An instant firming and anti-wrinkle composition and a method for preparing the same

By incorporating specific ingredients into anti-wrinkle products, this composition addresses the problem of existing anti-wrinkle products neglecting firming effects, achieving significant immediate firming and anti-wrinkle effects, and improving skin's moisture content, elasticity, and firmness.

CN117618307BActive Publication Date: 2025-11-21RENHE GLOBAL (SHANGHAI) GRAND HEALTH RESEARCH INSTITUTE CO LTD
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Patent Information

Application Number
CN202311630185.X
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2023-11-30
Publication Date
2025-11-21
Estimated Expiration
2043-11-30

AI Technical Summary

Technical Problem

In existing technologies, anti-wrinkle products mainly focus on anti-wrinkle effects while neglecting skin firming effects, and cannot comprehensively improve skin condition, especially the firming and anti-wrinkle effects of the skin around the eyes.

Method used

A combination of moisturizers, conopeptides, acetylglucosamine, hydroxypropyl tetrahydropyranotriol, centella asiatica extract, thyme flower/leaf extract, and Buddleja officinalis extract was used to prepare an instant firming and anti-wrinkle eye composition, which enhances the skin's immediate moisturizing, firming, and anti-wrinkle effects.

Benefits of technology

It significantly increases the moisture content of the stratum corneum, improves skin elasticity, reduces the length, depth, and roughness of crow's feet, and enhances skin firmness; the effects are visible within 30 minutes.

✦ Generated by Eureka AI based on patent content.

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Abstract

The application discloses an instant firming and anti-wrinkle eye composition and a preparation method thereof. The composition comprises the following components: a moisturizing agent, a conotoxin, an acetylated chitosan, a hydroxypropyl tetrahydropyran triol, a gynura extract, a satureja montana flower / leaf extract and a buddleja globosa extract. The application adds the effective components of the conotoxin, the acetylated chitosan, the hydroxypropyl tetrahydropyran triol, the gynura extract, the satureja montana flower / leaf extract and the buddleja globosa extract on the basis of the moisturizing agent to prepare the eye composition with instant moisturizing, firming and anti-wrinkle effects. The skin horny layer moisture content improvement rate reaches 58.43-65.23%, the R2 value improvement rate reaches 9.43-13.25%, the F4 value reduction rate reaches 8.62-11.94%, the fish tail wrinkle length, depth and Ra value reduction rates are more than 22.68%, more than 5.62% and more than 16.52% respectively.
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Description

Technical Field

[0001] This invention relates to the field of cosmetic technology, specifically to an instant firming and anti-wrinkle eye makeup composition and its preparation method. Background Technology

[0002] Because of direct contact with the external environment, skin is stimulated by various stressors such as oxidation, dryness, and ultraviolet radiation, leading to aging and sagging. Furthermore, with increasing age, climate change, and rising work and life pressures, these signs of aging become more pronounced. To maintain healthy skin, there is a growing demand for firming and anti-wrinkle products.

[0003] Existing patent document CN114796062A describes a composition comprising Euglena polysaccharide, chicory root extract, acetyl hexapeptide-8, hydrolyzed collagen, and sodium polyglutamate. The essence water prepared using this composition has a good anti-wrinkle effect, with an immediate (5 min) skin wrinkle improvement rate of 12.2%-20.3% and a long-term (28 d) skin wrinkle improvement rate of 14.6%-21.5%.

[0004] Existing patent document CN115212134A discloses an anti-aging nanocomposition, its preparation method, and its use. The anti-aging nanocomposition comprises 5-10 parts by weight of acetyl hexapeptide-8, 1-10 parts by weight of snake venom-like tripeptide, 5-15 parts by weight of conopeptide, 0.5-3 parts by weight of acetylglucosamine, and 5-15 parts by weight of Tremella fuciformis fruiting body extract. Its measured anti-wrinkle efficacy is: an improvement rate of 5.5-9.49% in the area of ​​crow's feet wrinkles 15 minutes after use.

