Toothpaste with functions of strengthening teeth and protecting gingiva and preparation process of toothpaste

Abstract

The invention discloses toothpaste with tooth-strengthening and gum-protecting functions and a preparation process thereof, and relates to the technical field of toothpaste production and processing. The facial cleanser is prepared from the following components: 50% of a humectant, 22.00% of hydrated silica, 18.40% of water, 3.00% of polyethylene glycol-400, 2.1% of a cleaning agent, 0.80% of an Ilex rotunda extract, 0.60% of essence, 0.60% of cellulose gum, 0.50% of hydroxyapatite, 0.36% of menthol, 0.30% of xanthan gum, 0.30% of CI 77891, 0.30% of tetrasodium pyrophosphate, 0.24% of menthane formylethylamine, 0.20% of saccharin sodium salt and 0.15% of methylparaben. The toothpaste disclosed by the invention not only has excellent cleaning ability, but also has the functions of protecting and improving gingival health, so that multiple effects are integrated; a nanometer grinding technology is adopted, so that the seepage force and the taste of the components are improved, and meanwhile, the sanitation and the stability of the product are ensured through a sterile filling and vacuum technology.

Description

Technical Field

[0001] The invention relates to the technical field of toothpaste production and processing, and in particular to a toothpaste with the function of strengthening teeth and protecting gums and a preparation process thereof. Background Art

[0002] With the development of modern society and the advancement of science and technology, people are pursuing higher and higher oral health. Teeth and gums are important parts of the oral cavity, and their health status directly affects the normal function of the oral cavity. The main function of traditional toothpaste is to clean teeth and reduce the incidence of caries by removing stains and food residues on the surface of teeth. However, they usually do not have the function of caring for gums. After long-term use, they may cause gum problems such as gingivitis and gum recession.

[0003] After searching, the application scheme with Chinese patent application number 202210677569.6 discloses a whitening and cleaning toothpaste composition and a preparation method thereof, wherein the toothpaste composition includes 5.1~35wt.% of abrasive, 0.25~0.35wt.% of tetrasodium pyrophosphate, 1.2~1.4wt.% of adhesive, 0.9~1.1wt.% of preservative, 0.67~0.71wt.% of anti-caries agent, 35~41wt.% of moisturizer, 1.25~1.55wt.% of flavoring agent, 4.1~4.5wt.% of surfactant, 0.45~0.55wt.% of sunscreen, 0.45%~2% of Yunnan Baiyao extract, and the balance is water; the abrasive is a compound of hydrated silica and friction cellulose, hydrated silica accounts for 5~35wt.% of the total mass of the whitening and cleaning toothpaste composition, and friction cellulose accounts for 0.1~15wt.% of the total mass of the whitening and cleaning toothpaste composition. The toothpaste composition in the above patent has the following deficiencies: although it has the functions of whitening and cleaning, it is still insufficient in terms of gum care. Summary of the invention

[0004] The purpose of the present invention is to solve the shortcomings of the prior art and to propose a toothpaste with the function of strengthening teeth and protecting gums and a preparation process thereof.

[0005] In order to achieve the above object, the present invention adopts the following technical solutions: A toothpaste with the function of protecting teeth and gums, comprising: Humectant 50%, hydrated silica 22.00%, water 18.40%, polyethylene glycol-400 3.00%, detergent 2.1%, iron holly extract 0.80%, fragrance 0.60%, cellulose gum 0.60%, hydroxyapatite 0.50%, menthol 0.36%, xanthan gum 0.30%, CI 77891 0.30%, tetrasodium pyrophosphate 0.30%, menthane carboxamide 0.24%, sodium saccharin 0.20%, methylparaben 0.15%, dipotassium glycyrrhizinate 0.10%, propylparaben 0.05; Wherein, the moisturizing agent includes: sorbitol 41.00%, maltitol 4.50%, mannitol 4.50%; Wherein, the cleaning agent comprises: 1.995% sodium lauryl sulfate, 0.042% sodium sulfate, 0.0105% C12-16 alcohol, and 0.0525% water.

[0006] Preferably: the preparation process of the toothpaste comprises the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Check the pH value of the mixture and adjust it to a pH range suitable for the oral environment, with the pH value controlled at 6.5-7.5; Step 5: Pour the final mixture into a toothpaste tube and seal it for storage.

