A control system for preparing impregnation liquid for metal treatment

By designing the processing control system for metal treatment, the stirring parameters of the preparation and addition of active ingredients in the infiltration liquid are monitored and dynamically corrected in real time, the problem of low reliability in the setting of process parameters in the prior art is solved, and production quality and efficiency are improved.

CN118846928BActive Publication Date: 2025-05-09XUZHOU MATTSON NEW MATERIALS RES INST CO LTD
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Patent Information

Application Number
CN202411328222.6
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-09-24
Publication Date
2025-05-09
Estimated Expiration
2044-09-24

AI Technical Summary

Technical Problem

The existing monitoring methods for preparing leachate for metal treatment are insufficient subjectivity and accuracy, resulting in low reliability in setting process parameters, unqualified production quality or reduced production efficiency.

Method used

Design a processing control system for preparing and processing for metal treatment, including initial setting, adjustment and judgment of stirring parameters for the preparation of infiltration liquid and addition of active ingredients, and improve the control accuracy of process parameters through real-time monitoring and dynamic correction.

Benefits of technology

By scientifically and reasonably setting and adjusting the stirring parameters of the preparation of infiltration liquid and the addition of active ingredients, ensure that the infiltration liquid is fully mixed and improve the production quality and production efficiency of the infiltration liquid for metal treatment.

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Abstract

The invention relates to the field of metal treatment impregnation liquid preparation processing control, and specifically discloses a metal treatment impregnation liquid preparation processing control system. The invention selects appropriate stirring parameters for preparing the impregnation liquid according to information of an impregnating agent and a solvent, and considers various influencing factors such as viscosity and volatility; selects appropriate stirring parameters for adding the active ingredient according to information of adding an active ingredient, and considers various influencing factors such as the solubility and reaction rate of the active ingredient, thereby making the setting of stirring parameters for preparing the impregnation liquid and adding the active ingredient more reliable; in combination with the actual production conditions of preparing the impregnation liquid and adding the active ingredient, the stirring parameters for preparing the impregnation liquid and adding the active ingredient are dynamically corrected to form a closed-loop control, thereby improving the control accuracy of the stirring parameters for preparing the impregnation liquid and adding the active ingredient, thereby ensuring the production quality and production efficiency of the metal treatment impregnation liquid preparation.
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Description

Technical Field

[0001] The invention relates to the field of preparation and processing control of an impregnation liquid for metal treatment, and in particular to a preparation and processing control system of an impregnation liquid for metal treatment. Background Art

[0002] Metal treatment impregnation fluid is a chemical solution used to improve the surface properties of metals. The impregnation process involves immersing the metal in the solution so that the active ingredients in the solution penetrate the metal surface and react chemically with it, thereby changing the properties of the metal surface. It is usually used for metal processing, surface treatment and lubrication. Metal treatment impregnation fluid can improve the surface quality and durability of metals and extend the service life of metals.

[0003] Monitoring the preparation process of metal treatment impregnation liquid can ensure product quality, safety and cost control, improve production efficiency, and is of great significance to the smooth progress of the production process and the stability of product quality.

[0004] There are some shortcomings in the existing monitoring methods for the preparation of impregnation liquid for metal treatment: First, when initially setting the process parameters for the preparation of impregnation liquid for metal treatment, they are often set based on the experience of the operator, which is subjective and does not combine the characteristics of the raw materials, such as dosage and material, to conduct quantitative analysis to obtain matching process parameters. As a result, the setting of process parameters is not reliable enough, which can easily make the production quality of the impregnation liquid for metal treatment unqualified or reduce production efficiency.

[0005] Secondly, after the process parameters for preparing the impregnation liquid for metal treatment are running according to the set initial values, the actual production situation is not monitored in real time. Due to the influence of factors such as equipment aging, production environment, and raw material quality, the actual production status may not meet expectations. At this time, it is necessary to dynamically correct the initially set process parameters, which makes the existing method for regulating the process parameters not very accurate and unable to guarantee the production quality and production efficiency of the impregnation liquid for metal treatment. Summary of the invention

[0006] In view of the above problems, the present invention proposes a control system for the preparation and processing of an impregnation liquid for metal treatment, which realizes the function of controlling the preparation and mixing processing of the impregnation liquid for metal treatment.

[0007] The technical solution adopted by the present invention to solve its technical problem is: the present invention provides an impregnation liquid preparation and processing control system for metal treatment, including an impregnation liquid preparation and stirring parameter initial setting module, an impregnation liquid preparation and stirring parameter adjustment and judgment module, an impregnation liquid preparation and stirring parameter dynamic correction module, an active ingredient addition and stirring parameter initial setting module, an active ingredient addition and stirring parameter adjustment and judgment module, an active ingredient addition and stirring parameter dynamic correction module and a database.

