An efficient energy-saving nitric acid evaporation and concentration device
By designing a combination of components such as liquid storage chamber, evaporation chamber and drive motor, the problem of difficulty in adjusting the amount of gas and nitric acid in existing equipment is solved, and the stability and energy saving of the nitric acid evaporation and concentration process are achieved.
Patent Information
- Application Number
- CN202411688131.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-11-25
- Publication Date
- 2025-07-25
- Estimated Expiration
- 2044-11-25
AI Technical Summary
Existing nitric acid evaporation and concentration equipment requires multiple adjustment mechanisms, making it difficult to adjust the amount of gas and nitric acid, resulting in excessive energy consumption.
The combination design of components such as liquid storage chamber, evaporation chamber, drive motor, gear, ratchet and peristaltic pump rod is adopted. The gear drives the rotary ring to rotate, realize automatic adjustment of infusion and gas, and use the exhaust gas impeller to cut foam to avoid energy waste.
The stability and energy saving of the nitric acid evaporation and concentration process are achieved, the adjustment accuracy and stability of the equipment are improved, and energy consumption is reduced.
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Figure CN119185969B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of nitric acid evaporation and concentration, and particularly to an efficient and energy-saving nitric acid evaporation and concentration device. Background Art
[0002] An evaporator is essentially a heat exchanger. Inside the evaporator, heat exchange occurs between the material and the heat source. Part of the solvent in the material becomes gaseous and is separated, and the concentration of the material increases to achieve the purpose of evaporation and concentration. During the evaporation and concentration of nitric acid, a device is also needed to evaporate nitric acid. However, existing evaporation devices have some deficiencies. For example:
[0003] A method and device for denitrifying and evaporating and concentrating radioactive nitric acid waste liquid with the publication number of CN116013569A eliminates the phenomenon of bumping by introducing nitrogen oxide gas during the denitrifying evaporation reaction of radioactive nitric acid waste liquid. And during the denitrifying evaporation reaction of radioactive nitric acid waste liquid, there is no salt and no impurity ions are introduced. It has the characteristics of stable process, wide applicability, and less equipment modification. However, during actual use, since this device requires a variety of adjustment mechanisms to add raw materials such as nitric acid and gas, it may be difficult to adjust the amounts of gas and nitric acid during actual use of this device, and during the evaporation and concentration process, there may be a situation of excessive energy consumption;
[0004] Therefore, we propose an efficient and energy-saving nitric acid evaporation and concentration device to solve the problems mentioned above. Summary of the Invention
[0005] The purpose of the present invention is to provide an efficient and energy-saving nitric acid evaporation and concentration device to solve the problems in the above background art that most current nitric acid evaporation and concentration devices on the market require a variety of adjustment mechanisms to add raw materials such as nitric acid and gas, which may lead to difficulties in adjusting the amounts of gas and nitric acid during actual use of the device, and there may be a problem of excessive energy consumption during the evaporation and concentration process.
[0006] To achieve the above purpose, the present invention provides the following technical solution: An efficient and energy-saving nitric acid evaporation and concentration device, including a liquid storage bin and an evaporation bin connected to the liquid storage bin; the top of the liquid storage bin is fixedly connected to the evaporation bin, and a liquid delivery valve is provided at the bottom of the liquid storage bin. A driving motor is connected to the top of the liquid storage bin, a first gear is connected to the top of the driving motor, a lower ratchet is connected to the top of the first gear, an upper ratchet is attached to the top of the lower ratchet, a first spring shaft is connected to the top of the upper ratchet, a connecting shaft is connected to the top of the first spring shaft, and a gas-dispersing impeller is provided at the top of the connecting shaft. A heating cylinder is provided outside the gas-dispersing impeller, a check valve is provided in the middle of the heating cylinder, and the top of the heating cylinder is connected to the evaporation bin;
