Preparation process of copper-based composite materials by drawing, rolling, and ultrasonic friction bonding

By employing a graphene coating and inert gas protection process involving drawing, rolling, and ultrasonic friction consolidation, the corrosion problem of copper-based composite materials in oxidizing environments has been solved, enabling the preparation of high-performance copper-based composite materials.

CN115846451BActive Publication Date: 2026-03-10YANTAI IND RES XINHE NEW MATERIAL CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2022-11-07
Publication Date
2026-03-10

AI Technical Summary

Technical Problem

Copper-based composite materials are prone to oxidation in the presence of oxygen, which leads to corrosion and affects their performance and usability.

Method used

High-performance copper-based composite materials were prepared by using graphene as an anti-corrosion coating and combining drawing, rolling and ultrasonic friction consolidation processes, through graphene immersion, inert gas protection and high-frequency vibration rolling.

Benefits of technology

It effectively prevents the oxidation of copper-based materials, improves conductivity and strength, enhances material performance, and shortens the production process.

✦ Generated by Eureka AI based on patent content.

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Abstract

This invention discloses a process for preparing a copper-based composite material using drawing, rolling, and ultrasonic friction consolidation. The process includes the following steps: copper wire from a winding machine is introduced into a wire polishing machine for polishing; a graphene aqueous solution is prepared in a graphene immersion tank; after immersion, the copper wire is removed, and the graphene aqueous solution on the surface of the copper wire is dried using a hot air blower; several copper wires in a rolling groove are initially compressed using a pressure roller; the compression of the copper wires by the pressure roller achieves initial consolidation; finally, the initially consolidated copper wires are rolled using an ultrasonic roller, ultimately forming a high-performance copper-based composite material. The process involves rolling the copper wires, using a pressure roller for initial consolidation, and using an ultrasonic roller to perform high-frequency vibration rolling on the initially consolidated copper matrix, thus rapidly obtaining a high-performance copper-based composite material with high conductivity.
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Description

TECHNICAL FIELD

[0001] The application belongs to the technical field of copper-based material, and particularly relates to a drawing, rolling and ultrasonic friction consolidation composite copper-based composite material preparation process. BACKGROUND

[0002] In the preparation of the copper-based composite material, when the copper wire is used in an oxygen environment, a challenge is that the surface of the copper-based material will be oxidized over time, which eventually causes corrosion. It is found in research that graphene can be used as a candidate material for an anti-corrosion coating of the surface of the copper-based material. The use of graphene can protect the copper wire from deep penetrating oxidation, greatly reducing the oxidation rate of the copper, and becoming the first process in the preparation process of the copper-based composite material. The excellent performance of the copper-based composite material can enhance the use performance of the copper-based material.

[0003] Patent CN202011217598.1 discloses a copper-based composite material and a preparation method thereof. The copper-based composite material comprises a copper matrix and first ceramic particles, second ceramic particles and ceramic whiskers dispersed in the copper matrix. The first ceramic particles, micron-sized second ceramic particles and ceramic whiskers are coupled with each other. The first ceramic particles are used to enhance the strength and hardness of the matrix, and further enhance the holding force of the copper matrix on the second ceramic particles and the ceramic whiskers. Finally, the strength and wear resistance of the copper-based composite material are enhanced while the electrical conductivity of the material is ensured. Patent CN201210095598.8 discloses a preparation method of a carbon nanotube reinforced copper-based composite material. The composite material is prepared by using carbon nanotubes, pure copper powder and additives as raw materials, and by following the process flow of high-energy ball milling, reduction annealing, pressing forming, vacuum sintering and obtaining the carbon nanotube reinforced copper-based composite material. The copper-based composite material with high strength and high hardness is prepared. The problem of uniform dispersion of carbon nanotubes in the copper-based composite material is solved. The copper-based material is easily oxidized in a normal environment, which affects the functionality and usability of the copper-based material. In order to improve the excellent performance of the copper-based material in use, enhance the electrical conductivity of the material and shorten the process flow in production, a drawing, rolling and ultrasonic friction consolidation composite copper-based composite material preparation process is proposed.