[0008] The impregnation liquid preparation stirring parameter adjustment and judgment module is respectively connected to the impregnation liquid preparation stirring parameter initial setting module and the impregnation liquid preparation stirring parameter dynamic correction module, the active ingredient addition stirring parameter initial setting module is respectively connected to the impregnation liquid preparation stirring parameter dynamic correction module and the active ingredient addition stirring parameter adjustment and judgment module, the active ingredient addition stirring parameter dynamic correction module is connected to the active ingredient addition stirring parameter adjustment and judgment module, and the database is respectively connected to the impregnation liquid preparation stirring parameter initial setting module and the active ingredient addition stirring parameter initial setting module.

[0009] The initial setting module of the stirring parameters for the preparation of the impregnation liquid is used to obtain the raw material information for the preparation of the impregnation liquid for metal treatment, analyze the stirring parameters of the impregnation liquid preparation process in the production process of the impregnation liquid for metal treatment, where the stirring parameters of the impregnation liquid preparation process include the stirring speed, stirring time and stirring temperature, and set the stirring parameters of the impregnation liquid preparation process.

[0010] The module for adjusting and judging the stirring parameters of the impregnation liquid preparation is used to obtain the sediment volume and the number of bubbles in the impregnation liquid at each sampling time point during the monitoring period of the impregnation liquid preparation, and to judge whether the stirring parameters of the impregnation liquid preparation process need to be adjusted.

[0011] Dynamic correction module for stirring parameters of impregnation liquid preparation: used to obtain the adjustment direction and adjustment amount of stirring parameters of the impregnation liquid preparation process, and correct the stirring parameters of the impregnation liquid preparation process.

[0012] Active ingredient adding stirring parameter initial setting module: used to obtain the active ingredient information added to the metal treatment impregnation liquid, analyze the stirring parameters of the active ingredient adding process in the production process of the metal treatment impregnation liquid, where the stirring parameters of the active ingredient adding process include stirring speed, stirring time and stirring temperature, and set the stirring parameters of the active ingredient adding process.

[0013] Active ingredient addition stirring parameter adjustment judgment module: used to obtain the number of bubbles and the amount of active ingredient dissolved in the impregnation liquid at each sampling time point during the active ingredient addition monitoring period, and determine whether the stirring parameters of the active ingredient addition process need to be adjusted.

[0014] Active ingredient addition stirring parameter dynamic correction module: used to obtain the adjustment direction and adjustment amount of the stirring parameters of the active ingredient addition process, and correct the stirring parameters of the active ingredient addition process.

[0015] Database: used to store historical production information of impregnation fluids for metal treatment.

[0016] Compared with the prior art, the preparation and processing control system of an impregnation liquid for metal treatment described in the present invention has the following beneficial effects: 1. The present invention selects appropriate stirring speed, stirring time and stirring temperature for preparing the impregnation liquid according to the type and amount of the impregnation agent and solvent for preparing the impregnation liquid for metal treatment, and considers various influencing factors such as viscosity, volatility, reaction intensity, density and surface tension, thereby making the setting of the process parameters of the impregnation liquid preparation process more reliable, thereby ensuring that the impregnation liquid is fully mixed and evenly, achieving the ideal impregnation effect, and ensuring the production quality of the impregnation liquid for metal treatment.

[0017] 2. The present invention selects a suitable stirring speed, stirring time and stirring temperature for adding the active ingredient according to the type, concentration and amount of the active ingredient added to the impregnation solution for metal treatment, and takes into account various influencing factors such as the solubility and reaction rate of the active ingredient, thereby making the setting of the process parameters of the active ingredient adding process more reliable, thereby ensuring that the active ingredient is fully and evenly mixed and guaranteeing the production and preparation quality of the impregnation solution for metal treatment.

[0018] 3. The present invention monitors the sediment volume and the number of bubbles in the impregnation liquid during the preparation of the impregnation liquid, determines whether the stirring parameters of the impregnation liquid preparation process need to be adjusted, and further obtains the adjustment direction and adjustment amount of the stirring parameters of the impregnation liquid preparation process. It can dynamically correct the stirring parameters of the impregnation liquid preparation process in combination with actual production conditions to form a closed-loop control, thereby improving the control accuracy of the stirring parameters of the impregnation liquid preparation process, thereby ensuring the production quality and production efficiency of the preparation of the impregnation liquid for metal treatment.

[0019] 4. The present invention monitors the number of bubbles in the impregnation liquid and the dissolution of the active ingredient during the process of adding the active ingredient, determines whether the stirring parameters of the active ingredient adding process need to be adjusted, and further obtains the adjustment direction and adjustment amount of the stirring parameters of the active ingredient adding process. It can dynamically correct the stirring parameters of the active ingredient adding process in combination with the actual production situation to form a closed-loop control, thereby improving the control accuracy of the stirring parameters of the active ingredient adding process, thereby ensuring the production quality and production efficiency of the preparation of the impregnation liquid for metal treatment. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required for describing the embodiments are briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0021] Figure 1 This is a system module connection diagram of the present invention. DETAILED DESCRIPTION

[0022] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0023] See also Figure 1 As shown, the present invention provides an impregnation liquid preparation and processing control system for metal treatment, including an impregnation liquid preparation and stirring parameter initial setting module, an impregnation liquid preparation and stirring parameter adjustment and judgment module, an impregnation liquid preparation and stirring parameter dynamic correction module, an active ingredient addition and stirring parameter initial setting module, an active ingredient addition and stirring parameter adjustment and judgment module, an active ingredient addition and stirring parameter dynamic correction module and a database.