[0007] The top of the liquid storage bin is connected with an infusion tube, and the top of the liquid storage bin is connected with a first fixing plate, and the first fixing plate fixes the infusion tube. The top of the first fixing plate is connected with a first peristaltic pump rod, and the top of the first peristaltic pump rod is connected with a first rotating shaft. And a second spring shaft is arranged outside the first rotating shaft, the outside of the second spring shaft is connected with a first clamping block, and the top of the first rotating shaft is connected with a second rotating shaft. And a third spring shaft is arranged outside the second rotating shaft, the outside of the third spring shaft is connected with a second clamping block. The top of the second rotating shaft is connected with a second peristaltic pump rod, and the top of the second peristaltic pump rod is connected with a second fixing plate. The bottom of the second fixing plate is connected with an air delivery pipe, and the air delivery pipe is attached to the second peristaltic pump rod, and the air delivery pipe is connected with a heating cylinder. The infusion tube is connected with the bottom of the evaporation chamber;
[0008] The left side of the first gear meshes with the second gear, and a rotating ring is connected inside the second gear. And a first ratchet groove is arranged at the bottom inside the rotating ring, and the first ratchet groove can be snap-connected with the first clamping block. And a second ratchet groove is connected to the top inside the rotating ring, and the second ratchet groove can be snap-connected with the second clamping block;
[0009] The top of the liquid storage bin is connected with a fixing ring, and the fixing ring is slidably connected with the outside of the rotating ring. And a steam collector is arranged at the top of the evaporation chamber, a detection mechanism is arranged on the right side of the evaporation chamber, and a discharge port is arranged at the bottom of the evaporation chamber.
[0010] Driving the rotating ring to rotate through the second gear can make the first ratchet groove drive the first clamping block to rotate when the rotating ring rotates clockwise, so that the first rotating shaft drives the first peristaltic pump rod to squeeze the infusion tube, so that the infusion tube conveys liquid to the evaporation chamber. And when the second gear drives the rotating ring to rotate counterclockwise, the second ratchet groove will drive the second clamping block to rotate, so that the second clamping block drives the second rotating shaft to rotate, and the second rotating shaft drives the second peristaltic pump rod arranged at the top to rotate and squeeze the air delivery pipe, so as to convey the pure oxygen inside the air delivery pipe to the inside of the heating cylinder for heating;
[0011] When the heating cylinder finishes heating the pure oxygen inside, the pure oxygen will be input into the evaporation chamber. Since the driving motor is rotating at this time, the lower ratchet and the upper ratchet will be clamped and fixed, so that the upper ratchet drives the connecting shaft and the air-dispersing impeller to rotate. When the gas forms foam at the bottom of the evaporation chamber, the heat-dissipating impeller can cut it, so as to avoid the foam being too large and affecting the evaporation and concentration operation inside the evaporation chamber.
[0012] As a preferred technical solution of the present invention, the detection mechanism includes a U-shaped tube, and the U-shaped tube is fixedly connected with the evaporation chamber, and a concentration detector is arranged in the middle of the U-shaped tube.
[0013] Adopting the above technical solution enables the device to be more convenient when detecting the concentration of nitric acid liquid, thereby increasing the accuracy of the device during detection.
[0014] As a preferred technical solution of the present invention, a filter block is connected to the bottom of the liquid storage tank, and a precipitation tank is connected to the bottom of the filter block, and the precipitation tank is connected to the infusion valve.
[0015] Adopting the above technical solution enables impurities inside the nitric acid liquid to be intercepted by the filter block when the nitric acid liquid enters the liquid storage tank, and then precipitate in the precipitation tank, making the nitric acid liquid purer.
[0016] As a preferred technical solution of the present invention, a fixed rod is connected to the top of the liquid storage tank, and the liquid storage tank is fixedly connected to the evaporation tank through the fixed rod.
[0017] Adopting the above technical solution can make the connection between the liquid storage tank and the evaporation tank more stable through the setting of the fixed rod, increasing the firmness of the device.
[0018] As a preferred technical solution of the present invention, a heating resistance wire is provided inside the heating cylinder, and the inner top of the heating cylinder is fixedly connected to the one-way valve.
[0019] Adopting the above technical solution enables the heating cylinder to be more convenient when heating pure oxygen or other gases, thereby increasing the convenience of the device when heating gases.
[0020] As a preferred technical solution of the present invention, the ratchet slots of the first ratchet slot and the second ratchet slot are opposite, and the orientations of the first latch and the second latch are opposite.
