A filtering and distilling device for fine chemical organic synthesis and its use method

Abstract

The present invention discloses a filtering and distilling device for fine chemical organic synthesis and a method for using the same, and relates to the technical field of chemical filtering and distilling, including a stage, a vertical plate, a sinking table, a distillation flask, a condenser, and a recovery cylinder. The present invention sequentially and fixedly arranges a first connecting plate and a second connecting plate in the vertical direction of the vertical plate, and a circular groove is provided on the first connecting plate and the second connecting plate, and a supporting assembly for supporting a funnel is arranged inside the circular groove, and a common driving assembly that can drive multiple groups of supporting assemblies to rotate is arranged on the side of the vertical plate. When multiple groups of funnels are placed on the supporting assembly, when liquid is slowly and concentratedly poured into a place of filter paper inside the supporting funnel through a liquid guide hopper, the multiple groups of funnels can be rotated by the common driving assembly, so that the filter paper at various places inside the funnel can be fully utilized, which can effectively solve the problem that the concentrated pouring of liquid may not fully and effectively utilize the surface area of ​​the entire filter paper due to the funnel shape of the filter paper, thereby affecting the filtering effect.

Description

Technical Field

[0001] The invention relates to the technical field of chemical filtration and distillation, and in particular to a filtration and distillation device for fine chemical organic synthesis and a use method thereof. Background Art

[0002] Fine chemicals refers to the industrial field of producing fine chemicals, covering a series of high value-added chemical products such as medicines, pesticides, dyes, flavors and fragrances, additives, etc. Organic synthesis is an important branch in the field of chemistry, involving the process of converting simple elements, inorganic substances or simple organic substances into complex organic compounds by chemical methods. This process includes multiple reaction steps, such as addition reactions, substitution reactions, elimination reactions and rearrangement reactions.

[0003] During chemical experiments, when using filtering and distillation equipment, you first need to place the filter paper tightly in the funnel, and then pour the liquid to be filtered into the filter paper by manual pouring. In order to ensure the smoothness of the pouring process, it is usually recommended to pour the liquid slowly and concentratedly into one place of the filter paper. However, in the prior art, due to the funnel shape of the filter paper, concentrated pouring of the liquid may not fully and effectively utilize the surface area of ​​the entire filter paper, thereby affecting the filtration effect. This practice not only leads to low filtration efficiency, but also may increase experimental costs, because the underutilized filter paper needs to be replaced more frequently, thereby consuming more materials and time. Summary of the invention

[0004] The purpose of the present invention is to solve the problem in the prior art that in the process of chemical experiments, when using filtering and distilling equipment, first, the filter paper needs to be tightly placed in the funnel, and the liquid to be filtered is poured into the filter paper by manual pouring. In order to ensure the smoothness of the pouring process, it is usually recommended to slowly and concentratedly pour the liquid into one place of the filter paper. However, since the filter paper is in the shape of a funnel, concentrated pouring of the liquid may not fully and effectively utilize the surface area of ​​the entire filter paper, thereby affecting the filtering effect. This practice not only leads to low filtering efficiency, but also may increase the experimental cost, because the filter paper that is not fully utilized needs to be replaced more frequently, thereby consuming more materials and time. The present invention proposes a filtering and distilling equipment for fine chemical organic synthesis and a method for using the same.

[0005] In order to achieve the above object, the present invention adopts the following technical solutions:

[0006] A filtering and distillation device for fine chemical organic synthesis, comprising a stage, a vertical plate, a sinking platform, a distillation flask, a condenser, and a recovery cylinder, wherein a vertical plate is vertically fixedly arranged on the top of the stage, a sinking platform is provided at the top edge of the stage, a triangular plate is fixedly arranged on the top edge of the vertical plate, a liquid guide hopper is vertically fixedly arranged on the top of the triangular plate, a first connecting plate and a second connecting plate are fixedly arranged below the triangular plate in sequence, the first connecting plate and the second connecting plate are staggered in vertical direction, and the first connecting plate and the second connecting plate are arranged on the top edge of the vertical plate. A circular groove is provided on the top, and a supporting component for stably supporting the filter bucket is arranged inside the circular groove, a common driving component that can drive multiple supporting components to rotate is arranged at the bottom of the second connecting plate, an avoidance groove is provided on the top of the loading platform, and a multifunctional component for water bath heating the distillation flask is arranged on the loading platform below the avoidance groove, an air outlet pipe is obliquely fixed on the side of the distillation flask, a vertical groove is provided on the side of the vertical plate, and a closing avoidance component is arranged at the position of the vertical groove for closing the top opening of the distillation flask when the distillation flask is distilling.