[0005] The aforementioned patents only studied anti-wrinkle and anti-aging effects, without considering skin firming effects. Therefore, the purpose of this invention is to develop a composition that simultaneously possesses firming and anti-wrinkle effects, to more comprehensively improve the condition of the skin, especially the skin around the eyes. Summary of the Invention

[0006] To address the shortcomings of existing technologies, the present invention aims to provide an instant firming and anti-wrinkle eye makeup composition and its preparation method.

[0007] The objective of this invention is achieved through the following technical solution:

[0008] This invention provides an instant firming and anti-wrinkle eye composition comprising the following ingredients: moisturizer, conopeptide, acetyl glucosamine, hydroxypropyl tetrahydropyranotriol, centella asiatica extract, thyme flower / leaf extract, and Buddleja officinalis extract.

[0009] As a preferred embodiment, the instant firming and anti-wrinkle eye makeup composition comprises the following components in parts by weight: 5-20 parts of moisturizer, 2-8 parts of water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, 0.1-0.5 parts of acetylglucosamine / water, 0.01-0.1 parts of butylene glycol / hydroxypropyltetrahydropyranotriol / water, 0.01-0.1 parts of glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, and 0.001-0.02 parts of cyclodextrin / Centella asiatica extract.

[0010] As a preferred embodiment, the weight ratio of butylene glycol / hydroxypropyltetrahydropyranotriol / water to glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is 1:1.

[0011] As a preferred embodiment, the moisturizer comprises the following components: glycerin, butylene glycol, glyceryl polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate.

[0012] As a preferred embodiment, the weight ratio of glycerol, butylene glycol, glycerol polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate is 3-6:2-5:0.5-2:0.5-2:0.3-0.8:0.1-0.3:0.01-0.03.

[0013] As a preferred option, it also includes thickeners, pH adjusters, solubilizers, chelating agents, preservatives, fragrances, and solvents.

[0014] As a preferred embodiment, the components include the following parts by weight: 0.2-0.7 parts thickener, 0.1-0.5 parts pH adjuster, 0.1-0.3 parts solubilizer, 0.02-0.08 parts chelating agent, 2-3 parts preservative, 0.005-0.01 parts fragrance, and 70-90 parts solvent.

[0015] As a preferred embodiment, the thickener is selected from carbomer and xanthan gum;

[0016] The pH adjuster is selected from arginine;

[0017] The solubilizer is selected from PPG-26-butanol polyether-26 / PEG-40 hydrogenated castor oil / water;

[0018] The chelating agent is selected from disodium EDTA;

[0019] The preservative is selected from isopentyl glycol / p-hydroxyacetophenone / 1,2-hexanediol;

[0020] The fragrance is selected from triethyl citrate / bergamot fruit oil / North African cedar bark oil / star anise oil;

[0021] The solvent is selected from water.

[0022] As a preferred embodiment, the composition is an essence.

[0023] The present invention also provides a method for preparing the aforementioned instant firming and anti-wrinkle eye composition, comprising the following steps: weighing each component in proportion and stirring evenly to obtain the final product.

[0024] Compared with the prior art, the present invention has the following beneficial effects:

[0025] This invention, by adding active ingredients such as conopeptide, acetyl glucosamine, hydroxypropyl tetrahydropyrantriol, Centella asiatica extract, thyme flower / leaf extract, and Buddleja officinalis extract to a moisturizer, produces an eye care composition with immediate moisturizing, firming, and anti-wrinkle effects. The composition increases skin stratum corneum moisture content by 58.43%-65.23%, skin elasticity R2 value by 9.43-13.25%, skin firmness F4 value by 8.62-11.94%, crow's feet wrinkle length by over 22.68%, crow's feet wrinkle depth by over 5.62%, and crow's feet wrinkle roughness Ra value by over 16.52%. Attached Figure Description

[0026] Other features, objects, and advantages of the present invention will become more apparent from the following detailed description of non-limiting embodiments with reference to the accompanying drawings:

[0027] Figure 1 It is a three-level laughter chart;

[0028] Figure 2 This is a typical example of Antera 3D images of crow's feet (level 3 smile lines) of two subjects before use (T0) and 30 minutes after use (T30min) using the serum of Example 1 as the test sample. Detailed Implementation

[0029] The present invention will now be described in detail with reference to specific embodiments. These embodiments will help those skilled in the art to further understand the present invention, but do not limit the invention in any way. It should be noted that those skilled in the art can make various modifications and improvements without departing from the concept of the present invention. These all fall within the scope of protection of the present invention.

