Pet nutritional supplement granule and preparation method thereof
By using the explosive core material and nutrient layer in pet nutritional supplement granules, combined with Antarctic krill oil, DHA algae oil and pumpkin seed oil, the problems of poor palatability and single nutritional components for pets are solved, and the efficient use of Antarctic krill oil and a variety of nutrients are achieved, which relieves allergic reactions and improves palatability.
Patent Information
- Application Number
- CN202510488934.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-04-18
- Publication Date
- 2025-06-10
- Estimated Expiration
- 2045-04-18
AI Technical Summary
The existing Antarctic krill oil supplement for pets has poor palatability, low utilization rate, and may cause pet allergic reactions. It has a single nutritional component, making it difficult to supplement multiple nutrients at the same time.
Pet nutritional supplement particles composed of a burst bead core material and a nutrient layer coated on its surface. The core liquid contains 75-85% Antarctic krill oil, 15-25% DHA algae oil and 5-10% pumpkin seed oil. The nutrient layer contains flavor masking pellets and a variety of nutrients.
It improves the utilization rate of Antarctic krill oil, reduces pet resistance to Antarctic krill oil, allergic reactions, and improves palatability and achieves sustained release function through the design of taste masking micropills.
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Figure CN120113731A_ABST
Abstract
Description
Technical Field
[0001] The present disclosure relates to the technical field of pet food, and particularly to a pet nutritional supplement granule and a preparation method thereof. Background Art
[0002] Antarctic krill oil is a natural oil extracted from Antarctic krill and is rich in various nutritional components beneficial to pet health. The ω-3 fatty acids it contains, especially EPA and DHA, have strong anti-inflammatory properties, can effectively reduce joint inflammation, relieve pain and swelling caused by diseases such as arthritis, and its lubricating effect can effectively prevent the occurrence of joint diseases for pets that often exercise or are older. However, existing Antarctic krill oil supplements for pets usually exist in the forms of soft capsules, capsules, dripping pills, etc., with poor palatability for pets, and there are also problems such as low utilization rate of Antarctic krill oil, and allergic reactions such as soft stools, skin itching, erythema, and ear infections in some pets after consumption.
[0003] Moreover, the above-mentioned Antarctic krill oil products have a single nutritional component. If other types of nutrients, such as calcium, iron, zinc and other nutrient elements, need to be supplemented, additional feeding is required.
[0004] Therefore, how to provide a product with good palatability, which can simultaneously supplement Antarctic krill oil and other nutrient elements, and improve the utilization rate of Antarctic krill oil, pet palatability, and relieve allergic reactions has become an urgent problem to be solved currently. Summary of the Invention
[0005] To solve the above technical problems, the present disclosure provides a pet nutritional supplement granule and a preparation method thereof.
[0006] In a first aspect, the present disclosure provides a pet nutritional supplement granule, including a bursting bead core material and a nutritional layer coated on the surface of the bursting bead core material;
[0007] The bursting bead core material includes a wall material and a core liquid wrapped inside the wall material;
[0008] By weight, the core liquid includes 75 - 85 parts of Antarctic krill oil, 15 - 25 parts of DHA algal oil, and 5 - 10 parts of pumpkin seed oil;
[0009] The components of the nutritional layer include taste-masking pellets, and the taste-masking pellets include a pellet core and a coating layer coated on the surface of the pellet core;
[0010] The pellet core contains vitamins;
[0011] The components of the coating layer include first animal-source meat, amino acids, table salt, sodium alginate, polyethylene glycol, hydroxypropyl methylcellulose, and zein.
[0012] Among them, the weight parts of Antarctic krill oil are such as 75 parts, 77 parts, 80 parts, 82 parts or 85 parts, etc.; the weight parts of DHA algal oil are such as 15 parts, 17 parts, 20 parts, 23 parts or 25 parts, etc.; the weight parts of pumpkin seed oil are such as 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts, etc., but are not limited to the listed values, and other unlisted values within the above range are equally applicable.