[0021] As a preferred technical solution of the present invention, a corrugated pipe is provided on the right side of the steam collector, and corrugated-shaped slots are provided inside the corrugated pipe.
[0022] Adopting the above technical solution enables the contact area of water vapor to increase when the water vapor contacts the corrugated pipe, so that the condensed water is better adsorbed by the corrugated pipe and discharged to the condensed water discharge port, increasing the convenience of discharging the condensed water.
[0023] As a preferred technical solution of the present invention, a condensed water discharge port is provided at the bottom left of the corrugated pipe, and the condensed water discharge port is fixedly connected to the corrugated pipe.
[0024] As a preferred technical solution of the present invention, feet are provided at the bottom of the liquid storage tank, and heat preservation wall mechanisms are provided inside both the liquid storage tank and the evaporation tank.
[0025] Compared with the prior art, the beneficial effects of the present invention are as follows: By driving the rotating ring to rotate through the second gear, when the rotating ring rotates clockwise, the first ratchet groove can drive the first clamping block to rotate, so that the first rotating shaft drives the first peristaltic pump rod to squeeze the infusion tube, and then the infusion tube conveys liquid to the evaporation chamber for infusion work. When the second gear drives the rotating ring to rotate counterclockwise, the second ratchet groove will drive the second clamping block to rotate, so that the second clamping block drives the second rotating shaft to rotate, and the second rotating shaft drives the second peristaltic pump rod arranged at the top to rotate and squeeze the gas transmission tube, so as to transmit the pure oxygen inside the gas transmission tube to the heating cylinder for heating;
[0026] When the heating cylinder finishes heating the pure oxygen inside, the pure oxygen will be input into the evaporation chamber. Since the drive motor is rotating at this time, the lower ratchet and the upper ratchet will be engaged and fixed, so that the upper ratchet drives the connecting shaft and the air-dispersing impeller to rotate. When the gas forms foam at the bottom of the evaporation chamber, the heat-dissipating impeller can cut it, so as to prevent the foam from being too large and affecting the evaporation and concentration operation inside the evaporation chamber;
[0027] Furthermore, through the setting of the fixing ring, when the rotating ring rotates, the fixing ring can support it, so that the rotating ring can rotate more stably, thereby increasing the stability of the device during operation;
[0028] Even further, through the setting of the fixing rod, when the liquid storage chamber is fixedly connected to the evaporation chamber, it can be more stable, increasing the firmness of the device. BRIEF DESCRIPTION OF THE DRAWINGS
[0029] Figure 1 is the front elevation structure schematic diagram of the present invention;
[0030] Figure 2 is the front elevation structure schematic diagram of the front cross-section of the liquid storage tank of the present invention;
[0031] Figure 3 is the front elevation structure schematic diagram of the front cross-section of the heating cylinder of the present invention;
[0032] Figure 4 is the hierarchical elevation structure schematic diagram of the air-dispersing impeller of the present invention;
[0033] Figure 5 is the front elevation structure schematic diagram of the front cross-section of the rotating ring of the present invention;
[0034] Figure 6 is of the present invention Figure 5 enlarged structure schematic diagram at A;
[0035] Figure 7Schematic side elevation structure diagram of the rotating ring of the present invention;
[0036] Figure 8 Schematic elevation structure diagram of the front view section of the evaporation chamber of the present invention;
[0037] Figure 9 Detailed front elevation structure diagram of the first peristaltic pump rod of the present invention.
[0038] In the figure: 1, liquid storage chamber; 2, evaporation chamber; 3, infusion valve; 4, precipitation chamber; 5, filter block; 6, drive motor; 7, first gear; 8, heating cylinder; 9, check valve; 10, lower ratchet; 11, first spring shaft; 12, upper ratchet; 13, connecting shaft; 14, air-dispersing impeller; 15, second gear; 16, rotating ring; 17, infusion tube; 18, first fixed disk; 19, first peristaltic pump rod; 20, first rotating shaft; 21, second spring shaft; 22, first clamping block; 23, first ratchet groove; 24, second rotating shaft; 25, third spring shaft; 26, second clamping block; 27, second ratchet groove; 28, second peristaltic pump rod; 29, gas transmission tube; 30, second fixed disk; 31, discharge port; 32, U-shaped tube; 33, concentration detector; 34, steam collector; 35, corrugated pipe; 36, condensate discharge port; 37, fixed rod; 38, fixed ring. Detailed implementation mode
[0039] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments.
