Online pH meter cleaning and checking device

The online pH meter cleaning and calibration device solves the problem of pH meter cleaning and calibration in continuous reactor production, enabling cleaning and probe replacement without stopping the machine, and is suitable for toxic and harmful reactions.

CN224142217UActive Publication Date: 2026-04-21SHANDONG YUANLIAN CHEM CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
SHANDONG YUANLIAN CHEM CO LTD
Filing Date
2025-05-21
Publication Date
2026-04-21

AI Technical Summary

Technical Problem

In the existing technology, pH meters cannot be cleaned and calibrated during continuous reactor production, and pH probes cannot be replaced without shutting down the machine.

Method used

Design an online pH meter cleaning and calibration device, including a ball valve, nitrogen and liquid inlet valves and an outlet valve on a continuous reactor to achieve a closed cleaning process, and protect the pH meter probe with a sealing packing to support replacement without shutting down the system.

Benefits of technology

It enables the cleaning and calibration of pH meters without shutting down the reactor, ensuring that the reaction liquid inside the reactor does not flow out. It is especially suitable for toxic and harmful reactions and supports rapid probe replacement.

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Abstract

The utility model discloses an on-line pH meter cleaning and checking device which comprises a continuous kettle, a first ball valve and a second ball valve are respectively sleeved on the continuous kettle close to the left side and the right side, and the right side of the continuous kettle is connected with a pH meter probe. A nitrogen exhaust port valve and a flushing fluid and checking fluid exhaust port valve are respectively arranged at the bottom of the continuous kettle close to the right side of the first ball valve, and a flushing fluid and checking fluid inlet valve and a nitrogen inlet valve are arranged at the top of the continuous kettle close to the second ball valve; the first ball valve and the second ball valve are arranged in a bilateral symmetry mode with the central axis of the continuous kettle as the symmetry axis, and a sealing packing is arranged on the right side of the continuous kettle. According to the technical scheme, the defect that the pH meter cannot be cleaned and checked in the continuous kettle production process is overcome, the whole cleaning process is completely closed, no reaction liquid in the kettle flows out, the device is particularly suitable for toxic and harmful reactions, and if a pH meter probe is damaged, the pH probe can be replaced in a non-stop state.
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Description

Technical Field

[0001] This utility model relates to the field of pH meter technology, and in particular to an online pH meter cleaning and calibration device. Background Technology

[0002] A continuous stirred tank reactor, also known as a continuous stirred tank reactor, is a specialized piece of equipment used in chemical production to achieve continuous material flow and chemical reactions. Its core characteristic is that the material input, reaction, and product output are all uninterrupted continuous processes. Existing continuous stirred tank reactor technologies cannot address the shortcomings of pH meters not being able to be cleaned and calibrated during continuous reactor production, nor can pH probes be replaced without shutting down the reactor. Therefore, we propose an online pH meter cleaning and calibration device. Utility Model Content

[0003] The purpose of this invention is to at least solve one of the technical problems existing in the prior art, and to provide an online pH meter cleaning and calibration device that is applicable to online pH cleaning and calibration in continuous reactor production processes.

[0004] To achieve the above objectives, an online pH meter cleaning and calibration device is provided, comprising: a continuous vessel, wherein a first ball valve and a second ball valve are respectively sleeved on the left and right sides of the continuous vessel, a pH meter probe is connected to the right side of the continuous vessel, and a nitrogen exhaust valve and a rinsing liquid and calibration liquid discharge valve are respectively provided at the bottom of the continuous vessel near the right side of the first ball valve.

[0005] According to the online pH meter cleaning and calibration device, the top of the continuous reactor is provided with a rinsing liquid and calibration liquid inlet valve and a nitrogen inlet valve near the second ball valve, and the first ball valve and the second ball valve are arranged symmetrically about the central axis of the continuous reactor.

[0006] According to the online pH meter cleaning and calibration device, a sealing packing is provided on the right side of the continuous vessel, and the sealing packing is sleeved between the pH meter probe and the inner wall of the continuous vessel.

[0007] According to the online pH meter cleaning and calibration device, the nitrogen exhaust valve and the rinsing liquid and calibration liquid discharge valve are arranged on the left and right sides of the bottom of the continuous reactor.

[0008] According to the online pH meter cleaning and calibration device, the rinsing fluid and calibration fluid inlet valves and the nitrogen inlet valve are arranged on the left and right sides of the top of the continuous reactor.

[0009] The above solution has at least one of the following beneficial effects:

[0010] 1. This technical solution solves the problem of pH meters being unable to be cleaned and calibrated during continuous reactor production;

[0011] 2. This technical solution completely seals the entire cleaning process, preventing any outflow of the reaction liquid from the vessel, making it particularly suitable for toxic and harmful reactions;

[0012] 3. This technical solution allows for the replacement of the pH meter probe without shutting down the system if the probe is damaged.

