Film thickness deviation measuring method, film thickness deviation measuring device, film manufacturing method, and film manufacturing device
The background-directed schlieren method allows for non-contact, safe, and cost-effective measurement of film thickness deviation using a light source and optical sensor array, addressing the limitations of existing methods.
Patent Information
- Application Number
- JP2025551802
- Authority / Receiving Office
- JP · JP
- Patent Type
- Patents
- Current Assignee / Owner
- Priority Date
- 2024-06-04
- Filing Date
- 2025-04-21
- Publication Date
- 2025-12-01
- Estimated Expiration
- 2045-04-21
AI Technical Summary
Existing methods for film thickness measurement, such as those using X-rays or optical interference, pose safety concerns or require complex and expensive device configurations.
Applying the background-directed schlieren method to measure film thickness deviation using a point or line light source and a one-dimensional or two-dimensional optical sensor array, calculating film thickness gradient without complex cross-correlation functions, enabling a simple and safe device configuration.
Enables non-contact measurement of film thickness deviation with a simple and safe device, reducing measurement complexity and cost.
Smart Images

Figure 0007777746000078 
Figure 0007777746000079 
Figure 0007777746000080
Abstract
Description
[Technical Field]
[0001] The present invention relates to a method and apparatus for measuring film thickness deviation, a method and apparatus for producing a film, and a method and apparatus for producing a film. [Background technology]
[0002] A widely used method for in-line, non-contact measurement of the thickness of a resin film involves transmitting light such as X-rays or infrared rays through the film and calculating the thickness in accordance with the Beer-Lambert law based on the attenuation rate of the transmitted light (see, for example, Patent Documents 1 and 2). Patent Document 3 also describes an optical interference film thickness measurement method in which a film is irradiated with white parallel light and the film thickness is calculated from the spectral intensity of the reflected light. [Prior art documents] [Patent documents]
[0003] [Patent Document 1] Japanese Patent Application Laid-Open No. 2006-275750 [Patent Document 2] Japanese Patent Application Publication No. 60-224002 [Patent Document 3] Japanese Patent Application Publication No. 7-280523 Summary of the Invention [Problem to be solved by the invention]
[0004] The method of transmitting X-rays and measuring the attenuation rate of transmitted light described in Patent Document 1 generally requires a controlled area, which poses a safety problem. Also, the optical interference method described in Patent Document 3 has a problem in that the device configuration is complex, which tends to make the device expensive.
[0005] The present invention has been made in light of the above-mentioned problems, and aims to provide a film thickness deviation measurement method and device that can obtain film thickness deviation in a non-contact manner using a simple and safe device configuration, as well as a film manufacturing method and device that use the measurement method and device. [Means for solving the problem]
[0006] The inventors conducted extensive research to solve the above-mentioned problems. As a result, they came up with the idea of applying the background-directed schlieren method, which is used to calculate the density gradient of a fluid, to measuring the thickness deviation of a solid film. However, the background-directed schlieren method typically calculates the amount of movement of a background image between two photographs using a cross-correlation function, which requires a large number of calculations. Therefore, the inventors came up with the idea of using a point or line light source instead of a background image, and acquiring the position of the light source detected by a one-dimensional or two-dimensional optical sensor array instead of calculating the amount of movement of the background image between two photographs. This enabled them to calculate a thickness deviation profile with a small amount of calculation, without the need for the calculation of a cross-correlation function, which requires a large number of calculations. Based on this knowledge, the inventors were able to calculate a film thickness deviation profile with a simple and safe device configuration, and further research led to the completion of the present invention.
[0007] That is, the gist of the present invention is as follows.
[0008] [1] A method for measuring the deviation of film thickness, the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point or line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and the one-point film thickness gradient measurement step of calculating the film thickness gradient from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the light source; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising:
number
number
number
[0009] [2] The method for measuring film thickness deviation according to [1], wherein the position of the optical sensor array is changed in accordance with the change in the position of the light source in the multi-point film thickness gradient measuring step. [3] A method for measuring the deviation of a film thickness, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point or line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and the one-point film thickness gradient measurement step of calculating the film thickness gradient from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the optical sensor array; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the optical sensor array and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising:
number
number
number
[0010] [4] The method for measuring film thickness deviation according to [3], wherein in the multipoint film thickness gradient measurement step, the position of the light source is changed in accordance with the change in the position of the optical sensor array.
[0011] [5] A method for measuring the deviation of a film thickness, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point or line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and the one-point film thickness gradient measurement step of calculating the film thickness gradient from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the irradiation direction of the light source; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the irradiation points of the light source and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising:
number
number
number
[0012] [6] The method for measuring film thickness deviation according to [5], wherein in the multipoint film thickness gradient measurement step, the position of the optical sensor array is changed in accordance with a change in the irradiation direction of the light source.
[0013] [7] A method for measuring the deviation of a film thickness, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point or line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and the one-point film thickness gradient measurement step of calculating the film thickness gradient from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the detection direction of the optical sensor array; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence between the detection direction of the optical sensor array and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising:
number
number
number
[0014] [8] The method for measuring film thickness deviation according to [7], wherein in the multipoint film thickness gradient measurement step, the position of the light source is changed in accordance with a change in the detection direction of the optical sensor array.
[0015] [9] the film is transported to pass between the light source and the photosensor array; The method for measuring a film thickness deviation according to any one of [1] to [8], wherein the integral path C is a line segment that is substantially perpendicular to the conveyance direction of the object to be measured.
[0016]
[10] An apparatus for measuring the deviation of a film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a light source position changing means for changing the position of the light source; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following equation (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the light source using the light source position changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure.
number
number
number
[0017]
[11] The film thickness deviation measuring device according to
[10] , further comprising an optical sensor position changing means for changing the position of the optical sensor array.
[0018]
[12] An apparatus for measuring the deviation of a film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; an optical sensor position changing means for changing the position of the optical sensor array; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following equation (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the optical sensor array using the optical sensor position changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure.
number
number
number
[0019]
[13] An apparatus for measuring the deviation of a film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a light source irradiation direction changing means for changing the irradiation direction of the light source; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following equation (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the irradiation direction of the light source using the light source irradiation direction changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure.
number
number
number
[0020]
[14] The film thickness deviation measuring device according to
[13] , further comprising an optical sensor position changing means for changing the position of the optical sensor array.
[0021]
[15] An apparatus for measuring the deviation of a film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a sensor detection direction changing means for changing the detection direction of the optical sensor array; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following equation (1): a multi-point film thickness gradient measuring unit that performs a multi-point film thickness gradient measuring step in which the single-point film thickness gradient measuring step is performed a plurality of times by changing the detection direction of the optical sensor array using the sensor detection direction changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure.
number
number
number
[0022]
[16] The film thickness deviation measuring device according to
[15] , further comprising a light source position changing means for changing the position of the light source.