[0007] Optionally, the support assembly includes a support ring, a driven pulley, and a bottom limit ring. The support ring is movably inserted into the circular groove, a driven pulley is fixedly provided at the top edge of the support ring, and the support ring is fixed with a bottom limit ring at the bottom of the second connecting plate using vertical bolts.

[0008] Optionally, the common drive component includes a vertical shaft, a top pulley, a bottom pulley, a short belt, and a long belt. The bottom pulley and the driven pulley on the first connecting plate are commonly sleeved with a short belt, and the top pulley and the driven pulley on the second connecting plate are commonly sleeved with a long belt. The bottom pulley and the top pulley are commonly fixed on the vertical shaft, and the vertical shaft is fixedly connected to the output end of the drive motor, and the drive motor is fixedly set at the bottom of the second connecting plate.

[0009] Optionally, the multifunctional component includes a water bath, a supporting ball net, and a guide plate. The loading platform is provided with an insertion slot below the avoidance slot, and a bottom connection platform is fixedly arranged on the loading platform directly above the avoidance slot. A neck slot is provided on the top of the bottom connection platform, and a guide plate is movably inserted into the insertion slot. A water bath is fixedly arranged on the top of the guide plate, and a transverse shifting hand is fixedly arranged in the middle position of the side of the water bath. A supporting ball net is movably inserted into the top of the water bath, and a circular array of release holes is provided on the top of the supporting ball net. A drain pipe is fixedly arranged at an angle on the bottom of the side of the water bath, and a guide elbow is movably inserted into the end of the condenser. The end of the guide elbow is suspended on the top of the recovery tube, and the recovery tube is movably placed on the top of the sinking platform. The loading platform is provided with a composite support component for limiting the direction of the cooling water inlet pipe of the condenser and fixing the condenser below the condenser.

[0010] Optionally, the composite support assembly includes a support frame, an auxiliary support seat, and a positioning seat. A transverse movement groove is opened at the bottom of the support frame, and the transverse movement groove passes through the mounting bolt. The bottom thread of the mounting bolt is screwed into the top of the worktable. An auxiliary support seat is fixedly arranged on the top of the support frame, and a positioning seat is fixedly arranged on the side of the auxiliary support seat. The positioning seat and the auxiliary support seat are both provided with supporting arc grooves on the top, and a positioning groove is vertically opened on the side of the top of the positioning seat, and a bottom ring is vertically fixed on the bottom of the positioning seat.

[0011] Optionally, the closed avoidance assembly includes a closed cylinder, an extension rod, a closed head, a top support plate, a mounting plate, a micro switch, and a trigger rod. The mounting plate is fixedly arranged on the rear side of the vertical plate, and a micro switch is fixedly arranged on the top of the mounting plate.

[0012] Optionally, the servo motor is vertically fixed on the top of the loading platform, a top support plate is fixedly provided at the output end of the servo motor, a closed cylinder is fixedly provided on the top of the top support plate, and an extension rod is vertically fixedly provided at the output end of the closed cylinder.

[0013] Optionally, a closed head is vertically fixedly provided at the end of the extension rod, a trigger rod is fixedly provided on the outer wall of the output end of the servo motor, and the end of the trigger rod contacts the side of the micro switch.

[0014] Optionally, a controller is fixedly arranged at the bottom of the front side of the loading platform, the micro switch is connected to the closed cylinder control circuit, and the closed cylinder, the drive motor and the servo motor are all connected to the controller.

[0015] A method for using a filtering and distilling device for fine chemical organic synthesis comprises the following steps:

[0016] S1: Filtration. Workers introduce the liquid to be filtered and distilled into the liquid guiding bucket, put the filter bucket into the circular grooves on the staggered first connecting plate and the second connecting plate, put filter paper in the filter bucket, start the common drive component, and open the valve at the bottom of the liquid guiding bucket. The common drive component drives the two filter buckets to rotate, and the liquid to be processed is evenly poured on various places of the filter paper and filtered by the multi-stage filter buckets. The filtered liquid falls into the distillation flask.

[0017] S2: Distillation. The worker controls the closed avoidance component through the controller to close the opening of the distillation flask, and then starts the water bath. The water bath distills the distillation flask. The gas distilled from the distillation flask is cooled by the condenser and finally flows back into the recovery cylinder.