[0030] The terms "preferred," "more preferably," and "more suitable" used in this invention refer to embodiments of the invention that provide certain beneficial effects under certain circumstances. However, other embodiments may also be preferred under the same or other circumstances. Furthermore, the description of one or more preferred embodiments does not imply that other embodiments are unavailable, nor is it intended to exclude other embodiments from the scope of this invention.

[0031] It should be understood that, except in any operational instance or otherwise indicated, all figures representing the amounts of ingredients used, for example, in the specification and claims, should be understood to be modified in all cases by the term "about". Therefore, unless otherwise stated, the numerical parameters set forth in the following specification and appended claims are approximations varying with the desired performance to be obtained according to the invention. It is not at all an attempt to limit the application of the doctrine of equivalents to the scope of the claims; each numerical parameter should be interpreted at least according to the number of significant figures reported and by applying ordinary rounding techniques.

[0032] Although the numerical ranges and parameters illustrating the broad scope of the invention are approximate, the values ​​listed in the specific examples are reported as precisely as possible. However, any numerical value inherently contains some error that is necessarily caused by the standard deviation found in their respective test measurements.

[0033] The following embodiments provide an instant firming and anti-wrinkle eye composition comprising the following components: moisturizer, conopeptide, acetylglucosamine, hydroxypropyl tetrahydropyrantriol, centella asiatica extract, thyme flower / leaf extract, Buddleja officinalis extract, thickener, pH adjuster, solubilizer, chelating agent, preservative, fragrance, and solvent.

[0034] The moisturizer comprises the following components: glycerin, butylene glycol, glyceryl polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate.

[0035] In one specific embodiment, the instant firming and anti-wrinkle eye makeup composition comprises the following components in parts by weight: 5-20 parts moisturizer, 2-8 parts water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, 0.1-0.5 parts acetylglucosamine / water, 0.01-0.1 parts butylene glycol / hydroxypropyltetrahydropyranotriol / water, 0.01-0.1 parts glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, 0.001-0.02 parts cyclodextrin / Centella asiatica extract, 0.2-0.7 parts thickener, 0.1-0.5 parts pH adjuster, 0.1-0.3 parts solubilizer, 0.02-0.08 parts chelating agent, 2-3 parts preservative, 0.005-0.01 parts fragrance, and 70-90 parts solvent.

[0036] In one specific embodiment, the instant firming and anti-wrinkle eye makeup composition comprises the following components in parts by weight: 3-6 parts glycerin, 2-5 parts butylene glycol, 0.5-2 parts glyceryl polyether-26, 0.5-2 parts trehalose, 0.3-0.8 parts panthenol, 0.1-0.3 parts allantoin, 0.01-0.03 parts hydrolyzed sodium hyaluronate, 2-8 parts water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, 0.1-0.5 parts acetylglucosamine / water, 0.01-0.1 parts butylene glycol / hydroxypropyltetrahydropyranotriol / water, 0.01-0.1 parts glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, and 0.01-0.1 parts cyclodextrin / Centella asiatica extract. 0.02 parts, Carbomer 0.1-0.5 parts, Xanthan Gum 0.1-0.2 parts, Arginine 0.1-0.5 parts, PPG-26-Butyl Ether-26 / PEG-40 Hydrogenated Castor Oil / Water 0.1-0.3 parts, Disodium EDTA 0.02-0.08 parts, Isoamyl Glycol / p-Hydroxyacetophenone / 1,2-Hexanediol 2-3 parts, Triethyl Citrate / Berberis Fruit Oil / North African Cedar Bark Oil / Star Anise Oil 0.005-0.01 parts, Water to 100 parts.

