A hydrogenation sodium hydrogen self-absorption dispersion reaction device

Abstract

The utility model belongs to the field of chemical production technology especially sodium hydride hydrogenation self -absorption dispersion reaction unit, including the stirring bucket, the circular arc surface fixed mounting of stirring bucket has the support rod, multiple support rod around the circular arc surface of stirring bucket is circular array setting, be provided with fully stirring mechanism in stirring bucket, fully stirring mechanism realizes sodium hydride hydrogenation fully complete stirring action. This sodium hydride hydrogenation self -absorption dispersion reaction unit, through setting fully stirring mechanism, can make sodium hydride liquid and hydrogen in stirring bucket carry out fully stirring reaction, make stirring main shaft and stirring vice axle mutual cooperation, realize two angle liquid stirring, make the liquid quality after stirring reaction is completed higher.

Description

Technical Field

[0001] This utility model relates to the field of chemical production technology, and in particular to a sodium hydride hydrogenation self-absorption dispersion reaction device. Background Technology

[0002] In existing technologies, such as the self-priming automatic hydrogenation and stirring device for sodium hydride liquid disclosed on the Chinese patent website (publication number CN216396319U), this device is used for stirring and processing sodium hydride liquid. The entire set of equipment adopts a quantitative liquid level float trigger structure design, which ensures that the sodium hydride liquid automatically starts the hydrogenation mechanism at the set capacity. In addition, with the gas flow monitoring, the hydrogen injection can be controlled, making the reaction synthesis ratio more accurate, thereby improving the quality of sodium hydride liquid reaction synthesis, saving costs, reducing equipment wear and tear, extending service life, avoiding safety hazards caused by over-reaction, and making it safer and more reliable.

[0003] However, in practical applications, the stirring mechanism of this device is poorly designed and cannot fully stir the sodium hydride liquid, which can easily lead to incomplete reactions during the stirring process and affect the quality of the final product. Utility Model Content

[0004] To address the technical problem that existing stirring devices cannot fully and completely stir sodium hydride, this invention proposes a sodium hydride hydrogenation self-absorption dispersion reaction device.

[0005] This utility model proposes a sodium hydride hydrogenation self-absorption dispersion reaction device, including a stirring tank. A support rod is fixedly installed on the arc surface of the stirring tank, and multiple support rods are arranged in a circumferential array around the arc surface of the stirring tank. A thorough stirring mechanism is provided inside the stirring tank; the thorough stirring mechanism realizes the stirring action of fully and completely hydrogenating sodium hydride.

[0006] Preferably, the mixing mechanism includes a mixing main shaft, the upper end of which is rotatably connected to the inner top surface of the mixing tank via a ball bearing. The upper end of the mixing main shaft extends through and out of the upper part of the mixing tank. A motor is fixedly installed on the upper part of the mixing tank. The output end of the motor is fixedly connected to the upper part of the mixing main shaft via a coupling. A mixing secondary shaft is rotatably connected to the arc surface of the mixing main shaft via a ball bearing. The two ends of the mixing secondary shaft extend through and out of the two sides of the mixing main shaft, respectively. The angle between the axis of the mixing secondary shaft and the axis of the mixing main shaft is set to 40°.

[0007] The above technical solution involves setting a motor to drive the main stirring shaft to rotate. The rotation of the main stirring shaft can drive the secondary stirring shaft to rotate around the main stirring shaft. The angle between the axis of the secondary stirring shaft and the axis of the main stirring shaft is set to 40°, so that the secondary stirring shaft and the main stirring shaft can stir the sodium hydride in different directions, making the sodium hydride stirring reaction in the stirring tank more complete.

[0008] Preferably, a C-shaped stirring rod is fixedly installed at the lower end of the stirring sub-shaft, and a plurality of the C-shaped stirring rods are arranged in a circumferential array around the arc surface of the stirring sub-shaft, and a self-priming fan blade is fixedly installed on the lower arc surface of the stirring main shaft.

[0009] The above technical solution enables the main stirring shaft to drive the secondary stirring shaft to rotate while the secondary stirring shaft itself can also rotate. This allows the C-shaped stirring rod at the bottom of the secondary stirring shaft to stir the sodium hydride liquid. The self-priming fan blades fixed on the main stirring shaft draw hydrogen gas from the mixing tank into the sodium hydride liquid for stirring and reaction.