[0018] Compared with the prior art, the present invention has the following advantages:

[0019] 1. The present invention sequentially and fixedly arranges a first connecting plate and a second connecting plate on the vertical direction of the vertical plate, and circular grooves are provided on the first connecting plate and the second connecting plate, and a supporting assembly for supporting the funnel is provided inside the circular groove, and a common driving assembly capable of driving a plurality of supporting assemblies to rotate is provided on the side of the vertical plate. When the plurality of funnels are placed on the supporting assembly, when liquid is slowly and concentratedly poured into a place of the filter paper inside the supporting funnel through the liquid guiding hopper, the plurality of funnels can be rotated by the common driving assembly, so that the filter paper at various places inside the funnel can be fully utilized, which can thoroughly and effectively solve the problem that the concentrated pouring of liquid may not fully and effectively utilize the surface area of ​​the entire filter paper due to the funnel shape of the filter paper, thereby affecting the filtering effect. This practice not only leads to low filtering efficiency, but also may increase the experimental cost, because the filter paper that is not fully utilized needs to be replaced more frequently, thereby consuming more materials and time.

[0020] 2. In the present invention, a first connecting plate and a second connecting plate are fixedly arranged in sequence in the vertical direction of the vertical plate. Circular grooves are opened on the first connecting plate and the second connecting plate. A supporting assembly for supporting the funnel is arranged inside the circular groove. Since the first connecting plate and the second connecting plate are staggered and two groups of supporting assemblies are provided, they can be used to accommodate two funnels, thereby realizing step-by-step and multi-stage filtration of the distillate to be filtered, which can improve the filtration efficiency. Each stage removes particles of a specific size, and finally obtains a filtrate with higher purity, and finally extends the life of the filter material. By removing larger particles first, the subsequent filter material is not easy to be blocked, thereby reducing the replacement frequency.

[0021] 3. The present invention provides a closed avoidance component on the top of the distillation flask. The closed avoidance component can close the top opening of the distillation flask when the distillation flask is distilling. When the distillation flask is receiving the filtrate, the closed avoidance component can open the top of the distillation flask and be removed from the top of the distillation flask to avoid interfering with the funnel dripping the filtrate into the distillation flask. During the distillation process, the top of the distillation flask can be sealed to prevent external pollutants from entering and substances from volatilizing; when the filtrate is receiving, the top component can be opened and removed to facilitate the funnel to drip the filtrate into the distillation flask, avoid frequent disassembly and installation, and improve the convenience and efficiency of operation. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] Figure 1 It is a schematic diagram of the overall structure of the present invention.

[0023] Figure 2 for Figure 1 Another perspective structural diagram of .

[0024] Figure 3 for Figure 2 Schematic diagram of the enlarged structure at B.

[0025] Figure 4 for Figure 2 Another perspective structural diagram of .

[0026] Figure 5 It is a schematic diagram of the structure of a water bath and its connecting parts.

[0027] Figure 6 A closure assembly is provided to close the distilling flask.

[0028] Figure 7 for Figure 6 Schematic diagram of the local enlarged structure at A.

[0029] Figure 8 It is a structural schematic diagram of the condenser and its positioning support assembly.

[0030] Fig. 9 for Figure 8 Schematic diagram of the semi-exploded structure.

[0031] Fig.10 Schematic diagram of the structure of the composite drive component.

[0032] Fig.11 A schematic diagram of the structure of the support assembly for supporting the filter bucket.

[0033] In the figure: 1, loading platform; 2, horizontal hand; 3, sinking platform; 4, bottom connecting platform; 5, neck groove; 6, avoidance groove; 61, distillation flask; 610, air outlet pipe; 7, insertion groove; 8, controller; 9, vertical plate; 10, first connecting plate; 11, circular groove; 12, second connecting plate; 13, recovery cylinder; 14, liquid guide bucket; 15, triangular plate; 16, vertical groove; 17, release hole; 18, water bath; 19, support net; 20, drainage pipe; 21, guide plate; 22, top support plate; 23, closed cylinder; 24, extension rod; 2 5. Closing head; 26. Trigger rod; 27. Micro switch; 28. Mounting plate; 29. ​​Servo motor; 30. Auxiliary support seat; 31. Condenser; 32. Support frame; 320. Mounting bolt; 33. Transverse groove; 34. Guide elbow; 35. Positioning groove; 36. Support arc groove; 37. Bottom ring; 38. Positioning seat; 39. Top pulley; 40. Short belt; 41. Vertical shaft; 42. Bottom pulley; 43. Driving motor; 44. Long belt; 45. Driven pulley; 46. Support ring; 47. Bottom limit ring; 48. Vertical bolt. DETAILED DESCRIPTION