[0037] In one specific embodiment, the water / 1,2-pentanediol / 1,2-hexanediol / conospiropeptide is derived from commercial products. Conopeptide 02 (manufactured by Dongguan Weiqi Technology Co., Ltd.) consists of water, 1,2-pentanediol, 1,2-hexanediol, and conopeptide.

[0038] In one specific embodiment, the acetyl glucosamine / water is derived from commercial NAG (acetyl glucosamine) (manufactured by Shanghai Huixin Biotechnology Co., Ltd.), and its components are acetyl glucosamine and water. Other acetyl glucosamine products from different manufacturers can also be used in this invention, and this invention does not impose any particular limitation.

[0039] In one specific embodiment, the butanediol / hydroxypropyltetrahydropyranotriol / water is derived from commercial products. S-30 (manufactured by Shanghai Keqin Technology Co., Ltd.) consists of: butanediol, hydroxypropyltetrahydropyranotriol, and water.

[0040] In one specific embodiment, the glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is derived from commercial products. NECTAPURE PF (manufactured by DSM Nutritional Products Ltd.). Its ingredients are: glycerin, water, thyme flower / leaf extract, and Buddleja officinalis extract. The ratio of thyme flower / leaf extract to Buddleja officinalis extract is 1:1.

[0041] In one specific embodiment, the cyclodextrin / Centella asiatica extract is derived from the commercially available Redummatte ASC-II (manufactured by Shanghai Jiakai Biotechnology Co., Ltd.). Its components are cyclodextrin and Centella asiatica extract.

[0042] In the following embodiments of the present invention, all other raw materials used are commercially available.

[0043] In the following embodiments, the instant firming and anti-wrinkle eye composition is a serum, which can be prepared using conventional methods, and the present invention does not impose any particular limitations.

[0044] Example 1

[0045] This embodiment provides an instant firming and anti-wrinkle eye serum, comprising the following components: moisturizer, conopeptide, acetylglucosamine, hydroxypropyl tetrahydropyrantriol, Centella asiatica extract, thyme flower / leaf extract, Buddleja officinalis extract, thickener, pH adjuster, solubilizer, chelating agent, preservative, fragrance, and solvent; wherein the moisturizer includes glycerin, butylene glycol, glyceryl polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate. The composition and weight ratio of each corresponding raw material (total weight parts: 100 parts) are shown in Table 1. The specific steps for preparing the serum are as follows:

[0046] 1. Add some water, glycerin, glyceryl polyether-26, trehalose, panthenol, allantoin, hydrolyzed sodium hyaluronate, carbomer, xanthan gum, and disodium EDTA to a water pot, heat and stir until dissolved to obtain phase A. Then, pump phase A into the main pot and heat the main pot to 80-85℃.

[0047] 2. When the main pot temperature drops to 65℃, add the pre-dissolved arginine (pre-dissolved in water) as phase B into the main pot and stir thoroughly.

[0048] 3. Mix and dissolve butylene glycol, PPG-26-butanol polyether-26 / PEG-40 hydrogenated castor oil / water, triethyl citrate / bergamot fruit oil / North African cedar bark oil / star anise oil until homogeneous to form phase C1; mix the remaining water, water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, acetyl glucosamine / water, butylene glycol / hydroxypropyl tetrahydropyranotriol / water, glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, cyclodextrin / Centella asiatica extract until homogeneous to form phase C2.

[0049] 4. Cool the main pot after step 2 to 45°C, then add C1 phase and C2 phase, as well as isopentyl glycol / p-hydroxyacetophenone / 1,2-hexanediol, and stir thoroughly to dissolve evenly;

[0050] 5. Once the main pot has cooled to 38°C, vacuum it, filter it, and you will get the instant firming and anti-wrinkle essence.

[0051] Example 2

[0052] This embodiment provides an instant firming and anti-wrinkle eye serum, the composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 1. The preparation steps of the serum are the same as in Embodiment 1.