[0040] Embodiment 1:
[0041] Please refer to Figures 1-9 , the present invention provides a technical solution: an efficient energy-saving nitric acid evaporation and concentration device, including a liquid storage chamber 1 and an evaporation chamber 2 connected to the liquid storage chamber 1; the top of the liquid storage chamber 1 is fixedly connected to the evaporation chamber 2, and an infusion valve 3 is provided at the bottom of the liquid storage chamber 1, and a drive motor 6 is connected to the top of the liquid storage chamber 1, a first gear 7 is connected to the top of the drive motor 6, and a lower ratchet 10 is connected to the top of the first gear 7, and an upper ratchet 12 is attached to the top of the lower ratchet 10, a first spring shaft 11 is connected to the top of the upper ratchet 12, a connecting shaft 13 is connected to the top of the first spring shaft 11, and an air-dispersing impeller 14 is provided at the top of the connecting shaft 13, a heating cylinder 8 is provided outside the air-dispersing impeller 14, and a check valve 9 is provided in the middle of the heating cylinder 8, and the top of the heating cylinder 8 is connected to the evaporation chamber 2;
[0042] The top of the liquid storage chamber 1 is connected to an infusion tube 17, and the top of the liquid storage chamber 1 is connected to a first fixing plate 18. The first fixing plate 18 fixes the infusion tube 17. The top of the first fixing plate 18 is connected to a first peristaltic pump rod 19, and the top of the first peristaltic pump rod 19 is connected to a first rotating shaft 20. A second spring shaft 21 is arranged outside the first rotating shaft 20. The outside of the second spring shaft 21 is connected to a first clamping block 22. The top of the first rotating shaft 20 is connected to a second rotating shaft 24. A third spring shaft 25 is arranged outside the second rotating shaft 24. The outside of the third spring shaft 25 is connected to a second clamping block 26. The top of the second rotating shaft 24 is connected to a second peristaltic pump rod 28. The top of the second peristaltic pump rod 28 is connected to a second fixing plate 30. The bottom of the second fixing plate 30 is connected to an air delivery tube 29. The air delivery tube 29 is in contact with the second peristaltic pump rod 28. The air delivery tube 29 is connected to the heating cylinder 8. The infusion tube 17 is connected to the bottom of the evaporation chamber 2;
[0043] The left side of the first gear 7 meshes with a second gear 15. The second gear 15 is internally connected to a rotating ring 16. A first ratchet groove 23 is arranged at the bottom inside the rotating ring 16. The first ratchet groove 23 can be snap-connected with the first clamping block 22. The top inside the rotating ring 16 is connected to a second ratchet groove 27. The second ratchet groove 27 can be snap-connected with the second clamping block 26;
[0044] The top of the liquid storage chamber 1 is connected to a fixing ring 38. The fixing ring 38 is slidably connected to the outside of the rotating ring 16. A steam collector 34 is arranged at the top of the evaporation chamber 2. A detection mechanism is arranged on the right side of the evaporation chamber 2. A discharge port 31 is arranged at the bottom of the evaporation chamber 2;
[0045] When using the nitric acid evaporation and concentration device, first, the nitric acid liquid is transmitted into the liquid storage chamber 1 through the infusion valve 3. Subsequently, the driving motor 6 is started, so that the driving motor 6 drives the first gear 7 to rotate counterclockwise. Since the first gear 7 meshes with the second gear 15, the second gear 15 will rotate clockwise, so that the first ratchet groove 23 arranged at the bottom of the rotating ring 16 drives the first clamping block 22 to snap and rotate. The first clamping block 22 rotates with the first rotating shaft 20 as the center and drives the first rotating shaft 20 to rotate. Thus, the first rotating shaft 20 drives the first peristaltic pump rod 19 to rotate, squeezing the infusion tube 17. Due to extrusion and pressure, the nitric acid liquid inside the liquid storage chamber 1 is discharged into the evaporation chamber 2 through the infusion tube 17;