[0013] On the one hand, in view of the problems of low utilization rate of Antarctic krill oil and causing allergies in some pets in the prior art, by adding DHA algal oil and pumpkin seed oil, the two act synergistically, not only improving the utilization rate of Antarctic krill oil, but also effectively alleviating diarrhea, skin itching, erythema and ear infections caused by allergies; at the same time, through the encapsulation of the nutrient layer, the resistance of pets to Antarctic krill oil is reduced; on the other hand, the present disclosure also solves the resistance psychology of pets when eating vitamin supplements by making the vitamin raw materials with too strong taste into taste-masked pellets and adding them to the nutrient layer, and also improves the palatability without additionally increasing the taste layer by adjusting the formula of the taste-masked pellets, and at the same time realizes the sustained-release function and relieves the gastrointestinal pressure of pets.
[0014] In the present disclosure, the addition content of pumpkin seed oil should not be too much. Excessive addition not only has limited improvement on the utilization rate of Antarctic krill oil, but also increases the risk of pet allergies.
[0015] The following are the preferred technical solutions of the present disclosure, but do not limit the technical solutions provided by the present disclosure. Through the following technical solutions, the technical purposes and beneficial effects of the present disclosure can be better achieved and realized.
[0016] As a preferred technical solution of the present disclosure, in the bursting bead core material, the mass ratio of the wall material to the core liquid is (0.3 - 0.4):1.
[0017] As a preferred technical solution of the present disclosure, the diameter of the bursting bead core material is 5 - 6 mm, such as 5 mm, 5.2 mm, 5.4 mm, 5.6 mm, 5.8 mm or 6 mm, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0018] The components of the wall material include glycerol, sorbitol and edible glue.
[0019] Preferably, the added mass ratio of glycerol, sorbitol and edible glue is (80 - 100):(20 - 40):(2800 - 3200), such as 90:30:300, 80:20:2800, 100:40:3200 or 95:35:2900, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0020] Preferably, the composition of the wall material further includes a colorant.
[0021] The colorant is a food coloring and can be added as appropriate according to requirements.
[0022] Preferably, the edible glue includes gelatin.
[0023] As a preferred technical solution of the present disclosure, the vitamins include one or more of vitamin B1, vitamin B2, vitamin B6, vitamin B12, calcium D-pantothenate or niacin.
[0024] Preferably, the vitamins further include one or more of vitamin A, vitamin D3, vitamin K or folic acid.
[0025] In the present disclosure, the types of vitamins are not limited to the above substances, and other vitamins beneficial to pets can be added.
[0026] Preferably, the composition of the nutrition layer further includes a first auxiliary material, and the first auxiliary material includes one or more of starch, maltodextrin or granulated sugar.
[0027] In the present disclosure, the types of vitamins are not limited to the above. Existing vitamins required by pets can be added and prepared as needed. Moreover, the addition amount of the second vitamin can also be adjusted according to product requirements, which will not be elaborated here.
[0028] As a preferred technical solution of the present disclosure, the first animal-source meat includes one or more of chicken, chicken liver or beef.
[0029] Preferably, the amino acids include one or more of taurine, proline, lysine, glycine or glutamic acid.
[0030] As a preferred technical solution of the present disclosure, by mass percentage, the components of the coating layer include 60-75wt% of the first animal-derived meat, 10-20wt% of amino acids, 1-3wt% of table salt, 5-15wt% of sodium alginate, 1-5wt% of polyethylene glycol, 3-7wt% of hydroxypropyl methylcellulose, and 5-15wt% of zein. Among them, the content of the first animal-derived meat is such as 60wt%, 60-75wt%, 70wt% or 75wt%, etc.; the content of amino acids is such as 10wt%, 12wt%, 14wt%, 16wt%, 18wt% or 20wt%, etc.; the content of table salt is such as 1wt%, 2wt% or 3wt%, etc.; the content of sodium alginate is such as 5wt%, 7wt%, 10wt%, 13wt% or 15wt%, etc.; the content of polyethylene glycol is such as 1wt%, 2wt%, 3wt%, 4wt% or 5wt%, etc.; the content of hydroxypropyl methylcellulose is such as 3wt%, 4wt%, 5wt%, 6wt% or 7wt%, etc.; the content of zein is such as 5wt%, 10wt%, 12wt% or 15wt%, etc. However, it is not limited to the listed values, and other unlisted values within the above range are equally applicable.