[0024] The impregnation liquid preparation stirring parameter adjustment and judgment module is respectively connected to the impregnation liquid preparation stirring parameter initial setting module and the impregnation liquid preparation stirring parameter dynamic correction module, the active ingredient addition stirring parameter initial setting module is respectively connected to the impregnation liquid preparation stirring parameter dynamic correction module and the active ingredient addition stirring parameter adjustment and judgment module, the active ingredient addition stirring parameter dynamic correction module is connected to the active ingredient addition stirring parameter adjustment and judgment module, and the database is respectively connected to the impregnation liquid preparation stirring parameter initial setting module and the active ingredient addition stirring parameter initial setting module.

[0025] The module for initially setting stirring parameters for preparing the impregnation liquid is used to obtain information on raw materials for preparing the impregnation liquid for metal treatment, analyze stirring parameters of the impregnation liquid preparation process during the production of the impregnation liquid for metal treatment, wherein the stirring parameters of the impregnation liquid preparation process include stirring speed, stirring time and stirring temperature, and set the stirring parameters of the impregnation liquid preparation process.

[0026] Furthermore, the specific working process of the initial setting module of the stirring parameters for preparing the impregnation liquid includes: extracting the historical production information of the impregnation liquid for metal treatment stored in the database, obtaining the preparation raw material information of each historical production of the impregnation liquid for metal treatment and the stirring parameters of the impregnation liquid preparation process, analyzing the relationship between the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process and the type and amount of the impregnating agent and solvent for preparing the metal treatment impregnation liquid, and constructing a prediction model for the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process.

[0027] As a preferred solution, the relationship between the stirring parameters of the impregnation solution preparation process and the raw material information of the impregnation solution for metal treatment can be presented in the form of a table, a graph, a function, etc.

[0028] The raw material information for preparing the impregnation liquid for metal treatment is obtained, and the types and amounts of the impregnation agent and solvent for preparing the impregnation liquid for metal treatment are obtained, and the information is substituted into the prediction model of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process to obtain the reference stirring speed, reference stirring time and reference stirring temperature of the impregnation liquid preparation process.

[0029] Furthermore, the specific working process of the initial setting module of the stirring parameters for preparing the impregnation liquid further includes: obtaining the viscosity of the impregnation agent, the surface tension of the impregnation agent, the volatility of the solvent and the surface tension of the solvent for preparing the impregnation liquid for metal treatment, and recording them as , and obtain the reaction intensity and density difference of the impregnant and solvent for preparing the metal treatment impregnation solution, which are recorded as .

[0030] As a preferred solution, before preparing the metal treatment impregnation liquid, the impregnation agent and solvent are tested to obtain the viscosity of the impregnation agent, the surface tension of the impregnation agent, the volatility of the solvent and the surface tension of the solvent, as well as the reaction intensity and density difference between the impregnation agent and the solvent.

[0031] By analyzing the formula Obtain the stirring speed influencing factor of the impregnation solution preparation process ,in They represent the preset viscosity of the impregnant, the surface tension of the impregnant, the thresholds of the volatility of the solvent and the surface tension of the solvent, and the thresholds of the intensity of the reaction between the impregnant and the solvent and the density difference, respectively. They represent the weights of the preset viscosity of the impregnant, the surface tension of the impregnant, the volatility of the solvent, the surface tension of the solvent, the intensity of the reaction between the impregnant and the solvent, and the density difference. .

[0032] By analyzing the formula Obtain the stirring time influencing factor of the impregnation solution preparation process .

[0033] Similarly, according to the analysis method of the influencing factor of the stirring time in the impregnation liquid preparation process, the influencing factor of the stirring temperature in the impregnation liquid preparation process is obtained and recorded as Specifically, since the stirring temperature and stirring time have the same relationship with the viscosity of the impregnating agent, the surface tension of the impregnating agent, the volatility of the solvent, the surface tension of the solvent, the intensity of the reaction between the impregnating agent and the solvent, and the density difference, and The analytical formula is the same.

[0034] As a preferred solution, a high-viscosity impregnant requires a longer stirring time and a slower stirring speed to ensure that the impregnant and the solvent are fully mixed. At the same time, for a high-viscosity impregnant, increasing the temperature can significantly reduce its viscosity, making it easier to mix.

[0035] As a preferred solution, a highly volatile solvent requires a shorter stirring time and a slower stirring speed to avoid solvent volatilization. At the same time, for a highly volatile solvent, too high a temperature will cause its volatilization speed to be too fast, affecting the mixing effect.

[0036] As a preferred solution, highly reactive impregnants and solvents require shorter stirring times and slower stirring speeds to avoid reactions. At the same time, for highly reactive impregnants and solvents, excessively high temperatures can lead to excessively fast reaction rates and may even cause explosions.

