A high-efficiency and low-energy consumption amino acid evaporation crystallization equipment and process

By using a structure combining a heating cylinder and a preheating cylinder in the amino acid evaporation and crystallization equipment, the evaporation gas is recycled and used for insulation and preheating, and automatic material extraction is achieved using scrapers and pressure rollers. The problem of low thermal vapor emission and amino acid extraction efficiency is solved, and the high-efficiency and low-energy consumption of amino acid evaporation and crystallization process is achieved.

CN117732092BActive Publication Date: 2025-04-08SHANDONG XIANGRUI PHARMA
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Patent Information

Application Number
CN202410144470.9
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-02-01
Publication Date
2025-04-08
Estimated Expiration
2044-02-01

AI Technical Summary

Technical Problem

The existing amino acid evaporation and crystallization equipment generates direct discharge of hot steam during the evaporation process, resulting in environmental thermal pollution and energy waste. At the same time, the crystallized amino acids are difficult to be efficiently taken out, affecting the crystallization efficiency.

Method used

A highly efficient and low-energy-consuming amino acid evaporation and crystallization equipment is designed. The structure of a combination of a heating cylinder and a preheating cylinder is used to recover and insulate and preheat the evaporate gas through a spiral groove and a transition tube, and the scraper and a press-pressure roller are used to achieve automatic material collection.

Benefits of technology

It effectively reduces the heat exchange and waste heat pollution to the environment by the outer wall of the heating cylinder, while improving the efficiency and safety of evaporation and crystallization, and reducing the cumbersomeness and risk of manual removal of amino acids.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present application relates to the technical field of amino acid evaporation crystallization, and in particular to a high-efficiency and low-energy consumption amino acid evaporation crystallization device and process, comprising a heating cylinder, an air outlet pipe, a transition pipe and a spiral groove. In the heating cylinder designed by the present invention, water vapor evaporated from the interior thereof enters the interior of the spiral groove through the air outlet pipe and the transition pipe, and then the water vapor in the spiral groove can play a role in heat preservation for the heating cylinder, reduce the heat exchange between the outer wall of the heating cylinder and the external environment, and reduce the pollution of waste heat to the environment; when the water in the sodium glutamate solution is completely evaporated to obtain sodium glutamate powder, the scraper can rotate to scrape the sodium glutamate powder outward from the discharge trough, thereby reducing the tediousness of taking out the sodium glutamate powder by manual methods, and at the same time can reduce the risk of workers entering the interior of the heating cylinder.
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Description

Technical Field

[0001] The present application relates to the technical field of amino acid evaporation crystallization, and in particular to a high-efficiency and low-energy consumption amino acid evaporation crystallization device and process. Background Art

[0002] Amino acids are the main units that make up proteins in living organisms. In order to obtain amino acids with higher purity, crystallization is often used to purify amino acids. Amino acids obtained by crystallization are of high quality, and the purification process is highly efficient and safe. Among them, glutamic acid is a common non-essential amino acid.

[0003] Among them, sodium glutamate is a salt formed by sodium ions and glutamate ions, which is often used to make seasonings such as MSG to enhance the flavor. Sodium glutamate can also be obtained by evaporation and crystallization during the preparation process.

[0004] The utility model with the publication number CN206746030U discloses a device for amino acid evaporation crystallization, including a crystallization tank, a heating ring with a hollow structure is sleeved on the outer side of the crystallization tank, the heating ring can slide down along the crystallization tank by itself under the action of gravity, the height of the heating ring is 1 / 5 to 1 / 4 of the height of the crystallization tank, the hollow structure of the heating ring is filled with heat transfer oil, the inlet and outlet of the heat transfer oil and the center of the heating ring are on the same straight line; at least two wire seats are fixedly connected to the support frame, each of which is respectively connected to a screw rod extending vertically upward to the bottom surface of the heating ring through a thread, the screw rod provides support for the heating ring, and the screw rod is evenly distributed along the circumference of the heating ring. This patent application uses a heating ring to heat the liquid in the crystallization tank layer by layer from top to bottom. As the liquid level decreases, the heating ring is moved downward by rotating the screw rod. Since the liquid heated each time is in the uppermost layer, it evaporates directly after the temperature is reached, which greatly shortens the time used for crystallization and improves the crystallization efficiency.