[0031] As a preferred technical solution of the present disclosure, the diameter of the taste-masking pellets is 0.9-1.1mm, such as 0.9mm, 1.0mm or 1.1mm, etc. However, it is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0032] Preferably, the thickness of the nutrition layer is 2-3mm, such as 2mm, 2.2mm, 2.4mm, 2.6mm, 2.8mm or 3mm, etc. However, it is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0033] As a preferred technical solution of the present disclosure, the pet nutrition supplement granules further include a taste layer coated on the surface of the nutrition layer.
[0034] Preferably, the components of the taste layer include the second animal-derived meat and the second auxiliary material.
[0035] Preferably, the second animal-derived meat includes one or more of chicken, beef or chicken liver.
[0036] Preferably, the second auxiliary material includes starch and / or maltodextrin.
[0037] Preferably, the thickness of the taste layer is 2-3mm, such as 2mm, 2.2mm, 2.4mm, 2.6mm, 2.8mm or 3mm, etc. However, it is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0038] Second aspect, the present disclosure also provides a preparation method of the pet nutritional supplement granules as described in the first aspect, and the preparation method includes the following steps:
[0039] (1) Prepare the core liquid and the wall material glue liquid, and use the microcapsule embedding technology to form concentric droplets of the core liquid and the wall material glue liquid, and drop them into the coagulating liquid to form wet pills. The obtained wet pills are dried to obtain the core material of the popping beads;
[0040] (2) Prepare powdery vitamins and obtain pill cores by centrifugal granulation; then, coat the obtained pill cores to obtain taste-masked pellets;
[0041] (3) Prepare the powder for the nutrition layer, and use centrifugal granulation to form a nutrition layer on the surface of the core material of the popping beads obtained in step (1), and then dry to obtain the pet nutritional supplement granules;
[0042] Wherein, the powder for the nutrition layer includes taste-masked pellets.
[0043] Wherein, steps (1) and (2) are not in a sequential order.
[0044] The finished product prepared by using the preparation method described in the present disclosure has a stable structure, good powder wrapping property, and a simple production process, which is beneficial to industrial application.
[0045] As a preferred technical solution of the present disclosure, the preparation method further includes: after drying in step (3), use centrifugal granulation to form a taste layer on the surface of the nutrition layer, and then dry to obtain the pet nutritional supplement granules.
[0046] As a preferred technical solution of the present disclosure, the drying temperature in step (1) is 25-35°C, such as 25°C, 30°C or 35°C, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0047] Preferably, after drying in step (1), the water content of the obtained core material of the popping beads is below 8wt%, such as 2wt%, 4wt%, 6wt% or 8wt%, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0048] Preferably, the drying temperature in step (3) is 60-80°C, such as 60°C, 65°C, 70°C, 75°C or 80°C, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0049] Preferably, after drying in step (3), the water content of the obtained pet health food granules is below 8wt%, such as 2wt%, 4wt%, 6wt% or 8wt%, etc., but is not limited to the listed values, and other unlisted values within this range are equally applicable.
[0050] As a preferred technical solution of the present disclosure, the specific operation of step (1) includes:
[0051] S1: Prepare the core liquid
[0052] Between 15 - 35 °C, mix 75 - 85 parts by weight of Antarctic krill oil, 15 - 25 parts by weight of DHA algal oil, and 5 - 10 parts by weight of pumpkin seed oil;
[0053] S2: Prepare the wall material glue liquid
[0054] Mix glycerol, sorbitol, and edible glue with water at 50 - 70 °C according to the mass ratio of (80 - 100):(20 - 40):(2800 - 3200), stir evenly, and then heat to 80 - 85 °C, with the heating time being 1.5 - 2.5 h;
[0055] S3: Add the core liquid and the wall material glue liquid to the oil pot and glue pot of the pill dropping machine respectively, set the dropping speed of the dropper to 45 - 55 HZ, and the generated concentric liquid droplets (i.e., the wall material glue liquid includes the core liquid) fall into the coagulating liquid to form wet pills; then dry the wet pills at 25 - 35 °C, and at the same time use absorbent paper to remove the coagulating liquid on the surface of the wet pills until the water content is below 8 wt%, obtaining the core material of the bursting beads.