[0037] As a preferred solution, the impregnants and solvents with large density differences require longer stirring time and faster stirring speed to ensure uniform mixing. At the same time, for the impregnants and solvents with large density differences, increasing the temperature can reduce their density differences and make them easier to mix.

[0038] As a preferred solution, impregnants and solvents with high surface tension require longer stirring time and faster stirring speed to reduce surface tension. At the same time, for impregnants and solvents with high surface tension, increasing the temperature can significantly reduce their surface tension, making them easier to mix.

[0039] Furthermore, the specific working process of the initial setting module for the mixing parameters of the impregnation liquid preparation also includes: The stirring speed of the impregnation solution preparation process is obtained ,in Indicates the reference stirring speed of the impregnation liquid preparation process, Indicates the compensation amount of the stirring speed in the impregnation liquid preparation process, Represents a natural constant.

[0040] Similarly, according to the analysis method of the stirring speed of the impregnation liquid preparation process, the stirring time and stirring temperature of the impregnation liquid preparation process are obtained, and the stirring parameters of the impregnation liquid preparation process are further set.

[0041] It should be noted that the present invention selects appropriate stirring speed, stirring time and stirring temperature for preparing the impregnation liquid according to the type and amount of the impregnation agent and solvent for preparing the impregnation liquid for metal treatment, and takes into account various influencing factors such as viscosity, volatility, reaction intensity, density and surface tension, so as to make the setting of the process parameters of the impregnation liquid preparation process more reliable, thereby ensuring that the impregnation liquid is fully mixed and evenly, achieving the ideal impregnation effect, and ensuring the production quality of the impregnation liquid for metal treatment.

[0042] The impregnation liquid preparation stirring parameter adjustment judgment module is used to obtain the sediment volume and bubble quantity in the impregnation liquid at each sampling time point in the impregnation liquid preparation monitoring period, and judge whether the stirring parameters of the impregnation liquid preparation process need to be adjusted.

[0043] Furthermore, the specific working process of the impregnation liquid preparation stirring parameter adjustment judgment module is: obtaining the sediment volume and the number of bubbles in the impregnation liquid at each sampling time point during the impregnation liquid preparation monitoring period, and recording them as , Indicates The number of the sampling time point, .

[0044] As a preferred scheme, the volume of sediment and the number of bubbles in the infiltration liquid at each sampling time point during the monitoring period of the infiltration liquid preparation are obtained. The specific method is: set the duration of the monitoring period of the infiltration liquid preparation, and set each sampling time point during the monitoring period of the infiltration liquid preparation according to the preset equal time interval principle, collect images of the infiltration liquid at each sampling time point during the monitoring period of the infiltration liquid preparation, and obtain the volume of sediment and the number of bubbles in the infiltration liquid at each sampling time point during the monitoring period of the infiltration liquid preparation.

[0045] In a specific embodiment, the duration of the monitoring period of the preparation of the impregnation liquid is the total duration of the preparation process of the impregnation liquid. or .

[0046] As a preferred solution, the container used for preparing the impregnation liquid is made of transparent glass.

[0047] As a preferred solution, by acquiring images of the impregnation liquid at various angles, images of the precipitate in the impregnation liquid at various angles are obtained, a spatial model of the precipitate in the impregnation liquid is constructed, and the volume of the precipitate in the impregnation liquid is obtained.

[0048] By analyzing the formula Get the stirring degree coefficient of the impregnation solution preparation process ,in It indicates the correction factor of the stirring degree coefficient of the preset impregnation liquid preparation process. Respectively represent the weights of the preset sediment volume and bubble quantity, , represents the number of sampling time points, Respectively represent the first The volume of sediment and the number of bubbles in the infiltration solution at each sampling time point.

[0049] The stirring degree coefficient of the impregnation liquid preparation process is compared with the preset reference range of the stirring degree coefficient of the impregnation liquid preparation process. If the stirring degree coefficient of the impregnation liquid preparation process does not fall within the preset reference range of the stirring degree coefficient of the impregnation liquid preparation process, the stirring parameters of the impregnation liquid preparation process need to be adjusted.

[0050] The impregnation liquid preparation stirring parameter dynamic correction module is used to obtain the adjustment direction and adjustment amount of the stirring parameter of the impregnation liquid preparation process, and correct the stirring parameter of the impregnation liquid preparation process.

[0051] Furthermore, the specific working process of the dynamic correction module for the stirring parameters of the impregnation liquid preparation is: obtaining the difference between the stirring degree coefficient of the impregnation liquid preparation process and the median of the preset reference range of the stirring degree coefficient of the impregnation liquid preparation process, and recording it as the stirring degree coefficient deviation of the impregnation liquid preparation process.

[0052] The sign of the deviation of the stirring degree coefficient in the impregnation liquid preparation process is obtained, and the adjustment direction of the stirring speed, stirring time and stirring temperature in the impregnation liquid preparation process is analyzed.

[0053] As a preferred scheme, the adjustment direction of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process is analyzed. The specific method is: obtain the sign of the stirring degree coefficient deviation of the impregnation liquid preparation process. If it is a positive sign, the adjustment direction of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process is to decrease; if it is a negative sign, the adjustment direction of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process is to increase.

