Efficient stirring reaction kettle for organic silicon production

Abstract

The utility model discloses an efficient stirring reaction kettle for organic silicon production, which comprises a kettle body, a motor of the kettle body is connected with a vertical pipe, the vertical pipe is rotatably arranged on a cover of the kettle body through a first bearing, the vertical pipe is arranged in the kettle body, pesticide spraying ports are uniformly distributed on the position of the vertical pipe in the kettle body, and the pesticide spraying ports are communicated with the kettle body. A vertical pipe is arranged in the kettle body, round holes are uniformly distributed in the position, outside the kettle body, of the vertical pipe, a round pipe is rotatably mounted outside the vertical pipe through a third bearing, the round pipe is sleeved outside the round holes, a connecting port is formed in the side wall of the round pipe, and a connecting pipe is connected in the connecting port. The vertical pipe is driven to rotate in the kettle body, a medium in the kettle body is stirred, meanwhile, a catalyst is sprayed into the stirred kettle body through a one-way valve, the vertical pipe adopts a hollow stirring shaft as a catalyst conveying channel, and an external buffer box and a feeding pipe are combined, so that uniform distribution of the catalyst is ensured, and the reaction consistency and efficiency are improved.

Description

Technical Field

[0001] This utility model relates to the field of organosilicon production technology, specifically to a high-efficiency stirred reactor for organosilicon production. Background Technology

[0002] Organosilicon, or organosilicon compounds, refers to compounds containing Si-C bonds, with at least one organic group directly bonded to a silicon atom. Compounds whose organic groups are bonded to silicon atoms via oxygen, sulfur, nitrogen, etc., are also commonly considered organosilicon compounds. Among these, polysiloxanes, with a silicon-oxygen bond (-Si-O-Si-) backbone, are the most numerous, most extensively studied, and most widely used type of organosilicon compound, accounting for over 90% of total usage. However, the production of organosilicon requires stirred reaction vessels.

[0003] However, in the current stirred reactors used for organosilicon production, the catalyst is delivered through the feeding port at the top of the reactor, which makes it difficult for the catalyst to be evenly distributed in the medium of the reactor. This reduces the consistency of the reaction and the reaction efficiency between the catalyst and the medium in the reactor. Utility Model Content

[0004] The purpose of this invention is to provide a high-efficiency stirred reactor for organosilicon production, which solves the problem that in current stirred reactors for organosilicon production, the catalyst is delivered through the feeding port at the top of the reactor body, making it difficult for the catalyst to be evenly distributed in the medium of the reactor body, thereby reducing the consistency of the reaction and the reaction efficiency between the catalyst and the medium in the reactor body.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a high-efficiency stirred reactor for organosilicon production, comprising a reactor body, a vertical pipe connected to a motor of the reactor body, the vertical pipe being rotatably mounted on the lid of the reactor body via a first bearing, and the vertical pipe being placed inside the reactor body, with spray nozzles evenly distributed on the vertical pipe within the reactor body, and circular holes evenly distributed around the vertical pipe outside the reactor body, a circular pipe being rotatably mounted on the outside of the vertical pipe via a third bearing, and the circular pipe being fitted over the circular holes, with a connection port on the side wall of the circular pipe, and a connecting pipe connected to the connection port.

[0006] Preferably, a stirring structure is installed at the position where the vertical tube is placed inside the vessel body. The stirring structure includes a shell, a driving component, a worm gear, a rotating shaft, blades, a second bearing, and a worm wheel.

[0007] The housing is installed on the side wall of the vertical tube, the drive unit is installed inside the housing, the worm is installed on the output shaft of the drive unit, the rotating shaft passes through the vertical tube and the housing, and the connection points of the rotating shaft with the vertical tube and the housing are all connected by a second bearing. There are no fewer than three rotating shafts, and blades are installed at both ends of the rotating shaft. A worm wheel is installed at the position of the rotating shaft inside the housing, and the worm is meshed with the worm wheel.

[0008] Preferably, a control unit is installed inside the housing, and the control unit controls the drive components.

[0009] Preferably, the spray nozzles are located at the front, rear, and left side of the vertical pipe, and the spray nozzles are arranged in four rows from top to bottom.

[0010] Preferably, a one-way valve is installed inside the spray nozzle, and the one-way valve corresponds to a spray nozzle in a one-to-one manner.

[0011] Preferably, the blades and the shaft are connected by a connecting structure, which corresponds one-to-one with the blades, and the connecting structure includes bolts and threaded holes;

[0012] The bolt is installed on the rotating shaft, the threaded hole is opened on the blade, and the bolt is sleeved in the threaded hole.