[0056] Among them, set the temperature of the oil pot to 15 - 30 °C, and set the temperature of the glue pot to 70 - 90 °C.
[0057] As a preferred technical solution of the present disclosure, the specific operation of step (2) includes:
[0058] Prepare the pill core: Place the powdered vitamin in a centrifugal granulating machine for rounding, and then dry to obtain a pill core with a water content of 8 - 10 wt%;
[0059] Prepare the coating liquid: Dissolve 60 - 75 wt% of the first animal - source meat powder, 10 - 20 wt% of amino acids, 1 - 3 wt% of table salt, 5 - 15 wt% of sodium alginate, 1 - 5 wt% of polyethylene glycol, 3 - 7 wt% of hydroxypropyl methylcellulose, and 5 - 15 wt% of zein in water to obtain the coating liquid;
[0060] Place the pill core in a bottom - spray fluidized bed coater, turn on the bottom spray atomizer for coating until the taste - masking pellets with a set diameter are obtained.
[0061] In the present disclosure, the addition amount of water in the coating liquid can be determined by those skilled in the art according to experience as long as the coating state can be achieved.
[0062] As a preferred technical solution of the present disclosure, the specific operation of step (3) includes:
[0063] Prepare the powder for the nutrient layer: Mix the taste-masked pellets obtained in step (2) with the first excipient to obtain the powder for the nutrient layer;
[0064] Place the core material of the bursting bead obtained in step (1) in a centrifugal granulation machine, set the rotation speed to 35 - 45 HZ, spray water to moisten the surface of the core material of the bursting bead, spray the powder for the nutrient layer for rounding, take it out after reaching the set diameter, and dry it at 60 - 80 °C until the moisture content is below 8 wt%, to obtain the required pet nutritional supplement granules.
[0065] As a preferred technical solution of the present disclosure, in the preparation process of each step, good products meeting the standard size are screened out through a standard sieve.
[0066] As a preferred technical solution of the present disclosure, in the process of preparing the core material of the bursting bead, after good products meeting the standard size are screened out through a standard sieve, unqualified products with irregular circles, air leakage and damage are further screened out manually.
[0067] The technical solution provided by the embodiment of the present disclosure has the following advantages compared with the prior art:
[0068] (1) Aiming at the problems of low utilization rate of Antarctic krill oil and causing allergies in some pets in the prior art, the present disclosure adds DHA algal oil and pumpkin seed oil, and the two act synergistically, not only improving the utilization rate of Antarctic krill oil, but also effectively alleviating diarrhea, skin itching, erythema, and ear infections caused by allergies; at the same time, through the encapsulation of the nutrient layer, the resistance of pets to Antarctic krill oil is reduced;
[0069] (2) The present disclosure also makes the vitamin raw materials with too strong taste into taste-masked pellets and adds them to the nutrient layer, solving the resistance psychology of pets when eating vitamin supplements, and also improving the palatability without adding a flavor layer by adjusting the formula of the taste-masked pellets, and at the same time realizing the sustained-release function and alleviating the gastrointestinal pressure of pets;
[0070] (3) The finished product prepared by the present disclosure has a stable structure, good powder encapsulation, and a simple production process, which is conducive to industrial application. BRIEF DESCRIPTION OF THE DRAWINGS
[0071] The accompanying drawings here are incorporated into the specification and form a part of this specification, showing embodiments consistent with the present disclosure, and are used together with the specification to explain the principles of the present disclosure.
[0072] In order to more clearly illustrate the technical solutions in the embodiments of the present disclosure or the prior art, the following will briefly introduce the accompanying drawings required for the description of the embodiments or the prior art. Obviously, for those of ordinary skill in the art, other drawings can be obtained based on these drawings without creative efforts.