[0010] Preferably, a fixing ring is fixedly installed on the inner top surface of the mixing tank, a fixing helical gear is fixedly installed on the outer arc surface of the fixing ring, a fixing plate is fixedly installed on the arc surface of the mixing main shaft, the arc surface of the mixing secondary shaft is rotatably connected to the outer surface of the fixing plate through ball bearings, and a rotating helical gear is rotatably connected to the upper arc surface of the mixing secondary shaft through ball bearings, the tooth groove of the rotating helical gear meshing with the teeth of the fixing helical gear.

[0011] By using the above technical solution, a fixed plate is set up to make the rotation of the stirring main shaft and the stirring secondary shaft more stable and safe. The rotating helical gear and the fixed helical gear mesh, so that the rotation of the stirring secondary shaft causes the rotating helical gear to rotate around the fixed helical gear, so that the stirring secondary shaft can rotate on its own axis while rotating, and the C-shaped stirring rod can stir the sodium hydride liquid.

[0012] Preferably, the upper part of the mixing tank is provided with an air inlet, an air pump is fixedly installed on the upper part of the mixing tank, an air supply pipe is fixedly installed on the output end of the air pump, one end of the air supply pipe is fixedly connected to the upper part of the air inlet, and one end of the air supply pipe passes through and extends into the interior of the air inlet. The upper part of the mixing tank is also provided with a feed inlet, and the lower part of the mixing tank is fixedly installed with a discharge valve.

[0013] The above technical solution involves setting up an air pump, which, when activated, delivers hydrogen to the mixing tank through a gas pipe and an air inlet, allowing the hydrogen to react with the sodium hydride liquid. An inlet is provided to add the sodium hydride liquid to be mixed into the mixing tank, and a discharge valve is provided to discharge the liquid after mixing.

[0014] The beneficial effects of this utility model are as follows:

[0015] By setting up a sufficient stirring mechanism, the sodium hydride liquid and hydrogen gas in the stirring tank can be fully stirred and reacted. The stirring main shaft and stirring secondary shaft work together to achieve liquid stirring at two angles, resulting in higher quality liquid after the stirring reaction is completed. This solves the technical problem that existing stirring devices cannot fully and completely stir sodium hydride. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of a sodium hydride hydrogenation self-absorption dispersion reaction device proposed in this utility model;

[0017] Figure 2 This is a three-dimensional view of the stirring shaft structure of a sodium hydride hydrogenation self-absorption dispersion reaction device proposed in this utility model;

[0018] Figure 3 This is a three-dimensional view of the stirring shaft structure of a sodium hydride hydrogenation self-absorption dispersion reaction device proposed in this utility model.

[0019] In the diagram: 1. Mixing tank; 2. Support rod; 3. Mixing main shaft; 4. Motor; 5. Mixing auxiliary shaft; 6. C-shaped mixing rod; 7. Self-priming fan blade; 8. Fixing ring; 9. Fixing helical gear; 10. Fixing plate; 11. Rotating helical gear; 12. Air inlet; 13. Air pump; 14. Air supply pipe; 15. Feed inlet; 16. Discharge valve. Detailed Implementation

[0020] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments.

[0021] Reference Figures 1-3 A sodium hydride hydrogenation self-absorption dispersion reaction device includes a stirring tank 1. A support rod 2 is fixedly installed on the arc surface of the stirring tank 1. Multiple support rods 2 are arranged in a circumferential array around the arc surface of the stirring tank 1. A thorough stirring mechanism is provided inside the stirring tank 1. The thorough stirring mechanism realizes the thorough stirring action of hydrogenation of sodium hydride.