[0053] Example 3

[0054] This embodiment provides an instant firming and anti-wrinkle eye serum, the composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 1. The preparation steps of the serum are the same as in Embodiment 1.

[0055] Example 4

[0056] This embodiment provides an instant firming and anti-wrinkle eye serum, the composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 1. The preparation steps of the serum are the same as in Embodiment 1.

[0057] Example 5

[0058] This embodiment provides an instant firming and anti-wrinkle eye serum, the composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 1. The preparation steps of the serum are the same as in Embodiment 1.

[0059] Example 6

[0060] This embodiment provides an instant firming and anti-wrinkle eye serum, the composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 1. The preparation steps of the serum are the same as in Embodiment 1.

[0061] Table 1

[0062]

[0063]

[0064] Comparative Example 1

[0065] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared with Example 2, only the water / 1,2-pentanediol / 1,2-hexanediol / conopeptide are not added. The preparation steps of the serum are the same as those in Example 1.

[0066] Comparative Example 2

[0067] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared with Example 2, only acetylglucosamine / water is not added. The preparation steps of the serum are the same as those in Example 1.

[0068] Comparative Example 3

[0069] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared with Example 2, only butylene glycol / hydroxypropyltetrahydropyranotriol / water are not added. The preparation steps of the serum are the same as those in Example 1.

[0070] Comparative Example 4

[0071] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared with Example 2, only cyclodextrin / centella asiatica extract is not added. The preparation steps of the serum are the same as those in Example 1.

[0072] Comparative Example 5

[0073] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared to Example 2, it only omits the addition of glycerin / water / thymus vulgaris flower / leaf extract / Buddleja davidii extract. The preparation steps of the serum are the same as in Example 1.

[0074] Comparative Example 6

[0075] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared to Example 2, it does not contain glycerin / water / thymus vulgaris flower / leaf extract / Buddleja davidii extract, and the content of butylene glycol / hydroxypropyltetrahydropyranotriol / water is 0.1 parts. The preparation steps of the serum are the same as in Example 1.

[0076] Comparative Example 7

[0077] This comparative example provides an instant firming and anti-wrinkle eye serum. The composition and weight ratio of its ingredients (total weight parts: 100 parts) are shown in Table 2. Compared to Example 2, butylene glycol / hydroxypropyltetrahydropyranotriol / water are not added, and the content of glycerin / water / thymus (THYMUS VULGARIS) flower / leaf extract / Buddleja davidii extract is 0.1 parts. The preparation steps of the serum are the same as in Example 1.

[0078] Table 2

[0079]

[0080]

[0081] Efficacy verification:

[0082] The serums prepared in Examples 1-6 and Comparative Examples 1-7 were used as test samples, and recruited subjects who met the criteria were used as test subjects. The test subjects were divided into different test groups. Each test subject first cleansed their face with the specified cleansing sample and sat quietly for 30 minutes in a laboratory at a temperature of 21±1℃ and a humidity of 50±10% RH. The baseline values ​​of various indicators of the skin around the eyes (before use) were measured. Then, the test subjects took an appropriate amount of the test sample and gently applied it to the skin around the eyes. After 30 minutes or 1 hour of application, the test values ​​of various indicators were measured (after use).

[0083] 1) Test subjects: Healthy women / men aged 25-55, with crow's feet, under-eye wrinkles (wrinkle grade ≥2, refer to "Skin Aging Atlas"), and dry and loose skin around the eyes.

[0084] 2) Test indicators and instruments

[0085] The moisture content of the stratum corneum was measured using a Corneometer CM825, with the test site being the outer corner of the eye. The higher the measured value, the higher the moisture content of the stratum corneum.

[0086] Skin elasticity R2 value and skin firmness F4 value were measured using a Cutometer dual MPA580. The test site was the outer corner of the eye. The larger the R2 value, the better the skin elasticity; the smaller the F4 value, the better the skin firmness.