[0073] Figure 1 This is a schematic cross-sectional view of the pet nutritional supplement granules described in Embodiment 1 of the present disclosure.
[0074] Among them, 1 is the core material of the bursting bead; 1-1 is the wall material; 1-2 is the core liquid; 2 is the nutrition layer; 2-1 is the taste-masking pellet; 2-1-1 is the coating layer; 2-1-2 is the pellet core. Specific Embodiments
[0075] In order to more clearly understand the above-mentioned objects, features, and advantages of the present disclosure, the solutions of the present disclosure will be further described below. It should be noted that, without conflict, the embodiments of the present disclosure and the features in the embodiments can be combined with each other.
[0076] In the following description, many specific details are set forth in order to fully understand the present disclosure, but the present disclosure can also be implemented in other ways different from those described herein; obviously, the embodiments in the specification are only a part of the embodiments of the present disclosure, rather than all of the embodiments.
[0077] Embodiment 1
[0078] This embodiment provides a pet nutritional supplement granule, and its schematic cross-sectional view is as Figure 1 shown, including a bursting bead core material 1 with a diameter of 5 mm and a nutrition layer 2 with a thickness of 3 mm coated on the surface of the bursting bead core material 1;
[0079] The bursting bead core material 1 includes a wall material 1-1 and a core liquid 1-2 wrapped inside the wall material 1-1;
[0080] By weight, the core liquid 1-2 includes 85 parts of Antarctic krill oil, 20 parts of DHA algal oil, and 5 parts of pumpkin seed oil;
[0081] The components of the nutrition layer 2 include taste-masking pellets 2-1 with a diameter of 1 mm, starch, maltodextrin, and granulated sugar;
[0082] The taste-masking pellet 2-1 includes a pellet core 2-1-2 and a coating layer 2-1-1 coated on the surface of the pellet core 2-1-2;
[0083] The pellet core 2-1-2 contains vitamins;
[0084] The components of the coating layer 2-1-1 include 25 wt% chicken, 20 wt% chicken liver, 20 wt% beef, 3 wt% taurine, 1 wt% proline, 2 wt% lysine, 1 wt% glycine, 3 wt% glutamic acid, 1 wt% table salt, 5 wt% sodium alginate, 1 wt% polyethylene glycol, 5 wt% hydroxypropyl methylcellulose and 13 wt% zein.
[0085] The preparation method includes the following steps:
[0086] (1) Prepare the core material 1 of the bursting bead
[0087] S1: Prepare the core liquid 1-2
[0088] At 25 °C, mix 20 kg of Euphausia superba oil, 5 kg of DHA algal oil and 1.25 kg of pumpkin seed oil to obtain the core liquid 1-2;
[0089] S2: Prepare the glue liquid (raw material of the wall material 1-1)
[0090] At 60 °C, add 90 g of glycerol, 30 g of sorbitol solution and 3 kg of gelatin to 20 kg of purified water in sequence, stir evenly, then heat to 80 °C, and the heating time is 2 h to obtain the glue liquid;
[0091] S3: Add the core liquid 1-2 to the oil pan of the pill dropping machine, add the glue liquid to the glue pan of the pill dropping machine. After the glue liquid stands for 2 h to completely defoam, start dropping. Set the dropping speed of the dropper head to 50 HZ. The generated concentric liquid drops (i.e., the glue liquid wraps the core liquid 1-2) fall into the liquid paraffin oil to form wet pills; then put the wet pills into a rotary cage drying machine for drying, and at the same time use oil absorbent paper to absorb the surface paraffin oil. When the water content is below 8 wt%, obtain the core material 1 of the bursting bead;
[0092] The obtained core material 1 of the bursting bead is screened with a standard sieve to select the qualified products of 5 mm, and then the unqualified products with irregular circles, air leakage and breakage are manually selected. The discharge amount of the core material 1 of the bursting bead is 26 kg;
[0093] (2) Coating the nutrient layer 2
[0094] S3: Prepare the pill core 2-1-2:
[0095] Put 1.5 g of powdered vitamin A, 5 g of powdered vitamin D3, 1 g of powdered vitamin B1, 2 g of powdered vitamin B2, 1 g of powdered vitamin B6, 0.02 g of powdered vitamin B12, 10 g of powdered nicotinic acid, 0.2 g of powdered folic acid, and 10 g of powdered D-calcium pantothenate into a centrifugal granulation machine for rolling, and then dry to obtain the pill core 2-1-2 with a water content of 9 wt%;
[0096] S4: Preparation of coating solution: Dissolve 2.5 kg of chicken powder, 2 kg of chicken liver powder, 2 kg of beef powder, 0.3 kg of taurine, 0.1 kg of proline, 0.2 kg of lysine, 0.1 kg of glycine, 0.3 kg of glutamic acid, 0.1 kg of table salt, 0.5 kg of sodium alginate, 0.1 kg of polyethylene glycol 400, 0.5 kg of hydroxypropyl methylcellulose and 1.3 kg of zein into 56 kg of water to obtain the coating solution;
[0097] S5: Preparation of taste-masking pellets 2-1
[0098] Place 100 kg of pellet cores 2-1-2 in a bottom-spray fluidized bed coater, turn on the bottom spray atomizer for coating to obtain taste-masking pellets 2-1 with a diameter of 1 mm;
[0099] S6: Preparation of mixed powder (raw materials for nutritional layer 2)
[0100] Mix 50 kg of maltodextrin, 30 kg of pregelatinized corn starch and 20 kg of taste-masking pellets 2-1 to obtain the mixed powder;
[0101] S7: Place the qualified bead core material 1 obtained in step (1) in a centrifugal granulator, set the rotation speed to 100 HZ, spray water to wet the surface of the bead core material 1, spray the mixed powder for rounding, take it out after the diameter reaches 8 mm, and dry it at 70 °C until the moisture content is below 8 wt% to obtain pet nutritional supplement granules.
[0102] Example 2
[0103] This example provides a pet nutritional supplement granule and its preparation method. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 1, and the difference is only that: the core liquid 1-2 includes 18.75 kg of Antarctic krill oil, 6.25 kg of DHA algal oil and 2.5 kg of pumpkin seed oil.
[0104] The preparation method refers to the preparation method in Example 1, and the difference is only that: in step S1, 18.75 kg of Antarctic krill oil, 6.25 kg of DHA algal oil and 2.5 kg of pumpkin seed oil are mixed at 25 °C to obtain the core liquid 1-2.
[0105] The discharge amount of the bead core material 1 in this preparation process is 24.5 kg.
[0106] Example 3
[0107] This embodiment provides a pet nutritional supplement granule and a preparation method thereof. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 1, with the only difference being that the core liquid 1-2 includes 21.25 kg of Antarctic krill oil, 3.75 kg of DHA algal oil, and 2 kg of pumpkin seed oil.
[0108] The preparation method refers to the preparation method in Example 1, with the only difference being that in step S1, at 25°C, 21.25 kg of Antarctic krill oil, 3.75 kg of DHA algal oil, and 2 kg of pumpkin seed oil are mixed to obtain the core liquid 1-2.
[0109] In this preparation process, the discharge amount of the bead core material 1 is 22 kg.
[0110] Comparative Example 1
[0111] This comparative example provides a pet nutritional supplement granule and a preparation method thereof. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 1, with the only difference being that the core liquid 1-2 only includes 26.25 kg of Antarctic krill oil.
[0112] The preparation method refers to the preparation method in Example 1, with the only difference being that in step S1, at 25°C, the core liquid 1-2 only includes 26.25 kg of Antarctic krill oil.
[0113] In this preparation process, the discharge amount of the bead core material 1 is 15 kg.
[0114] Comparative Example 2
[0115] This comparative example provides a pet nutritional supplement granule and a preparation method thereof. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 1, with the only difference being that the core liquid 1-2 includes 21 kg of Antarctic krill oil and 5.25 kg of DHA algal oil.
[0116] On the premise of ensuring the total mass of the core liquid remains unchanged, the reduced weight of the pumpkin seed oil is added to the Antarctic krill oil and DHA algal oil in proportion.