[0005] The above patent application still has the following problems in the process of amino acid evaporation and crystallization: 1. When evaporating and crystallizing amino acids, the above patent application directly discharges hot steam into the air, which may cause thermal pollution to the environment. At the same time, the discharged hot steam is not recycled, which will cause energy waste.

[0006] 2. After evaporation and crystallization, the amino acids adhere to the bottom of the crystallization tank. At this time, it is necessary to take out the crystallized amino acids through external equipment or manually, which takes a long time and affects the evaporation and crystallization efficiency of the amino acids.

[0007] Based on this, and in accordance with the above-mentioned viewpoints, the existing technology for the evaporation and crystallization of amino acids still has room for improvement. Summary of the invention

[0008] In order to solve the above technical problems, the present application provides a high-efficiency and low-energy consumption amino acid evaporation crystallization equipment and process, which adopts the following technical solutions:

[0009] In the first aspect, a high-efficiency and low-energy consumption amino acid evaporation and crystallization device includes a heating cylinder, an air outlet pipe is installed on the upper end surface of the heating cylinder, a spiral groove is opened inside the side wall of the heating cylinder, a transition pipe is installed on the air outlet pipe and is connected to the spiral groove.

[0010] The upper end surface of the heating cylinder is penetrated by a rotating shaft extending up and down, the upper end surface of the rotating shaft is installed with a driving motor, the part of the rotating shaft located inside the heating cylinder is penetrated by a moving block extending left and right and moving up and down, a scraper is installed on the right side of the moving block, the lower end surface of the heating cylinder is provided with a discharge trough penetrating up and down, and the upper end surface of the heating cylinder is installed with an electronic hygrometer.

[0011] Preferably, the front end surface of the rotating shaft located inside the heating cylinder is equipped with a stirring rod facing forward horizontally, and a plurality of stirring rods evenly distributed from front to back are installed on the lower side of the circumferential surface of the stirring rod.

[0012] Preferably, a preheating cylinder is arranged on the right side of the heating cylinder, and an inlet is installed on the right side of the upper end surface of the preheating cylinder, the heating cylinder and the preheating cylinder are connected by a horizontal frame, a water pump is installed on the horizontal frame, the water outlet of the water pump is connected with the heating cylinder through a water outlet pipe, the water inlet of the water pump is connected with the preheating cylinder through a water inlet pipe, and a preheating pipe matching with the air outlet pipe is installed on the preheating cylinder.

[0013] Preferably, the preheating tubes are evenly arranged in multiple circumferential directions and are of a vertically through-connected structure. A transition box that is through-connected is installed on the upper ends of the preheating tubes, and the end of the air outlet pipe away from the heating tube is through-connected with the transition box.

[0014] Preferably, a rotating coupling is provided inside the preheating tube, the upper end of which is installed on the top of the preheating tube through a bearing, a spiral blade is installed on the circumferential surface of the rotating coupling, and a pulley is installed at one end of the rotating coupling located in the transition box, and the pulleys are connected by belt transmission.

[0015] Preferably, an elastic telescopic rod is installed on the lower end surface of the moving block, a moving connecting block is installed on the end of the elastic telescopic rod away from the moving block, a pressing roller extending left and right is installed on the left end surface of the moving connecting block through a bearing, a counterweight is installed on the side of the pressing roller away from the moving connecting block, an annular bevel rack plate is installed on the bottom of the heating cylinder, and a bevel gear matching the annular bevel rack plate is installed on the right side of the pressing roller.

[0016] Preferably, a bidirectional threaded groove is provided on the circumferential surface of the pressing roller, an L-shaped fixed frame is arranged on the left side of the upper end surface of the movable connecting block, the vertical section of the fixed frame is fixedly connected to the movable connecting block, the horizontal section of the fixed frame is located directly above the pressing roller, and a scraping plate that slides left and right is arranged on the lower end surface of the horizontal section of the fixed frame, and a scraping protrusion that cooperates with the bidirectional threaded groove is arranged on the lower end surface of the scraping plate.

[0017] In a second aspect, a high-efficiency and low-energy consumption amino acid evaporation crystallization process, the use method of which comprises the following steps:

[0018] S1: Blocking treatment, pumping sodium glutamate solution into the preheating cylinder through the outlet, blocking the discharge trough, and pumping sodium glutamate solution into the heating cylinder through a water pump.