[0013] Compared with the prior art, the beneficial effects of this utility model are: the high-efficiency stirred reactor for organosilicon production has the following advantages compared with traditional technology:

[0014] 1. The driving vertical pipe rotates inside the vessel, stirring the medium inside the vessel. At the same time, the catalyst is injected into the stirred vessel through a one-way valve. The vertical pipe uses a hollow stirring shaft as the catalyst delivery channel. Combined with the external buffer tank and the feed pipe, it ensures that the catalyst is evenly distributed, which helps to improve the consistency and efficiency of the reaction.

[0015] 2. The drive tube rotates inside the vessel, while the manual control unit controls the drive component to rotate periodically in both directions. The drive component drives the worm gear to rotate, and through the meshing force between the worm gear and the worm wheel, the rotating shaft rotates on the vertical tube through the second sealed bearing. The rotating shaft drives the blades to rotate, achieving simultaneous vertical and horizontal stirring, which can evenly stir the medium inside the vessel. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of the structure of this utility model;

[0017] Figure 2 for Figure 1 Schematic diagram of the central shaft, blades, and second bearing;

[0018] Figure 3 for Figure 1 A schematic diagram of the structure of the central vertical tube, the circular tube, and the third bearing;

[0019] Figure 4 for Figure 1 A schematic diagram of the structure of the bolt, threaded hole, shaft and blade.

[0020] In the diagram: 1. Kettle body; 2. First bearing; 3. Stirring structure; 4. Vertical pipe; 5. Shell; 6. Drive component; 7. Worm gear; 8. Rotating shaft; 9. Blade; 10. Second bearing; 11. Worm wheel; 12. Control unit; 13. Spray nozzle; 14. One-way valve; 15. Circular pipe; 16. Third bearing; 17. Connection port; 18. Connecting pipe; 19. Circular hole; 20. Connecting structure; 21. Bolt; 22. Threaded hole. Detailed Implementation

[0021] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0022] Those skilled in the art can connect the components in this case sequentially. The specific connection and operation sequence should refer to the working principle described below. The detailed connection methods are well-known technologies in the field. The working principle and process are mainly described below.

[0023] In current stirred reactors used for organosilicon production, the catalyst is delivered through a feeding port at the top of the reactor. This makes it difficult for the catalyst to be evenly distributed within the reactor medium, thus reducing the consistency of the reaction and the reaction efficiency between the catalyst and the medium in the reactor.

[0024] In view of this, the present invention provides a high-efficiency stirred reactor for organosilicon production. The driving vertical tube rotates inside the reactor, stirring the medium inside the reactor. At the same time, the catalyst is injected into the stirred reactor through a one-way valve. The vertical tube uses a hollow stirring shaft as the catalyst delivery channel. Combined with an external buffer tank and a feed pipe, it ensures uniform distribution of the catalyst, which helps to improve the consistency and efficiency of the reaction.

[0025] Please see Figures 1-4This utility model provides a technical solution: a high-efficiency stirred reactor for organosilicon production, including a reactor body 1. The reactor body 1 is a special reactor for organosilicon production, which is existing technology and therefore not described in detail. A vertical pipe 4 is connected to the motor of the reactor body 1. The vertical pipe 4 is closed at both ends. The vertical pipe 4 is rotatably mounted on the cover of the reactor body 1 through a first bearing 2, and the vertical pipe 4 is placed inside the reactor body 1. The reactor body 1 and the cover are connected by bolts and can be disassembled. They are sealed with a sealing gasket. Spray nozzles 13 are evenly distributed on the vertical pipe 4 inside the reactor body 1. Circular holes 19 are evenly distributed around the vertical pipe 4 outside the reactor body 1. A circular pipe 15 is rotatably mounted on the outside of the vertical pipe 4 through a third bearing 16, and the circular pipe 15 is sleeved on the outside of the circular holes 19. There are third bearings 16 on both sides of the circular pipe 15. A connection port 17 is opened on the side wall of the circular pipe 15. A connecting pipe 18 is connected to the connection port 17. The connecting pipe 18 is connected to the pump body of the external catalyst tank.

[0026] A stirring structure 3 is installed in the position where the vertical tube 4 is placed inside the vessel body 1. The stirring structure 3 includes a shell 5, a driving component 6, a worm gear 7, a rotating shaft 8, a blade 9, a second bearing 10, and a worm wheel 11.

[0027] The housing 5 is installed on the side wall of the vertical tube 4. The drive unit 6 is installed inside the housing 5. The drive unit 6 is a servo motor. The worm gear 7 is installed on the output shaft of the drive unit 6. The rotating shaft 8 passes through the vertical tube 4 and the housing 5. The connection points of the rotating shaft 8 with the vertical tube 4 and the housing 5 are all connected by the second bearing 10. There are no fewer than three rotating shafts. The two ends of the rotating shaft 8 are respectively equipped with blades 9. The worm wheel 11 is installed in the position of the rotating shaft 8 inside the housing 5. The worm gear 7 is meshed with the worm wheel 11. The control unit 12 is installed inside the housing 5. The control unit 12 is a battery and a remote control switch. The battery can be of large capacity and the charging port extends to the outside of the housing 5 and is sealed by a seal. It can be charged during maintenance and cleaning. The control unit 12 controls the drive unit 6.