[0117] The preparation method refers to the preparation method in Example 1, with the only difference being that in step S1, at 25°C, 21 kg of Antarctic krill oil and 5.25 kg of DHA algal oil are mixed to obtain the core liquid 1-2.
[0118] In this preparation process, the discharge amount of the bead core material 1 is 15.4 kg.
[0119] Comparative Example 3
[0120] This comparative example provides a pet nutritional supplement granule and a preparation method thereof. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 1, with the only difference being that the core liquid 1-2 comprises 24.71 kg of Antarctic krill oil and 1.54 kg of pumpkin seed oil.
[0121] On the premise of ensuring that the total mass of the core liquid remains unchanged, the reduced weight of DHA algal oil is added to Antarctic krill oil and pumpkin seed oil in proportion.
[0122] The preparation method refers to the preparation method in Example 1, with the only difference being that in step S1, 24.71 kg of Antarctic krill oil and 1.54 kg of pumpkin seed oil are mixed at 25°C to obtain the core liquid 1-2.
[0123] The discharge amount of the bursting bead core material 1 in this preparation process is 15.6 kg.
[0124] Comparative Example 4
[0125] This comparative example provides a pet nutritional supplement granule and a preparation method thereof. The pet nutritional supplement granule refers to the pet nutritional supplement granule in Example 2, with the only difference being that the core liquid 1-2 comprises 18.38 kg of Antarctic krill oil, 6.12 kg of DHA algal oil, and 3 kg of pumpkin seed oil.
[0126] On the premise of ensuring that the total mass of the core liquid remains unchanged, the increased weight of pumpkin seed oil is proportionally reduced by Antarctic krill oil and DHA algal oil.
[0127] The preparation method refers to the preparation method in Example 1, with the only difference being that in step S1, 18.38 kg of Antarctic krill oil, 6.12 kg of DHA algal oil, and 3 kg of pumpkin seed oil are mixed at 25°C to obtain the core liquid 1-2.
[0128] The discharge amount of the bursting bead core material 1 in this preparation process is 15 kg.
[0129] Product performance test
[0130] Determine the utilization rate of Antarctic krill oil in the pet nutritional supplement granules obtained in Examples 1-3 and Comparative Examples 1-4.
[0131] Utilization rate of Antarctic krill oil % = total discharge mass of bursting bead core material / (total mass of core liquid materials + total mass of edible glue materials) × 100%, where the edible glue refers to gelatin, and the amounts of glycerol and sorbitol are not counted.
[0132] The results of the utilization rate of Antarctic krill oil in the pet nutritional supplement granules obtained in Examples 1-3 and Comparative Examples 1-4 are shown in Table 1.
[0133] Table 1
[0134]
[0135] Conclusion:
[0136] From the measurement results, it can be seen that adding DHA algal oil and pumpkin seed oil to the pet nutritional supplement granule product of the present application in the Antarctic krill oil bursting beads ensures the structural stability of the product, thereby effectively improving the utilization rate of Antarctic krill oil, increasing it from 49% to over 73%.
[0137] There is only Antarctic krill oil in the core liquid of the bursting bead core material of Comparative Example 1, resulting in a low utilization rate.
[0138] In Comparative Examples 2 and 3, only one of DHA algal oil or pumpkin seed oil was added, and the two could not play a synergistic role, resulting in limited improvement in the utilization rate of Antarctic krill oil.
[0139] In Comparative Example 4, the addition amount of pumpkin seed oil was too much, which instead reduced the utilization rate of Antarctic krill oil and increased the risk of pet allergy.
[0140] It should be noted that in this article, relational terms such as "first" and "second" are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variant thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements not only includes those elements, but also includes other elements not expressly listed, or also includes elements inherent to such process, method, article or device. Without further limitation, an element defined by the statement "including a..." does not exclude the existence of additional identical elements in the process, method, article or device including the said element.
[0141] The above are only specific embodiments of the present disclosure, enabling those skilled in the art to understand or implement the present disclosure. Various modifications to these embodiments will be obvious to those skilled in the art, and the general principles defined herein can be implemented in other embodiments without departing from the spirit or scope of the present disclosure. Therefore, the present disclosure will not be limited to these embodiments described herein, but will conform to the broadest scope consistent with the principles and novel features disclosed herein.
