A non-breakage, body-boosting hair care composition, its preparation and use

Abstract

The application discloses a hair nourishing and breakage preventing composition, a preparation method and application thereof, and comprises the following raw materials in percentage by mass: Candida oleaginosus / glucose / fermentation product of rapeseed oil acid methyl ester 1-2%; camellia seed oil 1-2%; sorbitol 8-15%; hair conditioner 8-16%; emulsifier 5-13%; and deionized water in excess. The hair nourishing and breakage preventing composition provides rich nutrients for hair, improves the moisturizing, repairing and anti-inflammatory effects of hair / scalp, effectively improves dry, damaged and inflammatory problems of hair, and mainly uses natural ingredients as active ingredients, is safe and non-irritating, and reduces damage of hair / scalp.

Description

TECHNICAL FIELD

[0001] The present application relates to the technical field of daily chemicals, in particular to a hair growth and breakage prevention hair care composition and a preparation method and application thereof. BACKGROUND

[0002] With the development of the beauty industry, people's hair dyeing and perming frequency is increasing, and hair dyeing and perming and other hair beauty behaviors can greatly damage the hair and scalp, making the hair very fragile and prone to dry, brittle, and frizzy hair. Therefore, various hair care products such as hair care shampoo and hair essence have emerged in the market.

[0003] At present, hair care products are endowed with various functions by adding active ingredients such as antidandruff agents, moisturizing agents, sunscreen agents, and nutrient agents, so that the hair can be soft, easy to comb, anti-static, and shiny when using the hair care products, so that the damaged hair due to hair dyeing and perming can be repaired to some extent. However, current hair care products are mainly chemical synthetic substances, and long-term use can cause chemical components to accumulate on the scalp, thereby damaging the scalp. Therefore, there is an urgent need for a safe and non-irritating hair care product that can be used long-term. SUMMARY

[0004] The present application provides a hair growth and breakage prevention hair care composition and a preparation method and application thereof to repair hair damage and enhance hair quality to achieve breakage prevention effect, and can be used long-term safely and non-irritating.

[0005] In order to solve the above technical problems, in a first aspect, the present application provides a hair growth and breakage prevention hair care composition, comprising the following raw materials in mass percentage:

[0006] Candida oleaginosus / glucose / canola oil acid methyl ester fermentation product 1-2%;

[0007] Camellia seed oil 1-2%;

[0008] Sorbitol 8-15%;

[0009] Hair conditioner 8-16%;

[0010] Emulsifier 5-13%;

[0011] Deionized water balance.

[0012] The fermentation product of Candida melibiosica / glucose / methyl oleate is a secondary metabolite of microorganism produced by fermentation of sugar and plant oil as carbon source under certain conditions, and is a biological surfactant.

[0013] The camellia seed oil is the main component of camellia seed, which is rich in nutrients, fatty acids (unsaturated fatty acids 93%, including oleic acid 82% and linoleic acid 11%), camellin, tea polyphenol, saponin, tannin, and is rich in antioxidants and squalene with anti-inflammatory effect. Squalene and flavonoids have excellent effect on anticancer. Camellia oil is also rich in vitamin E, calcium, iron, zinc and other trace elements. The zinc element, which is praised by medical scientists and nutritionists as "the flower of life", is 10 times that of soybean oil. The types of amino acids contained in tea oil are the most among all edible oils.

[0014] The sorbitol (glucose alcohol) is a slowly metabolized sugar alcohol by human, which is similar in structure to monosaccharide and can be obtained by reducing the aldehyde group of glucose to hydroxyl group. It is stable in chemical properties, not easy to be oxidized by air, not easy to be fermented by various microorganisms, and has good heat resistance and does not decompose at high temperature (200℃). The six hydroxyl groups in the sorbitol molecule can effectively combine some free water, and the addition has certain effect on improving the water content of the product and reducing the water activity.

[0015] In some embodiments, the following raw materials are included in mass percentage:

[0016] The fermentation product of Candida melibiosica / glucose / methyl oleate is 1% to 1.5%;

[0017] The camellia seed oil is 1% to 1.5%;

[0018] The sorbitol is 10% to 12%;

[0019] The hair conditioner is 10% to 13%;

[0020] The emulsifier is 8% to 10%;

[0021] The deionized water is the balance.

