Preparation system capable of rapidly purifying compound

By combining a graphene stirring paddle and a cooling mechanism, the problem of wasted water cooling resources during distillation and purification is solved, enabling rapid cooling of the condenser and recycling of water resources, which is suitable for the rapid purification of compounds.

CN224166932UActive Publication Date: 2026-04-28HUBEI TIANSHU PHARMA CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
HUBEI TIANSHU PHARMA CO LTD
Filing Date
2025-02-12
Publication Date
2026-04-28

AI Technical Summary

Technical Problem

In existing distillation and purification processes, water cooling requires a large amount of fresh water, resulting in significant resource waste and hindering recycling.

Method used

By employing a graphene stirring paddle and a cooling mechanism, and using circulating water to cool the condenser tubes, rapid cooling and water resource recycling are achieved.

Benefits of technology

It achieves rapid cooling of the condenser tube, reduces the consumption of fresh water, saves resources, and is especially suitable for areas with scarce water resources.

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Abstract

The preparation system comprises a heating box and a motor, a gas collecting hood is arranged at one end above the heating box, a condensation pipe is arranged at one end of the side face of the gas collecting hood, a cooling mechanism is arranged at one end of the side face of the condensation pipe, and a water tank is arranged at one end of the side face of the heating box. A stirring mechanism is arranged at one end in the water tank, and a backflow pipe is arranged between the condensation pipe and the heating box; through the water tank, the cooling mechanism, the stirring mechanism and the like, water in the water tank can be matched with the cooling mechanism to cool the condensation pipe, the water can be circulated back to the water tank through the cooling mechanism, and then the water in the water tank can be stirred through the stirring mechanism; and therefore, water in the water tank can be rapidly cooled, the requirement for cooling the condensation pipe can be met, recycling can be achieved, and more resources are saved.
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Description

Technical Field

[0001] This invention relates to the field of compound preparation technology, specifically a preparation system capable of rapidly purifying compounds. Background Technology

[0002] A compound is a pure substance composed of two or more different elements, as opposed to elements and mixtures. These elements are bonded together by chemical bonds, such as covalent bonds and ionic bonds, to form a substance with a fixed composition and specific properties. The elements in a compound exist in a certain proportion, and the properties of a compound usually differ from those of its constituent elements. Compounds have wide applications in many fields, including daily life, industrial production, and scientific research.

[0003] However, some compounds require distillation purification during the production process. In general, the condenser needs to be rapidly cooled during distillation purification. Water cooling is usually used in distillation purification, but it is usually directly connected to an external water source, which consumes a large amount of water and is not conducive to recycling. Therefore, further improvement is needed. Utility Model Content

[0004] The purpose of this invention is to provide a preparation system for rapidly purifying compounds in order to solve the problems mentioned in the background art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a preparation system for rapidly purifying compounds, comprising: a heating chamber and a motor; a gas collecting hood is provided at one end of the upper part of the heating chamber; a condenser is provided at one end of the side of the gas collecting hood; a cooling mechanism is provided at one end of the side of the condenser; a water tank is provided at one end of the side of the heating chamber; a stirring mechanism is provided at one end inside the water tank; and a reflux pipe is provided between the condenser and the heating chamber. The heating chamber is existing technology and can heat the compound to be purified and the reagent to form water vapor. By cooperating with other components, multiple distillations can be performed to purify the compound.

[0006] As a further embodiment of this utility model: the stirring mechanism includes a main shaft fixedly connected to the output shaft below the motor, a first fixing block fixedly connected to one side end of the main shaft, a graphene stirring paddle fixedly connected to one side end of the first fixing block, a second fixing block fixedly connected to one side end of the main shaft, a rotating plate rotatably connected to one side end of the second fixing block, and a gear fixedly connected to one side end of the rotating plate.

[0007] As a further embodiment of this utility model: the water tank includes a water tank body disposed at one end of the side of the heating box, a connecting block is fixedly connected to one end of the interior of the water tank body, a gear ring is fixedly connected to one end of the side of the connecting block, the gear meshes with the gear ring, a support plate is fixedly connected to one end of the upper part of the water tank body, a water inlet is opened at one end of the side of the water tank body, and a water outlet is opened at one end of the side of the water tank body.

[0008] As a further embodiment of this utility model: the cooling mechanism includes a pump disposed at one end of the side of the water tank, an inlet pipe disposed at one end of the side of the pump, a cooling chamber disposed at one end of the side of the inlet pipe, and an outlet pipe disposed between the cooling chamber and the water tank.

[0009] As a further improvement of this utility model: the water tank is adapted to the stirring mechanism, and the cooling mechanism is adapted to the condenser tube.