[0034] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0035] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating the orientation or position relationship are based on the orientation or position relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0036] Reference Figure 1-11 A filtering and distilling device for fine chemical organic synthesis and a method of using the same include a stage 1, a vertical plate 9, a sinking platform 3, a distillation flask 61, a condenser 31, and a recovery cylinder 13. The condenser 31 of the distillation flask 61 is a device for cooling and condensing steam into a liquid. The specific structure includes an outer shell, an inner tube, a cooling water inlet and outlet, and a cooling water interlayer. Cooling water flows in the interlayer between the outer shell and the inner tube to condense the steam in the inner tube. The steam enters the inner tube through the steam inlet, condenses into a liquid after cooling, and is discharged through the condensate outlet. The distillation flask 61 and the condenser 31 are both common glass experimental instruments in laboratories, so the specific structure of the condenser 31 is not disclosed in detail in this application document.

[0037] A vertical plate 9 is vertically fixed on the top of the stage 1, a sinking platform 3 is provided at the top edge of the stage 1, a triangular plate 15 is fixed on the top edge of the vertical plate 9, a liquid guide bucket 14 is vertically fixed on the top of the triangular plate 15, a first connecting plate 10 and a second connecting plate 12 are fixed on the vertical plate 9 in sequence below the triangular plate 15, the first connecting plate 10 and the second connecting plate 12 are staggered in the vertical direction, a circular groove 11 is provided on the top of the first connecting plate 10 and the second connecting plate 12, a supporting assembly for stably supporting the filter bucket is provided inside the circular groove 11,

[0038] The support assembly includes a support ring 46, a driven pulley 45, and a bottom limit ring 47. The support ring 46 is movably inserted into the circular groove 11. The driven pulley 45 is fixedly provided at the top edge of the support ring 46. The support ring 46 is fixedly provided with a bottom limit ring 47 at the bottom of the second connecting plate 12 by a vertical bolt 48. The diameter of the bottom limit ring 47 is larger than the diameter of the circular groove 11. The bottom limit ring 47 and the driven pulley 45 limit the support ring 46 in the circular groove 11. In order to reduce the wear of the filter bucket placed on the support ring 46, a rubber ring can be additionally inlaid on the top of the support ring 46.

[0039] Therefore, when the two supporting components are placed in the glass filter funnel, the bottom of the filter funnel on the first connecting plate 10 is suspended on the top edge of the filter funnel on the second connecting plate 12. The liquid guide funnel 14 is a common separatory funnel in the laboratory, which can temporarily store the test solution to be filtered and distilled. A valve is provided at the bottom of the separatory funnel to control the release of the test solution in the separatory funnel.

[0040] At this time, the bottom of the liquid guiding funnel 14 is at the top edge of the filter funnel on the first connecting plate 10. When the circular grooves 11 opened on the tops of the first connecting plate 10 and the second connecting plate 12 are both placed in the filter funnel, funnel-shaped filter papers are placed in the filter funnels, and the pore size of the filter paper on the first connecting plate 10 is larger than that on the second connecting plate 12. The two filter funnels form a multi-stage step-by-step filtration of the test solution, and particles of a specific size are removed step by step, and finally a higher purity filtrate is obtained, and finally the life of the filter material is extended. By removing larger particles first, the subsequent filter material is not easy to be blocked, thereby reducing the replacement frequency.

[0041] A common driving component that can drive multiple supporting components to rotate is arranged at the bottom of the second connecting plate 12, and the common driving component includes a vertical shaft 41, a top pulley 39, a bottom pulley 42, a short belt 40, and a long belt 44. The bottom pulley 42 and the driven pulley 45 on the first connecting plate 10 are commonly sleeved with the short belt 40, and the top pulley 39 and the driven pulley 45 on the second connecting plate 12 are commonly sleeved with the long belt 44.