[0023]
[17] A film manufacturing method in which a molten resin is discharged from a die having a plurality of lip gap adjustment means to form a film, The film discharged from the die is transported along a preset path line, the film is turned on between a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, without placing the film therebetween, and the original position, which is the position of the light source detected by the optical sensor array, is acquired; and the film is placed between the light source and the optical sensor array, and the light source is turned on, and the apparent position, which is the position of the light source detected by the optical sensor array, is acquired; and the one-point film thickness gradient measurement step is used to determine the film thickness gradient of the film from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the light source from the light source; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; a lip gap adjusting step of operating the lip gap adjusting means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value; A film manufacturing method comprising:
number
number
number
[0024]
[18] A film manufacturing apparatus that extrudes molten resin from a die having a plurality of lip gap adjustment means to form a film, a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, which are arranged opposite each other across a pass line along which the film discharged from the die is transported; A calculation unit for calculating a film thickness deviation of the film, a one-point film thickness gradient measurement unit that performs an original position acquisition step of turning on the light source without placing the film between the light source and the optical sensor array and acquiring the original position, which is the position of the light source detected by the optical sensor array, and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and then performs a one-point film thickness gradient measurement step of determining the film thickness gradient from the acquired original position and apparent position using the following equation (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the light source; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; a calculation unit having a lip gap adjusting unit that operates the lip gap adjusting means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value; A film manufacturing apparatus comprising:
number
number
number
[0025]
[19] The film manufacturing apparatus according to
[18] , further comprising a stretching machine for stretching the film downstream of the position on the pass line sandwiched between the light source and the optical sensor array. [Effects of the Invention]
[0026] According to the present invention, it is possible to obtain the film thickness deviation of a film in a non-contact manner using a simple and safe device configuration. [Brief explanation of the drawings]
[0027] [Figure 1] FIG. 1 is a conceptual diagram of an optical system for background-directed Schlieren imaging in a fluid. [Figure 2] 1 is a diagram showing a schematic configuration of an example of a film thickness deviation measuring device according to the present invention. [Figure 3] FIG. 2 is a diagram showing the configuration of a calculation unit in the film thickness deviation measuring device. [Figure 4] 1 is a diagram showing a schematic configuration of an example of a film manufacturing apparatus according to the present invention. [Figure 5] FIG. 1 is a diagram showing a schematic configuration of a film thickness deviation measuring device in an example. [Figure 6] FIG. 10 is a diagram showing a film thickness deviation profile obtained in an example. DETAILED DESCRIPTION OF THE INVENTION
[0028] Hereinafter, an embodiment of the present invention will be described with reference to the drawings. Note that the embodiment described below is an example of the present invention, and the invention is not limited to the following content.
[0029] In this invention, the background-oriented Schlieren method (hereinafter referred to as the "BOS method"), which is used to calculate the density gradient of a fluid, is applied to measuring the thickness deviation of a solid film. The BOS method for fluids measures the density gradient of a fluid by utilizing the phenomenon in which, when the background is viewed through the fluid, the background appears shifted due to a refractive index difference caused by the density gradient. Compared to the conventional Schlieren method, the BOS method for fluids has two advantages: the optical system for measurement is simple, and the density gradient can be quantified.
[0030] A conceptual diagram of the optical system of the BOS method for fluids is shown in Figure 1. As shown in Figure 1, the optical system for the BOS method for fluids consists of a measured object 11 made of fluid, a background image 12, and an imaging means 13. Figure 1 shows an apparent optical path 14 from the imaging means 13 and an actual optical path 15 due to the presence of the measured object 11. In this BOS method, a background image 12 is captured through the measured object 11. At this time, the position of the background image on the image captured by the imaging means 13 is shifted in proportion to the density gradient of the measured object 11.
[0031] In the phenomenon where the background image is captured with a deviation, the total deflection angle ε can be approximated by the ratio of the amount of deviation Δh of the background image 12 in the captured image to the distance d between the object under test 11 and the background image 12. In other words, it can be expressed as ε=Δh / d.
[0032] The total deflection angle ε is expressed by the following equation (3) by integrating the gradient ∂n / ∂x of the refractive index n of the object 11 in the direction perpendicular to the optical axis over the thickness (2 × Δz) of the object 11. Note that n0 in equation (3) is the refractive index experienced by light parallel to the optical axis.
number
[0033] Furthermore, the refractive index n and density ρ of the object 11 satisfy the relationship n=ρG+1, where G is the constant of the Gladstone-Dale law. Therefore, the density gradient ∂ρ / ∂x of the object 11 is expressed by the following equation (4).
number
[0034] In this invention, the optical system of the BOS method is used to obtain the gradient of the film thickness t of a solid film (film thickness deviation in the in-plane direction of the film), but the Gladstone-Dale law is not used. Instead, it is approximated that the only place where the in-plane gradient of the refractive index n of the object 11 to be measured occurs is at the part of the film thickness that comes into contact with air. This makes it possible to obtain the following equation (5):
number
[0035] where x is a position vector within the film plane, t(x) is the film thickness deviation obtained by subtracting the film thickness of the object 11 at the origin x=0 from the film thickness of the object 11 at the position x within the film plane, dt(x) / dx is the film thickness gradient expressed by the total in-plane differential of the film thickness deviation t(x), and n target is the refractive index of the film, n air is the refractive index of the atmosphere,
[0036] Furthermore, by substituting ε=Δh / d into equation (5), the following equation (1) is obtained.
number
number
[0037] where v is the unit tangent vector of the path C,
number
[0038] Specific examples of the integral path C include a line segment parallel to or perpendicular to the long or short side of the film, and a reciprocating scanning path in which the film is scanned parallel to one side, then slightly moved in a direction perpendicular to that side, and then scanned in the opposite direction parallel to that side, repeating this process.
[0039] (Film thickness deviation measuring device) Next, an example of a film thickness deviation measuring device of the present invention will be described. Fig. 2 shows a schematic configuration of an example of a film thickness deviation measuring device of the present invention. The film thickness deviation measuring device 20 shown in Fig. 2 comprises a light source 22 which is a point light source or a line light source, a one-dimensional or two-dimensional optical sensor array 23, a calculation unit 24, and a light source position changing means (not shown). The film 21 to be measured is placed between the light source 22 and the optical sensor array 23. It is preferable that the film thickness deviation measuring device 20 be installed in a dark room in order to accurately detect only the light emitted from the light source 22.