[0007] Preferably, the preparation process of the toothpaste is replaced by the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Finely grind the mixture using nano-grinding technology to improve taste and enhance penetration of ingredients; Step 5: Place the mixture into a vacuum device and perform vacuuming to ensure that there are no bubbles in the toothpaste and to make the ingredients more evenly distributed; Step 6: The toothpaste is aged in a refrigerated environment at 5°C for 48 hours to stabilize the chemical properties and improve storage stability; Step 7: After removal, conduct final quality inspection, including pH testing and microbiological testing, to ensure that the product meets the safety standards for oral products.

[0008] Step 8: Under sterile conditions, fill the toothpaste into a pre-sterilized toothpaste tube; Preferably: the step 1 specifically includes: S11: placing the weighed moisturizer, hydrated silica and water in a mixer according to the proportion; S12: Preliminary stirring at room temperature for 5 minutes to completely disperse the solid components; S13: Raise the mixer temperature to 60°C and continue heating and stirring for 30 minutes to ensure that all ingredients are fully dissolved.

[0009] Preferably: the step 2 specifically includes: S21: naturally cooling the mixture obtained in step 1 to room temperature; S22: Slowly add detergent while stirring rapidly to avoid forming lumps; S23: Continue stirring for 10 minutes until the mixture is homogeneous.

[0010] Preferably: the step three specifically includes: S31: adding holly extract, flavor, cellulose gum and other active ingredients in sequence; S32: After each addition, stir at 60r / min for 5 minutes to ensure uniform blending; S33: After adding all ingredients, stir at 120 r / min for 5 minutes to ensure the homogeneity of the mixture.

[0011] Preferably: the step 4 specifically includes: S41: transferring the mixture into a nano grinder; S42: Grind in a grinder at 3000 rpm for 30 minutes to ensure fine and uniform particles; S43: The ground mixture is tested for particle size to ensure that it meets nanometer standards.

[0012] Preferably: the step five specifically includes: S51: placing the mixture into a vacuum device to perform vacuuming; S52: Pull until the vacuum degree is -0.094MPa, open the air vent valve to exhaust, remove bubbles, and make the toothpaste more compact; The step six specifically includes: S61: placing the vacuumed toothpaste in a constant temperature cold storage room at 5°C; S62: Maintain for 48 hours for aging treatment to stabilize the composition and properties of the toothpaste.

[0013] Preferably: the step seven specifically includes: S71: Conduct pH test to ensure it is within the safe range for oral products; S72: Conduct microbiological testing to ensure there is no bacterial contamination; S73: Conduct comprehensive quality assessment before final packaging to ensure that every tube of toothpaste meets production standards.

[0014] Preferably: the step eight specifically includes: S81: Pour toothpaste into a pre-sterilized toothpaste tube under a sterile operating table; S82: Use automatic filling machines to avoid manual contact and ensure product hygiene; S83: Seal immediately after filling to ensure that the product is not contaminated by the outside world.

[0015] The beneficial effects of the present invention are: The toothpaste of the present invention not only has excellent cleaning ability, but also has the function of protecting and improving gum health, achieving multiple effects in one; the nano-grinding technology is used to improve the penetration and taste of the ingredients, while the hygiene and stability of the product are ensured through aseptic filling and vacuum technology. The present invention selects natural extracts and mild detergents to reduce irritation to the oral mucosa and is suitable for long-term use; through aging treatment and strict quality testing, the stability and safety of the product during storage and use are ensured. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 The present invention provides a flow chart of a process for preparing a toothpaste having the function of strengthening teeth and protecting gums. DETAILED DESCRIPTION

[0017] The technical solution of the present invention is further described in detail below in conjunction with specific implementation methods.

[0018] Embodiment 1: A toothpaste with the function of protecting teeth and gums, comprising: Humectant 50%, hydrated silica 22.00%, water 18.40%, polyethylene glycol-400 3.00%, detergent 2.1%, ILEX ROTUNDA extract 0.80%, fragrance 0.60%, cellulose gum 0.60%, hydroxyapatite 0.50%, menthol 0.36%, xanthan gum 0.30%, CI 77891 0.30%, tetrasodium pyrophosphate 0.30%, menthane carboxamide 0.24%, sodium saccharin 0.20%, methylparaben 0.15%, dipotassium glycyrrhizinate 0.10%, propylparaben 0.05; Wherein, the moisturizing agent includes: sorbitol 41.00%, maltitol 4.50%, mannitol 4.50%; Wherein, the cleaning agent comprises: 1.995% sodium lauryl sulfate, 0.042% sodium sulfate, 0.0105% C12-16 alcohol, and 0.0525% water.