[0019] S2: Heating treatment: the sodium glutamate is heated by the heating tube, and at the same time, the evaporated water vapor enters the spiral groove through the outlet pipe and the transition pipe to keep the heating tube warm.

[0020] S3: Preheating treatment: excess water vapor enters the preheating tube through the outlet pipe and the transition box to preheat the glutamic acid ammonia solution in the preheating tube.

[0021] S4: material taking process. When the sodium glutamate solution is evaporated and dried to obtain sodium glutamate powder, the discharging trough is opened and the sodium glutamate powder is taken out from the discharging trough by a scraper.

[0022] In summary, the present application includes at least one of the following beneficial technical effects:

[0023] 1. In the heating cylinder designed by the present invention, the water vapor evaporated from the inside enters the spiral groove through the air outlet pipe and the transition pipe, and then the water vapor in the spiral groove can keep the heating cylinder warm, reduce the heat exchange between the outer wall of the heating cylinder and the external environment, and reduce the pollution of waste heat to the environment; when the water in the sodium glutamate solution is completely evaporated to obtain the sodium glutamate powder, the scraper can rotate to scrape the sodium glutamate powder out of the discharge trough, reducing the tediousness of taking out the sodium glutamate powder by manual methods, and at the same time can reduce the risk of workers entering the heating cylinder.

[0024] 2. The water vapor discharged from the heating cylinder enters the preheating tube through the exhaust pipe and the transition box, and then the water vapor and the preheating tube cooperate with each other to preheat the sodium glutamate solution in the preheating tube. At the same time, the waste heat of the water vapor can be utilized, which not only reduces the pollution of waste heat to the environment, but also makes the evaporation and crystallization efficiency of the preheated sodium glutamate solution higher after entering the heating cylinder.

[0025] 3. The pressing roller of the present invention can also rotate itself during the circumferential rotation around the rotating axis, and the pressing roller can crush the sodium glutamate after evaporation and crystallization to obtain sodium glutamate powder during the rotation process, thereby avoiding agglomeration of sodium glutamate after evaporation and crystallization, which affects the subsequent removal of sodium glutamate. BRIEF DESCRIPTION OF THE DRAWINGS

[0026] Figure 1 It is a three-dimensional structural schematic diagram of the present invention.

[0027] Figure 2 It is a schematic diagram of the external three-dimensional structure of the heating tube of the present invention.

[0028] Figure 3 It is a schematic diagram of the internal three-dimensional structure of the heating tube of the present invention.

[0029] Figure 4 It is a schematic diagram of the three-dimensional installation structure between the rotating shaft, the scraper, etc. of the present invention.

[0030] Figure 5 The present invention Figure 4 A partial enlarged view of point A in the middle.

[0031] Figure 6 The present invention Figure 4 A partial enlarged view of point B in the middle.

[0032] Figure 7 It is a schematic diagram of the internal three-dimensional structure of the preheating cylinder of the present invention.

[0033] Figure 8 The present invention Figure 8 A partial enlarged view of point C in the middle.

[0034] Fig. 9 The present invention is a flow chart of the high-efficiency and low-energy consumption amino acid evaporation crystallization method.

[0035] Explanation of the reference numerals: 1. heating cylinder; 11. rotating shaft; 111. stirring connecting rod; 112. stirring rod; 12. driving motor; 13. moving block; 131. elastic telescopic rod; 132. moving connecting block; 133. pressing roller; 134. counterweight; 135. annular bevel rack plate; 136. bevel gear; 137. bidirectional threaded groove; 138. fixed frame; 139. scraper plate; 130. scraper protrusion; 14. scraper; 15. discharge trough; 16. electronic hygrometer; 2. air outlet pipe; 3. spiral groove; 4. transition pipe; 5. preheating cylinder; 51. inlet; 52. horizontal frame; 53. water pump; 54. water outlet pipe; 55. water inlet pipe; 56. preheating pipe; 561. rotating connecting shaft; 562. spiral blade; 563. pulley; 564. belt; 57. transition box. DETAILED DESCRIPTION

[0036] The following is combined with Figures 1 to 9This application is described in further detail.