[0022] In some embodiments, the mass ratio between the fermentation product of Candida melibiosica / glucose / methyl oleate, the camellia seed oil and the sorbitol is 1:1:8.

[0023] In some embodiments, the leave-on conditioner includes glycerin and propylene glycol, and one or more of polyurethane-10 and phenoxyethanol, one or more of polyethylene glycol-90M, butylated hydroxytoluene, and silica.

[0024] In some embodiments, the emulsifier includes one or more of stearyltrimethylammonium chloride, PEG-40 glyceryl stearate, glyceryl stearate, potassium cetyl phosphate, stearic acid, hydrogenated lecithin, phytosteol, and tocopheryl acetate.

[0025] In some embodiments, one or more of thickening agents, preservatives, nutrients, and fragrances are further included.

[0026] In some embodiments, the thickening agent includes one or more of guar hydroxypropyltrimonium chloride and hydroxyethylcellulose.

[0027] The preservative includes one or more of benzyl alcohol, phenoxyethanol, benzoic acid, and sorbic acid.

[0028] The nutrient is one or more of hydrolyzed protein, vitamins, and shea butter.

[0029] In a second aspect, the present application further provides a method for preparing the hair conditioning composition of the first aspect, comprising the following steps:

[0030] Step one, weighing the raw materials of the hair conditioning composition;

[0031] Step two, adding sorbitol to deionized water, stirring and heating to 68-75°C to obtain solution A;

[0032] Step three, stirring and heating the Candida oleaginosus / glucose / methyl oleate fermentation product, camellia seed oil, and emulsifier to 68-75°C to obtain solution B;

[0033] Step four, adding solution A to solution B under stirring, continuing to stir, and naturally cooling to a temperature of 40-45°C;

[0034] Step five, adding the remaining raw materials at 40-45°C, continuing to stir for 15-20 min, cooling to room temperature, and filtering to obtain the hair conditioning composition.

[0035] In some embodiments, the stirring temperature of steps two and three is 70°C, the stirring temperature of steps four and five is 45°C, and the stirring time of step five is 15 min.

[0036] In a third aspect, the present application further provides use of the hair conditioning composition of the first aspect in the preparation of a hair care product.

[0037] Compared with the prior art, the present application has the following beneficial effects:

[0038] The volume breakage-preventing hair care composition of the present application can enhance hair quality and is safe and non-irritating, and the combination of Candida bombicola / glucose / methyl oleate fermentation product, camellia seed oil and sorbitol can have a synergistic effect, providing rich nutrients for the hair, improving the moisturizing, repairing and anti-inflammatory effects of the hair / skin, effectively improving the dryness, damage and inflammation of the hair, and the active ingredients of the present application are mainly natural ingredients, safe and non-irritating, reducing the damage to the hair / skin. DETAILED DESCRIPTION

[0039] In order to make the above-mentioned purposes, features and advantages of the present application more obvious and easy to understand, the specific embodiments of the present application are described in detail below. In the following description, a large number of specific details are set forth in order to fully understand the present application. However, the present application can be implemented in many other ways different from those described herein, and those skilled in the art can make similar improvements without departing from the scope of the present application, so the present application is not limited to the specific embodiments disclosed below.

[0040] The term "prepared from" as used herein is synonymous with "comprising". The terms "comprising", "including", "having" "with" "contain" or any other similar forms are intended to cover non-exclusive inclusion. For example, a composition, step, method, article or device comprising the listed elements does not necessarily limit to only those elements, but can include other elements not explicitly listed or inherent to such composition, step, method, article or device.