[0087] Crow's feet wrinkles (level 3 smile lines) were measured using Antera 3D for image acquisition. Skin texture was reconstructed from shape through coloring, and spatial and spectral analysis was performed using 24 LEDs at 7 different wavelengths to achieve a realistic 3D skin surface reconstruction. The level 3 smile atlas is shown below. Figure 1 As shown.

[0088] 3) Test Results

[0089] 3.1 Based on the length, depth, and roughness Ra value of crow's feet (level 3 smile lines) measured before (0h) and 30min after using the test sample, the reduction rate of crow's feet length (level 3 smile lines) ((length of crow's feet before use - length of crow's feet after use) / length of crow's feet before use * 100%), the reduction rate of crow's feet depth (level 3 smile lines) ((depth of crow's feet before use - depth of crow's feet after use) / depth of crow's feet before use * 100%), and the reduction rate of crow's feet roughness Ra value (level 3 smile lines) ((Ra value of crow's feet before use - Ra value of crow's feet after use) / Ra value of crow's feet before use * 100%) were calculated for each test sample group.

[0090] The test group results for Examples 1-4 and Comparative Examples 1-5 are shown in Table 3 (the results are average values).

[0091] Table 3

[0092]

[0093]

[0094] As can be seen from the results in Table 3, after using the serums prepared in Examples 1-4 as test samples for 30 minutes, compared with before use, the length, depth, and roughness Ra value of crow's feet (level 3 smile lines) all decreased significantly. Figure 1 Examples 1 and 2 in the text are Antera 3D images of crow's feet (level 3 smile lines) of two subjects before use (T0) and 30 minutes after use (T30min) using the essence of Example 1 as the test sample. Figure 1 It is evident that crow's feet (level 3 smile lines) are significantly improved after use.

[0095] As can be seen from the comparison of the effects of Example 2 and Comparative Examples 1-4, when the serum does not contain water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, acetyl glucosamine / water, butylene glycol / hydroxypropyl tetrahydropyranotriol / water, or cyclodextrin / Centella asiatica extract, the reduction rates of crow's feet length, depth, and roughness Ra value all decrease to varying degrees. This indicates that water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, acetyl glucosamine / water, butylene glycol / hydroxypropyl tetrahydropyranotriol / water, and cyclodextrin / Centella asiatica extract can significantly improve crow's feet (level 3 smile lines) through their combined action, achieving a significant anti-wrinkle effect.

[0096] 3.2 Based on the skin stratum corneum moisture content, R2 value, and F4 value measured before (0h) and 1h after using the test sample, the following calculations were made for each test sample group: skin stratum corneum moisture content increase rate ((skin stratum corneum moisture content after use - skin stratum corneum moisture content before use) / skin stratum corneum moisture content before use * 100%), skin elasticity R2 value increase rate ((R2 value after use - R2 value before use) / R2 value before use * 100%), and skin firmness F4 value decrease rate ((F4 value before use - F4 value after use) / F4 value before use * 100%). The test group results for Examples 1-6 and Comparative Examples 1-7 are shown in Table 4 (the results are average values).

[0097] Table 4

[0098]

[0099]

[0100] As can be seen from the results in Table 4, after using the serums prepared in each embodiment as test samples for 1 hour, compared with before use, the skin stratum corneum moisture content increased significantly, the skin elasticity R2 value increased significantly, and the skin firmness F4 value decreased significantly.

[0101] Furthermore, a comparison of the effects of Example 2 with Comparative Examples 1-5 shows that when the serum does not contain water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, acetyl glucosamine / water, butylene glycol / hydroxypropyl tetrahydropyranotriol / water, glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract or cyclodextrin / Centella asiatica extract, the rate of increase in skin elasticity R2 value and the rate of decrease in skin firmness F4 value both decrease to varying degrees. A comparison of Example 2 with Comparative Examples 6-7 shows that when glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is not added and the content of butylene glycol / hydroxypropyl tetrahydropyranotriol / water is increased to 0.1 parts, or when butylene glycol / hydroxypropyl tetrahydropyranotriol / water is not added and the content of glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is increased to 0.1 parts, the rate of increase in skin elasticity R2 value and the rate of decrease in skin firmness F4 value both decrease to varying degrees. This demonstrates that the present invention, by employing a combination of water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, acetyl glucosamine / water, butylene glycol / hydroxypropyltetrahydropyranotriol / water, glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, and cyclodextrin / Centella asiatica extract, achieves a synergistic effect, significantly increasing the R2 value and decreasing the F4 value, thus giving the serum a significant immediate firming effect.