[0042] It should be added that the diameters of the top pulley 39 and the bottom pulley 42 are much smaller than the diameter of the driven pulley 45. The bottom pulley 42 and the top pulley 39 are fixedly arranged on a vertical shaft 41. The vertical shaft 41 is fixedly connected to the output end of a drive motor 43. The drive motor 43 is fixedly arranged at the bottom of the second connecting plate 12. The drive motor 43 will only very slowly drive the filter buckets on the two supporting assemblies to rotate slowly, so that the test solution is slowly and evenly introduced into various places on the surface of the bucket-shaped filter paper, thereby making full use of the filter paper.

[0043] An avoidance groove 6 is provided on the top of the stage 1, and a multifunctional component for water bath heating of the distillation flask 61 is arranged below the avoidance groove 6 on the stage 1, the multifunctional component includes a water bath pot 18, a support ball net 19, and a guide plate 21. An insertion groove 7 is provided below the avoidance groove 6 on the stage 1, and a bottom connecting platform 4 is fixedly provided on the stage 1 just above the avoidance groove 6. A neck groove 5 is provided on the top of the bottom connecting platform 4, and a guide plate 21 is movably inserted into the insertion groove 7. A water bath pot 18 is fixedly provided on the top of the guide plate 21, and a transverse movement hand 2 is fixedly provided in the middle position of the side of the water bath pot 18. A support ball net 19 is movably inserted into the top of the water bath pot 18, and a circular array of release holes 17 are provided on the top of the support ball net 19. The support ball net 19 cooperates with the bottom connecting platform 4 to stably support the distillation flask 61 placed in the water bath pot 18.

[0044] An air outlet pipe 610 is fixedly arranged at an angle on the side of the distillation flask 61, a vertical groove 16 is opened on the side of the vertical plate 9, and a closing avoidance component is arranged at the position of the vertical groove 16 for closing the top opening of the distillation flask 61 when the distillation flask 61 is distilling. A drain pipe 20 is fixedly arranged at an angle on the bottom of the side of the water bath pot 18, a guide elbow 34 is movably inserted into the end of the condenser 31, and the end of the guide elbow 34 is suspended on the top of the recovery cylinder 13, and the recovery cylinder 13 is movably placed on the top of the sinking platform 3, and the top height of the sinking platform 3 is lower than the top height of the loading platform 1.

[0045] A composite support assembly for limiting the direction of the cooling water inlet pipe of the condenser 31 and fixing the condenser 31 is provided on the stage 1 below the condenser 31. The composite support assembly includes a support frame 32, an auxiliary support seat 30, and a positioning seat 38. A transverse groove 33 is provided at the bottom of the support frame 32. The transverse groove 33 passes through the mounting bolt 320. The bottom thread of the mounting bolt 320 is screwed into the top of the stage 1. An auxiliary support seat 30 is fixedly provided on the top of the support frame 32. A positioning seat 38 is fixedly provided on the side of the auxiliary support seat 30 of the support frame 32. Support arc grooves 36 are provided on the tops of the positioning seat 38 and the auxiliary support seat 30. The auxiliary support seat 30 is used for auxiliary support of the exhaust pipe 610. A positioning groove 35 is vertically provided on the side of the top of the positioning seat 38. A bottom ring 37 is vertically fixedly provided at the bottom of the positioning seat 38. The positioning groove 35 is used for positioning the cooling water pipe of the condenser 31, and the bottom ring 37 is used for fixing the head of the condenser 31.

[0046] The closed avoidance component includes a servo motor 29, a closed cylinder 23, an extension rod 24, a closed head 25, a top support plate 22, a mounting plate 28, a micro switch 27, and a trigger rod 26. The mounting plate 28 is fixedly arranged on the rear side of the vertical plate 9, and a micro switch 27 is fixedly arranged on the top of the mounting plate 28. The servo motor 29 is vertically fixedly arranged on the top of the stage 1. The output end of the servo motor 29 is fixedly arranged with a top support plate 22, and the top of the top support plate 22 is fixedly arranged with a closed cylinder 23. The output end of the closed cylinder 23 is vertically fixedly arranged with an extension rod 24, and the end of the extension rod 24 is vertically fixedly arranged with a closed head 25. The closed head 25 is a stepped head, and the material is selected to be rubber material. The diameter of the narrow section of the closed head 25 is slightly larger than the top opening diameter of the distillation flask 61.

[0047] A trigger rod 26 is fixedly provided on the outer wall of the output end of the servo motor 29, and the end of the trigger rod 26 contacts the side of the micro switch 27. A controller 8 is fixedly provided on the bottom of the front side of the loading platform 1. The micro switch 27 is connected to the control circuit of the closed cylinder 23. The closed cylinder 23, the drive motor 43, and the servo motor 29 are all connected to the controller 8.