[0004] The information disclosed in this Background section is only for the purpose of increasing the understanding of the background of the application and should not be taken as an acknowledgement or any form of suggestion that this information forms prior art that is already known in this field. SUMMARY

[0005] The purpose of the present application is to provide a drawing, rolling and ultrasonic friction consolidation composite copper-based composite material preparation process to solve the above problems in the prior art.

[0006] In order to achieve the above object, the application provides a drawing, rolling, ultrasonic friction consolidation composite high-performance copper-based composite material preparation equipment, which comprises the following steps:

[0007] One, preparation stage of high-performance copper-based composite material preparation:

[0008] S1, first introduce the copper wire on the winding machine into the wire polishing machine, polish the copper wire by using the wire polishing machine, and cut the copper wire into a plurality of equal length copper wires;

[0009] S2, prepare a graphene water solution in the graphene soaking pool, put the cut copper wires into the drain groove in the graphene soaking pool, and soak for 25 minutes;

[0010] S3, after soaking, take out the drain groove from the graphene soaking pool, take out the copper wire with graphene water solution on the surface, and bind it on the baffle in the drying box, and use the air heater to dry the graphene water solution on the surface of the copper wire, and after drying, place the copper wires side by side in the rolling groove of the high-carbon steel rolling die, and use the fixing mechanism to tension and fix the two ends of the copper wire;

[0011] Two, consolidation stage of high-performance copper-based composite material preparation:

[0012] S4, first cover the sealing cover, start the first motor, make the first motor drive the first connecting shaft to rotate, the first connecting shaft drives the pressure wheel to rotate, at the same time, drives the first gear at both ends to rotate, makes the first gear roll back and forth on the straight rack, uses the pressure wheel to preliminarily compress the plurality of copper wires in the rolling groove, through the compression of the pressure wheel to the copper wire, makes the plurality of copper wires realize the preliminary consolidation state;

[0013] S5, start the second motor to work, make the second motor drive the two second connecting shafts on the same side to rotate, use the rotation of the two second connecting shafts to drive the second gear to roll back and forth on the straight rack on each side, and use the second connecting shaft to drive the ultrasonic roller and the vibration sub inside to rotate at the same time, make the vibration sub rotate to produce high-frequency vibration, and conduct the high-frequency vibration to the outer wall of the ultrasonic roller, finally use the ultrasonic roller to roll the preliminarily consolidated copper wire, and finally consolidate to form high-performance copper-based composite material;

[0014] S6, while the ultrasonic roller is working, use the inert gas in the inert gas tank to protect the copper wire rolling area, spray inert gas into the rolling groove through the air pipe, prevent the copper-based from being oxidized.

[0015] The copper-based material composite equipment body comprises a supporting table and a sealing cover, a concave cavity is formed in the center of the top of the supporting table, a high-carbon steel rolling die is arranged at the top end of the concave cavity, a rolling groove for placing copper wires is arranged on the high-carbon steel rolling die, a fixing mechanism for fixing the end of the copper wire is arranged at the front and rear ends of the high-carbon steel rolling die, a solidification mechanism for solidifying the copper wire is arranged at the left and right ends of the supporting table, the solidification mechanism comprises a pressure wheel arranged at the upper end of the rolling groove and an ultrasonic roller, an inert gas tank is arranged at the top of the sealing cover, a breather pipe is arranged at the rear end of the inert gas tank, the breather pipe penetrates through the top of the sealing cover and extends to the rear side of the rolling groove, a lifting mechanism for adjusting the height of the high-carbon steel rolling die is arranged in the concave cavity, the lifting mechanism comprises a lead screw rotatably connected to the front and rear walls of the concave cavity, a short shaft sleeved on the bottom of the high-carbon steel rolling die and an adjusting disc fixed to the first end of the lead screw.

[0016] In the technical scheme of the present application, the bottom of the high-carbon steel rolling die is also provided with two guide holes matched with the size of the short shaft, and an arc-shaped piece is fixed to the bottom of the high-carbon steel rolling die in front of each guide hole.