[0019] The preparation process of the toothpaste comprises the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Check the pH value of the mixture and adjust it to a pH range suitable for the oral environment (about 6.5-7.5); Step 5: Pour the final mixture into a toothpaste tube and seal it for storage.

[0020] Embodiment 2: A toothpaste with the function of protecting teeth and gums. This embodiment is based on the embodiment 1, and the following improvements are made: The preparation process of the toothpaste is replaced by the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Finely grind the mixture using nano-grinding technology to improve taste and enhance penetration of ingredients; Step 5: Place the mixture into a vacuum device and perform vacuuming to ensure that there are no bubbles in the toothpaste and to make the ingredients more evenly distributed; Step 6: The toothpaste is aged in a refrigerated environment at 5°C for 48 hours to stabilize the chemical properties and improve storage stability; Step 7: After removal, conduct final quality inspection, including pH test and microbiological test, to ensure that the product meets the safety standards for oral products; Step 8: Under sterile conditions, fill the toothpaste into the pre-sterilized toothpaste tube.

[0021] Wherein, the step 1 specifically includes: S11: placing the weighed moisturizer, hydrated silica and water in a mixer according to the proportion; S12: Preliminary stirring at room temperature for 5 minutes to completely disperse the solid components; S13: Raise the mixer temperature to 60°C and continue heating and stirring for 30 minutes to ensure that all ingredients are fully dissolved.

[0022] Wherein, the step 2 specifically includes: S21: naturally cooling the mixture obtained in step 1 to room temperature; S22: Slowly add detergent while stirring rapidly to avoid forming lumps; S23: Continue stirring for 10 minutes until the mixture is homogeneous.

[0023] Wherein, the step three specifically includes: S31: adding holly extract, flavor, cellulose gum and other active ingredients in sequence; S32: After each addition, stir at 60r / min for 5 minutes to ensure uniform blending; S33: After adding all ingredients, stir at 120 r / min for 5 minutes to ensure the homogeneity of the mixture.

[0024] Wherein, the step 4 specifically includes: S41: transferring the mixture into a nano grinder; S42: Grind in a grinder at 3000 rpm for 30 minutes to ensure fine and uniform particles; S43: The ground mixture is tested for particle size to ensure that it meets nanometer standards.

[0025] Wherein, the step five specifically includes: S51: placing the ground paste into a vacuum device; S52: Pull until the vacuum degree is -0.094MPa, open the air vent valve to exhaust, remove bubbles, and make the toothpaste more compact.

[0026] Wherein, the step six specifically includes: S61: Place the toothpaste in a constant temperature refrigerator at 5°C; S62: Maintain for 48 hours for aging treatment to stabilize the composition and properties of the toothpaste.

[0027] Wherein, the step seven specifically includes: S71: Conduct pH test to ensure it is within the safe range for oral products; S72: Conduct microbiological testing to ensure there is no bacterial contamination; S73: Conduct comprehensive quality assessment before final packaging to ensure that every tube of toothpaste meets production standards.

[0028] Wherein, the step eight specifically includes: S81: Pour toothpaste into a pre-sterilized toothpaste tube under a sterile operating table; S82: Use automatic filling machines to avoid manual contact and ensure product hygiene; S53: Seal immediately after filling to ensure that the product is not contaminated by the outside world.

[0029] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A toothpaste with the function of protecting teeth and gums, characterized in that the ingredients include: Humectant 50%, hydrated silica 22.00%, water 18.40%, polyethylene glycol-4003.00%, detergent 2.1%, holly extract 0.80%, fragrance 0.60%, cellulose gum 0.60%, hydroxyapatite 0.50%, menthol 0.36%, xanthan gum 0.30%, CI 778910.30%, tetrasodium pyrophosphate 0.30%, menthane carboxamide 0.24%, saccharin sodium 0.20%, methylparaben 0.15%, dipotassium glycyrrhizinate 0.10%, propylparaben 0.05; Wherein, the moisturizing agent comprises: sorbitol 41.00%, maltitol 4.50%, mannitol 4.50%; The cleaning agent includes: 1.995% sodium lauryl sulfate, 0.042% sodium sulfate, 0.0105% C12-16 alcohol, and 0.0525% water.