[0054] As a preferred solution, the stirring speed, stirring time and stirring temperature in the impregnation liquid preparation process are adjusted in the same direction.

[0055] The absolute value of the deviation of the stirring degree coefficient of the impregnation liquid preparation process is obtained, and it is substituted into the relationship function between the absolute value of the deviation of the stirring degree coefficient of the impregnation liquid preparation process and the adjustment amount of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process to obtain the adjustment amount of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process.

[0056] It should be noted that the present invention monitors the sediment volume and the number of bubbles in the impregnation liquid during the preparation of the impregnation liquid, determines whether the stirring parameters of the impregnation liquid preparation process need to be adjusted, and further obtains the adjustment direction and adjustment amount of the stirring parameters of the impregnation liquid preparation process. It can dynamically correct the stirring parameters of the impregnation liquid preparation process in combination with the actual production situation to form a closed-loop control, thereby improving the control accuracy of the stirring parameters of the impregnation liquid preparation process, thereby ensuring the production quality and production efficiency of the preparation of the impregnation liquid for metal treatment.

[0057] The active ingredient addition stirring parameter initial setting module is used to obtain the active ingredient information added to the metal treatment impregnation liquid, analyze the stirring parameters of the active ingredient addition process in the production process of the metal treatment impregnation liquid, wherein the stirring parameters of the active ingredient addition process include stirring speed, stirring time and stirring temperature, and set the stirring parameters of the active ingredient addition process.

[0058] Furthermore, the specific working process of the active ingredient addition stirring parameter initial setting module includes: obtaining a prediction model of the stirring speed, stirring time and stirring temperature of the active ingredient addition process.

[0059] As a preferred scheme, a prediction model for the stirring speed, stirring time and stirring temperature of the active ingredient adding process is obtained. The specific method is: extracting the historical production information of the metal treatment impregnation liquid stored in the database, obtaining the active ingredient information added to the metal treatment impregnation liquid in each historical production and the stirring parameters of the active ingredient adding process, analyzing the relationship between the stirring speed, stirring time and stirring temperature of the active ingredient adding process and the type, concentration and amount of the active ingredient added to the metal treatment impregnation liquid, and constructing a prediction model for the stirring speed, stirring time and stirring temperature of the active ingredient adding process.

[0060] The information of active ingredients added to the impregnation liquid for metal treatment is obtained, and the type, concentration and dosage of the active ingredients added to the impregnation liquid for metal treatment are obtained, and the information is substituted into the prediction model of the stirring speed, stirring time and stirring temperature of the active ingredient adding process to obtain the reference stirring speed, reference stirring time and reference stirring temperature of the active ingredient adding process.

[0061] Furthermore, the specific working process of the active ingredient addition stirring parameter initial setting module also includes: obtaining the solubility and reaction rate of the active ingredient added to the metal treatment impregnation solution, analyzing the influencing factors of the stirring temperature, stirring speed and stirring time of the active ingredient addition process, and recording them as , , .

[0062] As a preferred solution, the influencing factors of the stirring temperature, stirring speed and stirring time of the active ingredient adding process are analyzed. The specific method is: the solubility and reaction rate of the active ingredient added to the metal treatment impregnation solution are obtained, and they are recorded as .

[0063] By analyzing the formula Obtain the stirring temperature influencing factor of the active ingredient addition process ,in Respectively represent the preset thresholds of solubility and reaction rate of the active ingredient, Represent the preset solubility and reaction rate weights, .

[0064] Similarly, according to the analysis method of the stirring temperature influencing factor of the active ingredient addition process, the stirring speed influencing factor and the stirring time influencing factor of the active ingredient addition process are obtained and recorded as Specifically, since the stirring temperature, stirring speed and stirring time have the same relationship with the solubility and reaction rate of the active ingredient added to the metal treatment impregnation solution, and The analytical formula is the same.

[0065] As a preferred solution, for active ingredients with lower solubility and slower reaction rate, a higher temperature is required to completely dissolve them and fully react with the solvent.

[0066] As a preferred solution, for active ingredients with lower solubility and slower reaction rate, a faster stirring speed is required to dissolve them quickly.

[0067] As a preferred solution, for active ingredients with lower solubility and slower reaction rate, longer stirring time is required to completely dissolve them.

[0068] By analyzing the formula Get the stirring temperature of the active ingredient addition process ,in Indicates the reference stirring temperature for the active ingredient addition process. Indicates the compensation amount for the stirring temperature in the active ingredient addition process.

[0069] Similarly, according to the analysis method of the stirring temperature of the active ingredient adding process, the stirring speed and stirring time of the active ingredient adding process are obtained, and the stirring parameters of the active ingredient adding process are further set.