[0022] The mixing mechanism includes a mixing main shaft 3. The upper end of the mixing main shaft 3 is rotatably connected to the inner top surface of the mixing tank 1 via ball bearings. The upper end of the mixing main shaft 3 extends through and out of the upper part of the mixing tank 1. A motor 4 is fixedly installed on the upper part of the mixing tank 1. The output end of the motor 4 is fixedly connected to the upper part of the mixing main shaft 3 via a coupling. A mixing auxiliary shaft 5 is rotatably connected to the arc surface of the mixing main shaft 3 via ball bearings. The two ends of the mixing auxiliary shaft 5 extend through and out of the two sides of the mixing main shaft 3, respectively. The included angle between the axis of the mixing auxiliary shaft 5 and the axis of the mixing main shaft 3 is set to 40°.

[0023] By setting the motor 4 to drive the stirring main shaft 3 to rotate, the rotation of the stirring main shaft 3 can drive the stirring auxiliary shaft 5 to rotate around the stirring main shaft 3, and the angle between the axis of the stirring auxiliary shaft 5 and the axis of the stirring main shaft 3 is set to 40°, so that the stirring auxiliary shaft 5 and the stirring main shaft 3 can stir the sodium hydride in different directions, making the sodium hydride stirring reaction in the stirring tank 1 more complete.

[0024] A C-shaped stirring rod 6 is fixedly installed at the lower end of the stirring sub-shaft 5. Multiple C-shaped stirring rods 6 are arranged in a circular array around the arc surface of the stirring sub-shaft 5. A self-priming fan blade 7 is fixedly installed on the lower arc surface of the stirring main shaft 3.

[0025] By rotating the main stirring shaft 3 and the auxiliary stirring shaft 5 simultaneously, the auxiliary stirring shaft 5 itself can also rotate, causing the C-shaped stirring rod 6 at the bottom of the auxiliary stirring shaft 5 to stir the sodium hydride liquid. The self-priming fan blades 7 fixed on the main stirring shaft 3 draw hydrogen gas from the stirring tank 1 into the sodium hydride liquid for stirring and reaction.

[0026] To enable the stirring sub-shaft 5 to rotate, a fixing ring 8 is fixedly installed on the inner top surface of the stirring tank 1. A fixing helical gear 9 is fixedly installed on the outer arc surface of the fixing ring 8. A fixing plate 10 is fixedly installed on the arc surface of the stirring main shaft 3. The arc surface of the stirring sub-shaft 5 and the outer surface of the fixing plate 10 are rotatably connected by ball bearings. A rotating helical gear 11 is rotatably connected to the upper arc surface of the stirring sub-shaft 5 by ball bearings. The tooth groove of the rotating helical gear 11 meshes with the teeth of the fixing helical gear 9.

[0027] By setting the fixed plate 10, the rotation of the stirring main shaft 3 driving the stirring secondary shaft 5 is made more stable and safe. The rotating helical gear 11 and the fixed helical gear 9 mesh, so that the rotation of the stirring secondary shaft 5 causes the rotating helical gear 11 to rotate around the fixed helical gear 9, so that the stirring secondary shaft 5 can rotate on its own while rotating, and the U-shaped stirring rod 6 stirs the sodium hydride liquid.

[0028] An air inlet 12 is provided at the upper part of the mixing tank 1. An air pump 13 is fixedly installed at the upper part of the mixing tank 1. An air supply pipe 14 is fixedly installed at the output end of the air pump 13. One end of the air supply pipe 14 is fixedly connected to the upper part of the air inlet 12. The other end of the air supply pipe 14 passes through and extends into the interior of the air inlet 12. A feed inlet 15 is also provided at the upper part of the mixing tank 1. A discharge valve 16 is fixedly installed at the lower part of the mixing tank 1.

[0029] By setting up an air pump 13, starting the air pump 13 can deliver hydrogen to the inside of the mixing tank 1 through the gas delivery pipe 14 and the air inlet 12, so that the hydrogen and sodium hydride liquid can be stirred and reacted. The feed inlet 15 is set up to add the sodium hydride liquid that needs to be stirred into the mixing tank 1, and the discharge valve 16 is set up to discharge the liquid after the stirring is completed.