[0048] The specific implementation steps and principles of the present invention are:

[0049] In the initial state, the extension rod 24 rotates to a position parallel to the vertical plate 9, and the closing head 25 is not directly above the top opening of the distillation flask 61. The worker introduces the liquid to be filtered and distilled into the liquid guide bucket 14, puts the filter bucket into the circular grooves 11 on the staggered first connecting plate 10 and the second connecting plate 12, puts the filter paper into the filter bucket, starts the common drive component, and opens the valve at the bottom of the liquid guide bucket 14. The drive motor 43 in the common drive component drives the two filter buckets placed on the support ring 46 to rotate through the top pulley 39, the short belt 40, the bottom pulley 42, and the long belt 44. The liquid to be processed is evenly poured on various places on the filter paper and filtered by the multi-stage filter buckets. The filtered liquid falls into the distillation flask 61.

[0050] The worker controls the closing avoidance assembly to close the opening of the distillation flask 61 through the controller 8. Specifically, the controller 8 first controls the servo motor 29 to rotate until the trigger rod 26 of the vertical section of the servo motor 29 presses the micro switch 27. At this time, the closing head 25 at the bottom of the extension rod 24 moves to the top of the distillation flask 61. At this time, the closing cylinder 23 can move, driving the closing head 25 to press into the top opening of the distillation flask 61, and then start the water bath 18. The water bath 18 distills the distillation flask 61. The gas distilled from the distillation flask 61 is cooled by the condenser 31 and finally flows back to the inside of the recovery cylinder 13.

[0051] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A filtering and distilling device for fine chemical organic synthesis, comprising a stage (1), a vertical plate (9), a sinking table (3), a distillation flask (61), a condenser (31), and a recovery cylinder (13), characterized in that: A vertical plate (9) is vertically fixedly arranged on the top of the loading platform (1), a sinking platform (3) is provided at the top edge of the loading platform (1), a triangular plate (15) is fixedly arranged on the top edge of the vertical plate (9), a liquid guide hopper (14) is vertically fixedly arranged on the top of the triangular plate (15), a first connecting plate (10) and a second connecting plate (12) are fixedly arranged in sequence below the triangular plate (15), the first connecting plate (10) and the second connecting plate (12) are staggered in the vertical direction, and the first connecting plate (10) and the second connecting plate (12) are staggered in the vertical direction. ), a circular groove (11) is provided on the top of the second connecting plate (12), a supporting assembly for stably supporting the filter bucket is arranged inside the circular groove (11), a common driving assembly capable of driving a plurality of supporting assemblies to rotate is arranged at the bottom of the second connecting plate (12), an avoidance groove (6) is provided on the top of the loading platform (1), a multifunctional assembly for water bath heating the distillation flask (61) is arranged on the loading platform (1) below the avoidance groove (6), an air outlet pipe (610) is arranged on the side of the distillation flask (61) in an inclined manner, and a side of the vertical plate (9) is provided with a plurality of supporting assemblies for rotating the supporting assemblies. A vertical groove (16) is provided, and a sealing avoidance component is provided at the position of the vertical groove (16) for sealing the top opening of the distillation flask (61) when the distillation flask (61) is distilling. The sealing avoidance component comprises a servo motor (29), a sealing cylinder (23), an extension rod (24), a sealing head (25), a top support plate (22), a mounting plate (28), a micro switch (27), and a trigger rod (26). The mounting plate (28) is fixedly arranged on the rear side of the vertical plate (9), and the micro switch (27) is fixedly arranged on the top of the mounting plate (28). ), the servo motor (29) is vertically fixedly arranged on the top of the loading platform (1), a top support plate (22) is fixedly arranged on the output end of the servo motor (29), a closed cylinder (23) is fixedly arranged on the top of the top support plate (22), an extension rod (24) is vertically fixedly arranged on the output end of the closed cylinder (23), a closed head (25) is vertically fixedly arranged on the end of the extension rod (24), a trigger rod (26) is fixedly arranged on the outer wall of the output end of the servo motor (29), and the end of the trigger rod (26) contacts the side of the micro switch (27).