[0070] It should be noted that the present invention selects appropriate stirring speed, stirring time and stirring temperature for adding active ingredients according to the type, concentration and amount of active ingredients added to the impregnation solution for metal treatment, and takes into account various influencing factors such as the solubility and reaction rate of the active ingredients, thereby making the setting of the process parameters of the active ingredient addition process more reliable, thereby ensuring that the active ingredients are fully and evenly mixed and ensuring the production and preparation quality of the impregnation solution for metal treatment.

[0071] The active ingredient addition stirring parameter adjustment judgment module is used to obtain the number of bubbles and the amount of active ingredient dissolved in the impregnation liquid at each sampling time point in the active ingredient addition monitoring period, and judge whether the stirring parameters of the active ingredient addition process need to be adjusted.

[0072] Furthermore, the specific working process of the active ingredient addition stirring parameter adjustment judgment module is: obtaining the number of bubbles and the amount of active ingredient dissolved in the impregnation liquid at each sampling time point within the active ingredient addition monitoring period, and analyzing the stirring degree coefficient of the active ingredient addition process.

[0073] As a preferred solution, the stirring degree coefficient of the active ingredient addition process is analyzed. The specific method is as follows: the duration of the monitoring period of active ingredient addition is set, and each sampling time point is set within the monitoring period of active ingredient addition according to the preset equal time interval principle, the number of bubbles and the amount of active ingredient dissolved in the impregnation liquid at each sampling time point within the monitoring period of active ingredient addition are obtained, and the average number of bubbles in the impregnation liquid within the monitoring period of active ingredient addition, the maximum number of bubbles growth rate, and the maximum active ingredient dissolution growth rate are analyzed, and they are recorded as .

[0074] By analyzing the formula Get the stirring degree coefficient of the active ingredient addition process ,in Indicates the threshold value of the number of bubbles in the impregnation liquid during the preset active ingredient addition monitoring period. They respectively represent the thresholds of the preset maximum bubble number growth rate and the maximum active ingredient dissolution growth rate.

[0075] As a preferred solution, the average number of bubbles in the impregnation liquid at each sampling time point during the active ingredient addition monitoring period is calculated to obtain the average number of bubbles in the impregnation liquid during the active ingredient addition monitoring period.

[0076] As a preferred solution, curves showing the number of bubbles in the impregnation liquid and the amount of active ingredient dissolved over time during the active ingredient addition monitoring period are plotted respectively, and the maximum bubble number growth rate and the maximum active ingredient dissolved amount growth rate of the impregnation liquid during the active ingredient addition monitoring period are further obtained.

[0077] The stirring degree coefficient of the active ingredient adding process is compared with the preset reference range of the stirring degree coefficient of the active ingredient adding process. If the stirring degree coefficient of the active ingredient adding process does not fall within the preset reference range of the stirring degree coefficient of the active ingredient adding process, the stirring parameters of the active ingredient adding process need to be adjusted.

[0078] The active ingredient addition stirring parameter dynamic correction module is used to obtain the adjustment direction and adjustment amount of the stirring parameter of the active ingredient addition process, and correct the stirring parameter of the active ingredient addition process.

[0079] Furthermore, the specific working process of the active ingredient addition stirring parameter dynamic correction module is: obtaining the difference between the stirring degree coefficient of the active ingredient addition process and the median of the preset active ingredient addition process stirring degree coefficient reference range, and recording it as the stirring degree coefficient deviation of the active ingredient addition process.

[0080] The sign of the deviation of the stirring degree coefficient of the active ingredient addition process is obtained, and the adjustment direction of the stirring speed, stirring time and stirring temperature of the active ingredient addition process is analyzed.

[0081] As a preferred scheme, the adjustment direction of the stirring speed, stirring time and stirring temperature of the active ingredient addition process is analyzed. The specific method is: obtain the sign of the stirring degree coefficient deviation of the active ingredient addition process. If it is a positive sign, the adjustment direction of the stirring speed, stirring time and stirring temperature of the active ingredient addition process is to decrease. If it is a negative sign, the adjustment direction of the stirring speed, stirring time and stirring temperature of the active ingredient addition process is to increase.

[0082] The absolute value of the deviation of the stirring degree coefficient of the active ingredient addition process is obtained, and the absolute value is substituted into the relationship function between the absolute value of the deviation of the stirring degree coefficient of the active ingredient addition process and the adjustment amount of the stirring speed, stirring time and stirring temperature of the active ingredient addition process to obtain the adjustment amount of the stirring speed, stirring time and stirring temperature of the active ingredient addition process.

[0083] It should be noted that the present invention determines whether the stirring parameters of the active ingredient adding process need to be adjusted by monitoring the number of bubbles in the impregnation liquid and the dissolution of the active ingredient during the process of adding the active ingredient, and further obtains the adjustment direction and adjustment amount of the stirring parameters of the active ingredient adding process. It can dynamically correct the stirring parameters of the active ingredient adding process in combination with the actual production situation to form a closed-loop control, thereby improving the control accuracy of the stirring parameters of the active ingredient adding process, thereby ensuring the production quality and production efficiency of the preparation of the impregnation liquid for metal treatment.

[0084] The database is used to store historical production information of the impregnation solution for metal treatment.