[0017] In the technical scheme of the present application, the fixing mechanism comprises a bottom plate fixed to the top of the supporting table, an open slot is formed in the middle of the top of the bottom plate, a top plate is arranged at the upper end of the bottom plate, a clamping block is integrally formed on the bottom plate, the clamping block is in clamping engagement with the open slot, two tightening pieces are arranged on the outer side of the top plate, and the ends of the tightening pieces penetrate through the top plate and are in threaded connection with the outer wall of the bottom plate.

[0018] In the technical scheme of the present application, the solidification mechanism comprises mounting boxes fixed to the left and right sides of the supporting table and straight racks arranged in each mounting box, and a sliding groove is formed in the upper end of the left and right walls of the mounting box.

[0019] In the technical scheme of the present application, a first connecting shaft is rotatably connected to the pressure wheel, first gears are sleeved on the left and right ends of the first connecting shaft, a first motor is coaxially connected to the right end of the first connecting shaft, and the first gears on each side are in engagement with the straight racks on the same side.

[0020] In the technical scheme of the present application, the ultrasonic roller is internally provided with a vibration sub and a rotating shaft rotatably connected to the vibration sub, two symmetrically arranged second connecting shafts are rotatably connected to the left and right ends of the rotating shaft, a flange plate is arranged at the first end of the second connecting shaft, the left and right outer ends of the ultrasonic roller are fixedly connected with the two flange plates through bolts, second gears are sleeved on the ends of the second connecting shafts, each second gear is in engagement with the straight rack on the same side, and a second motor is coaxially fixed to the end of the second connecting shaft on the right side of the ultrasonic roller.

[0021] In the technical scheme of the present application, the inert gas tank is provided with a plurality of mounting seats, and the inert gas tank is fixed on the top of the sealing cover through the mounting seats.

[0022] In the technical scheme of the present application, the two first bevel gears are connected and fixed to the screw rod body through keys, the second bevel gears meshing with each first bevel gear are connected and fixed to the bottom of the two short shafts through keys, and the convex round pieces matched with the arc-shaped pieces are arranged on the top surface of each second bevel gear.

[0023] In summary, due to the adoption of the above technical scheme, the present application has the following beneficial effects:

[0024] 1、In the present application, the consolidation mechanism is provided to roll the copper wire, the pressure wheel is provided to preliminarily consolidate the copper wire, and the ultrasonic roller is provided to vibrate and roll the copper base formed by preliminary consolidation at a high frequency, so that a high-performance copper base composite material with high conductivity can be quickly obtained.

[0025] 2、In the present application, the lifting mechanism is provided to ensure that the height of the high-carbon steel rolling die can be adjusted according to the different diameters of the copper wire during use, and then the rolling degree of the copper wire by the pressure wheel and the ultrasonic roller can be adjusted, so that the strength of the copper base composite material is increased.

[0026] 3、In the present application, the graphene soaking pool and the inert gas tank are provided to ensure that when the copper base is prepared, the copper wire is soaked in the graphene aqueous solution, so that the conductivity, hardness and strength of the copper wire can be enhanced, and the inert gas tank is provided to ensure that when the copper base is consolidated, the inert gas is introduced to enhance the corrosion resistance of the rolling area of the copper base and prevent oxidation with the outside world. BRIEF DESCRIPTION OF DRAWINGS

[0027] Figure 1 It is a schematic diagram of the overall structure of the present application;

[0028] Figure 2 It is a structure diagram of the copper base material composite equipment body in the present application;

[0029] Figure 3 It is an internal structure diagram of the copper base material composite equipment body in the present application;

[0030] Figure 4 It is a structure diagram of the high-carbon steel rolling die and the fixing mechanism in the present application;

[0031] Figure 5 It is a partial structure diagram of the copper base material composite equipment body in the present application;

[0032] Figure 6Exploded view of the fixing mechanism in the application;

[0033] Figure 7 Structure diagram of the fixing mechanism in the application;

[0034] Figure 8 Structure diagram of the pressure wheel in the application;

[0035] Figure 9 Structure of the ultrasonic roller in the application;

[0036] Figure 10 Structure diagram of the ultrasonic roller and the second connecting shaft in the application;

[0037] Figure 11 Structure diagram of the inert gas tank in the application;

[0038] Figure 12 Structure diagram of the lifting mechanism in the application;