[0046] When the nitric acid liquid inside the evaporation chamber 2 reaches a specified height, the driving motor 6 drives the first gear 7 to rotate clockwise, enabling the second gear 15 to drive the rotating ring 16 to rotate counterclockwise. At this time, the first ratchet groove 23 will disconnect from the first latch 22, and the first latch 22 will retract under the drive of the second spring shaft 21. The first rotating shaft 20 will not drive the first peristaltic pump rod 19 to rotate, while the rotating ring 16 will drive the second ratchet groove 27 to rotate counterclockwise, causing the second ratchet groove 27 to engage with the second latch 26 and drive the second latch 26 to rotate around the second rotating shaft 24 as the center, thereby causing the second rotating shaft 24 and the second peristaltic pump rod 28 to rotate, enabling the second peristaltic pump rod 28 to fit and squeeze the gas transmission pipe 29, so that the gas transmission pipe 29 transports pure oxygen or other gases into the heating cylinder 8;
[0047] When the first gear 7 rotates counterclockwise, the lower ratchet 10 will disconnect from the upper ratchet 12, and the upper ratchet 12 will retract upward under the drive of the first spring shaft 11. When the first gear 7 rotates clockwise, the lower ratchet 10 will engage with the upper ratchet 12, thereby enabling the first gear 7 to drive the connecting shaft 13 and the air-diffusing impeller 14 to rotate, causing the heated gas to be cut into smaller bubbles by the air-diffusing impeller 14 after forming bubbles through the one-way valve 9;
[0048] The detection mechanism includes a U-shaped tube 32, and the U-shaped tube 32 is fixedly connected to the evaporation chamber 2, and a concentration detector 33 is provided in the middle of the U-shaped tube 32; a filter block 5 is connected to the bottom of the liquid storage chamber 1, and a sedimentation chamber 4 is connected to the bottom of the filter block 5, and the sedimentation chamber 4 is connected to the infusion valve 3; a fixed rod 37 is connected to the top of the liquid storage chamber 1, and the liquid storage chamber 1 is fixedly connected to the evaporation chamber 2 through the fixed rod 37;
[0049] The heating cylinder 8 is internally provided with a heating resistance wire, and the inner top of the heating cylinder 8 is fixedly connected to the one-way valve 9; the ratchet groove positions of the first ratchet groove 23 and the second ratchet groove 27 are opposite, and the orientations of the first latch 22 and the second latch 26 are opposite; a corrugated pipe 35 is provided on the right side of the steam collector 34, and the corrugated pipe 35 is internally provided with corrugated-shaped slots; a condensate discharge port 36 is provided at the bottom left end of the corrugated pipe 35, and the condensate discharge port 36 is fixedly connected to the corrugated pipe 35; the bottom of the liquid storage chamber 1 is provided with feet, and heat insulation wall mechanisms are provided on the inner sides of both the liquid storage chamber 1 and the evaporation chamber 2;
[0050] When the infusion valve 3 transfers nitric acid liquid to the liquid storage bin 1, the nitric acid liquid will pass through the precipitation bin 4, and the impurities inside the nitric acid liquid will be filtered out by the filter block 5, so that the impurities in the nitric acid liquid will be reduced when it is transferred to the liquid storage bin 1. When the nitric acid liquid in the evaporation bin 2 reaches a certain water level, the excess liquid will be transferred to the U-shaped tube 32 and detected by the concentration detector 33, so as to judge the concentration of the nitric acid liquid. When the evaporation bin 2 discharges steam, the steam will enter the corrugated pipe 35 through the steam collector 34. Due to the corrugated grooves provided inside the corrugated pipe 35, the contact area of the steam will increase, so that the corrugated grooves will adsorb the condensed water and drain it into the condensed water discharge port 36 through the flow direction.