Claims
1. A pet nutritional supplement granule, characterized in that: It comprises a blasting bead core material and a nutrient layer coated on the surface of the blasting bead core material; The popping bead core material includes a wall material and a core liquid wrapped inside the wall material; In parts by weight, the core liquid comprises 75-85 parts of Antarctic krill oil, 15-25 parts of DHA algae oil and 5-10 parts of pumpkin seed oil; The ingredients of the nutrient layer include taste-masked pellets, and the taste-masked pellets include a pellet core and a coating layer coated on the surface of the pellet core; The pellet core contains vitamins; The coating layer comprises first animal source meat, amino acids, salt, sodium alginate, polyethylene glycol, hydroxypropyl methylcellulose and corn protein.
2. The pet nutritional supplement granules according to claim 1, characterized in that: The diameter of the blasting bead core material is 5-6 mm; Preferably, the wall material comprises glycerin, sorbitol and edible gum; Preferably, the added mass ratio of glycerol, sorbitol and edible gum is (80-100):(20-40):(2800-3200); Preferably, the composition of the wall material further includes a colorant; Preferably, the edible gum comprises gelatin.
3. The pet nutritional supplement granules according to claim 1 or 2, characterized in that: The vitamins include one or more of vitamin B1, vitamin B2, vitamin B6, vitamin B12, D-calcium pantothenate or niacin; Preferably, the vitamins further include one or more of vitamin A, vitamin D3, vitamin K or folic acid; Preferably, the ingredients of the nutrient layer further include a first auxiliary material, and the first auxiliary material includes one or more of starch, maltodextrin or white sugar.
4. The pet nutritional supplement granules according to any one of claims 1 to 3, characterized in that: The first animal source meat includes one or more of chicken, chicken liver or beef; Preferably, the amino acids include one or more of taurine, proline, lysine, glycine or glutamic acid.
5. The pet nutritional supplement granules according to claim 4, characterized in that: In terms of mass percentage, the ingredients of the coating layer include 60-75wt% of first animal source meat, 10-20wt% of amino acids, 1-3wt% of salt, 5-15wt% of sodium alginate, 1-5wt% of polyethylene glycol, 3-7wt% of hydroxypropyl methylcellulose and 5-15wt% of zein.
6. The pet nutritional supplement granules according to any one of claims 1 to 5, characterized in that: The diameter of the taste-masked pellets is 0.9-1.1 mm; Preferably, the thickness of the nutrient layer is 2-3 mm.
7. A method for preparing the pet nutritional supplement particles according to any one of claims 1 to 6, characterized in that: The preparation method comprises the following steps: (1) preparing a core liquid and a glue for a wall material, using microencapsulation technology to form concentric droplets of the core liquid and the glue for the wall material, dropping the droplets into a coagulation liquid to form wet pellets, and drying the obtained wet pellets to obtain a bursting bead core material; (2) preparing powdered vitamins and preparing pellet cores by centrifugal granulation; then coating the obtained pellet cores to obtain taste-masked pellets; (3) preparing a powder for a nutritional layer, using a centrifugal granulation method to form a nutritional layer on the surface of the popping bead core material obtained in step (1), and then drying to obtain pet nutritional supplement particles; Wherein, the powder for the nutrient layer includes taste-masking micro-pellets.
8. The preparation method according to claim 7, characterized in that: The preparation method further comprises: after drying in step (3), forming a flavor layer on the surface of the nutrition layer by a centrifugal granulation method, and then drying to obtain pet nutritional supplement particles.
9. The preparation method according to claim 7 or 8, characterized in that: The drying temperature in step (1) is 25-35° C. Preferably, after the drying in step (1), the moisture content of the obtained popping bead core material is below 8 wt %.
10. The preparation method according to any one of claims 7 to 9, characterized in that: The drying temperature in step (3) is 60-80° C. Preferably, after the drying in step (3), the moisture content of the obtained pet health food particles is below 8 wt %.
Citation Information
Patent Citations
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