[0010] As a further improvement of this utility model: the interior of the cooling chamber is hollow, and the side in contact with the condenser tube is made of copper.

[0011] Compared with the prior art, the beneficial effects of this utility model are:

[0012] This invention utilizes a water tank, a cooling mechanism, and a stirring mechanism. The water in the tank, in conjunction with the cooling mechanism, cools the condenser tube. The cooling mechanism allows the water to circulate back into the water tank, and the stirring mechanism agitates the water, rapidly lowering its temperature to meet the cooling requirements of the condenser tube. This allows for recycling and greater resource conservation. Attached Figure Description

[0013] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0014] Figure 2 This is a schematic diagram of the overall structure from a second perspective in this utility model;

[0015] Figure 3 This is a schematic diagram of the water tank structure in this utility model;

[0016] Figure 4 This is a schematic diagram of the stirring mechanism in this utility model.

[0017] In the diagram: 1. Heating box; 2. Gas collection hood; 3. Condenser pipe; 4. Cooling mechanism; 41. Pump; 42. Water inlet pipe; 43. Cooling chamber; 44. Water outlet pipe; 5. Water tank; 51. Water tank body; 52. Connecting block; 53. Gear ring; 54. Support plate; 55. Water inlet; 56. Water outlet; 6. Motor; 7. Stirring mechanism; 71. Main shaft; 72. First fixed block; 73. Graphene stirring paddle; 74. Second fixed block; 75. Rotating plate; 76. Gear; 8. Return pipe. Detailed Implementation

[0018] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0019] In the description of this utility model, it should be noted that the terms "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," and "outer," etc., indicating the orientation or positional relationship, are based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and should not be construed as indicating or implying relative importance. In the description of this utility model, it should be noted that unless otherwise explicitly specified and limited, the terms "installation," "connection," "linking," and "setting" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; and they can refer to the internal connection of two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model based on the specific circumstances. The embodiments of this utility model will be described below based on its overall structure.

[0020] Reference Figures 1 to 4 In this embodiment of the present invention, a preparation system for rapidly purifying compounds includes: a heating chamber 1 and a motor 6. A gas collecting hood 2 is provided at one end of the upper part of the heating chamber 1. A condenser 3 is provided at one end of the side of the gas collecting hood 2. A cooling mechanism 4 is provided at one end of the side of the condenser 3. A water tank 5 is provided at one end of the side of the heating chamber 1. A stirring mechanism 7 is provided at one end of the interior of the water tank 5. A reflux pipe 8 is provided between the condenser 3 and the heating chamber 1.

[0021] The stirring mechanism 7 includes a main shaft 71 fixedly connected to the output shaft below the motor 6. A first fixing block 72 is fixedly connected to one side end of the main shaft 71. A graphene stirring paddle 73 is fixedly connected to one side end of the first fixing block 72. The graphene stirring paddle 73 is a metal stirring paddle with a graphene coating on its surface, which has good heat absorption performance. A second fixing block 74 is fixedly connected to one side end of the main shaft 71. A rotating plate 75 is rotatably connected to one side end of the second fixing block 74. A gear 76 is fixedly connected to one side end of the rotating plate 75.

[0022] The water tank 5 includes a water tank body 51 located at one side of the heating box 1. A connecting block 52 is fixedly connected to one end of the water tank body 51. A toothed ring 53 is fixedly connected to one side of the connecting block 52. A support plate 54 is fixedly connected to one upper end of the water tank body 51. A water inlet 55 is opened at one side of the water tank body 51. A water outlet 56 is opened at one side of the water tank body 51.

[0023] The above scheme is adopted: the motor 6 drives the main shaft 71 to rotate, thereby driving the first fixed block 72 and the graphene stirring paddle 73 to rotate. Then, when the main shaft 71 rotates, it drives the second fixed block 74 fixed to the side to rotate, thereby driving the rotating plate 75 connected to the side to revolve. Then, when the rotating plate 75 revolves, the gear 76 fixed to the side meshes with the gear ring 53, thereby driving the rotating plate 75 to rotate on its own axis. The rotation direction is not the same as that of the graphene stirring paddle 73, so that the water in the water tank 5 can be cooled down more quickly.

[0024] The cooling mechanism 4 includes a pump 41 located at one side of the water tank 5, an inlet pipe 42 located at one side of the pump 41, a cooling chamber 43 located at one side of the inlet pipe 42, and an outlet pipe 44 located between the cooling chamber 43 and the water tank 5.