[0051] Working principle: When using the nitric acid evaporation and concentration equipment, first transfer the nitric acid liquid to the inside of the liquid storage bin 1 through the infusion valve 3, and then start the drive motor 6, so that the drive motor 6 drives the first gear 7 to rotate counterclockwise. Since the first gear 7 meshes with the second gear 15, the second gear 15 will rotate clockwise, so that the first ratchet groove 23 provided at the bottom of the rotating ring 16 drives the first latch 22 to engage and rotate, so that the first latch 22 rotates around the first rotating shaft 20 as the center and drives the first rotating shaft 20 to rotate. Thus, the first rotating shaft 20 drives the first peristaltic pump rod 19 to rotate, squeezes the infusion tube 17, so that the infusion tube 17 discharges the nitric acid liquid inside the liquid storage bin 1 into the evaporation bin 2 due to extrusion and pressure;
[0052] When the nitric acid liquid in the evaporation bin 2 reaches the specified height, the drive motor 6 drives the first gear 7 to rotate clockwise, which can make the second gear 15 drive the rotating ring 16 to rotate counterclockwise. At this time, the first ratchet groove 23 will disconnect from the first latch 22, and the first latch 22 will retract under the drive of the second spring shaft 21, and the first rotating shaft 20 will not drive the first peristaltic pump rod 19 to rotate, while the rotating ring 16 will drive the second ratchet groove 27 to rotate counterclockwise, so that the second ratchet groove 27 engages with the second latch 26 and drives the second latch 26 to rotate around the second rotating shaft 24 as the center, so that the second rotating shaft 24 and the second peristaltic pump rod 28 rotate, so that the second peristaltic pump rod 28 fits and squeezes the gas transmission tube 29, so that the gas transmission tube 29 transfers pure oxygen or other gases to the inside of the heating cylinder 8;
[0053] When the first gear 7 rotates counterclockwise, the lower ratchet 10 will disconnect from the upper ratchet 12, and the upper ratchet 12 will retract upward under the drive of the first spring shaft 11. When the first gear 7 rotates clockwise, the lower ratchet 10 will engage with the upper ratchet 12, so that the first gear 7 drives the connecting shaft 13 and the air-dispersing impeller 14 to rotate, so that the heated gas is cut into smaller bubbles by the air-dispersing impeller 14 after forming bubbles through the one-way valve 9;
[0054] When the infusion valve 3 transfers nitric acid liquid to the liquid storage bin 1, the nitric acid liquid will pass through the precipitation bin 4, and the impurities in the nitric acid liquid will be filtered out by the filter block 5, so that the impurities in the nitric acid liquid will be reduced when it is transferred to the liquid storage bin 1. When the nitric acid liquid in the evaporation bin 2 reaches a certain water level, the excess liquid will be transferred to the U-shaped tube 32 and detected by the concentration detector 33, so as to judge the concentration of the nitric acid liquid. When the evaporation bin 2 discharges steam, the steam will enter the corrugated pipe 35 through the steam collector 34. Due to the corrugated grooves provided inside the corrugated pipe 35, the contact area of the steam will increase, so that the corrugated grooves will adsorb the condensed water and drain it into the condensed water discharge port 36 through the flow direction.
[0055] Thus, a series of operations are completed. The content not described in detail in this specification belongs to the prior art well-known to those skilled in the art.
[0056] For those skilled in the art, it is obvious that the present invention is not limited to the details of the above-described exemplary embodiments, and the present invention can be implemented in other specific forms without departing from the spirit or basic characteristics of the present invention. Therefore, from any point of view, the embodiments should be regarded as exemplary and non-restrictive. The scope of the present invention is defined by the appended claims rather than the above description. Therefore, all changes falling within the meaning and scope of the equivalent elements of the claims are intended to be embraced by the present invention. Any reference signs in the claims should not be regarded as limiting the claims involved.