[0040] <Film> The film 21 to be measured, which is the object to be measured, is made of a material such as resin or glass that transmits light from the light source 21. This film includes thick resin or glass that is sometimes called a sheet.
[0041] The film 21 is disposed between the light source 22 and the optical sensor array 23 with its thickness direction being approximately parallel to the line connecting the light source 22 and the optical sensor array 23 .
[0042] <Light source> The light source 22 is either a point light source or a line light source. The light source 22 may be a display made of liquid crystal, LED, or organic EL that can be regarded as a point light source by illuminating only one or a few light-emitting elements, or a line light source that can be regarded as a line light source by illuminating only one or a few rows of light-emitting elements. The point light source or line light source may be, for example, an omnidirectional light source (i.e., one that does not irradiate only in a specific direction) or a directional light source (i.e., one that irradiates only in a specific direction).
[0043] The diameter of the point light source or the line width of the line light source is preferably 1 μm or more and 1000 μm or less, and more preferably 5 μm or more and 300 μm or less. By making the diameter or line width of the light source 22 1 μm or more, it is possible to reduce measurement errors in the position of the light source 22 while preventing the appearance of interference fringes. Furthermore, by making the diameter or line width of the light source 22 1000 μm or less, it is possible to reduce position measurement errors due to the size of the light source itself. It is more preferable that the diameter of the light source 22 or the line width of the line light source be 5 μm or more and 300 μm or less.
[0044] <Optical sensor array> The optical sensor array 23 is a collection of optical sensors 231, in which a plurality of optical sensors 231 are arranged one-dimensionally or two-dimensionally, and is disposed opposite the light source 22. For example, an image sensor can be used as the optical sensor array 23. Alternatively, an optical fiber cable for guiding detected light to the optical sensor 231 may be installed at the position of the optical sensor array 23 shown in FIG. 2, with the actual optical sensor array 23 being installed in a separate location. By providing an optical fiber cable in this manner, for example, when the light source 22, film 21, and optical sensor array 23 are arranged vertically from below in this order, the main body of the optical sensor array 23 can be installed separately, thereby simplifying the support material for the optical sensor array 23.
[0045] The optical sensor 231 detects light emitted from the light source 22, and the position of the light source 22 is obtained based on which optical sensor 231 in the optical sensor array 23 detects the light emitted from the light source 22. The optical sensor array 23 may output the position of the optical sensor 231 that detected the light with the highest intensity, or, as is more commonly used, may output the intensity of light detected by all of the optical sensors 231 in the optical sensor array 23. The output of the optical sensor array 23 is input to the calculation unit 24 and used to calculate the film thickness deviation profile of the film 21. The optical sensor 231 must be able to detect the wavelength of the light emitted from the light source 22.
[0046] In the optical sensor array 23, the smaller the interval between the optical sensors 231, the higher the resolution, which is preferable.
[0047] The width (area) of the optical sensor array 23 can be the width of the entire position where the optical sensor 231 can detect the light source 22. In other words, it is calculated from an extension line connecting the light source 22, whose position or irradiation direction is changed, and the film 21, and the total deflection angle ε obtained from the maximum film thickness gradient expected for the film 21. Alternatively, when the position of the optical sensor array 23 is changed in accordance with a change in the position or irradiation direction of the light source 22, the width of the optical sensor array 23 can be made narrower than the width when the position of the optical sensor 231 is not changed. In other words, it is sufficient that the width be centered on the irradiation direction of the light source 22 and be the total deflection angle ε obtained from the maximum film thickness gradient expected for the film 21.
[0048] <Arithmetic section> The calculation unit 24 executes a process of calculating the film thickness deviation of the film 21 based on the position of the light source 22 detected by the optical sensor array 23. As shown in FIG. 3, the calculation unit 24 has a single-point film thickness gradient measurement unit 241, a multi-point film thickness gradient measurement unit 242, and a film thickness deviation calculation unit 243.
[0049] <<One-point film thickness gradient measurement unit>> The one-point film thickness gradient measurement unit 241 performs an original position acquisition step in which the light source 22 is turned on without placing the film 21 between the light source 22 and the optical sensor array 23, and acquires the original position, which is the position of the light source 22 detected by the optical sensor array 23. It also performs an apparent position acquisition step in which the film 21 is placed between the light source 22 and the optical sensor array 23, the light source 22 is turned on, and an apparent position, which is the position of the light source 22 detected by the optical sensor array 23. Then, it performs a one-point film thickness gradient measurement step in which the film thickness gradient of the film 21 is calculated using the following equation (1) from the acquired original position and apparent position, and outputs the result.
number
[0050] If the optical sensor array 23 outputs the position of the optical sensor 231 that detected the light with the highest intensity, the output of the optical sensor array 23 may be input as the position of the light source 22. Alternatively, if the optical sensor array 23 outputs the intensities of light detected by all of the optical sensors 231, the position of the optical sensor 231 with the highest detected intensity may be calculated and input. Alternatively, the light intensity distribution may be approximated by, for example, a Gaussian distribution, and the position of the light source 22 may be calculated for continuous values including intermediate positions between the optical sensors 231 and input. By comparing the input position of the light source 22 with and without the film 21, it is possible to obtain a vector Δh that represents the amount of displacement from the actual position to the apparent position.
[0051] Refractive index n target and n air may be a fixed value, or may be calculated or manually input based on the temperature or the material of film 21. Furthermore, distance d between light source 22 and film 21 may be measured in advance and set to a fixed value. If the relative positions of light source 22 and film 21 change, distance d may be a variable value calculated or measured each time. In particular, if the direction of light irradiation from light source 22 is changed, the distance from light source 22 to the irradiation position on film 21 changes, so it is preferable to calculate or measure it each time.
[0052] <<Multi-point film thickness gradient measurement unit>> The multi-point film thickness gradient measurement unit 242 performs a multi-point film thickness gradient measurement process in which the single-point film thickness gradient measurement process for determining the film thickness gradient of the film 21 performed by the single-point film thickness gradient measurement unit 241 is repeated multiple times by changing the position of the light source 22, and outputs the results.
[0053] <<Film Thickness Deviation Profile Calculation Unit>> The film thickness deviation profile calculation unit 243 outputs the film thickness deviation t(x) of the film 21 calculated from the correspondence between the position of the light source 22 and the film thickness gradient of the film 21 output from the multipoint film thickness gradient measurement unit 242 using the following equation (2):
number
[0054] When determining the film thickness deviation profile t(x) of the film 21, the integral path C is not particularly limited, but can be a line segment parallel to or perpendicular to the long or short side of the film 21. Another example is a reciprocating scanning path in which the film 21 is scanned parallel to one side, then slightly moved in a direction perpendicular to that side, and then scanned in the opposite direction parallel to that side, repeating this process.