[0039] Figure 13 Enlarged view of A in the application Figure 12

[0040] Figure 14 Structure diagram of the copper-based material composite equipment body part two in the application

[0041] Explanation of reference numerals:

[0042] 1. Copper-based material composite equipment body; 10, support table; 101, concave cavity; 11, sealing cover; 12, high-carbon steel rolling die; 121, rolling groove; 122, guide hole; 123, arc-shaped part; 13, fixing mechanism; 130, bottom plate; 1301, open slot; 131, top plate; 1310, clamping block; 132, tightening part;

[0043] 2. Fixing mechanism; 20, mounting box; 201, sliding groove; 21, straight rack; 22, pressure wheel; 220, first connecting shaft; 221, first motor; 222, first gear; 23, ultrasonic roller; 230, vibration sub; 231, rotating shaft; 24, second connecting shaft; 241, flange; 242, second gear; 243, second motor;

[0044] 3. Inert gas tank; 30, mounting seat; 31, air pipe;

[0045] 4. Lifting mechanism; 40, lead screw; 401, first bevel gear; 41, short shaft; 410, second bevel gear; 411, convex round part; 42, adjusting disc;

[0046] 5. Copper wire; 50, copper wire;

[0047] 6. Graphene soaking pool; 60, leakage groove;​

[0048] 7. Drying oven;

[0049] 8. Hot air blower; Detailed Implementation

[0050] The specific embodiments of the present invention will now be described in detail with reference to the accompanying drawings, but it should be understood that the scope of protection of the present invention is not limited to the specific embodiments.

[0051] Unless otherwise expressly stated, throughout the specification and claims, the term "comprising" or its variations such as "including" or "comprises" shall be understood to include the stated elements or components without excluding other elements or other components.

[0052] Please see Figures 1 to 14 As shown, this invention provides a high-performance copper-based composite material preparation equipment using a drawing, rolling, and ultrasonic friction consolidation composite process. The equipment includes a copper-based material composite equipment body 1, which comprises a support platform 10 and a sealing cover 11. A cavity 101 is formed at the center of the top of the support platform 10. A high-carbon steel rolling mold 12 is provided at the top of the cavity 101. The high-carbon steel rolling mold 12 has a rolling groove 121 for placing copper wires 50. Fixing mechanisms 13 for fixing the ends of the copper wires 50 are provided at both ends of the high-carbon steel rolling mold 12. The sealing cover 11, made of tempered transparent glass, prevents leakage of inert gas and avoids inhalation and injury. A tail gas port is provided at the rear end of the sealing cover 11 for connecting to a tail gas absorption device to remove excess tail gas from the copper-based material composite equipment body 1 before opening the sealing cover 11. The bottom of the rolling groove 121 is arc-shaped on both sides to facilitate the removal of the consolidated copper matrix.

[0053] In this invention, the bottom of the high carbon steel rolling die 12 is also provided with two guide holes 122 that match the size of the short shaft 41. An arc-shaped part 123 is fixed to the bottom of the high carbon steel rolling die 12 located in front of each guide hole 122. The bottom of the high carbon steel rolling die 12 is placed into the cavity 101, and the high carbon steel rolling die 12 is fixed on the short shaft 41 through the guide holes 122.

[0054] Specifically, the fixing mechanism 13 includes a base plate 130 fixed to the top of the support platform 10. An opening groove 1301 is provided in the middle of the top of the base plate 130. A top plate 131 is provided at the upper end of the base plate 130. A locking block 1310 is integrally formed on the base plate 130. The locking block 1310 is engaged with the opening groove 1301. Two tightening members 132 are provided on the outer side of the top plate 131. The end of each tightening member 132 passes through the top plate 131 and is threaded to the outer wall of the base plate 130. In the preparation stage of the high-performance copper-based composite material preparation, the ends of several copper wires 50 are placed into the opening groove 1301, and the locking block 1310 on the inner side of the top plate 131 is locked into the opening groove 1301. The base plate 130 and the top plate 131 are fixed by using the tightening members 132, which can limit the two ends of the copper wires 50 and tighten the copper wires 50 to facilitate the subsequent rolling operation.

