A plum-scented tobacco liner and its preparation method

By using natural plum juice extract to prepare a flavoring for cigarette grease fittings, the problem of odor during combustion of grease fittings has been solved, the aroma and taste of cigarettes have been improved, and a richer aroma style and a better sensory experience have been achieved.

CN117562290BActive Publication Date: 2026-04-03ETABONG QINGDAO INDAL
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2023-11-21
Publication Date
2026-04-03

AI Technical Summary

Technical Problem

Existing cigarette sealing adhesives produce unpleasant odors during combustion, affecting the sensory and smoking quality of cigarettes. Furthermore, existing flavorings have poor aroma richness and are not harmonious.

Method used

Using natural plum juice extract as the main aroma component, combined with lactic acid, palmitic acid and polysaccharide solution, a plum-scented flavoring for tobacco grease is prepared to improve the burning smell and aroma style of grease.

Benefits of technology

It enhances the aroma and flavor of cigarettes, reduces irritation, strengthens fruity and sweet aromas, improves the richness and natural fragrance of the smoke, and enhances the sensory evaluation of cigarettes.

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Abstract

This invention belongs to the field of cigarette adhesives, specifically relating to a plum-scented cigarette grease and its preparation method. The plum-scented cigarette grease flavoring, by weight, comprises the following components: 0.1-0.4 parts lactic acid, 0.05-0.15 parts palmitic acid, 2-10 parts natural plum juice extract, 70-80 parts polysaccharide solution, and 9.45-27.85 parts water. This invention uses natural plum juice extract as the main aroma component of the cigarette grease flavoring, providing the grease with a rich aroma profile including fruity and sweet notes. The grease has a natural aroma and reduces the unpleasant odor and irritation caused by burning cigarette grease. The use of the plum-scented tobacco grease flavoring of this invention improves the aroma, taste, and flavor profile of cigarettes, enhancing their overall aroma and reducing impurities. It also makes cigarettes smoother and more delicate, effectively reducing irritation and residue, and contributing to a richer and more fruity, sweeter aroma, and more delicate fragrance.
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Description

Technical Field

[0001] This invention belongs to the field of cigarette adhesives, specifically relating to a cigarette adhesive with a plum flavor and its preparation method. Background Technology

[0002] The information disclosed in this background section is intended only to enhance understanding of the overall background of the invention and is not necessarily to be construed as an admission or in any way implying that such information constitutes prior art known to those skilled in the art.

[0003] Cigarette adhesives are generally divided into filter tip adhesive, sealing adhesive, and packaging adhesive. Filter tip adhesive is used to bond the cigarette filter to the tipping paper; packaging adhesive is used for the packaging of cigarette packs and cartons; and sealing adhesive is used to bond the cigarette paper. Filter tip adhesive and packaging adhesive do not participate in the combustion process of the cigarette, while sealing adhesive does. Currently, the domestic cigarette industry mostly uses vinyl acetate-ethylene copolymer emulsion (VAE emulsion) as cigarette adhesive. VAE emulsion is a high-molecular-weight synthetic adhesive, which is prone to producing unpleasant odors during combustion, affecting the sensory and smoking quality of the cigarette.

[0004] Adding flavoring to the sealing glue can compensate for the odor defects caused by its combustion. Current technologies often use flavorings formulated primarily from monomeric compounds. While these flavorings are effective in masking off-flavors and improving taste, they lack richness in aroma, have a noticeable chemical odor, and are incompatible with the aroma of tobacco. Summary of the Invention

[0005] To address the shortcomings of existing technologies, the present invention aims to provide a cigarette grease with a plum aroma and its preparation method. The cigarette grease flavoring of the present invention contains natural plum juice extract, providing a fresh, fruity, and sweet aroma profile, reducing unpleasant odors from cigarette grease combustion, decreasing the irritation in cigarette sensory evaluation, and enhancing the sweetness of the smoke.

[0006] To achieve the above objectives, the present invention is implemented through the following technical solution:

[0007] In a first aspect, the present invention provides a flavoring for tobacco grease with a plum aroma, characterized in that, by weight, it comprises the following components:

[0008] Lactic acid 0.1-0.4 parts, palmitic acid 0.05-0.15 parts, natural plum juice extract 2-10 parts, polysaccharide solution 70-80 parts, solvent water 9.45-27.85 parts.

[0009] Preferably, the preparation method of the natural plum juice extract includes the following steps:

[0010] The green plums and bayberries were crushed and sieved to obtain plum juice for later use. Ethanol was added to the plum juice and stirred to extract it. The supernatant was collected by centrifugation and then concentrated to obtain the natural plum juice extract.

