through the feeding hole 209, and the feeding port 402 is fixedly installed on the top of the feeding pipe 401. The sealing cover 403 is located on the top of the feeding port 402. The fixed column 404 is fixedly connected to one side of the feeding port 402, and the fixed column 404 is movably sleeved inside the clamping device 406 through the fixed shaft 405. One end of the clamping device 406 is fixedly connected to one side of the sealing cover 403, which facilitates opening the sealing cover 403 to the left and prevents it from falling off.
[0022] The pressurization assembly 5 includes a pressurizer 501, a hydrolysis connecting pipe 502, a gas connecting pipe 503, a hydrolysis pressurization motor 504, and a gas pressurization motor 505. The pressurizer 501 is fixedly installed on one side of the top of the workbench assembly 1, and the pressurizer 501 is connected to the hydrolysis tank 201 and the inert gas tank 301 through the hydrolysis connecting pipe 502 and the gas connecting pipe 503, respectively. The hydrolysis pressurization motor 504 and the gas pressurization motor 505 are symmetrically arranged inside the pressurizer 501, which is beneficial to promote the hydrolysis reaction and improve the reaction rate and product yield.
[0023] The display control component 6 includes a bracket 601, a CNC controller 602, a gas pressure sensor 603, a hydrolysis pressure sensor 604, and a temperature sensor 605. The bracket 601 is fixedly installed on the top side of the workbench component 1, and the CNC controller 602 is located on the top of the bracket 601. The gas pressure sensor 603 is fixedly installed on the top inside the inert gas tank 301. The hydrolysis pressure sensor 604 and the temperature sensor 605 are symmetrically arranged on the top side inside the hydrolysis tank 201, which is beneficial for detecting the temperature and pressure inside the hydrolysis tank 201 and the inert gas tank 301.
[0024] The working principle of this utility model:
[0025] First, place the equipment on a level surface and introduce inert gas into the inert gas tank 301 through the air inlet 304. The operator controls the gas booster motor 505 to start using the CNC 602, and increases the internal pressure of the inert gas tank 301 through the gas connection pipe 503. Then, flip the sealing cover 403 to the left to open it. Mix an appropriate amount of p-nitrophenol and water in a certain proportion, and add it into the hydrolysis tank 201 through the feed inlet 402 and close the sealing cover 403.
[0026] Next, the operator starts the stirring motor 203 via the CNC 602. The output shaft of the stirring motor 203 drives the transmission shaft, which in turn drives the stirring rod 205 and the heater 206 to rotate, so that the reactants are evenly mixed in the pressure cylinder. The heater 206 is started and the temperature is set. As the temperature rises, p-nitrophenol begins to undergo a hydrolysis reaction. At the same time, the gas supply motor 306 is started via the CNC 602. The output shaft of the gas supply motor 306 drives the transmission shaft, which in turn drives the blocking device 307 to rotate, so that the gas supply hole 308 on the blocking device 307 is connected to the gas supply pipe 302, allowing the inert gas in the inert gas tank 301 to enter the hydrolysis tank 201 through the gas supply pipe 302, providing an inert environment for the hydrolysis process. When the temperature reaches the set value, the hydrolysis booster motor 504 is started via the CNC 602 to apply a certain pressure to the mixture in the hydrolysis tank 201, which is beneficial to promote the hydrolysis reaction and improve the reaction rate and product yield.
[0027] Finally, the pressure and temperature in the hydrolysis tank 201 and the inert gas tank 301 are detected by the gas pressure sensor 603, the hydrolysis pressure sensor 604, and the temperature sensor 605, respectively. If the pressure and temperature are abnormal, the feedback will be displayed on the display on the CNC 602, so that the staff can make timely adjustments by controlling the corresponding devices through the CNC 602 to ensure the effective hydrolysis of p-nitrophenol. After the hydrolysis is completed, the hydrolyzed product is discharged through the discharge port 207.
[0028] Finally, the following points should be noted: First, in the description of this application, it should be noted that, unless otherwise specified and limited, the terms "installation", "connection", and "linkage" should be interpreted broadly, and can be mechanical or electrical connections, or internal connections between two components, or direct connections. "Up", "down", "left", "right", etc. are only used to indicate relative positional relationships. When the absolute position of the described object changes, the relative positional relationship may change.
[0029] Secondly: The accompanying drawings of the embodiments disclosed in this utility model only involve the structures involved in the embodiments disclosed in this utility model. Other structures can refer to the general design. In the absence of conflict, the same embodiment and different embodiments of this utility model can be combined with each other.
[0030] Finally: The above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.