[0055] The film 21 can be configured to be transported so as to pass between the light source 22 and the optical sensor array 23, and the integration path C is a line segment that is approximately perpendicular to the transport direction of the film 21. In this case, the above equation (2) can be simplified to the following equation (6).
number
[0056] Since the position of the light source 22 is discrete, the discrete amount corresponding to each position of the light source 22 is expressed as x=kΔx in the above equation (6).
[0057] <Means for changing the light source position> The light source position changing means changes the position of the light source 22. Any means capable of changing the position of the light source 22 can be used as the light source position changing means. Such means include a means for mounting the light source 22 on an O-frame, C-frame, or the like and moving the light source 22 in a one-dimensional direction. Another example of the light source position changing means is a means for suspending the light source 22 on a two-axis actuator, as in a 3D printer, and moving it two-dimensionally. Furthermore, a means for moving the light source 22 three-dimensionally can also be used as the light source position changing means.
[0058] A single film thickness deviation measuring device 20 may have a plurality of light sources 22. In this case, in order to avoid confusing the plurality of light sources 22 with one another, it is preferable to stagger the light emission timing of the light sources 22, change the wavelength of the light sources 22, or install the light sources 22 at a distance sufficient to prevent confusion with one another. If the plurality of light sources 22 are sufficiently separated in terms of wavelength and physical distance, multiple points can be measured simultaneously, which is advantageous in terms of the scanning mechanism and time.
[0059] Furthermore, the film thickness deviation measuring device 20 may further include an optical sensor position changing means for changing the position of the optical sensor array 22. This allows the size (area) of the sensor array 23 to be reduced.
[0060] The above-described film thickness deviation measuring device is provided with a light source position changing means for changing the position of the light source 22. However, instead, an optical sensor position changing means for changing the position of the optical sensor array 23 may be provided. In this case, the position of the optical sensor array 23 is changed when performing the multi-point film thickness gradient measurement process. Examples of such a means include a means for mounting the optical sensor array 23 on an O-frame, C-frame, or the like and moving the optical sensor array 23 in a one-dimensional direction. Another example of the optical sensor position changing means is a means for suspending the optical sensor array 23 on a biaxial actuator, as in a 3D printer, and moving it two-dimensionally. Another example of the optical sensor position changing means is a means for moving the optical sensor array 23 three-dimensionally. In this case, the film thickness deviation measuring device 20 may further include a light source position changing means for changing the position of the light source 22. This allows the size (area) of the light source 22 to be reduced.
[0061] Furthermore, instead of providing a light source position changing means, a light source irradiation direction changing means for changing the irradiation direction of the light source 22 may be provided, and the irradiation direction of the light source 22 may be changed when performing the multi-point film thickness gradient measurement process. An example of the light source irradiation direction changing means is a means for changing the irradiation direction of light from the light source 22 by changing the orientation of the light source 22 itself or a support material on which the light source 22 is installed. In this case, the film thickness deviation measuring device 20 may further include an optical sensor position changing means for changing the position of the optical sensor array 23. This allows the size (area) of the optical sensor array 23 to be reduced.
[0062] Furthermore, instead of providing a light source position changing means, a sensor detection direction changing means for changing the detection direction of the optical sensor array 23 may be provided, and the detection direction of the optical sensor array 23 may be changed when performing the multi-point film thickness gradient measurement process. An example of the sensor detection direction changing means is a means for changing the detection direction of the optical sensor array 23 by changing the orientation of the optical sensor array 23 itself or the support material on which the optical sensor array 23 is installed. In this case, the film thickness deviation measuring device 20 may further include a light source position changing means for changing the position of the light source 22. This allows the size (area) of the light source 22 to be reduced.
[0063] (Method for measuring film thickness deviation) The method for measuring film thickness deviation according to the present invention includes an original position acquisition step of turning on a light source, which is a point or line light source disposed opposite to a light source, and a one-dimensional or two-dimensional optical sensor array without placing a film to be measured, and acquiring an original position, which is the position of the light source detected by the optical sensor array; an apparent position acquisition step of placing the film between the light source and the optical sensor array, turning on the light source, and acquiring an apparent position, which is the position of the light source detected by the optical sensor array; a single-point film thickness gradient measurement step of determining a film thickness gradient of the film using the following equation (1) from the acquired original position and apparent position; a multi-point film thickness gradient measurement step of performing the single-point film thickness gradient measurement step multiple times by changing the position at which light from the light source is irradiated onto the film; and a film thickness deviation profile calculation step of determining a film thickness deviation profile of the film using the following equation (2) from the correspondence between the position at which light from the light source is irradiated onto the film obtained by the multi-point film thickness gradient measurement step and the film thickness gradient of the film. Equipped with.
number
number
[0064] <One-point film thickness gradient measurement process> A one-point film thickness gradient measurement process is performed, which includes an actual position acquisition process and an apparent position acquisition process.
[0065] <<Original position acquisition process>> First, the light source 22, which is a point or line light source arranged opposite to the one-dimensional or two-dimensional optical sensor array 23, is turned on without placing the film 21 to be measured, and the original position, which is the position of the light source 22 detected by the optical sensor array 23, is obtained.
[0066] <<Apparent position acquisition process>> Next, the film 21 is placed between the light source 22 and the optical sensor array 23, the light source 22 is turned on, and the apparent position, which is the position of the light source 22 detected by the optical sensor array 23, is obtained.
[0067] Then, the film thickness gradient of the film 21 is calculated using the above formula (1) from the acquired real position and apparent position.
[0068] <Multi-point film thickness gradient measurement process> The one-point film thickness gradient measurement process is carried out multiple times by changing the position where the light from the light source 22 is irradiated onto the film 21 .
[0069] <Thickness deviation profile calculation process> Next, the thickness deviation profile of the film 21 is calculated using the above formula (2) from the correspondence relationship between the position of the light source 22 and the thickness gradient of the film 21 obtained in the multipoint thickness gradient measurement process.
[0070] In the multipoint film thickness gradient measurement process, the position of the optical sensor array 23 can be changed in accordance with the change in the position of the light source 22. This allows the size (area) of the sensor array 23 to be reduced.
[0071] In the above-described film thickness deviation measurement method, the position of the light source 22 is changed in the multi-point film thickness gradient measurement step, but instead, the position of the optical sensor array 23 may be changed. In this case, in the film thickness deviation profile calculation step, the film thickness deviation profile is calculated using the above formula (2) based on the correspondence between the position of the optical sensor array 23 and the film thickness gradient. Furthermore, in the multi-point film thickness gradient measurement step, the position of the light source 22 can be configured to be changed in accordance with the change in the position of the optical sensor array 23. This allows the size (area) of the light source 22 to be reduced.