[0037] The embodiment of the present application discloses a high-efficiency and low-energy consumption amino acid evaporation crystallization device and process, which recovers the water vapor generated by the evaporation of sodium glutamate solution and performs heat preservation treatment on the sodium glutamate during the evaporation and crystallization process; at the same time, the present invention can take out the sodium glutamate after evaporation and crystallization without manual methods, and has higher efficiency and safety.

[0038] Embodiment 1:

[0039] See also Figure 1 as well as Figure 2 A high-efficiency and low-energy consumption amino acid evaporation crystallization device comprises a heating cylinder 1, an air outlet pipe 2 is installed on the upper end surface of the heating cylinder 1, a spiral groove 3 is opened inside the side wall of the heating cylinder 1, a transition pipe 4 connected with the air outlet pipe 2 is installed on the air outlet pipe 2, and the end of the transition pipe 4 away from the air outlet pipe 2 is connected with the spiral groove 3.

[0040] See also Figure 2 , Figure 3 as well as Figure 5 A rotating shaft 11 extending vertically is rotatably installed on the upper end surface of the heating cylinder 1, a driving motor 12 is installed on the upper end surface of the rotating shaft 11, a moving block 13 extending left and right and moving up and down is installed on the part of the rotating shaft 11 located inside the heating cylinder 1, a scraper 14 is installed on the right side of the moving block 13, a discharge trough 15 penetrating vertically is provided on the lower end surface of the heating cylinder 1, and an electronic hygrometer 16 is installed on the upper end surface of the heating cylinder 1.

[0041] The lower end of the spiral groove 3 is connected to the outside. During operation, the discharge groove 15 is sealed, and in the initial state, the heating cylinder 1 is filled with sodium glutamate solution. The heating cylinder 1 is heated by an external heating device (resistance wire, etc.). The water vapor generated during the heating process can enter the spiral groove 3 through the air outlet pipe 2 and the transition pipe 4, and then the water vapor in the spiral groove 3 can keep the heating cylinder 1 warm, reduce the heat exchange between the outer wall of the heating cylinder 1 and the external environment, and reduce the pollution of waste heat to the environment.

[0042] After the water vapor condenses inside the spiral groove 3, the inside of the heating tube 1 is in a negative pressure state. Under the negative pressure state, the humidity inside the heating tube 1 is low and the water vapor evaporates quickly, further accelerating the evaporation rate of the sodium glutamate solution water, and the condensed water droplets flow out through the bottom of the spiral groove 3.

[0043] See also Figures 3 to 5An elastic telescopic rod 131 is installed on the lower end surface of the moving block 13, and a moving connecting block 132 is installed on the end of the elastic telescopic rod 131 away from the moving block 13. A pressing roller 133 extending left and right is installed on the left end surface of the moving connecting block 132 through a bearing, which can press the sodium glutamate solid at the bottom of the heating cylinder 1. A counterweight block 134 is installed on the side of the pressing roller 133 away from the moving connecting block 132 to ensure that the pressing roller 133 will not be displaced in the up and down directions when pressing the sodium glutamate. An annular bevel rack plate 135 is installed at the bottom of the heating cylinder 1, and a bevel gear 136 matching the annular bevel rack plate 135 is installed on the right side of the pressing roller 133.

[0044] After heating for a period of time, the electronic hygrometer 16 is manually observed. If the reading of the electronic hygrometer 16 reaches a certain value, it indicates that the sodium glutamate solution inside the heating cylinder 1 is completely evaporated and dry sodium glutamate is obtained. At this time, the moving block 13 is pushed downward by an external driving force (electric push rod, etc.). During the downward movement of the moving block 13, the elastic telescopic rod 131 drives the moving connecting block 132 to move downward.

[0045] The bevel gear 136 can rotate relatively around the pressing roller 133 at a small angle to ensure that the bevel gear 136 and the annular bevel rack plate 135 can be adaptively fine-tuned to mesh, avoid the problem of tooth jamming between the bevel gear 136 and the annular bevel rack plate 135, and improve the use effect of the device.