[0102] A comparison of Examples 3 and 5-6 shows that when the ratio of butylene glycol / hydroxypropyltetrahydropyranotriol / water and glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is 1:1, the increase rate of skin elasticity R2 value (from 9.22% and 11.56% to 12.62%) and the decrease rate of skin firmness F4 value (from 8.76% and 9.23% to 11.94%) can be further improved, achieving better immediate firming effect.

[0103] Furthermore, the results of human trials of the serums prepared in the various embodiments and comparative examples of the present invention showed that the skin reactions of the subjects were all grade 0, and no adverse reactions occurred.

[0104] This invention has many specific applications, and the above description is only a preferred embodiment. It should be noted that the above embodiments are for illustrative purposes only and are not intended to limit the scope of protection of this invention. For those skilled in the art, several improvements can be made without departing from the principle of this invention, and these improvements should also be considered within the scope of protection of this invention.

Claims

1. An instant firming and anti-wrinkle eye makeup composition, characterized in that, The ingredients include the following components in parts by weight: 5-20 parts moisturizer, 2-8 parts water / 1,2-pentanediol / 1,2-hexanediol / conopeptide, 0.1-0.5 parts acetylglucosamine / water, 0.01-0.1 parts butylene glycol / hydroxypropyltetrahydropyranotriol / water, 0.01-0.1 parts glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract, and 0.001-0.02 parts cyclodextrin / Centella asiatica extract. The weight ratio of butylene glycol / hydroxypropyltetrahydropyranotriol / water to glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is 1:1; The moisturizer comprises the following components: glycerin, butylene glycol, glyceryl polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate. The weight ratio of glycerol, butylene glycol, glycerol polyether-26, trehalose, panthenol, allantoin, and hydrolyzed sodium hyaluronate is 3-6:2-5:0.5-2:0.5-2:0.3-0.8:0.1-0.3:0.01-0.03; The butanediol / hydroxypropyltetrahydropyranotriol / water is derived from the commercial Anallerg®--Proyouth® S-30; The glycerin / water / thyme flower / leaf extract / Buddleja officinalis extract is derived from the commercial ALPAFLOR® NECTAPURE PF.

2. The instant firming and anti-wrinkle eye makeup composition according to claim 1, characterized in that, It also includes thickeners, pH adjusters, solubilizers, chelating agents, preservatives, fragrances, and solvents.

3. The instant firming and anti-wrinkle eye makeup composition according to claim 2, characterized in that, It includes the following components in parts by weight: 0.2-0.7 parts thickener, 0.1-0.5 parts pH adjuster, 0.1-0.3 parts solubilizer, 0.02-0.08 parts chelating agent, 2-3 parts preservative, 0.005-0.01 parts fragrance, and 70-90 parts solvent.

4. The instant firming and anti-wrinkle eye makeup composition according to claim 2 or 3, characterized in that, The thickener is selected from carbomer and xanthan gum; The pH adjuster is selected from arginine; The solubilizer is selected from PPG-26-butanol polyether-26 / PEG-40 hydrogenated castor oil / water; The chelating agent is selected from disodium EDTA; The preservative is selected from isopentyl glycol / p-hydroxyacetophenone / 1,2-hexanediol; The fragrance is selected from triethyl citrate / bergamot fruit oil / North African cedar bark oil / star anise oil; The solvent is selected from water.

5. The instant firming and anti-wrinkle eye composition according to claim 1, characterized in that, The composition is an essence.

6. A method for preparing an instant firming and anti-wrinkle eye composition according to any one of claims 1-5, characterized in that, The process includes the following steps: weigh each component according to the specified proportions and stir until homogeneous.

Citation Information

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