[0025] The above scheme is adopted as follows: cold water is added to water tank 5, and then the reagent and the compound to be purified are placed in heating box 1 for heating to generate water vapor. The water vapor enters the condenser tube 3 through the gas collection hood 2, and then the cold water in water tank 5 is driven by pump 41 to enter the cooling chamber 43 through water inlet pipe 42 to cool the water vapor and condense it into water droplets. Then, it flows back into heating box 1 through reflux pipe 8 for circulating distillation. The water in cooling chamber 43 will flow back into water tank 5 through water outlet 56.

[0026] Water tank 5 is compatible with stirring mechanism 7, and cooling mechanism 4 is compatible with condenser tube 3.

[0027] The interior of the cooling chamber 43 is hollow, and the side that contacts the condenser tube 3 is made of copper.

[0028] The working principle of this invention is as follows: First, cold water is added to water tank 5. Then, the reagent and the compound to be purified are placed in heating chamber 1 for heating to generate water vapor. The water vapor enters the condenser tube 3 through the gas collection hood 2. Then, the cold water in water tank 5 is driven by pump 41 to enter the cooling chamber 43 through the water inlet pipe 42 to cool and condense the water vapor into water droplets. Then, the water flows back into heating chamber 1 through the return pipe 8 for circulating distillation. The water in cooling chamber 43 flows back into water tank 5 through water outlet 56. Then, the main shaft 71 is driven to rotate by motor 6, thereby driving the first fixed block 72 and the graphene stirring paddle 73 to rotate. Then, when the main shaft 71 rotates, it drives the second fixed block 74 fixed to the side to rotate, thereby driving the rotating plate 75 connected to the side to revolve. Then, when the rotating plate 75 revolves, the gear 76 fixed to the side meshes with the gear ring 53, thereby driving the rotating plate 75 to rotate on its own axis. The rotation direction is not the same as that of the graphene stirring paddle 73, so that the water in the water tank 5 can be cooled down more quickly. Water recycling helps to protect water resources and the ecological environment. Water recycling significantly reduces the consumption of fresh water, which is especially important for areas with scarce water resources. Through recycling, enterprises can significantly reduce water expenses.

[0029] The above description is only a preferred embodiment of the present utility model, but the protection scope of the present utility model is not limited thereto. Any equivalent substitutions or changes made by those skilled in the art within the technical scope disclosed in the present utility model, based on the technical solution and the inventive concept of the present utility model, should be included within the protection scope of the present utility model.

Claims

1. A preparation system for rapidly purifying compounds, comprising: The heating box (1) and the motor (6) are characterized in that a gas collecting hood (2) is provided at one end of the upper part of the heating box (1), a condenser pipe (3) is provided at one end of the side of the gas collecting hood (2), a cooling mechanism (4) is provided at one end of the side of the condenser pipe (3), a water tank (5) is provided at one end of the side of the heating box (1), a stirring mechanism (7) is provided at one end of the interior of the water tank (5), and a return pipe (8) is provided between the condenser pipe (3) and the heating box (1).

2. The preparation system for rapidly purifying compounds according to claim 1, characterized in that, The stirring mechanism (7) includes a main shaft (71) fixedly connected to the output shaft below the motor (6), a first fixing block (72) fixedly connected to one side end of the main shaft (71), a graphene stirring paddle (73) fixedly connected to one side end of the first fixing block (72), a second fixing block (74) fixedly connected to one side end of the main shaft (71), a rotating plate (75) rotatably connected to one side end of the second fixing block (74), and a gear (76) fixedly connected to one side end of the rotating plate (75).

3. The preparation system for rapidly purifying compounds according to claim 1, characterized in that, The water tank (5) includes a water tank body (51) disposed on one side of the heating box (1), a connecting block (52) is fixedly connected to one end inside the water tank body (51), a toothed ring (53) is fixedly connected to one side of the connecting block (52), a support plate (54) is fixedly connected to one upper end of the water tank body (51), a water inlet (55) is opened on one side of the water tank body (51), and a water outlet (56) is opened on one side of the water tank body (51).

4. The preparation system for rapidly purifying compounds according to claim 1, characterized in that, The cooling mechanism (4) includes a pump (41) disposed at one end of the side of the water tank (5), an inlet pipe (42) disposed at one end of the side of the pump (41), a cooling chamber (43) disposed at one end of the side of the inlet pipe (42), and an outlet pipe (44) disposed between the cooling chamber (43) and the water tank (5).

5. The preparation system for rapidly purifying compounds according to claim 1, characterized in that, The water tank (5) is adapted to the stirring mechanism (7), and the cooling mechanism (4) is adapted to the condenser (3).

6. The preparation system for rapidly purifying compounds according to claim 4, characterized in that, The cooling chamber (43) is hollow inside, and the side in contact with the condenser tube (3) is made of copper.