[0046] During the downward movement of the moving connecting block 132, the pressing roller 133 first contacts the sodium glutamate solid at the bottom of the heating cylinder 1. At this time, the bevel gear 136 and the annular bevel rack plate 135 are fine-tuned and meshed. During the rotation of the rotating shaft 11, the pressing roller 133 is driven to rotate circumferentially. During the circumferential rotation of the pressing roller 133 around the rotating shaft 11, the bevel gear 136 and the annular bevel rack plate 135 are meshed with each other and can also rotate on its own. Therefore, the pressing roller 133 during the rotation process can crush the sodium glutamate after evaporation and crystallization to obtain sodium glutamate powder, thereby avoiding agglomeration of sodium glutamate after evaporation and crystallization, which affects the subsequent removal of sodium glutamate.

[0047] When the sodium glutamate solid is pressed, the moving block 13 continues to move downward, and the elastic telescopic rod 131 contracts at this time to make way for the moving block 13, and the moving connecting block 132 no longer moves. During the downward movement of the moving block 13, the scraper 14 is driven to move downward and abut against the inner bottom surface of the heating cylinder 1. At this time, the discharge chute 15 is opened and the driving motor 12 is started. During the rotation of the driving motor 12, the rotating shaft 11 is driven to rotate. During the rotation of the rotating shaft 11, the scraper 14 is driven to rotate through the moving block 13. During the rotation of the scraper 14, the sodium glutamate powder can be scraped out from the discharge chute 15, thereby reducing the tediousness of removing the sodium glutamate powder by manual methods, and at the same time reducing the risk of workers entering the heating cylinder 1.

[0048] See also Figure 5 as well as Figure 6 In order to avoid relative sliding between the sodium glutamate solid and the pressing roller 133, a bidirectional thread groove 137 is provided on the circumferential surface of the pressing roller 133 of the present invention to increase the friction between the sodium glutamate and the pressing roller 133. An L-shaped fixed frame 138 is provided on the left side of the upper end surface of the movable connecting block 132. The vertical section of the fixed frame 138 is fixedly connected to the movable connecting block 132. The horizontal section of the fixed frame 138 is located directly above the pressing roller 133. A scraping plate 139 that slides left and right is provided on the lower end surface of the horizontal section of the fixed frame 138 to scrape off the sodium glutamate powder attached to the surface of the pressing roller 133. The scraping protrusion 130 that matches the bidirectional thread groove 137 is provided on the lower end surface of the scraping plate 139.

[0049] During specific operation, the sodium glutamate solid can be pressed during the rotation of the pressing roller 133. The bidirectional threaded groove 137 can increase the friction between the sodium glutamate and the pressing roller 133 during the rotation of the pressing roller 133, thereby avoiding the problem that the sodium glutamate solid and the pressing roller 133 remain relatively still and the pressing roller 133 cannot effectively press the sodium glutamate solid. At the same time, during the rotation of the pressing roller 133, the bidirectional threaded groove 137 synchronously drives the scraper plate 139 to move back and forth along the horizontal plate of the fixed frame 138, so that the scraper plate 139 can scrape off the sodium glutamate powder attached to the surface of the pressing roller 133, and the scraping protrusion 130 can scrape off the sodium glutamate powder inside the bidirectional threaded groove 137, thereby avoiding the problem that the sodium glutamate powder blocks the bidirectional threaded groove 137, resulting in a decrease in the friction between the sodium glutamate solid and the pressing roller 133.

[0050] Replay Figure 3 In order to ensure the uniformity of heating of the sodium glutamate solution during the evaporation and crystallization process, the rotating shaft 11 of the present invention is equipped with a horizontal forward stirring rod 111 on the front end surface located inside the heating cylinder 1, and a plurality of stirring rods 112 evenly distributed from front to back are installed on the lower side of the circumferential surface of the stirring rod 111.

[0051] During specific operation, the stirring rod 112 is driven to rotate by the stirring connecting rod 111 during the rotation of the rotating shaft 11. The sodium glutamate solution can be stirred during the rotation of the stirring rod 112, so that the sodium glutamate solution moves irregularly, thereby ensuring the uniformity of the sodium glutamate solution during the heating process.