[0041] When a range, a preferred range, or a range defined by a series of upper preferred values and lower preferred values for an equivalent, concentration, or other value or parameter is expressed, it should be understood that all ranges formed by any pairings of an upper range limit or preferred value with a lower range limit or preferred value, regardless of whether the range is explicitly disclosed, are specifically disclosed. For example, when the range "1 to 5" is disclosed, the described range should be interpreted to include the range "1 to 4", "1 to 3", "1 to 2", "1 to 2 and 4 to 5", "1 to 3 and 5", etc. When numerical ranges are described herein, unless otherwise stated, the range is intended to include its end values and all integers and fractions within the range, unless otherwise stated.

[0042] In addition, the indefinite articles "a" and "an" before an element or component of the present application are not intended to be limiting regarding the number of elements or components (i.e., one or at least one). Therefore, "a" or "an" should be interpreted to mean one or at least one, and the singular form of an element or component should include the plural unless the number is obviously meant to be singular.

[0043] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs. The terminology used in the description herein is for describing particular embodiments only and is not intended to be limiting of the application. As used herein, the term "and / or" includes any and all combinations of one or more of the associated listed items.

[0044] Example 1

[0045] A hair conditioning composition for preventing breakage and increasing volume, comprising the following raw materials by mass percentage:

[0046] Mycococcus / Mannitol / Methyl Canolaate Fermentation Product 1%;

[0047] Camellia Seed Oil 1%;

[0048] Sorbitol 8%;

[0049] Glycerin 5%;

[0050] Propylene Glycol 2%;

[0051] Polyurethane-10 0.5%;

[0052] Phenoxyethanol 0.5%;

[0053] Polyethylene Glycol 90M 0.05%;

[0054] Silica 0.05%;

[0055] Butylated Hydroxytoluene 0.05%;

[0056] Stearyltrimethylammonium Chloride 5%;

[0057] PEG-40 Glycerin Stearate 1%;

[0058] Deionized Water q.s.

[0059] A method for preparing a hair conditioning composition for preventing breakage and increasing volume, comprising the following steps:

[0060] Step 1, weighing the raw materials of the hair conditioning composition for preventing breakage and increasing volume;

[0061] Step 2, adding Sorbitol into deionized water, stirring and heating to 68°C to obtain solution A;

[0062] Step 3, adding Mycococcus / Mannitol / Methyl Canolaate Fermentation Product, Camellia Seed Oil and emulsifier into solution A, stirring and heating to 68°C to obtain solution B;

[0063] Step 4, adding solution A into solution B under stirring, continuing to stir and naturally cooling to 40°C;

[0064] Step five, add the remaining raw materials at 40℃, continue stirring for 15 min, cool to room temperature, filter, to obtain the lush breakage-preventing hair care composition.

[0065] Example 2

[0066] A lush breakage-preventing hair care composition comprising the following raw materials in percentage by mass:

[0067] Meyerozyma guiliardii / glucose / methyl canola oilate fermentation product 2%;

[0068] Camellia seed oil 2%;

[0069] Sorbitol 15%;

[0070] Glycerin 8%;

[0071] Propylene glycol 5%;

[0072] Polyurethane-10 1%;

[0073] Phenoxyethanol 1%;

[0074] Polyethylene glycol 90M 0.2%;

[0075] Silica 0.2%;

[0076] Butylated hydroxytoluene 0.2%;

[0077] Stearyl trimethylammonium chloride 10%;

[0078] Glycerin stearate 1%

[0079] Potassium cetyl phosphate 2%;

[0080] Deionized water q.s.

[0081] A method for preparing a lush breakage-preventing hair care composition comprising the following steps:

[0082] Step one, weigh the raw materials of the lush breakage-preventing hair care composition according to the amount;

[0083] Step two, add sorbitol to deionized water, stir and heat to 75℃ to obtain solution A;

[0084] Step three, stir and heat the Meyerozyma guiliardii / glucose / methyl canola oilate fermentation product, camellia seed oil and emulsifier to 75℃ to obtain solution B;

[0085] Step four, add solution A to solution B under stirring, continue stirring, and naturally cool to a temperature of 45℃;

[0086] Step five, add the remaining raw materials at 45℃, continue stirring for 20 min, cool to room temperature, filter, to obtain the hair care composition with volume and breakage prevention.