[0072] Furthermore, in the multi-point film thickness gradient measurement process, instead of changing the position of the light source 22, the irradiation direction of the light source 22 may be changed. In this case, in the multi-point film thickness gradient measurement process, the position of the optical sensor array 23 can be changed in accordance with the change in the irradiation direction of the light source 22. This allows the size (area) of the optical sensor array 22 to be reduced.
[0073] Furthermore, in the multi-point film thickness gradient measurement step, the detection direction of the optical sensor array 23 may be changed instead of changing the position of the light source 22. In this case, in the film thickness deviation profile calculation step, the film thickness deviation profile is calculated using the above formula (2) based on the correspondence between the detection direction of the optical sensor array 23 and the film thickness gradient. Also, in the multi-point film thickness gradient measurement step, the position of the light source 22 can be changed in accordance with the change in the detection direction of the optical sensor array 23. This allows the size (area) of the light source 22 to be reduced.
[0074] The film 21 is transported so as to pass between the light source 22 and the optical sensor array 23, and the integral path C used to calculate the above formula (2) can be a line segment that is approximately perpendicular to the transport direction of the film 21.
[0075] The thickness deviation of the film 21 obtained by the above method can be displayed using known visualization techniques. When the thickness deviation is calculated in only one specific direction, it is preferable to display it as a line graph. When the thickness deviation is calculated in an in-plane direction, it is preferable to display it as an overlaid line graph or a heat map. In this case, the thickness deviation is, for example, the thickness of the film 21 at the measurement point minus the thickness of the film 21 at the origin. For this reason, it may be more preferable to display the thickness as an absolute value by adding the thickness of the film 21 at the origin calculated by an appropriate method. Examples of methods for obtaining the thickness of the film 21 at the origin include measuring only one point using a known thickness meter such as a contact or transmission type, and using a nominal thickness regardless of the actual thickness.
[0076] (Film manufacturing equipment) Next, a film manufacturing apparatus according to the present invention will be described. The film manufacturing apparatus according to the present invention is a film manufacturing apparatus that extrudes molten resin from a die having a plurality of lip gap adjustment means to form a film, and includes a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, which are arranged opposite each other across a path line along which the film extruded from the die is transported, and a calculation unit that calculates a film thickness deviation of the film, and includes an original position acquisition step of turning on the light source without placing the film between the light source and the optical sensor array and acquiring an original position, which is the position of the light source detected by the optical sensor array, and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source, and acquiring an apparent position, which is the position of the light source detected by the optical sensor array. and a lip gap adjusting unit that operates the lip gap adjusting means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value.
number
number
[0077] Figure 4 shows a schematic configuration of an example of a film production apparatus according to the present invention. The film production apparatus 30 shown in Figure 4 includes an extruder 35, a T-die 36, a cooling roll 37, a stretching machine 38, and a winder 39. The T-die 36 has a plurality of lip gap adjustment means 361. The film production apparatus 30 also includes a film thickness deviation measurement device having a light source 22, an optical sensor array 23, and a calculation unit 24.
[0078] <Extruder> The extruder 35 is equipped with one or more feeders or hoppers, and melts and kneads multiple types of resins and fillers as necessary. The extruder 35 can be either a single-screw extruder or a twin-screw extruder, and may be a multi-stage extruder. Furthermore, multiple extruders 35 may be provided and connected to a T-die 36. Note that it is preferable to provide a filter, a vent, and a gear pump to improve the quality of the extruded resin and stabilize the extrusion rate. The extruder 35 may have a known configuration.
[0079] <Tダイ> The T-die 36 discharges the molten resin extruded from the extruder 35 through a gap and continuously forms a resin film 31 having a target thickness. If the film 31 to be produced has a multi-layer structure, either the feed block method or the multi-manifold method can be applied. The feed block method is a method in which the molten resin flows together before entering the T-die. The multi-manifold method is a method in which the single layers are spread inside the T-die and then joined together near the lip.
[0080] <<Lip gap adjustment means>> A plurality of lip gap adjusting means 361 are provided along the lip longitudinal direction of the T-die 36. The lip gap adjusting means 361 adjusts the width of the lip gap in accordance with a command from the lip gap adjusting unit 40 or manual operation, thereby adjusting the film thickness of the molten resin and the film.
[0081] A known configuration may be employed as the lip gap adjustment mechanism of the lip gap adjustment means 361. Suitable examples of such mechanisms include a method in which the amount of depression is changed by rotating a threaded bolt, a heat bolt type in which a cartridge heater is built in and the lip gap is thermally expanded and contracted, and a method in which adjustment is made by applying hydraulic pressure to a bolt or a T-die.
[0082] <Cooling roll> The cooling roll 37 cools and solidifies the molten resin extruded from the lip gap of the T-die 36, and forms it into a film.
[0083] The cooling roll 37 is preferably equipped with a pinning device such as an electrostatic application type, a suction chamber type, or an air knife type, or a touch roll, for the purposes of suppressing thickness variations and improving surface properties of the film 31. In addition, to increase the cooling rate of the molten resin, part of the cooling roll may be immersed in water or sprayed with water. <Stretching machine> The stretching machine 38 is a piece of equipment that is optionally installed in the film production apparatus 30 as needed, and is a device that stretches the film formed by the cooling roll 37. The stretching machine 38 is disposed downstream of the position on the pass line that is sandwiched between the light source 22 and the optical sensor array 23. Stretching of the film may be performed as needed, and the film to be produced does not need to be stretched.
[0084] When stretching is performed using the stretching machine 38, various stretching methods can be applied. That is, a method of stretching only in the machine direction (MD direction: longitudinal direction), a method of stretching only in the width direction (TD direction), a method of sequentially stretching in the MD direction and the TD direction, and a method of simultaneously stretching in the MD direction and the TD direction can be applied. Furthermore, for example, a method of sequentially stretching in the MD direction and the TD direction and then re-stretching in the MD direction or the TD direction can be applied. Regarding the stretching treatment, it is preferable to select and use a stretching method, including no stretching, depending on the type of resin of the film and the application.
[0085] Furthermore, for longitudinal stretching in the MD direction, either single-stage stretching using a pair of rolls with a speed difference or multi-stage stretching using multiple pairs of rolls can be suitably applied. Furthermore, for the method of heating the film for stretching, either a method using a preheating roll or a non-contact heating method using an infrared heater or the like can be suitably used. Furthermore, near the outlet of the stretching machine 38, the film may be subjected to a surface treatment such as a heat setting treatment for relaxing the film while heating or a corona treatment. The measured value of the film thickness deviation obtained by the film thickness deviation measuring device can also be used to control the stretching machine 38.