[0055] Furthermore, the left and right ends of the support platform 10 are provided with a fixing mechanism 2 for fixing the copper wire 50. The fixing mechanism 2 includes a pressure roller 22 and an ultrasonic roller 23 set on the upper end of the roller pressing groove 121. The fixing mechanism 2 includes a mounting box 20 fixed on the left and right sides of the support platform 10 and a straight rack 21 set inside each mounting box 20. The upper ends of the left and right walls of the mounting box 20 are provided with sliding grooves 201. The sliding grooves 201 limit the first connecting shaft 220 and the second connecting shaft 24, so that the ends of the first connecting shaft 220 and the ends of the second connecting shaft 24 roll in the opening groove 1301. The pressure roller 22 is used to perform preliminary fixing of the copper wire 50.

[0056] Furthermore, a first connecting shaft 220 is rotatably connected to the pressure roller 22. First gears 222 are sleeved on the rods at both ends of the first connecting shaft 220. A first motor 221 is coaxially connected to the right end of the first connecting shaft 220. Each first gear 222 meshes with its corresponding rack 21. The first motor 221 is connected to a power source via a wire, driving the first connecting shaft 220 to rotate. The first connecting shaft 220 drives the first gears 222 to roll on the rack 21, controlling the pressure roller 22 to move back and forth above the roller pressing groove 121. Simultaneously with the rotation of the first connecting shaft 220, the pressure roller 22 rotates, ensuring it is pressed against the copper wire 50 in the roller pressing groove 121. After the pressing, the pressure roller 22 rests at the front end of the high-carbon steel roller pressing mold 12, without affecting the subsequent ultrasonic roller 23 pressing operation.

[0057] It is worth noting that the ultrasonic roller 23 contains a vibrator 230 and a rotating shaft 231 rotatably connected to the vibrator 230. Both ends of the rotating shaft 231 have second connecting shafts 24, which are rotatably connected to each other. The first end of each second connecting shaft 24 has a flange 241. The left and right outer ends of the ultrasonic roller 23 are fixedly connected to the two flanges 241 by bolts, forming an integral structure between the two second connecting shafts 24 and the ultrasonic roller 23. The end of each second connecting shaft 24 is fitted with a second gear 242, which engages with a spur gear on the same side. The second motor 243 is coaxially fixed at the end of the second connecting shaft 24 located on the right side of the ultrasonic roller 23. The second motor 243 is connected to the power supply through a wire. The second motor 243 drives the second connecting shaft 24 on the same side to rotate, and drives the ultrasonic roller 23 to rotate. At the same time, it drives the vibrator 230 inside the ultrasonic roller 23 to generate high-frequency vibration. The high-frequency vibration generated by the vibrator 230 is transmitted to the outer wall of the ultrasonic roller 23. The ultrasonic roller 23 is used to roll the copper wire 50. Moreover, the pressure surface size of the ultrasonic roller 23 is the same as that of the pressure wheel 22 to ensure that the contact area with the copper wire 50 is consistent.

[0058] Specifically, an inert gas tank 3 is provided on the top of the sealing cover 11, and a vent pipe 31 is provided at the rear end of the inert gas tank 3. The end of the vent pipe 31 passes through the top of the sealing cover 11 and extends to the rear side of the roller pressing groove 121, so as to allow inert gas to be introduced into the rolling area during the ultrasonic roller 23 process. Several mounting seats 30 are provided on the inert gas tank 3, and the inert gas tank 3 is fixed to the top of the sealing cover 11 by several mounting seats 30. An inflation hole is provided at the front end of the inert gas tank 3 to facilitate inflation of the inert gas tank 3. A control valve is provided at the rear end of the inert gas tank 3, and the outlet of the control valve is fixed to the beginning of the vent pipe 31 to improve the gas flow capacity and facilitate timely corrosion protection of the solidified copper base.

[0059] Finally, a lifting mechanism 4 is provided inside the cavity 101. The height of the high carbon steel roller pressing mold 12 can be adjusted by the lifting mechanism 4, which facilitates the adjustment of the distance between the pressure roller 22, the ultrasonic roller 23 and the roller pressing groove 121, and can control the degree of pressing of the copper wire 50.