[0052] Example 2: See Figure 7 as well as Figure 8On the basis of the first embodiment, in order to further improve the utilization efficiency of water vapor in the evaporation and crystallization process, a preheating cylinder 5 is arranged on the right side of the heating cylinder 1 of the present invention, which can hold the sodium glutamate solution, and an inlet 51 is installed on the right side of the upper end surface of the preheating cylinder 5. The heating cylinder 1 and the preheating cylinder 5 are connected by a horizontal frame 52, and a water pump 53 is installed on the horizontal frame 52, which can pump the sodium glutamate solution in the preheating cylinder 5 into the heating cylinder 1. The water outlet of the water pump 53 is connected to the heating cylinder 1 through the water outlet pipe 54, and the water inlet of the water pump 53 is connected to the preheating cylinder 5 through the water inlet pipe 55. A preheating pipe 56 matched with the air outlet pipe 2 is installed on the preheating cylinder 5 to preheat the sodium glutamate solution.

[0053] There are multiple preheating tubes 56 evenly arranged around the circumference and the preheating tubes 56 are of a vertical through structure. A transition box 57 that is through is installed on the upper ends of the preheating tubes 56, and the end of the air outlet pipe 2 away from the heating tube 1 is through-connected with the transition box 57.

[0054] The diameter of the transition pipe 4 is smaller than that of the air outlet pipe 2, so a large amount of water vapor inside the air outlet pipe 2 remains after entering the transition pipe 4. During specific operation, before the sodium glutamate solution inside the heating cylinder 1 evaporates and crystallizes, the sodium glutamate solution is poured into the preheating cylinder 5 through the inlet 51. At this time, excess water vapor enters the transition box 57 through the air outlet pipe 2, and the water vapor enters the preheating tube 56 through the transition box 57. Then, the water vapor inside the preheating tube 56 can preheat the sodium glutamate solution. The preheating tube 56 is circumferentially provided with a plurality of sodium glutamate solution to make the sodium glutamate solution inside the preheating cylinder 5 more evenly heated.

[0055] Therefore, the water vapor and the preheating tube 56 cooperate with each other to preheat the sodium glutamate solution inside the preheating cylinder 5, and at the same time, the waste heat of the water vapor can be utilized, which not only reduces the pollution of waste heat to the environment, but also makes the evaporation and crystallization efficiency of the preheated sodium glutamate solution higher after entering the heating cylinder 1.

[0056] The water vapor condenses into water droplets inside the preheating tube 56 and adheres to the inside of the preheating tube 56 .

[0057] In order to prevent the water droplets attached to the inner wall of the preheating tube 56 from affecting the heat conduction effect of the preheating tube 56, a rotating coupling 561 is arranged inside the preheating tube 56 of the present invention. The upper end of the rotating coupling 561 is installed on the top of the preheating tube 56 through a bearing. A spiral blade 562 is installed on the circumferential surface of the rotating coupling 561, which is tightly attached to the inner wall of the preheating tube 56. A pulley 563 is installed at one end of the rotating coupling 561 located in the transition box 57, and the pulleys 563 are connected by a belt 564 for transmission.

[0058] Any one of the rotating couplings 561 is connected to the output shaft of an external motor (not shown in the figure). During specific operation, the external motor is started, and the output shaft of the external motor drives any one of the rotating couplings 561 to rotate during rotation. During rotation of the rotating coupling 561, the pulley 563 and the belt 564 cooperate with each other to drive the remaining rotating couplings 561 to rotate. During rotation of the rotating coupling 561, the spiral blade 562 is driven to rotate. During rotation of the spiral blade 562, the water droplets attached to the inside of the preheating tube 56 can be pushed downward and discharged from the bottom of the preheating tube 56 to prevent the water droplets attached to the inner wall of the preheating tube 56 from affecting the heat conduction effect of the preheating tube 56. At the same time, the spiral blade 562 can also push the water vapor downward to prevent the water vapor from being deposited and condensed inside the transition box 57, resulting in water droplets remaining inside the transition box 57 or even forming water nests, which affects the efficiency of water vapor entering the preheating tube 56.

[0059] When the sodium glutamate solution in the heating cylinder 1 is completely evaporated and crystallized, the actions of Example 1 are repeated and the water pump 53 is started. The water pump 53 can pump the sodium glutamate solution into the heating cylinder 1 through the cooperation of the water inlet pipe 55 and the water outlet pipe 54, thereby continuously evaporating and crystallizing the sodium glutamate solution.