[0086] <Rewinder 39> The winding machine 39 is a device that winds up the produced film into a roll. The film 31 wound into a roll becomes the product to be shipped.
[0087] It is preferable to install quality assurance equipment such as a surface inspection device, a pinhole inspection device, and a film thickness meter just before the winder 39. It is also preferable to trim the product to the desired width using a slitter or trimmer. Oscillation winding may be performed to prevent gauge bands during winding.
[0088] <Film thickness deviation measuring device> The film thickness deviation measuring device may have a similar configuration to the film thickness deviation measuring device 20 described above, and detailed description thereof will be omitted.
[0089] In the film manufacturing apparatus 30, the film 31 is transported along a preset path line, so that the integral path C is preferably a line segment that is approximately perpendicular to the transport direction of the film 31.
[0090] The light source 22 and the optical sensor array 23 are preferably positioned opposite each other across the pass line of the film 31. In the example shown in FIG. 4, the light source 22 and the optical sensor array 23 are positioned on the pass line between the chill roll 37 and the stretching machine 38, but they may also be positioned before or downstream of the stretching machine 38. That is, the film thickness deviation measurement unit consisting of the light source 22 and the optical sensor array 23 can be installed anywhere from downstream of the T-die 36 to upstream of the winding machine 39. However, considering the speed of feedback control and the possibility that the refractive index of the film 31 may change due to processing by the stretching machine 38, it is preferable to install the light source 22 and the optical sensor array 23 upstream of the stretching machine 38. Furthermore, if the distance between the lip of the T-die 36 and the chill roll 37 increases due to the installation of the light source 22 and the optical sensor array 23, there is a risk of film thickness unevenness in the MD and necking in the TD. For this reason, the film thickness deviation measurement unit is preferably installed downstream of the chill roll 37.
[0091] The light source 22 and the optical sensor array 23 are preferably installed on the same structure to prevent misalignment between the light source 22 and the optical sensor array 23 due to vibrations during operation, etc. Furthermore, it is more preferable that the installed structure can be pulled out offline during operation to calibrate the misalignment.
[0092] Other structures, such as glass windows, may be present in the gap between the film 31 and the light source 22, or between the film 31 and the optical sensor array 23. However, the structures must be able to transmit the light emitted from the light source 22 with sufficient intensity. If the other structures have a film thickness deviation, it is preferable to correct the calculated film thickness deviation of the film 31. However, if the distance between the light source 32 and the other structures is short and only has an acceptable effect on the calculated film thickness deviation of the film 31, correction may not be necessary. It is also more preferable that the other structures have no film thickness deviation.
[0093] The thickness deviation of the film 31 obtained by the above method can be displayed by a known visualization method. In the film manufacturing apparatus, it is preferable to display only the thickness deviation in the TD direction, from the viewpoint of feeding back the calculated thickness deviation information to the control of the lip gap adjustment means. Furthermore, in order to know the fluctuation of the thickness deviation over time, it is more preferable to display, for example, a line graph with the TD direction coordinate on the horizontal axis and the thickness deviation on the vertical axis, with the line color changing over time.
[0094] <Lip gap adjustment part> The lip gap adjustment unit 40 generates and outputs a command for feedback control of the film thickness based on information about the film thickness deviation in the width direction input from the calculation unit 24 of the film thickness deviation measuring device. The lip gap adjustment unit 40 compares the actual film thickness deviation profile of the film 31 input from the calculation unit 24 of the film thickness deviation measuring device with a pre-input ideal film thickness deviation profile of the film 31. Then, it controls the lip gap adjustment means 361 to increase the lip gap corresponding to the TD direction coordinate in order to thicken the portion where the actual film thickness deviation is thinner than the ideal film thickness deviation. It also controls the lip gap adjustment means 361 to decrease the lip gap corresponding to the TD direction coordinate in order to thin the portion where the actual film thickness deviation is thicker than the ideal film thickness deviation.
[0095] In this way, the lip gap adjustment unit 40 controls the actual film thickness deviation so that it approximates the ideal film thickness deviation. That is, the measured film thickness deviation profile is compared with the ideal film thickness deviation profile of the film 31 to determine the difference in film thickness at the position corresponding to each lip gap adjustment means 361 in the film width direction. Then, each lip gap adjustment means 361 is feedback-controlled so that the difference falls within a predetermined range.
[0096] Here, necking occurs in the film 31 when it is discharged from the T-die 36, for example. For this reason, the distance from the TD center to a specific position on the film 31 calculated by the calculation unit 24 of the film thickness deviation measuring device generally differs from the distance from the TD center to the specific position on the molten resin when it is discharged from the T-die lip. Therefore, it is preferable that the lip gap adjustment unit 40 use various known methods to determine which lip gap adjustment means 361 to issue a command to when the difference between the actual film thickness deviation and the ideal film thickness deviation is detected at a specific TD coordinate.
[0097] It is also known that accuracy is improved by simultaneously operating multiple lip gap adjustment means 361 in consideration of influence coefficients, rather than operating only one. For this reason, it is preferable to operate multiple lip gap adjustment means 361 simultaneously by weighting based on the results of calculations using various known methods.
[0098] (Film manufacturing method) Next, a film manufacturing method according to the present invention will be described. The film manufacturing method according to the present invention is a film manufacturing method in which molten resin is discharged from a die having a plurality of lip gap adjustment means to form a film, and the film discharged from the die is transported along a preset path line, and includes an original position acquisition step in which, without placing the film between a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, the light source is turned on and the original position, which is the position of the light source detected by the optical sensor array, is acquired, and an apparent position acquisition step in which, with the film placed between the light source and the optical sensor array, the light source is turned on and the apparent position, which is the position of the light source detected by the optical sensor array, is acquired. the position acquisition process, and the method comprises a single-point film thickness gradient measurement process for determining the film thickness gradient of the film using the following equation (1) from the acquired actual position and apparent position; a multi-point film thickness gradient measurement process for performing the single-point film thickness gradient measurement process multiple times by changing the position of the light source; a film thickness deviation profile calculation process for calculating the film thickness deviation profile using the following equation (2) from the correspondence between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement process; and a lip gap adjustment process for operating the lip gap adjustment means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value.
number
number
[0099] In the film manufacturing method according to the present invention, the original position acquisition process, apparent position acquisition process, single-point film thickness gradient measurement process, and multi-point film thickness gradient measurement process are the same as those in the film thickness deviation measurement method according to the present invention described above, and therefore their explanations will be omitted.