[0060] It is worth noting that the lifting mechanism 4 includes a lead screw 40 rotatably connected to the front and rear walls of the cavity 101, a short shaft 41 sleeved on the bottom of the high-carbon steel rolling die 12, and an adjusting plate 42 fixed to the head end of the lead screw 40. Two first bevel gears 401 are keyed and fixed on the body of the lead screw 40, and second bevel gears 410 are keyed to the bottom of the two short shafts 41. Each second bevel gear 410 has a convex round part 411 on its top surface that cooperates with the arc-shaped part 123. By rotating the adjusting plate 42, the adjusting plate 42 drives the lead screw 40 to rotate, and the first bevel gears 401... The screw 40 meshes with the second bevel gear 410, and drives the two first bevel gears 401 on its shaft to rotate, which in turn drives the second bevel gear 410 to rotate synchronously. When the second bevel gear 410 rotates, the convex round part 411 at the top of it abuts against the arc-shaped part 123 at the bottom of the high carbon steel rolling die 12. Since the bottom of the high carbon steel rolling die 12 is sleeved on two short shafts 41, when the convex round part 411 abuts against the arc-shaped part 123, it drives the high carbon steel rolling die 12 to move up and down along the cavity 101, thereby realizing the up and down adjustment of the high carbon steel rolling die 12.

[0061] This invention provides a process for preparing a copper-based composite material by drawing, rolling, and ultrasonic friction bonding, comprising the following steps:

[0062] I. Preparation stage for the preparation of high-performance copper-based composite materials:

[0063] S1. First, introduce the copper wire 5 on the winding machine into the wire polishing machine, polish the copper wire 5 using the wire polishing machine, and cut the copper wire 5 into several copper wires 50 of equal length and diameter between 0.05-0.5mm.

[0064] S2. Prepare a graphene aqueous solution in the graphene immersion tank 6, and put the cut copper wires 50 into the trough 60 in the graphene immersion tank 6 and immerse them for 25 minutes.

[0065] S3. After soaking, remove the trough 60 from the graphene soaking tank 6, take out the copper wire 50 with graphene aqueous solution on the surface, tie it to the partition in the drying oven 7, and use the hot air blower 8 to dry the graphene aqueous solution on the surface of the copper wire 50. After drying, place the copper wire 50 side by side in the rolling groove 121 of the high carbon steel rolling die 12, and use the fixing mechanism 13 to tighten and fix the two ends of the copper wire 50.

[0066] II. Consolidation Stage in the Preparation of High-Performance Copper-Based Composite Materials:

[0067] S4. First, close the sealing cover 11, then start the first motor 221, so that the first motor 221 drives the first connecting shaft 220 to rotate. The first connecting shaft 220 drives the pressure wheel 22 to rotate, and at the same time drives the first gears 222 at both ends to rotate, so that the first gears 222 roll back and forth on the rack 21. The pressure wheel 22 is used to initially press the copper wires 50 in the roller pressing groove 121. Through the pressing of the copper wires 50 by the pressure wheel 22, the copper wires 50 achieve a preliminary solidification state.

[0068] S5. Start the second motor 243 to drive the two second connecting shafts 24 on the same side to rotate. The rotation of the two second connecting shafts 24 drives the second gear 242 to roll back and forth on the rack 21 on each side. The second connecting shafts 24 drive the ultrasonic roller 23 and its internal vibrator 230 to rotate simultaneously. The vibrator 230 rotates to generate high-frequency vibration, and transmits the high-frequency vibration to the outer wall of the ultrasonic roller 23. Finally, the ultrasonic roller 23 is used to roll the initially solidified copper wire 50.

[0069] S6. While the ultrasonic roller 23 is working, the inert gas in the inert gas tank 3 is used to protect the rolling area of ​​the copper wire 50. The inert gas is sprayed into the rolling groove 121 through the air pipe 31 to prevent the copper base from oxidizing.