[0013] Additional aspects and advantages of this invention will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. Attached Figure Description

[0014] The present invention will be further described below with reference to the accompanying drawings and embodiments;

[0015] Figure 1 This is a schematic diagram of the cross-sectional structure of the present invention;

[0016] Figure 2 for Figure 1 A schematic diagram of a partial cross-sectional structure of components such as the first ball valve;

[0017] Figure 3 for Figure 1 A schematic diagram of a partial cross-sectional structure of components such as the pH meter probe.

[0018] Legend:

[0019] 1. Continuous reactor; 2. First ball valve; 3. Second ball valve; 4. Nitrogen inlet valve; 5. Nitrogen exhaust valve; 6. Rinse solution and calibration solution inlet valve; 7. Rinse solution and calibration solution outlet valve; 8. Sealing packing; 9. pH meter probe. Detailed Implementation

[0020] This section will describe in detail the specific embodiments of the present utility model. The preferred embodiments of the present utility model are shown in the accompanying drawings. The purpose of the drawings is to supplement the textual description with graphics, so that people can intuitively and vividly understand each technical feature and the overall technical solution of the present utility model, but they should not be construed as limiting the scope of protection of the present utility model.

[0021] Reference Figures 1 to 3 This utility model provides an online pH meter cleaning and calibration device, which includes a continuous vessel 1. A first ball valve 2 and a second ball valve 3 are respectively sleeved on the left and right sides of the continuous vessel 1. A pH meter probe 9 is connected to the right side of the continuous vessel 1. A nitrogen exhaust valve 5 and a rinsing liquid and calibration liquid discharge valve 7 are respectively provided at the bottom of the continuous vessel 1 near the right side of the first ball valve 2.

[0022] Near the second ball valve 3, the top of the continuous reactor 1 is equipped with a rinsing liquid and calibration liquid inlet valve 6 and a nitrogen inlet valve 4. The first ball valve 2 and the second ball valve 3 are symmetrically arranged about the central axis of the continuous reactor 1. The nitrogen exhaust valve 5 and the rinsing liquid and calibration liquid exhaust valve 7 are located on opposite sides of the bottom of the continuous reactor 1. The rinsing liquid and calibration liquid inlet valve 6 and the nitrogen inlet valve 4 are located on opposite sides of the top of the continuous reactor 1. This structure solves the problem of pH meters being unable to be cleaned and calibrated during continuous reactor production. The entire cleaning process is completely closed, with no outflow of reaction liquid from the reactor, making it particularly suitable for toxic and harmful reactions.

[0023] A sealing packing 8 is provided on the right side of the continuous reactor 1, and the sealing packing 8 is fitted between the pH meter probe 9 and the inner wall of the continuous reactor 1. With this structure, if the pH meter probe 9 is damaged, the pH probe can be replaced without stopping the reactor.

[0024] Working principle: When using this technical solution, first, pull the pH meter probe 9 rod to the cleaning position - close the first ball valve 2 - open the nitrogen inlet valve 4 - introduce nitrogen - open the nitrogen exhaust valve 5 - purge with nitrogen for 30 seconds - close the nitrogen exhaust valve 5 - close the nitrogen inlet valve 4 - open the rinsing fluid and calibration fluid inlet valve 6 - introduce the cleaning fluid - open the rinsing fluid and calibration fluid outlet valve 7 - drain the cleaning fluid - introduce the calibration fluid through the rinsing fluid and calibration fluid inlet valve 6 - calibration completed - close the rinsing fluid and calibration fluid inlet valve 6 and the rinsing fluid and calibration fluid outlet valve 7 - open the first ball valve 2 - insert the pH meter probe 9 rod into the working position.

[0025] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely illustrative of the principles of this utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claims. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. An on-line pH meter cleaning and calibration device, characterized by, include: A continuous reactor (1) is provided with a first ball valve (2) and a second ball valve (3) respectively fitted on the left and right sides of the continuous reactor (1). A pH meter probe (9) is connected to the right side of the continuous reactor (1). A nitrogen exhaust valve (5) and a rinsing liquid and calibration liquid discharge valve (7) are respectively provided at the bottom of the continuous reactor (1) near the right side of the first ball valve (2).

2. An on-line pH meter cleaning and calibration device according to claim 1, characterized in that, The top of the continuous reactor (1) is provided with a flushing liquid and a verification liquid inlet valve (6) and a nitrogen inlet valve (4) near the second ball valve (3), and the first ball valve (2) and the second ball valve (3) are arranged symmetrically about the central axis of the continuous reactor (1).

3. The on-line pH meter cleaning and calibration device of claim 1, wherein, A sealing packing (8) is provided on the right side of the continuous vessel (1), and the sealing packing (8) is fitted between the pH meter probe (9) and the inner wall of the continuous vessel (1).

4. The on-line pH meter cleaning and calibration device of claim 1, wherein, The nitrogen exhaust valve (5) and the flushing liquid and verification liquid exhaust valve (7) are set on the bottom of the continuous reactor (1), one on the left and one on the right.

5. The on-line pH meter cleaning and calibration device of claim 1, wherein, The flushing fluid and verification fluid inlet valve (6) and the nitrogen inlet valve (4) are located on the top of the continuous reactor (1), one on the left and one on the right.