[0028] The spray nozzles 13 are located in front of, behind and to the left of the vertical pipe 4. The spray nozzles 13 are arranged in four rows from top to bottom. One-way valves 14 are installed inside the spray nozzles 13, and one-way valves 14 correspond to one spray nozzle 13.

[0029] The blade 9 is connected to the shaft 8 via a connecting structure 20. The connecting structure 20 corresponds one-to-one with the blade 9. The connecting structure 20 includes a bolt 21 and a threaded hole 22.

[0030] Bolt 21 is installed on shaft 8, threaded hole 22 is opened on blade 9, and bolt 21 is fitted into threaded hole 22;

[0031] It is worth noting that the materials used in the design are all corrosion-resistant and high-temperature resistant, and all bearings used are sealed bearings.

[0032] When using this high-efficiency stirred reactor for organosilicon production, firstly, manually screw the threaded holes 22 on the blades 9 onto the bolts 21 on the rotating shaft 8 one by one. Then, extend the vertical pipe 4 into the reactor body 1 and seal it with the lid. Add organosilicon into the reactor body 1 and start the reactor body 1. Simultaneously, drive the vertical pipe 4 to rotate inside the reactor body 1. The manual control unit 12 controls the drive component 6 to rotate periodically in both directions. The drive component 6 drives the worm gear 7 to rotate. Through the meshing force between the worm gear 7 and the worm wheel 11, the rotating shaft 8 rotates on the vertical pipe 4 through the second bearing 10. The rotating shaft 8 drives the blades 9 to rotate, which can evenly stir the medium inside the reactor body 1. Meanwhile, the external pump works to pump the catalyst into the connecting pipe 18. The catalyst enters the circular pipe 15 and then enters the rotating vertical pipe 4 through the circular hole 19. The catalyst is sprayed into the stirred reactor body 1 through the one-way valve 14, ensuring uniform distribution of the catalyst and helping to improve the consistency and efficiency of the reaction.

[0033] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A high-efficiency stirred reactor for organosilicon production, comprising a reactor body (1), characterized in that: A vertical tube (4) is connected to the motor of the vessel body (1). The vertical tube (4) is rotatably mounted on the cover of the vessel body (1) through the first bearing (2). The vertical tube (4) is placed inside the vessel body (1). Spray nozzles (13) are evenly distributed in the position of the vertical tube (4) inside the vessel body (1). Circular holes (19) are evenly distributed in the position of the vertical tube (4) outside the vessel body (1). A circular tube (15) is rotatably mounted on the outside of the vertical tube (4) through the third bearing (16). The circular tube (15) is sleeved on the outside of the circular hole (19). A connection port (17) is opened on the side wall of the circular tube (15). A connecting pipe (18) is connected in the connection port (17).

2. The high-efficiency stirred reactor for organosilicon production according to claim 1, characterized in that: The vertical tube (4) is installed with a stirring structure (3) inside the vessel body (1). The stirring structure (3) includes a shell (5), a driving component (6), a worm gear (7), a rotating shaft (8), a blade (9), a second bearing (10), and a worm wheel (11). The housing (5) is installed on the side wall of the vertical tube (4), the drive (6) is installed inside the housing (5), the worm (7) is installed on the output shaft of the drive (6), the rotating shaft (8) passes through the vertical tube (4) and the housing (5), and the connection positions of the rotating shaft (8) with the vertical tube (4) and the housing (5) are all connected by the second bearing (10). There are no less than three rotating shafts (8), and blades (9) are installed at both ends of the rotating shaft (8). A worm wheel (11) is installed at the position of the rotating shaft (8) inside the housing (5), and the worm (7) is meshed with the worm wheel (11).

3. The high-efficiency stirred reactor for organosilicon production according to claim 2, characterized in that: A control unit (12) is installed inside the housing (5), and the control unit (12) controls the drive unit (6).

4. The high-efficiency stirred reactor for organosilicon production according to claim 1, characterized in that: The spray nozzles (13) are located in front, behind and to the left of the vertical pipe (4), and the spray nozzles (13) are arranged in four rows from top to bottom.

5. The high-efficiency stirred reactor for organosilicon production according to claim 4, characterized in that: A one-way valve (14) is installed inside the spray nozzle (13), and the one-way valve (14) corresponds one-to-one with the spray nozzle (13).

6. The high-efficiency stirred reactor for organosilicon production according to claim 2, characterized in that: The blade (9) is connected to the shaft (8) by a connecting structure (20), which corresponds one-to-one with the blade (9). The connecting structure (20) includes a bolt (21) and a threaded hole (22). The bolt (21) is installed on the rotating shaft (8), the threaded hole (22) is opened on the blade (9), and the bolt (21) is sleeved in the threaded hole (22).

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