[0087] Example 3

[0088] A hair care composition with volume and breakage prevention, comprising the following raw materials by mass percentage:

[0089] Mycococcus / Maltose / Methyl Canolaate Fermentation Product 1.5%;

[0090] Camellia Seed Oil 1.5%;

[0091] Sorbitol 12%;

[0092] Glycerin 6%;

[0093] Propylene Glycol 4%;

[0094] Polyurethane-10 0.8%;

[0095] Phenoxyethanol 0.8%;

[0096] Polyethylene Glycol 90M 0.1%;

[0097] Silica 0.1%;

[0098] Butylated Hydroxytoluene 0.1%;

[0099] Stearyltrimethylammonium Chloride 6%;

[0100] Hydrogenated Lecithin 1%;

[0101] Tocopheryl Acetate 1%;

[0102] Deionized Water q.s.

[0103] A method for preparing a hair care composition with volume and breakage prevention, comprising the following steps:

[0104] Step one, weigh the raw materials of the hair care composition with volume and breakage prevention according to the amount;

[0105] Step two, add sorbitol to deionized water, stir and heat to 70℃ to obtain solution A;

[0106] Step three, stir and heat Mycococcus / Maltose / Methyl Canolaate Fermentation Product, Camellia Seed Oil and emulsifier to 70℃ to obtain solution B;

[0107] Step four, add solution A to solution B under stirring, continue stirring and naturally cool to a temperature of 45℃;

[0108] Step five, add the remaining raw materials at 45℃, continue stirring for 15 min, cool to room temperature, filter, to obtain the hair care composition with volume and breakage prevention.

[0109] Comparative Example 1

[0110] The difference from Example 3 is that no Candida oleaginosus / glucose / canola fatty acid methyl ester fermentation product is added in Comparative Example 1.

[0111] Comparative Example 2

[0112] The difference from Example 3 is that no camellia seed oil is added in Comparative Example 2.

[0113] Comparative Example 3

[0114] The difference from Example 3 is that no sorbitol is added in Comparative Example 3.

[0115] I. Hair strength test

[0116] Test sample: the volumizing breakage-preventing hair care composition prepared in Example 3

[0117] Test purpose and principle: the ability of the sample to strengthen hair is evaluated by a hair multifunctional test system, the hair is stretched at a constant speed by the instrument until the hair breaks, and the test system calculates the work required to break a single hair. The greater the total work required to break the hair, the stronger the hair.

[0118] Test method: according to the method for evaluating the strengthening effect of hair care products in T / GDCC 012-2020, an ex vivo method is used. Take 10 bundles of commercially available human hair, wash and dry naturally at room temperature; blank group: take one hair from each bundle of hair to test the total stretching work and calculate the average value; test group: use the volumizing breakage-preventing hair care composition prepared in Example 3 to treat each bundle of hair, and then wash and dry naturally at room temperature. Take one hair from each bundle of hair to measure the total stretching work and calculate the average value.

[0119] Test results: as shown in Table 1.

[0120] Table 1: Hair stretching test results

[0121] Total work of stretching of single hair average value / J Total work of stretching of single hair average value / J Improvement rate 0.0136 0.0198 45.59％

[0122] It can be seen that the volumizing breakage-preventing hair care composition prepared in the present application has obvious improvement effect on hair strength.

[0123] II. Human test

[0124] Test sample: the volumizing breakage-preventing hair care composition prepared in Examples 1 to 3 and Comparative Examples 1 to 3 is made into a hair conditioner by adding a thickening agent, a preservative and a fragrance.

[0125] Test object: 60 volunteers aged 25 to 55 with hair frizz are recruited, and 10 people are randomly assigned to each example and comparative example.

[0126] Test procedure: register at the front desk, get the hair conditioner sample and commercially available shampoo; wash the hair with commercially available shampoo, wipe the hair until no water drops; take an appropriate amount of hair conditioner and evenly apply it on the hair, keep it for 8-15 minutes; wash it with clean water, dry it; go to the front desk and fill in the hair conditioner evaluation form, the score of each evaluation item is 1-10, the higher the score, the better the user experience.

[0127] Test results: calculate the average score of each item for the volunteers in the same example, and the score results are shown in Table 2.