[0100] <Lip gap adjustment process> Based on the film thickness deviation profile calculated in the film thickness deviation profile calculation step, the lip gap adjustment unit 40 is operated so that the film thickness deviation at each point on the film 31 is equal to or less than a target value.
[0101] In the above film manufacturing method, as in the film thickness deviation measuring method of the present invention, instead of changing the position of light source 22 in the multi-point film thickness gradient measuring step, the direction of irradiation of light from light source 22 onto film 21 can be changed. Furthermore, instead of changing the position of light source 22 in the multi-point film thickness gradient measuring step, this can be done by changing the position of film 21.
[0102] Furthermore, similarly to the film thickness deviation measuring method of the present invention, in the multipoint film thickness gradient measuring process, the position of the optical sensor array 23 can be changed in accordance with the change in the irradiation position of the light from the light source 22 onto the film 21. This allows the size (area) of the sensor array 23 to be reduced.
[0103] Although the embodiments of the present invention have been described above, the present invention is not limited to these, and various modifications are possible without departing from the spirit of the invention. Furthermore, the films 21 and 31 in the above description include a resin composition and glass that are generally called a sheet because they are relatively thick. [Example]
[0104] Examples of the present invention will be described below, but the present invention is not limited to these examples.
[0105] (Measurement conditions in this example) In this example, the film 21 to be measured was a PET film extruded using a T-die method with an average thickness of 86 μm and a standard deviation of 4 μm in the TD direction. The light source was a line light source, with only one row of light-emitting elements lit in the LCD. The LCD was 15.6 inches and had a Full HD (1920 × 1080) resolution. A CMOS camera was used as the optical sensor array. The CMOS camera had a resolution of 4000 × 3000. As shown in Figure 5, the LCD display 52, PET film 51, and CMOS camera 53 were arranged vertically in this order. The vertical direction is perpendicular to the surface of the film 51. The vertical distance between the PET film 51 and the LCD display 52 was 120 mm, and the vertical distance between the PET film 51 and the optical sensor array 53 was 550 mm. The TD direction of the PET film 51 and the light emitting element row 521 that illuminated the light emitting elements of the liquid crystal display 52 were arranged so as to be perpendicular to each other.
[0106] (Measurement process of film thickness deviation) First, without placing a PET film, only one specific row of light-emitting element rows 521 in the liquid crystal display 52 was turned on, and the position of the light-emitting element rows 521 was acquired by the CMOS camera 53 and determined as the original position. Furthermore, the lit light-emitting element rows 521 were moved row by row, and the correspondence relationship between the positions of the lit light-emitting element rows 521 on the liquid crystal display 52 and the original positions was acquired. Next, PET film 51 was placed between liquid crystal display 52 and CMOS camera 53 in the above-mentioned positional relationship. Then, only one specific row of light-emitting element rows 521 in liquid crystal display 51 was turned on, and the positions of the light-emitting elements were acquired by CMOS camera 53 and used as apparent positions. Furthermore, the lit light-emitting element rows 521 were moved row by row, and the correspondence between the positions of the lit light-emitting element rows 521 in liquid crystal display 52 and their apparent positions was acquired. Through the above operations, the original position and apparent position corresponding to the position of the lit light-emitting element row 521 could be obtained. Note that the above original position and apparent position are affected by the distortion of the CMOS camera, so the correspondence between pixel coordinates and actual coordinates is not constant across the entire field of view. Therefore, the camera was calibrated in advance, and the actual coordinates were calculated using the obtained camera matrix and distortion coefficients.
[0107] Next, from the acquired actual position and apparent position, Δh was calculated as the amount of displacement in the TD direction from the actual position to the apparent position, and the film thickness gradient dt(x) / dx of the PET film corresponding to the lit light-emitting element row 521 was calculated using the following equation (1).
number
[0108] Furthermore, the TD direction film thickness deviation profile t(x) of the PET film was calculated from the film thickness gradient dt(x) / dx of the PET film obtained above using the following equation (6).
number
[0109] The TD-direction film thickness deviation profile t(x) of the PET film obtained as described above is shown in Figure 6. For reference, Figure 6 also shows the film thickness profile obtained using a contact-type film thickness gauge with a dashed line. Note that the film thickness deviation measurement method of the present invention determines the amount of film thickness change from the origin, but not the absolute value of the film thickness. Therefore, for ease of viewing, a constant value has been added to the film thickness deviation profile t(x) in Figure 6 so that the absolute value roughly matches that of the contact-type film thickness profile. Figure 6 confirms that the film thickness deviation profile obtained using the film thickness deviation measurement method of the present invention and the film thickness profile obtained using a contact-type film thickness gauge generally match. As described above, it has been found that the present invention makes it possible to obtain film thickness deviation in a non-contact manner using a simple and safe device configuration. [Industrial Applicability]
[0110] According to the present invention, it is possible to obtain the film thickness deviation of a film in a non-contact manner using a simple and safe device configuration. [Explanation of symbols]
[0111] 11 Object to be measured 12 background images 13 Imaging means 14 Apparent light path 15 Actual light path 20 Film thickness deviation measuring device 21,31 Film 22 Light source 23 Optical sensor array 231 Optical Sensor 24 Arithmetic section 241 One-point film thickness gradient measurement unit 242 Multi-point film thickness gradient measurement unit 243 Film Thickness Deviation Calculation Unit 30 Film manufacturing equipment 35 Extruder 36 T-die 361 Lip gap adjustment means 37 Cooling Roll 38 Stretching machine 39 Winder 40 Lip gap adjustment part 51 PET film 52 LCD display 521 A row of light-emitting elements in a liquid crystal display 53 CMOS camera
Claims
1. A method for measuring film thickness deviation, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point light source or a line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and determining the film thickness gradient of the film from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the light source; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the position of the light source and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising: [Equation 1] [Equation 2] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 3] is.
2. 2. The method for measuring film thickness deviation according to claim 1, wherein the position of the optical sensor array is changed in accordance with the change in the position of the light source in the multi-point film thickness gradient measuring step.
3. A method for measuring film thickness deviation, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point light source or a line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and determining the film thickness gradient of the film from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the optical sensor array; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the optical sensor array and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising: [Equation 4] [Equation 5] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 6] is.
4. 4. The method for measuring film thickness deviation according to claim 3, wherein the position of the light source is changed in accordance with the change in the position of the optical sensor array in the multi-point film thickness gradient measuring step.