2. The filtration and distillation equipment for fine chemical organic synthesis according to claim 1, characterized in that: The support assembly comprises a support ring (46), a driven pulley (45), and a bottom limit ring (47); the support ring (46) is movably inserted into the circular groove (11); the driven pulley (45) is fixedly arranged at the top edge of the support ring (46); and the bottom limit ring (47) is fixedly arranged at the bottom of the second connecting plate (12) by vertical bolts (48).

3. The filtration and distillation equipment for fine chemical organic synthesis according to claim 1, characterized in that: The common drive assembly comprises a vertical shaft (41), a top pulley (39), a bottom pulley (42), a short belt (40), and a long belt (44); the bottom pulley (42) and a driven pulley (45) on the first connecting plate (10) are commonly sleeved with the short belt (40); the top pulley (39) and a driven pulley (45) on the second connecting plate (12) are commonly sleeved with the long belt (44); the bottom pulley (42) and the top pulley (39) are commonly fixedly arranged on the vertical shaft (41); the vertical shaft (41) is fixedly connected to the output end of a driving motor (43); and the driving motor (43) is fixedly arranged at the bottom of the second connecting plate (12).

4. The filtration and distillation equipment for fine chemical organic synthesis according to claim 1, characterized in that: The multifunctional component comprises a water bath (18), a supporting ball net (19), and a guide plate (21); the loading platform (1) is provided with an insertion groove (7) below the avoidance groove (6); the loading platform (1) is fixedly provided with a bottom connection platform (4) directly above the avoidance groove (6); the top of the bottom connection platform (4) is provided with a neck groove (5); the insertion groove (7) is movably inserted with a guide plate (21); the top of the guide plate (21) is fixedly provided with a water bath (18); a lateral movement hand (2) is fixedly provided at the middle position of the side of the water bath (18); the top of the water bath (18) is movably inserted with a neck groove (5); A supporting ball net (19) is movably inserted, and a circular array of release holes (17) are provided on the top of the supporting ball net (19). A drain pipe (20) is fixedly arranged at an angle on the bottom of the side of the water bath (18). A guide bend (34) is movably inserted into the end of the condenser (31), and the end of the guide bend (34) is suspended on the top of the recovery cylinder (13). The recovery cylinder (13) is movably placed on the top of the sinking platform (3). A composite support component for limiting the direction of the cooling water inlet pipe of the condenser (31) and fixing the condenser (31) is provided on the stage (1) below the condenser (31).

5. The filtration and distillation equipment for fine chemical organic synthesis according to claim 4, characterized in that: The composite support assembly comprises a support frame (32), an auxiliary support seat (30), and a positioning seat (38); a transverse displacement groove (33) is provided at the bottom of the support frame (32); the transverse displacement groove (33) passes through a mounting bolt (320); the bottom of the mounting bolt (320) is threadedly screwed into the top of the worktable (1); an auxiliary support seat (30) is fixedly provided at the top of the support frame (32); a positioning seat (38) is fixedly provided on the side of the auxiliary support seat (30) of the support frame (32); a supporting arc groove (36) is provided at the top of the positioning seat (38) and the auxiliary support seat (30); a positioning groove (35) is vertically provided on the side of the top of the positioning seat (38); and a bottom ring (37) is vertically fixedly provided at the bottom of the positioning seat (38).

6. The filtration and distillation equipment for fine chemical organic synthesis according to claim 5, characterized in that: A controller (8) is fixedly arranged at the bottom of the front side of the loading platform (1); the micro switch (27) is connected to the control circuit of the closed cylinder (23); and the closed cylinder (23), the drive motor (43), and the servo motor (29) are all connected to the controller (8).

7. The method for using the filtration and distillation equipment for fine chemical organic synthesis according to claim 6, characterized in that: The following steps are involved: S1: Filtration, a worker introduces the liquid to be filtered and distilled into the liquid guide bucket (14), places the filter bucket in the circular grooves (11) on the staggered first connecting plate (10) and the second connecting plate (12), places filter paper in the filter bucket, starts the common drive component, and opens the valve at the bottom of the liquid guide bucket (14). The common drive component drives the two filter buckets to rotate, and the liquid to be processed is evenly poured on all parts of the filter paper and filtered by the multi-stage filter buckets. The filtered liquid falls into the distillation bottle (61); S2: Distillation. The worker controls the closing avoidance component through the controller (8) to close the opening of the distillation flask (61), and then starts the water bath (18). The water bath (18) distills the distillation flask (61). The gas distilled from the distillation flask (61) is cooled by the condenser (31) and finally flows back into the recovery cylinder (13).

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