[0060] Finally, see Fig. 9 The present invention also provides a high-efficiency and low-energy consumption amino acid evaporation crystallization process, and its use method includes the following steps: S1: blocking treatment, pumping sodium glutamate solution into the preheating cylinder 5 through the outlet, blocking the discharge trough 15, and pumping sodium glutamate solution into the heating cylinder 1 through the water pump 53.

[0061] S2: Heating treatment, heating the heating tube 1 by an external heating device (resistance wire, etc.), the water vapor generated during the heating process can enter the spiral groove 3 through the outlet pipe 2 and the transition pipe 4, and the heating tube 1 is kept warm;

[0062] S3: Preheating treatment, excess water vapor enters the transition box 57 through the outlet pipe 2, and the water vapor enters the preheating tube 56 through the transition box 57, and then the water vapor in the preheating tube 56 can preheat the sodium glutamate solution.

[0063] S4: Material taking process, during the downward movement of the moving connecting block 132, the pressing roller 133 first contacts the sodium glutamate solid at the bottom of the heating cylinder 1, at which time the bevel gear 136 and the annular bevel rack plate 135 are fine-tuned and meshed, and the rotating shaft 11 drives the pressing roller 133 to rotate circumferentially during the rotation of the rotating shaft 11. During the circumferential rotation of the pressing roller 133 around the rotating shaft 11, the bevel gear 136 and the annular bevel rack plate 135 are meshed with each other and can also rotate on their own, and then the pressing roller 133 during the rotation process can crush the sodium glutamate after evaporation and crystallization to obtain sodium glutamate powder.

[0064] When the sodium glutamate solid is pressed, the moving block 13 continues to move downward, and the elastic telescopic rod 131 contracts at this time to make way for the moving block 13, and the moving connecting block 132 no longer moves. During the moving block 13 moving downward, the scraper 14 is driven to move downward and abut against the inner bottom surface of the heating cylinder 1. At this time, the discharge chute 15 is opened, and the driving motor 12 is started. During the rotation of the driving motor 12, the rotating shaft 11 is driven to rotate. During the rotation of the rotating shaft 11, the scraper 14 is driven to rotate through the moving block 13. During the rotation of the scraper 14, the sodium glutamate powder can be scraped out from the discharge chute 15.

[0065] It will be apparent to those skilled in the art that the invention is not limited to the details of the exemplary embodiments described above and that the invention can be implemented in other specific forms without departing from the spirit or essential features of the invention. Therefore, the embodiments should be considered exemplary and non-limiting in all respects, and the scope of the invention is defined by the appended claims rather than the foregoing description, and it is intended that all variations falling within the meaning and scope of the equivalent elements of the claims be included in the invention. Any reference numeral in a claim should not be considered as limiting the claim to which it relates.

[0066] In addition, it should be understood that although the present specification is described according to implementation modes, not every implementation mode contains only one independent technical solution. This description of the specification is only for the sake of clarity. Those skilled in the art should regard the specification as a whole. The technical solutions in each embodiment may also be appropriately combined to form other implementation modes that can be understood by those skilled in the art.

Claims

1. A high-efficiency and low-energy consumption amino acid evaporation crystallization device, comprising a heating cylinder (1), characterized in that: The upper end surface of the heating tube (1) is provided with an air outlet pipe (2), a spiral groove (3) is provided inside the side wall of the heating tube (1), a transition pipe (4) is provided on the air outlet pipe (2) and is connected therewith, and one end of the transition pipe (4) away from the air outlet pipe (2) is connected to the spiral groove (3), wherein; The upper end surface of the heating cylinder (1) is rotatably mounted with a rotating shaft (11) extending vertically, the upper end surface of the rotating shaft (11) is mounted with a driving motor (12), the portion of the rotating shaft (11) located inside the heating cylinder (1) is rotatably mounted with a moving block (13) extending leftwards and rightwards and moving vertically, a scraper (14) is mounted on the right side of the moving block (13), the lower end surface of the heating cylinder (1) is provided with a discharge trough (15) extending vertically, and the upper end surface of the heating cylinder (1) is mounted with an electronic hygrometer (16); The lower end surface of the moving block (13) is installed with an elastic telescopic rod (131), and the end of the elastic telescopic rod (131) away from the moving block (13) is installed with a moving connecting block (132). The left end surface of the moving connecting block (132) is installed with a pressing roller (133) extending left and right through a bearing, and a counterweight (134) is installed on the side of the pressing roller (133) away from the moving connecting block (132). An annular bevel rack plate (135) is installed at the bottom of the heating cylinder (1), and a bevel gear (136) matched with the annular bevel rack plate (135) is installed on the right side of the pressing roller (133); The circumferential surface of the pressing roller (133) is provided with a bidirectional thread groove (137); an L-shaped fixed frame (138) is arranged on the left side of the upper end surface of the movable connecting block (132); a vertical section of the fixed frame (138) is fixedly connected to the movable connecting block (132); a horizontal section of the fixed frame (138) is located directly above the pressing roller (133); a scraping plate (139) which slides left and right is arranged on the lower end surface of the horizontal section of the fixed frame (138); and a scraping protrusion (130) which cooperates with the bidirectional thread groove (137) is arranged on the lower end surface of the scraping plate (139).