[0011] Further preferred, the mass ratio of green plums to bayberries is 1.5-2.5:1.

[0012] Further preferred methods include using ethanol with a volume fraction of 40%-60%, a plum juice to ethanol ratio of 1g:25-35mL, an extraction temperature of 50-60℃, an extraction speed of 500r / min, and an extraction time of 1-2h.

[0013] Preferably, the concentration of polysaccharides in the polysaccharide solution is 9-11 g / L, and the polysaccharides include jujube polysaccharide and sea buckthorn polysaccharide in a mass ratio of 1:1.

[0014] In a second aspect, the present invention provides a method for preparing a plum-scented tobacco grease flavoring as described in the first aspect, comprising the following steps:

[0015] The product is obtained by mixing lactic acid, palmitic acid, natural plum juice extract, polysaccharide solution, and water, and then allowing it to stand.

[0016] Thirdly, the present invention provides the application of the plum-scented tobacco grease flavoring as described in the first aspect in the preparation of tobacco grease flavoring.

[0017] Fourthly, the present invention provides a tobacco grease with a plum flavor, comprising a grease and a tobacco grease flavoring with a plum flavor as described in any one of claims 1-5.

[0018] Preferably, the mass ratio of flavoring to adhesive for tobacco is 0.4-0.6g:1kg.

[0019] Fifthly, the present invention provides a method for preparing a plum-scented tobacco liner as described in the fourth aspect, comprising the following steps:

[0020] The plum-scented tobacco grease flavoring as described in any one of claims 1-5 is mixed evenly with the grease and left to stand.

[0021] The beneficial effects achieved by one or more technical solutions of the present invention are as follows:

[0022] This invention uses natural plum juice extract as the main aroma component of cigarette grease, providing the grease with a rich aroma style such as fruity and sweet, resulting in a natural aroma and reducing the unpleasant odor and irritation caused by the burning of cigarette grease.

[0023] The use of the plum-scented tobacco grease flavoring of this invention improves the aroma, taste, and flavor profile of cigarettes, enhancing their overall aroma and reducing impurities. It also makes cigarettes smoother and more delicate, effectively reducing irritation and residue, and contributing to a richer and more fruity, sweeter aroma, and more delicate fragrance. Detailed Implementation

[0024] To enable those skilled in the art to better understand the technical solution of the present invention, the technical solution of the present invention will be described in detail below with reference to specific embodiments and comparative examples.

[0025] Example 1

[0026] Fresh green plums and bayberries were crushed in a container at a mass ratio of 2:1 and passed through a 40-mesh sieve. The sieved plum juice was placed in a constant-temperature magnetic stirrer, and 40% ethanol was added. The material-to-liquid ratio was 1g:30ml. The temperature was set at 55℃ and the speed at 500r / min. The mixture was stirred and extracted for 90min. After cooling and reweighting, the supernatant was collected by centrifugation. The supernatant was then concentrated in a rotary evaporator at a concentration temperature of 55℃ and a vacuum degree of 110mbar to obtain the natural plum juice extract.

[0027] Weigh out 0.2g of lactic acid, 0.1g of palmitic acid, 5g of natural plum juice extract, 75g of polysaccharide solution (jujube polysaccharide and sea buckthorn polysaccharide mixed at a mass ratio of 1:1, concentration 10g / L), and 19.7g of water in sequence. Stir well and let stand to obtain a plum-scented tobacco grease flavoring for later use. Add 0.5g of the above tobacco grease flavoring to 1kg of grease while stirring. Let stand to obtain a plum-scented tobacco grease for later use. Roll cigarettes with the plum-scented tobacco grease using a rolling machine, and evaluate after equilibration in a constant temperature and humidity chamber for 24 hours.

[0028] Example 2

[0029] Fresh green plums and bayberries were crushed in a container at a mass ratio of 2:1 and passed through a 40-mesh sieve. The sieved plum juice was placed in a constant-temperature magnetic stirrer, and 40% ethanol was added. The material-to-liquid ratio was 1g:30ml. The temperature was set at 55℃ and the speed at 500r / min. The mixture was stirred and extracted for 90min. After cooling and reweighting, the supernatant was collected by centrifugation. The supernatant was then concentrated in a rotary evaporator at a concentration temperature of 55℃ and a vacuum degree of 110mbar to obtain the natural plum juice extract.