[0070] In the above process, the graphene aqueous solution in the graphene immersion tank 6 is composed of the following components by weight: 35 parts flake graphite, 3 parts sodium nitrate, 20 parts concentrated sulfuric acid, 2 parts potassium permanganate, 6 parts hydrogen peroxide, and 15 parts deionized water. The use of graphene can protect the copper wire from deep penetrating oxidation, greatly reducing the oxidation rate of copper. The copper wire 50 is initially compressed by the pressure roller 22, with the compression force generally between 5-20 kgf. After the pressure roller 22 is used for consolidation, the copper wires are initially bonded together. Then, the ultrasonic roller 23 is used for roll pressing and consolidation. During the ultrasonic roller 23 process, an inert gas is introduced into the rolling area for protection to prevent oxidation of the copper matrix. Finally, through this composite consolidation method, a high-performance copper-based composite material with high conductivity is quickly obtained.

[0071] The foregoing description of specific exemplary embodiments of the invention is for illustrative and explanatory purposes. These descriptions are not intended to limit the invention to the precise forms disclosed, and it will be apparent that many changes and variations can be made in accordance with the foregoing teachings. The exemplary embodiments were chosen and described in order to explain the specific principles of the invention and its practical application, thereby enabling those skilled in the art to implement and utilize various different exemplary embodiments of the invention, as well as various different choices and variations. The scope of the invention is intended to be defined by the claims and their equivalents.

Claims

1. A process for the production of a copper-based composite material by drawing, rolling, ultrasonic friction consolidation, characterized in that, Comprising the following steps: I. Preparation stage of high-performance copper-based composite material: S1, first introduce the copper wire (5) on the winding machine into the wire polishing machine, polish the copper wire (5) with the wire polishing machine, and cut the copper wire (5) into several copper wires (50) with equal length and diameter between 0.05-0.5mm; S2, prepare graphene aqueous solution in the graphene soaking pool (6), put the cut copper wires (50) into the leakage groove (60) in the graphene soaking pool (6), and soak for 25 minutes; S3, after soaking, take out the leakage groove (60) from the graphene soaking pool (6), take out the copper wire (50) with graphene aqueous solution on the surface, and bind it on the baffle in the drying box (7), and use the air heater (8) to dry the graphene aqueous solution on the surface of the copper wire (50), and then place the dried copper wire (50) side by side in the roller pressing groove (121) of the high-carbon steel roller pressing mold (12), and use the fixing mechanism (13) to tension and fix the two ends of the copper wire (50); II. Consolidation stage of high-performance copper-based composite material: S4, first cover the sealing cover (11), start the first motor (221), make the first motor (221) drive the first connecting shaft (220) to rotate, the first connecting shaft (220) drives the pressure wheel (22) to rotate, at the same time, drives the first gear (222) at both ends to rotate, makes the first gear (222) roll back and forth on the straight rack (21), uses the pressure wheel (22) to preliminarily press the copper wires (50) in the roller pressing groove (121), through the pressure wheel (22) to press the copper wire (50), makes the copper wire (50) realize the preliminary consolidation state; S5, start the second motor (243) to work, make the second motor (243) drive the two second connecting shafts (24) on the same side to rotate, use the rotation of the two second connecting shafts (24) to drive the second gear (242) to roll back and forth on the straight rack (21) on each side, and use the second connecting shaft (24) to drive the ultrasonic roller (23) and the vibration sub (230) inside it to rotate at the same time, make the vibration sub (230) rotate to produce high-frequency vibration, and conduct the high-frequency vibration to the outer wall of the ultrasonic roller (23), finally use the ultrasonic roller (23) to roll the preliminarily consolidated copper wire (50), and finally consolidate to form high-performance copper-based composite material; S6, while the ultrasonic roller (23) is working, use the inert gas in the inert gas tank (3) to protect the copper wire (50) rolling area, inject inert gas into the roller pressing groove (121) through the air pipe (31), prevent copper-based from oxidizing; The process adopts copper-based material composite equipment body (1) preparation, the copper-based material composite equipment body (1) includes support table (10) and sealing cover (11), the support table (10) top center is provided with recess cavity (101), the recess cavity (101) top is equipped with high carbon steel roller pressure mould (12), the high carbon steel roller pressure mould (12) is equipped with roller pressure groove (121) for placing copper wire (50) on, the high carbon steel roller pressure mould (12) front and back ends are equipped with the fixed mechanism (13) for the end of copper wire (50) fixed for, the support table (10) left and right ends are equipped with the consolidation mechanism (2) for consolidating copper wire (50), the consolidation mechanism (2) includes the pressure wheel (22) and ultrasonic roller (23) being arranged on the roller pressure groove (121) upper end, the sealing cover (11) top is equipped with inert gas tank (3), the inert gas tank (3) rear end is equipped with air pipe (31), the air pipe (31) tail end passes through the sealing cover (11) top and stretches to the back side of roller pressure groove (121); The first connecting shaft (220) is rotatably connected to the pressure wheel (22), the first connecting shaft (220) is provided with a first gear (222) on the left and right ends of the rod body, a first motor (221) is coaxially connected to the right end of the first connecting shaft (220), and the first gear (222) on each side is engaged with the straight rack (21) on the same side. The ultrasonic roller (23) is provided with a vibration sub (230) and a rotating shaft (231) rotatably connected to the vibration sub (230), the left and right ends of the rotating shaft (231) are rotatably connected to two second connecting shafts (24) arranged symmetrically, the first end of the second connecting shaft (24) is provided with a flange (241), the left and right outer ends of the ultrasonic roller (23) are fixedly connected to the two flanges (241) through bolts, the second connecting shaft (24) is provided with a second gear (242), and each second gear (242) is engaged with the straight rack (21) on the same side. The second motor (243) is coaxially fixed to the end of the second connecting shaft (24) on the right side of the ultrasonic roller (23).