Claims
1. A pressurized material mechanism for hydrolysis of p-nitrophenol, comprising a workbench assembly (1), a hydrolysis assembly (2), a gas storage assembly (3), a feeding assembly (4), a pressurization assembly (5) and a display control assembly (6), the hydrolysis assembly (2) is installed on the top of the workbench assembly (1), the gas storage assembly (3) is arranged on one side of the top of the workbench assembly (1), the feeding assembly (4) is connected to one side of the outer wall of the hydrolysis assembly (2), the pressurization assembly (5) is installed on one side of the top of the workbench assembly (1), and the display control assembly (6) is installed on one side of the top of the workbench assembly (1) close to the pressurization assembly (5), characterized in that: The hydrolysis assembly (2) comprises a hydrolysis barrel (201), a first protective shell (202), a stirring motor (203), a connecting body (204), a stirring rod (205), a heater (206), a discharge port (207), a first booster hole (208) and a feeding hole (209), the hydrolysis barrel (201) is fixedly installed at the middle position of the top of the workbench assembly (1), the first protective shell (202) is fixedly installed at the top of the hydrolysis barrel (201), and the inside of the first protective shell (202) is nested with the stirring motor (203), the output shaft of the stirring motor (203) is fixedly connected with the connecting body (204) through a shaft coupling, one side of the connecting body (204) is fixedly connected with the stirring rod (205), the heater (206) is installed at the bottom of the inside of the hydrolysis barrel (201), the discharge port (207) is formed in the left side of the hydrolysis barrel (201), and the feeding hole (209) is formed in the right side of the hydrolysis barrel (201), and the first booster hole (208) is formed in one side of the hydrolysis barrel (201).
2. The press mechanism for hydrolysis of p-nitrophenol according to claim 1, characterized in that: The gas storage assembly (3) comprises an inert gas barrel (301), a gas conveying pipe (302), a second booster hole (303), an air inlet hole (304), a second protective shell (305), a gas conveying motor (306), a blocker (307) and a gas conveying hole (308), the inert gas barrel (301) is fixedly installed at the top left side of the workbench assembly (1), and the inert gas barrel (301) is communicated with the hydrolysis barrel (201) through the gas conveying pipe (302), the second booster hole (303) is formed in one side of the inert gas barrel (301), the air inlet hole (304) is formed in the top side of the inert gas barrel (301), the second protective shell (305) is arranged at the middle of the outer wall of the gas conveying pipe (302), and the inside of the second protective shell (305) is nested with the gas conveying motor (306), the output shaft of the gas conveying motor (306) is fixedly connected with the blocker (307) through a shaft coupling, and the gas conveying hole (308) is formed in the blocker (307).
3. The press mechanism for hydrolysis of p-nitrophenol according to claim 1, characterized in that: The feeding assembly (4) comprises a feeding pipe (401), a feeding port (402), a sealing cover (403), a fixed column body (404), a fixed shaft (405) and a clamping device (406), the bottom of the feeding pipe (401) is communicated with the inside of the hydrolysis barrel (201) through the feeding hole (209), and the top of the feeding pipe (401) is fixedly installed with the feeding port (402), the sealing cover (403) is arranged at the top of the feeding port (402), the fixed column body (404) is fixedly connected to one side of the feeding port (402), and the fixed column body (404) is movably connected to the inside of the clamping device (406) through the fixed shaft (405), and one end of the clamping device (406) is fixedly connected to one side of the sealing cover (403).
4. The press mechanism for hydrolysis of p-nitrophenol according to claim 1, wherein: The booster assembly (5) comprises a booster (501), a hydrolysis connecting pipe (502), a gas connecting pipe (503), a hydrolysis booster motor (504) and a gas booster motor (505), the booster (501) is fixedly installed on one side of the top of the workbench assembly (1), and the booster (501) is communicated with the hydrolysis barrel (201) and the inert gas barrel (301) through the hydrolysis connecting pipe (502) and the gas connecting pipe (503) respectively, and the hydrolysis booster motor (504) and the gas booster motor (505) are symmetrically arranged in the booster (501).
5. The press mechanism for hydrolysis of p-nitrophenol according to claim 1, wherein: The display control assembly (6) comprises a support (601), a numerical controller (602), a gas pressure sensor (603), a hydrolysis pressure sensor (604) and a temperature sensor (605), the support (601) is fixedly installed on one side of the top of the workbench assembly (1), and the top of the support (601) is provided with the numerical controller (602), the gas pressure sensor (603) is fixedly installed on the top of the inside of the inert gas barrel (301), and the hydrolysis pressure sensor (604) and the temperature sensor (605) are symmetrically arranged on one side of the top of the inside of the hydrolysis barrel (201).