Claims
1. An efficient energy-saving nitric acid evaporation and concentration device, comprising a liquid storage bin (1) and an evaporation bin (2) connected to the liquid storage bin (1); characterized in that, The top of the liquid storage bin (1) is fixedly connected to the evaporation bin (2), and a liquid infusion valve (3) is provided at the bottom of the liquid storage bin (1). A driving motor (6) is connected to the top of the liquid storage bin (1). A first gear (7) is connected to the top of the driving motor (6), and a lower ratchet wheel (10) is connected to the top of the first gear (7). An upper ratchet wheel (12) is attached to the top of the lower ratchet wheel (10). A first spring shaft (11) is connected to the top of the upper ratchet wheel (12), a connecting shaft (13) is connected to the top of the first spring shaft (11), and a gas-dispersing impeller (14) is provided at the top of the connecting shaft (13). A heating cylinder (8) is provided outside the gas-dispersing impeller (14), a one-way valve (9) is provided in the middle of the heating cylinder (8), and the top of the heating cylinder (8) is connected to the evaporation bin (2); A liquid infusion pipe (17) is connected to the top of the liquid storage bin (1), and a first fixing plate (18) is connected to the top of the liquid storage bin (1). The first fixing plate (18) fixes the liquid infusion pipe (17). A first peristaltic pump rod (19) is connected to the top of the first fixing plate (18), a first rotating shaft (20) is connected to the top of the first peristaltic pump rod (19), and a second spring shaft (21) is provided outside the first rotating shaft (20). The outside of the second spring shaft (21) is connected to a first clamping block (22). A second rotating shaft (24) is connected to the top of the first rotating shaft (20), and a third spring shaft (25) is provided outside the second rotating shaft (24). The outside of the third spring shaft (25) is connected to a second clamping block (26). A second peristaltic pump rod (28) is connected to the top of the second rotating shaft (24), and a second fixing plate (30) is connected to the top of the second peristaltic pump rod (28). An air delivery pipe (29) is connected to the bottom of the second fixing plate (30). The air delivery pipe (29) is in contact with the second peristaltic pump rod (28) and is connected to the heating cylinder (8). The liquid infusion pipe (17) is connected to the bottom of the evaporation bin (2); A second gear (15) meshes with the left side of the first gear (7). A rotating ring (16) is connected inside the second gear (15). A first ratchet groove (23) is provided at the bottom inside the rotating ring (16). The first ratchet groove (23) can be snap-connected to the first clamping block (22). A second ratchet groove (27) is connected to the top inside the rotating ring (16), and the second ratchet groove (27) can be snap-connected to the second clamping block (26); A fixing ring (38) is connected to the top of the liquid storage bin (1). The fixing ring (38) is slidably connected to the outside of the rotating ring (16). A steam collector (34) is provided at the top of the evaporation bin (2). A detection mechanism is provided on the right side of the evaporation bin (2), and a discharge port (31) is provided at the bottom of the evaporation bin (2); A filter block (5) is connected to the bottom of the liquid storage bin (1). A precipitation bin (4) is connected to the bottom of the filter block (5), and the precipitation bin (4) is connected to the liquid infusion valve (3); A fixing rod (37) is connected to the top of the liquid storage bin (1). The liquid storage bin (1) is fixedly connected to the evaporation bin (2) through the fixing rod (37).
2. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 1, characterized in that, The detection mechanism includes a U-shaped tube (32), and the U-shaped tube (32) is fixedly connected to the evaporation chamber (2), and a concentration detector (33) is provided in the middle of the U-shaped tube (32).
3. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 1, characterized in that, A heating resistance wire is provided inside the heating cylinder (8), and the inner top of the heating cylinder (8) is fixedly connected to the one-way valve (9).
4. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 1, characterized in that, The ratchet groove positions of the first ratchet groove (23) and the second ratchet groove (27) are opposite, and the orientations of the first latch (22) and the second latch (26) are opposite.
5. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 1, characterized in that, A corrugated pipe (35) is provided on the right side of the steam collector (34), and corrugated slots are provided inside the corrugated pipe (35).
6. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 5, characterized in that, A condensate discharge port (36) is provided at the bottom left end of the corrugated pipe (35), and the condensate discharge port (36) is fixedly connected to the corrugated pipe (35).
7. The high-efficiency energy-saving nitric acid evaporation and concentration device according to claim 1, wherein The bottom of the liquid storage chamber (1) is provided with feet, and heat preservation wall mechanisms are provided inside both the liquid storage chamber (1) and the evaporation chamber (2). The infusion pipe (17) and the gas transmission pipe (29) are made of soft rubber structure. The top of the first fixing plate (18) is fixedly attached to the infusion pipe (17) through a protective plate, and the bottom of the second fixing plate (30) is also fixedly attached to the gas transmission pipe (29) through a protective plate.
Citation Information
Patent Citations
Denitration, evaporation and concentration method and device for radioactive nitric acid waste liquid
CN116013569A
Automatic feeding device and washing equipment
CN214529788U