2. The process for preparing a drawn, rolled, ultrasonically friction- consolidated copper-based composite material according to claim 1, wherein The recess cavity (101) is provided with a lifting mechanism (4) for adjusting the height of the high carbon steel roller pressure mould (12), the lifting mechanism (4) includes a lead screw (40) rotatably connected to the front and back walls of the recess cavity (101), a short shaft (41) sleeved to the bottom of the high carbon steel roller pressure mould (12), and an adjusting disc (42) fixed to the first end of the lead screw (40).

3. The process for preparing a drawn, rolled, ultrasonically friction- consolidated copper-based composite material according to claim 2, wherein The bottom of the high carbon steel roller pressure mould (12) is also provided with two guide holes (122) matching the size of the short shaft (41), and an arc-shaped part (123) is fixed to the front side of the bottom of the high carbon steel roller pressure mould (12) and located at each guide hole (122).

4. The process for preparing a drawn, rolled, ultrasonically friction- consolidated copper-based composite material according to claim 2, wherein The fixing mechanism (13) comprises a bottom plate (130) fixed on the top of the support table (10), an open slot (1301) is formed in the middle of the top of the bottom plate (130), a top plate (131) is arranged on the upper end of the bottom plate (130), a clamping block (1310) is integrally formed on the bottom plate (130), the clamping block (1310) is clamped and matched with the open slot (1301), two tightening members (132) are arranged on the outer side of the top plate (131), and the tail end of each tightening member (132) penetrates through the top plate (131) and is threadedly connected with the outer wall of the bottom plate (130).

5. The process for preparing a drawn, rolled, ultrasonically friction- consolidated copper-based composite material according to claim 3, wherein The fixing mechanism (2) comprises mounting boxes (20) fixed on the left and right sides of the support table (10) and straight racks (21) arranged in each mounting box (20), and the upper end of the left and right walls of the mounting box (20) is provided with a sliding groove (201).

6. The process for preparing a drawn, rolled, ultrasonically friction- consolidated copper-based composite material according to claim 2, wherein A plurality of mounting seats (30) are arranged on the inert gas tank (3), and the inert gas tank (3) is fixed on the top of the sealing cover (11) through the mounting seats (30).

7. The process for preparing a drawn, rolled, ultrasonically friction- consolidated composite copper-based composite material according to claim 3, characterized in that, The two first bevel gears (401) are arranged on the rod body of the lead screw (40) and are fixed by key connection, the two short shafts (41) are arranged at the bottom and are fixed by key connection, and the second bevel gear (410) meshed with each first bevel gear (401) is arranged on the bottom of the short shaft (41), the convex round piece (411) matched with the arc-shaped piece (123) is arranged on the top surface of each second bevel gear (410), and the convex round piece (411) is in abutment and rotation with the arc-shaped piece (123).

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