[0030] Working principle: First, the sodium hydride liquid to be stirred and reacted is poured into the stirring tank 1 through the feed inlet 15. Then, the feed inlet 15 is closed to prevent gas leakage. Next, the motor 4 is started to drive the stirring main shaft 3 to rotate. The rotation of the stirring main shaft 3 drives the stirring auxiliary shaft 5 to rotate around the stirring main shaft 3. The angle between the axis of the stirring auxiliary shaft 5 and the axis of the stirring main shaft 3 is set to 40°, so that the stirring auxiliary shaft 5 and the stirring main shaft 3 stir the sodium hydride in different directions, making the sodium hydride stirring and reaction in the stirring tank 1 more complete. Then, the air pump 13 is started to open the gas pump. Hydrogen gas is delivered into the mixing tank 1 through the gas supply pipe 14 and the gas inlet 12. The self-priming fan blades 7 fixed on the mixing main shaft 3 draw the hydrogen gas in the mixing tank 1 into the sodium hydride liquid for stirring and reaction. The rotation of the mixing sub-shaft 5 causes the rotating helical gear 11 to rotate around the fixed helical gear 9, so that the mixing sub-shaft 5 can rotate on its own axis while rotating. The C-shaped stirring rod 6 at the lower end of the mixing sub-shaft 5 stirs the sodium hydride liquid at an inclined angle, so that the stirring and reaction of the sodium hydride liquid is more complete. Finally, the fully stirred and reacted liquid is discharged through the discharge valve 16.

[0031] The above are merely preferred embodiments of this utility model, but the scope of protection of this utility model is not limited thereto. Any equivalent substitutions or modifications made by those skilled in the art within the scope of the technology disclosed in this utility model, based on the technical solution and inventive concept of this utility model, should be included within the scope of protection of this utility model.

Claims

1. A sodium hydride hydrogenation self-absorption dispersion reaction apparatus, comprising a stirring tank (1), characterized in that: A support rod (2) is fixedly installed on the arc surface of the mixing tank (1). Multiple support rods (2) are arranged in a circumferential array around the arc surface of the mixing tank (1). A fully stirring mechanism is provided inside the mixing tank (1). The fully stirring mechanism realizes the stirring action of fully and completely hydrogenating sodium hydride. The stirring mechanism includes a stirring main shaft (3), the upper end of which is rotatably connected to the inner top surface of the stirring tank (1) via ball bearings. The upper end of the stirring main shaft (3) extends through and out of the upper part of the stirring tank (1). A motor (4) is fixedly installed on the upper part of the stirring tank (1). The output end of the motor (4) is fixedly connected to the upper part of the stirring main shaft (3) via a coupling. A stirring auxiliary shaft (5) is rotatably connected to the arc surface of the stirring main shaft (3) via ball bearings. The two ends of the stirring auxiliary shaft (5) extend through and out of the two sides of the stirring main shaft (3). The angle between the axis of the stirring auxiliary shaft (5) and the axis of the stirring main shaft (3) is set to 40°. The lower end of the stirring sub-shaft (5) is fixedly installed with a C-shaped stirring rod (6), and multiple C-shaped stirring rods (6) are arranged in a circular array around the arc surface of the stirring sub-shaft (5). The lower part of the stirring main shaft (3) is provided with a self-priming fan blade (7). A fixing ring (8) is fixedly installed on the inner top surface of the mixing tank (1). A fixing helical gear (9) is fixedly installed on the outer arc surface of the fixing ring (8). A fixing plate (10) is fixedly installed on the arc surface of the mixing main shaft (3). The arc surface of the mixing sub-shaft (5) is rotatably connected to the outer surface of the fixing plate (10) through ball bearings. A rotating helical gear (11) is rotatably connected to the upper arc surface of the mixing sub-shaft (5) through ball bearings. The tooth groove of the rotating helical gear (11) meshes with the gear teeth of the fixing helical gear (9).

2. The sodium hydride hydrogenation self-absorption dispersion reaction apparatus according to claim 1, characterized in that: An air inlet (12) is provided at the upper part of the mixing tank (1). An air pump (13) is fixedly installed at the upper part of the mixing tank (1). An air supply pipe (14) is fixedly installed at the output end of the air pump (13). One end of the air supply pipe (14) is fixedly connected to the upper part of the air inlet (12). One end of the air supply pipe (14) passes through and extends into the interior of the air inlet (12). A feed inlet (15) is also provided at the upper part of the mixing tank (1). A discharge valve (16) is fixedly installed at the lower part of the mixing tank (1).

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