2. The high-efficiency and low-energy consumption amino acid evaporation and crystallization equipment according to claim 1 is characterized in that: The front end surface of the rotating shaft (11) located inside the heating cylinder (1) is equipped with a stirring rod (111) facing forward horizontally, and a plurality of stirring rods (112) evenly distributed from front to back are installed on the lower side of the circumferential surface of the stirring rod (111).

3. The high-efficiency and low-energy consumption amino acid evaporation and crystallization equipment according to claim 1 is characterized in that: A preheating cylinder (5) is arranged on the right side of the heating cylinder (1), and an inlet (51) is installed on the right side of the upper end surface of the preheating cylinder (5). The heating cylinder (1) and the preheating cylinder (5) are connected via a horizontal frame (52), a water pump (53) is installed on the horizontal frame (52), a water outlet of the water pump (53) is connected to the heating cylinder (1) via a water outlet pipe (54), a water inlet of the water pump (53) is connected to the preheating cylinder (5) via a water inlet pipe (55), and a preheating pipe (56) matching with the air outlet pipe (2) is installed on the preheating cylinder (5).

4. The high-efficiency and low-energy consumption amino acid evaporation and crystallization equipment according to claim 3 is characterized in that: The preheating tubes (56) are evenly arranged in a plurality in the circumferential direction and are of a vertically through-connected structure. A transition box (57) is installed at the upper end of the preheating tubes (56) and is through-connected therewith. The end of the air outlet pipe (2) away from the heating tube (1) is through-connected with the transition box (57).

5. The high-efficiency and low-energy consumption amino acid evaporation and crystallization equipment according to claim 4 is characterized in that: The preheating tube (56) is provided with a rotating shaft (561) inside. The upper end of the rotating shaft (561) is installed at the top of the preheating tube (56) through a bearing. A spiral blade (562) is installed on the circumferential surface of the rotating shaft (561). A pulley (563) is installed at one end of the rotating shaft (561) located in the transition box (57). The pulleys (563) are connected by a belt (564).

6. A high-efficiency and low-energy consumption amino acid evaporation crystallization process, comprising the high-efficiency and low-energy consumption amino acid evaporation crystallization device according to any one of claims 1, 3, 4 or 5, characterized in that: The method of use includes the following steps: S1: blocking treatment, pumping sodium glutamate solution into the preheating cylinder (5) through the outlet, blocking the discharge trough (15), and pumping sodium glutamate solution into the heating cylinder (1) through the water pump (53); S2: Heating treatment, wherein the sodium glutamate is heated by the heating cylinder (1), and at the same time, the evaporated water vapor enters the spiral groove (3) through the outlet pipe (2) and the transition pipe (4) to perform heat preservation treatment on the heating cylinder (1); S3: preheating treatment, the excess water vapor enters the preheating tube (56) through the gas outlet pipe (2) and the transition box (57) to preheat the glutamic acid ammonia solution in the preheating cylinder (5); S4: material taking process. When the sodium glutamate solution is evaporated and dried to obtain sodium glutamate powder, the discharging chute (15) is opened and the sodium glutamate powder is taken out from the discharging chute (15) by means of a scraper (14).

Citation Information

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