[0085] The above contents are merely examples and explanations of the concept of the present invention. Those skilled in the art may make various modifications or additions to the specific embodiments described or replace them in a similar manner. As long as they do not deviate from the concept of the invention or exceed the scope defined by the present invention, they shall all fall within the protection scope of the present invention.

Claims

1. A control system for preparing and processing an impregnation liquid for metal treatment, characterized in that: include: Initial setting module for mixing parameters of impregnation liquid preparation: The specific working process of the initial setting module for preparing and stirring parameters of the impregnation liquid includes: Extract the historical production information of the metal treatment impregnation solution stored in the database, obtain the raw material information of each historical production of the metal treatment impregnation solution and the stirring parameters of the impregnation solution preparation process, analyze the relationship between the stirring speed, stirring time and stirring temperature of the impregnation solution preparation process and the type and amount of the impregnation agent and solvent used to prepare the metal treatment impregnation solution, and construct a prediction model for the stirring speed, stirring time and stirring temperature of the impregnation solution preparation process; Obtaining raw material information for preparing the metal treatment impregnation solution, obtaining the type and amount of the impregnation agent and solvent for preparing the metal treatment impregnation solution, substituting the information into a prediction model of the stirring speed, stirring time and stirring temperature of the impregnation solution preparation process, and obtaining a reference stirring speed, reference stirring time and reference stirring temperature of the impregnation solution preparation process; The specific working process of the initial setting module for preparing and stirring parameters of the impregnation liquid also includes: Obtain the viscosity of the impregnating agent, the surface tension of the impregnating agent, the volatility of the solvent and the surface tension of the solvent for preparing the metal treatment impregnation solution, and record them as , and obtain the reaction intensity and density difference of the impregnant and solvent for preparing the metal treatment impregnation solution, which are recorded as ; By analyzing the formula Obtain the stirring speed influencing factor of the impregnation solution preparation process ,in They represent the preset viscosity of the impregnant, the surface tension of the impregnant, the thresholds of the volatility of the solvent and the surface tension of the solvent, and the thresholds of the intensity of the reaction between the impregnant and the solvent and the density difference, respectively. They represent the weights of the preset viscosity of the impregnant, the surface tension of the impregnant, the volatility of the solvent, the surface tension of the solvent, the intensity of the reaction between the impregnant and the solvent, and the density difference. ; By analyzing the formula Obtain the stirring time influencing factor of the impregnation solution preparation process ; Similarly, according to the analysis method of the influencing factor of the stirring time in the impregnation liquid preparation process, the influencing factor of the stirring temperature in the impregnation liquid preparation process is obtained and recorded as ; Influencing factors of stirring speed in the impregnation liquid preparation process , Stirring time influence factor and stirring temperature influence factors Further analysis revealed the stirring speed, stirring time and stirring temperature of the impregnation solution preparation process; The module for adjusting and judging the stirring parameters of the impregnation liquid preparation is used to obtain the sediment volume and the number of bubbles in the impregnation liquid at each sampling time point during the monitoring period of the impregnation liquid preparation, and to judge whether the stirring parameters of the impregnation liquid preparation process need to be adjusted; Dynamic correction module for stirring parameters of impregnation liquid preparation: used to obtain the adjustment direction and adjustment amount of stirring parameters of the impregnation liquid preparation process, and correct the stirring parameters of the impregnation liquid preparation process; Active ingredient adding stirring parameter initial setting module: used to obtain the active ingredient information added to the metal treatment impregnation solution, analyze the stirring parameters of the active ingredient adding process in the production process of the metal treatment impregnation solution, where the stirring parameters of the active ingredient adding process include stirring speed, stirring time and stirring temperature, and set the stirring parameters of the active ingredient adding process; Active ingredient addition stirring parameter adjustment judgment module: used to obtain the number of bubbles and the amount of active ingredient dissolved in the impregnation liquid at each sampling time point during the active ingredient addition monitoring period, and determine whether the stirring parameters of the active ingredient addition process need to be adjusted; Active ingredient addition stirring parameter dynamic correction module: used to obtain the adjustment direction and adjustment amount of the stirring parameters of the active ingredient addition process, and correct the stirring parameters of the active ingredient addition process; Database: used to store historical production information of impregnation fluids for metal treatment.

2. A metal treatment impregnation liquid preparation and processing control system according to claim 1, characterized in that: The specific working process of the initial setting module for preparing and stirring parameters of the impregnation liquid also includes: By analyzing the formula The stirring speed of the impregnation solution preparation process is obtained ,in Indicates the reference stirring speed of the impregnation liquid preparation process, Indicates the compensation amount of the stirring speed in the impregnation liquid preparation process, represents a natural constant; Similarly, according to the analysis method of the stirring speed of the impregnation liquid preparation process, the stirring time and stirring temperature of the impregnation liquid preparation process are obtained, and the stirring parameters of the impregnation liquid preparation process are further set.