2. The toothpaste with the function of strengthening teeth and protecting gums according to claim 1, characterized in that: The preparation process of the toothpaste comprises the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Check the pH value of the mixture and adjust it to a pH range suitable for the oral environment, with the pH value controlled at 6.5-7.5; Step 5: Pour the final mixture into a toothpaste tube and seal it for storage.

3. The toothpaste with the function of strengthening teeth and protecting gums according to claim 2, characterized in that: The preparation process of the toothpaste is replaced by the following steps: Step 1: Weigh the moisturizer, hydrated silica, water, and polyethylene glycol-400 in proportion, mix well, and heat to 60°C for 30 minutes to ensure complete dissolution; Step 2: Cool the mixture obtained in step 1 to room temperature, add detergent, and stir until completely blended; Step 3: Add holly extract, flavor, cellulose gum, hydroxyapatite, menthol, xanthan gum, CI 77891, tetrasodium pyrophosphate, menthane carboxamide, sodium saccharin, methylparaben, dipotassium glycyrrhizinate, and propylparaben to the mixture of step 2 in sequence, and stir thoroughly after each addition; Step 4: Finely grind the mixture using nano-grinding technology to improve taste and enhance penetration of ingredients; Step 5: Place the mixture into a vacuum device and perform vacuuming to ensure that there are no bubbles in the toothpaste and to make the ingredients more evenly distributed; Step 6: Aging the toothpaste in a cold storage environment controlled at 5°C; Step 7: After removal, conduct final quality inspection, including pH test and microbiological test, to ensure that the product meets the safety standards for oral products; Step 8: Under sterile conditions, fill the toothpaste into the pre-sterilized toothpaste tube.

4. The toothpaste with the function of strengthening teeth and protecting gums according to claim 3, characterized in that: The step 1 specifically includes: S11: placing the weighed moisturizer, hydrated silica and water in a mixer according to the proportion; S12: Preliminary stirring at room temperature for 5 minutes to completely disperse the solid components; S13: Raise the mixer temperature to 60°C and continue heating and stirring for 30 minutes to ensure that all ingredients are fully dissolved.

5. The toothpaste with the function of strengthening teeth and protecting gums according to claim 3, characterized in that: The step 2 specifically includes: S21: naturally cooling the mixture obtained in step 1 to room temperature; S22: Slowly add detergent while stirring rapidly to avoid forming lumps; S23: Continue stirring for 10 minutes until the mixture is homogeneous.

6. The toothpaste with the function of strengthening teeth and protecting gums according to claim 3, characterized in that: The step three specifically includes: S31: adding holly extract, flavor, cellulose gum and other active ingredients in sequence; S32: After each addition, stir at 60r / min for 5 minutes to ensure uniform blending; S33: After adding all ingredients, stir at 120 r / min for 5 minutes to ensure the homogeneity of the mixture.

7. The toothpaste with the function of strengthening teeth and protecting gums according to claim 3, characterized in that: The step 4 specifically includes: S41: transferring the mixture into a nano grinder; S42: Grind in a grinder at 3000 rpm for 30 minutes to ensure that the particles are fine and uniform; S43: The ground mixture is tested for particle size to ensure that it meets nanometer standards.

8. The toothpaste with teeth-health and gum-protecting functions according to claim 3, characterized in that: The step five specifically includes: S51: placing the ground mixture into a vacuum device; S52: When the vacuum degree reaches -0.094MPa, open the vent valve to exhaust air, remove bubbles, and make the toothpaste more compact.

9. The toothpaste with teeth-health and gum-protecting functions according to claim 3, characterized in that: The step six specifically includes: S61: placing the vacuumed toothpaste in a constant temperature cold storage room at 5°C; S62: Maintain for 48 hours for aging treatment to stabilize the composition and properties of the toothpaste.

10. The toothpaste with the function of strengthening teeth and protecting gums according to claim 3, characterized in that: The step seven specifically includes: S71: Conduct pH test to ensure it is within the safe range for oral products; S72: Conduct microbiological testing to ensure there is no bacterial contamination; S73: Conduct comprehensive quality assessment before final packaging to ensure that every tube of toothpaste meets production standards; The step eight specifically includes: S81: Pour the paste into a pre-sterilized toothpaste tube under a sterile operating table; S82: Use automatic filling machines to avoid manual contact and ensure product hygiene; S83: Seal immediately after filling to ensure that the product is not contaminated by the outside world.

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