[0030] Weigh out 0.1g of lactic acid, 0.05g of palmitic acid, 10g of natural plum juice extract, 70g of polysaccharide solution (jujube polysaccharide and sea buckthorn polysaccharide mixed at a mass ratio of 1:1, concentration 10g / L), and 19.85g of water. Stir well to obtain a plum-scented tobacco grease flavoring and set aside. Add 0.5g of the above tobacco grease flavoring to 1kg of grease while stirring. After setting aside, obtain a plum-scented tobacco grease flavoring. Roll cigarettes with the plum-scented tobacco grease using a rolling machine, equilibrate in a constant temperature and humidity chamber for 24 hours, and then evaluate.

[0031] Sensory evaluation was conducted on flavored cigarettes with added flavorings. The control sample was the same blank cigarette. The sensory evaluation scores for the blank cigarette were all recorded as 0 points. Positive scores indicated a good sensory evaluation, while negative scores indicated a poor one. The evaluation mainly included the aroma characteristics, taste characteristics, and aroma style of the flavored cigarettes with added flavorings. Aroma and taste were quantified using a scale of -5 to 5 points, with a scoring unit of 1 point. Aroma style was quantified using a scale of 0 to 3 points, with a scoring unit of 1 point. The evaluation result was the arithmetic mean of all judges (accurate to 0.1). Participants were required to have professional aroma-smelling skills and cigarette sensory evaluation qualifications. Seven judges participated. The results are shown in Table 1.

[0032] Table 1 Sensory Quality Evaluation Table for Tapered-Film Cigarettes

[0033]

[0034]

[0035] Table 1 shows that applying a plum-scented tobacco liner to cigarettes improves their aroma, taste, and overall flavor profile, enhancing the overall aroma and reducing impurities. The plum-scented liner makes the cigarette smoother and more delicate, effectively reducing irritation and residue, and contributing to a richer, more fruity, and sweet aroma profile, thus enhancing the overall richness of the cigarette's fragrance.

[0036] The above description is merely a preferred embodiment of the present invention and is not intended to limit the invention. Various modifications and variations can be made to the present invention by those skilled in the art. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present invention should be included within the scope of protection of the present invention.

Claims

1. A flavoring for tobacco grease fittings with a plum aroma, characterized in that, It consists of the following components in parts by weight: Lactic acid 0.1-0.4 parts, palmitic acid 0.05-0.15 parts, natural plum juice extract 2-10 parts, polysaccharide solution 70-80 parts, solvent water 9.45-27.85 parts; The preparation method of the natural plum juice extract includes the following steps: The green plums and bayberries were crushed and sieved to obtain plum juice for later use. Ethanol was added to the plum juice and stirred for extraction. The mixture was cooled, weighed, and centrifuged to obtain the supernatant. The supernatant was placed in a rotary evaporator for concentration at a temperature of 55 °C and a vacuum of 110 mbar to obtain a natural plum juice extract. The polysaccharide concentration in the polysaccharide solution is 10-11 g / L, and the polysaccharides include jujube polysaccharide and sea buckthorn polysaccharide in a mass ratio of 1:

1.

2. The flavoring for cigarette sealing adhesive as described in claim 1, characterized in that, The mass ratio of green plums to bayberries is 1.5-2.5:

1.

3. The flavoring for cigarette sealing adhesive as described in claim 1, characterized in that, The volume fraction of ethanol was 40%-60%, the ratio of plum juice to ethanol was 1 g: 25-35 mL, the extraction temperature was 50-60 ℃, the stirring speed was 500 r / min, and the extraction time was 1-2 h.

4. A method for preparing a plum-scented tobacco grease flavoring as described in any one of claims 1-3, characterized in that, Includes the following steps: The product is obtained by mixing lactic acid, palmitic acid, natural plum juice extract, polysaccharide solution, and water, and then allowing it to stand.

5. The use of the plum-scented tobacco grease flavoring as described in any one of claims 1-3 in the preparation of tobacco grease flavoring.

6. A tobacco sealing adhesive with a plum flavor, characterized in that, Includes grease fitting and the plum-scented grease fitting flavoring for tobacco as described in any one of claims 1-3.

7. The cigarette sealing adhesive as described in claim 6, characterized in that, The mass ratio of flavoring to adhesive for cigarette sealing is 0.4-0.6 g: 1 kg.

8. A method for preparing a plum-flavored tobacco liner as described in claim 6 or 7, characterized in that, Includes the following steps: The plum-scented tobacco grease flavoring as described in any one of claims 1-3 is mixed evenly with the grease and left to stand.

Citation Information

Patent Citations

  • Buccal type smokeless tobacco product with plum flavor

    CN103494320A

  • Lap adhesive suitable for external aroma type cigarettes and preparation method thereof

    CN108441137A

  • Characteristic essence with lotus fragrance and application of essence in cigarettes

    CN116676131A