3. The metal treatment impregnation liquid preparation and processing control system according to claim 1, characterized in that: The specific working process of the impregnation liquid preparation stirring parameter adjustment judgment module is as follows: Obtain the sediment volume and the number of bubbles in the infiltration solution at each sampling time point during the preparation and monitoring period of the infiltration solution, and record them as , Indicates The number of the sampling time point, ; By analyzing the formula Get the stirring degree coefficient of the impregnation solution preparation process ,in It indicates the correction factor of the stirring degree coefficient of the preset impregnation liquid preparation process. Respectively represent the weights of the preset sediment volume and bubble quantity, , represents the number of sampling time points, Respectively represent the first The volume of sediment and the number of bubbles in the infiltration solution at each sampling time point; The stirring degree coefficient of the impregnation liquid preparation process is compared with the preset reference range of the stirring degree coefficient of the impregnation liquid preparation process. If the stirring degree coefficient of the impregnation liquid preparation process does not fall within the preset reference range of the stirring degree coefficient of the impregnation liquid preparation process, the stirring parameters of the impregnation liquid preparation process need to be adjusted.

4. A metal treatment impregnation liquid preparation and processing control system according to claim 1, characterized in that: The specific working process of the dynamic correction module for the preparation and stirring parameters of the impregnation liquid is as follows: Obtaining a difference between the stirring degree coefficient of the impregnation liquid preparation process and the median of a preset reference range of the stirring degree coefficient of the impregnation liquid preparation process, and recording it as a deviation of the stirring degree coefficient of the impregnation liquid preparation process; Obtain the sign of the deviation of the stirring degree coefficient in the impregnation liquid preparation process, and analyze the adjustment direction of the stirring speed, stirring time and stirring temperature in the impregnation liquid preparation process; The absolute value of the deviation of the stirring degree coefficient of the impregnation liquid preparation process is obtained, and it is substituted into the relationship function between the absolute value of the deviation of the stirring degree coefficient of the impregnation liquid preparation process and the adjustment amount of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process to obtain the adjustment amount of the stirring speed, stirring time and stirring temperature of the impregnation liquid preparation process.

5. The metal treatment impregnation liquid preparation process control system according to claim 1, characterized in that: The specific working process of the active ingredient adding stirring parameter initial setting module includes: Obtain a prediction model for the stirring speed, stirring time and stirring temperature of the active ingredient addition process; The information of active ingredients added to the impregnation liquid for metal treatment is obtained, and the type, concentration and dosage of the active ingredients added to the impregnation liquid for metal treatment are obtained, and the information is substituted into the prediction model of the stirring speed, stirring time and stirring temperature of the active ingredient adding process to obtain the reference stirring speed, reference stirring time and reference stirring temperature of the active ingredient adding process.

6. A metal treatment impregnation liquid preparation process control system according to claim 5, characterized in that: The specific working process of the active ingredient adding stirring parameter initial setting module also includes: The solubility and reaction rate of the active ingredient added to the metal treatment impregnation solution were obtained, and the influencing factors of the stirring temperature, stirring speed and stirring time of the active ingredient addition process were analyzed and recorded as , , ; By analyzing the formula Get the stirring temperature of the active ingredient addition process ,in Indicates the reference stirring temperature for the active ingredient addition process. Indicates the compensation amount for the stirring temperature of the active ingredient addition process; Similarly, according to the analysis method of the stirring temperature of the active ingredient adding process, the stirring speed and stirring time of the active ingredient adding process are obtained, and the stirring parameters of the active ingredient adding process are further set.

7. The metal treatment impregnation liquid preparation process control system according to claim 1, characterized in that: The specific working process of the active ingredient adding stirring parameter adjustment judgment module is as follows: Obtain the number of bubbles and the amount of dissolved active ingredients in the impregnation liquid at each sampling time point during the active ingredient addition monitoring period, and analyze the stirring degree coefficient of the active ingredient addition process; The stirring degree coefficient of the active ingredient adding process is compared with the preset reference range of the stirring degree coefficient of the active ingredient adding process. If the stirring degree coefficient of the active ingredient adding process does not fall within the preset reference range of the stirring degree coefficient of the active ingredient adding process, the stirring parameters of the active ingredient adding process need to be adjusted.

8. A metal treatment impregnation liquid preparation process control system according to claim 7, characterized in that: The specific working process of the active ingredient addition stirring parameter dynamic correction module is as follows: Obtaining a difference between the stirring degree coefficient of the active ingredient adding process and the median of a preset reference range of the stirring degree coefficient of the active ingredient adding process, and recording the difference as a deviation of the stirring degree coefficient of the active ingredient adding process; Obtain the sign of the deviation of the stirring degree coefficient of the active ingredient addition process, and analyze the adjustment direction of the stirring speed, stirring time and stirring temperature of the active ingredient addition process; The absolute value of the deviation of the stirring degree coefficient of the active ingredient addition process is obtained, and the absolute value is substituted into the relationship function between the absolute value of the deviation of the stirring degree coefficient of the active ingredient addition process and the adjustment amount of the stirring speed, stirring time and stirring temperature of the active ingredient addition process to obtain the adjustment amount of the stirring speed, stirring time and stirring temperature of the active ingredient addition process.

Citation Information

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