5. A method for measuring film thickness deviation, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point light source or a line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and determining the film thickness gradient of the film from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the irradiation direction of the light source; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising: [Equation 7] [Equation 8] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 9] is.
6. 6. The method for measuring film thickness deviation according to claim 5, wherein the position of the optical sensor array is changed in accordance with a change in the irradiation direction of the light source in the multipoint film thickness gradient measuring step.
7. A method for measuring film thickness deviation, comprising: the film thickness gradient measurement step includes an original position acquisition step of turning on the light source without placing a film to be measured between a point light source or a line light source disposed opposite to the light source and a one-dimensional or two-dimensional optical sensor array, and acquiring the original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of turning on the light source with the film disposed between the light source and the optical sensor array, and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and determining the film thickness gradient of the film from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the detection direction of the optical sensor array; a thickness deviation profile calculation step of calculating a thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the detection direction of the optical sensor array and the thickness gradient of the film obtained by the multi-point thickness gradient measurement step; A method for measuring film thickness deviation comprising: [Equation 10] [0011] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [0012] is.
8. 8. The method for measuring film thickness deviation according to claim 7, wherein the position of the light source is changed in accordance with a change in the detection direction of the optical sensor array in the multipoint film thickness gradient measuring step.
9. the film is transported to pass between the light source and the photosensor array; 9. The film thickness deviation measuring method according to claim 1, wherein the integral path C is a line segment that is substantially perpendicular to the transport direction of the object to be measured.
10. An apparatus for measuring deviation in film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a light source position changing means for changing the position of the light source; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following formula (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the light source using the light source position changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure. [0013] [0014] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 15] is.
11. The film thickness deviation measuring device according to claim 10, further comprising an optical sensor position changing means for changing the position of the optical sensor array.
12. An apparatus for measuring deviation in film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; an optical sensor position changing means for changing the position of the optical sensor array; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following formula (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the optical sensor array using the optical sensor position changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure. [0016] [Equation 17] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 18] is.
13. An apparatus for measuring deviation in film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a light source irradiation direction changing means for changing the irradiation direction of the light source; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following formula (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the irradiation direction of the light source using the light source irradiation direction changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure. [Equation 19] [Equation 20] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 21] is.
14. The film thickness deviation measuring device according to claim 13, further comprising an optical sensor position changing means for changing the position of the optical sensor array.
15. An apparatus for measuring deviation in film thickness, a light source that is a point light source or a line light source; a one-dimensional or two-dimensional optical sensor array disposed opposite the light source; a sensor detection direction changing means for changing the detection direction of the optical sensor array; a calculation unit for calculating a film thickness deviation of the film, The calculation unit a one-point film thickness gradient measurement unit that performs a one-point film thickness gradient measurement step of determining a film thickness gradient of the film from the obtained original position and apparent position by turning on the light source without placing the film between the light source and the optical sensor array and obtaining an original position, which is the position of the light source detected by the optical sensor array; and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and obtaining an apparent position, which is the position of the light source detected by the optical sensor array, using the following formula (1): a multi-point film thickness gradient measuring unit that performs a multi-point film thickness gradient measuring step in which the single-point film thickness gradient measuring step is performed a plurality of times by changing the detection direction of the optical sensor array using the sensor detection direction changing means; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the light source irradiation points and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; A film thickness deviation measuring device having the above structure. [Equation 22] [Equation 23] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [0000] is.
16. The film thickness deviation measuring device according to claim 15, further comprising a light source position changing means for changing the position of the light source.
17. A film manufacturing method in which a molten resin is discharged from a die having a plurality of lip gap adjustment means to form a film, comprising: The film discharged from the die is transported along a preset path line, the film is turned on without placing a film between a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, and an original position acquisition step of acquiring the original position, which is the position of the light source detected by the optical sensor array; and the film is placed between the light source and the optical sensor array, and the light source is turned on, and an apparent position acquisition step of acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and a one-point film thickness gradient measurement step of calculating the film thickness gradient from the acquired original position and apparent position using the following formula (1): a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed a plurality of times by changing the position of the light source from the light source; a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following formula (2) based on the correspondence relationship between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; a lip gap adjusting step of operating the lip gap adjusting means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value; A film manufacturing method comprising: [Equation 25] [Equation 26] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [0000] is.
18. A film manufacturing apparatus that extrudes molten resin from a die having a plurality of lip gap adjustment means to form a film, a light source, which is a point light source or a line light source, and a one-dimensional or two-dimensional optical sensor array, which are arranged opposite each other across a pass line along which the film discharged from the die is transported; A calculation unit for calculating a film thickness deviation of the film, a one-point film thickness gradient measurement unit that performs an original position acquisition step of turning on the light source without placing the film between the light source and the optical sensor array and acquiring the original position, which is the position of the light source detected by the optical sensor array, and an apparent position acquisition step of placing the film to be measured between the light source and the optical sensor array and turning on the light source and acquiring the apparent position, which is the position of the light source detected by the optical sensor array, and then performs a one-point film thickness gradient measurement step of determining the film thickness gradient from the acquired original position and apparent position using the following equation (1): a multi-point film thickness gradient measurement unit that performs a multi-point film thickness gradient measurement step in which the single-point film thickness gradient measurement step is performed multiple times by changing the position of the light source; a film thickness deviation profile calculation unit that performs a film thickness deviation profile calculation step of calculating a film thickness deviation profile of the film using the following equation (2) based on the correspondence relationship between the position of the light source and the film thickness gradient of the film obtained by the multi-point film thickness gradient measurement step; a calculation unit having a lip gap adjusting unit that operates the lip gap adjusting means based on the film thickness deviation profile so that the film thickness deviation at each point on the film is equal to or less than a target value; A film manufacturing apparatus comprising: [0000] [0000] where: x: position vector in the plane of the film t(x): film thickness deviation obtained by subtracting the film thickness at the origin x = 0 from the film thickness at position x; dt(x) / dx: film thickness gradient expressed by the total in-plane differential of the film thickness deviation t n target : refractive index of the film n air : Refractive index of the atmosphere Δh: a vector representing the amount of displacement from the original position to the apparent position d: distance between the light source and the film v: unit tangent vector of path C [Equation 30] is.
19. The film manufacturing apparatus according to claim 18 , further comprising a stretching machine that stretches the film, located downstream of a position on the pass line that is sandwiched between the light source and the optical sensor array.
Citation Information
Patent Citations
Method for measuring see-through characteristics of plastic film
JP1992143641A
Defect inspection device
JP2001059795A
Illumination system for stereolithography apparatus
JP2015171820A
Imaging system for surface inspection
JP2024069627A
Machine direction line film inspection
US20210278347A1