[0128] Table 2 Hair conditioner use experience evaluation form

[0129] Evaluation item Example 1 Example 2 Example 3 Comparative Example 1 Comparative Example 2 Comparative Example 3 Tugging strength 9.1 9.2 9.4 7.1 6.9 7.8 Glossiness 9.1 8.9 9.5 5.4 4.6 7.7 Smoothness 9 8.8 9.3 4.8 6.1 8.4 Volume 8.8 9.2 9.6 4.5 6.7 8.9 Lightness 9.3 9 9.5 6.6 8.7 5.1 Easy washing 9.3 8.6 9.2 7.5 9.1 6.3 Irritation 9.9 9.8 9.9 9.6 9.7 9.6 Total score 64.5 63.5 66.4 45.5 51.8 53.8

[0130] From Table 2, it can be seen that the evaluation scores of Examples 1-3 are significantly better than those of Comparative Examples 1-3; comparison of Example 3 with Comparative Examples 1-3 shows that the fermentation product of Pseudozyma antarctica / glucose / rapeseed oil acid methyl ester, camellia seed oil and sorbitol as active ingredients can have a synergistic effect.

[0131] The technical features of the above-described examples can be combined in any manner, and to make the description concise, not all possible combinations of the technical features in the above-described examples are described, however, as long as the combinations of the technical features do not exist contradictions, they should be considered as the scope of the present disclosure.

[0132] The above-described specific examples further illustrate the purpose, technical solutions and beneficial effects of the present application, it should be understood that the above-described only for the specific embodiments of the present application, and not used to limit the scope of protection of the present application. It is particularly pointed out that for those skilled in the art, any modification, equivalent replacement, improvement, etc. made within the spirit and principles of the present application shall be included in the scope of protection of the present application.

Claims

1. A non-breakage, body- enhancing hair care composition characterized in that, consists of the following raw materials by mass percentage: Blastophagus fermentum / glucose / methyl rape seed oil acid fermentation product 1%~1.5%; Camellia seed oil 1%~1.5%; Sorbitol 10%~12%; Hair conditioner 10%~13%; Emulsifier 8%~10%; One or more of thickening agent, preservative, nutrient agent and fragrance in proper amount; Deionized water in residual amount; The mass ratio between the blastophagus fermentum / glucose / methyl rape seed oil acid fermentation product, camellia seed oil and sorbitol is 1:1:8; The hair conditioner is one or more of glycerin and propylene glycol, and one or more of polyurethane-10 and phenoxyethanol, one or more of polyethylene glycol-90M, butylated hydroxytoluene and silica; The emulsifier is one or more of steartrimonium chloride, PEG-40 glyceryl stearate, glyceryl stearate, potassium cetyl phosphate, stearic acid, hydrogenated lecithin, phytol and tocopheryl acetate; The thickening agent is one or more of guar hydroxypropyltrimonium chloride and hydroxyethyl cellulose; The preservative is one or more of benzyl alcohol, phenoxyethanol, benzoic acid and sorbic acid; The nutrient agent is one or more of hydrolyzed protein, vitamin and shea butter; The method for preparing the hair conditioning composition comprises the following steps: Step one, weighing the raw materials of the hair conditioning composition; Step two, adding sorbitol to deionized water, stirring and heating to 68~75℃ to obtain solution A; Step three, stirring and heating blastophagus fermentum / glucose / methyl rape seed oil acid fermentation product, camellia seed oil and emulsifier to 68~75℃ to obtain solution B; Step four, adding solution A to solution B under stirring, continuing to stir and naturally cooling to 40~45℃; Step five, adding the remaining raw materials at 40~45℃, continuing to stir for 15~20min, cooling to room temperature, filtering to obtain the hair conditioning composition.

2. The body- volume- preserving hair breakage- preventing hair composition of Claim 1 wherein The stirring temperature of step two and step three is 70℃, and the stirring temperature of step four and step five is 45℃, and the stirring time of step five is 15min.

3. The use of the hair conditioning composition according to claim 1 or 2 in the preparation of a hair care product.