Cooling agent composition, electronic atomization liquid and electronic atomization device

By combining WS-23, WS-27 and menthol in proportion to prepare electronic atomization liquid, the problem of single coolness of existing coolants is solved, and the richness and comfort of the cool parts are improved, and the user experience is improved.

CN120240697APending Publication Date: 2025-07-04SHENZHEN SMOORE TECH LTD
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Patent Information

Application Number
CN202410010907.X
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-01-03
Publication Date
2025-07-04

AI Technical Summary

Technical Problem

The coolant WS-23 in the existing electronic atomization device has a single cool effect area and a rough cool feeling, making it difficult to meet consumers' demand for a richer cool feeling.

Method used

WS-23, WS-27 and menthol are combined in a certain proportion to form a cooling agent composition, and mixed with solvents propylene glycol and glycerin to prepare an electronic atomization liquid to improve the richness and comfort of the cool part.

Benefits of technology

It enhances the richness and comfort of the cool feeling, enhances the user's experience of e-cigarettes, and avoids the generation of peculiar odors.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to a cooling agent composition, electronic atomization liquid and an electronic atomization device. The cooling agent composition is prepared from the following components in parts by mass: 30 to 45 parts of WS-23, 2 to 8 parts of WS-27 and 2 to 8 parts of menthol. According to the cooling agent composition, the WS-23, the WS-27 and the menthol are compounded according to a certain proportion for use, so that the cooling agent composition can be suitable for atomization, richness and comfort of a cool-feeling part are improved, and then the experience feeling of an electronic cigarette of a user is improved.
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Description

Technical Field

[0001] The present invention relates to the field of atomization, and particularly to a cooling flavor composition, an electronic atomization liquid, and an electronic atomization device. Background Art

[0002] The working mechanism of an electronic atomization device is to convert an electronic atomization liquid into an aerosol through an atomizer for human inhalation. The electronic atomization liquid is an important source of the flavor of the electronic atomization device. Adding a cooling flavor to the electronic atomization liquid can give consumers a cool feeling and enhance the richness of the flavor and taste. The commonly used traditional cooling flavor is WS-23 (N,2,3-trimethyl-2-isopropylbutyramide), but its cooling effect site is single and the cooling feeling is rough, which is difficult to meet the consumers' demand for a richer cooling feeling. Summary of the Invention

[0003] Based on this, some embodiments of the present invention provide a cooling flavor composition suitable for atomization, which can improve the richness and comfort of the cooling feeling.

[0004] A cooling flavor composition, by mass parts, includes: 30 parts to 45 parts of WS-23, 2 parts to 8 parts of WS-27, and 2 parts to 8 parts of menthol.

[0005] In some of these embodiments, by mass parts, it includes: 35 parts to 42 parts of WS-23, 3 parts to 6 parts of WS-27, and 3 parts to 6 parts of menthol.

[0006] In some of these embodiments, the mass ratio of the WS-23 to the WS-27 is (7 to 12):1; and / or,

[0007] the mass ratio of the WS-23 to the menthol is (7 to 12):1.

[0008] An electronic atomization liquid includes a solvent and the above-mentioned cooling flavor composition.

[0009] In some of these embodiments, the solvent includes one or more of propylene glycol and glycerol.

[0010] In some of these embodiments, based on 100% of the mass percentage of the electronic atomization liquid, the electronic atomization liquid includes 0.1% to 10% of the cooling flavor composition, 30% to 70% of propylene glycol, and 20% to 60% of glycerol.

[0011] In some of these embodiments, based on 100% of the mass percentage of the electronic atomization liquid, the electronic atomization liquid includes 2% to 6% of the cooling flavor composition, 35% to 50% of propylene glycol, and 48% to 60% of glycerol.

[0012] In some of these embodiments, the electronic atomization liquid further includes one or more of flavors, sweeteners, and nicotine salts.

[0013] In some of these embodiments, based on the mass percentage of the electronic atomization liquid being 100%, the mass percentage of the flavor is 0-30%, the mass percentage of the sweetener is 0-8%, and the mass percentage of the nicotine salt is 0-10%.

[0014] An electronic atomization device includes the above-mentioned electronic atomization liquid.

[0015] The above-mentioned cooling agent composition uses WS-23, WS-27, and menthol in a certain proportion, enabling the cooling agent composition to be suitable for atomization and improving the richness and comfort of the cooling sensation parts, thereby enhancing the user's experience of the electronic cigarette. Detailed Embodiments

[0016] To facilitate the understanding of the present invention, the present invention will be described more comprehensively below in conjunction with the detailed embodiments. Preferred embodiments of the present invention are given in the detailed embodiments. However, the present invention can be implemented in many different forms and is not limited to the embodiments described herein. On the contrary, the purpose of providing these embodiments is to make the understanding of the disclosure content of the present invention more thorough and comprehensive.

[0017] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by those skilled in the technical field to which the present invention belongs. The terms used in the specification of the present invention herein are only for the purpose of describing specific embodiments and are not intended to limit the present invention. The term "and / or" used herein includes any and all combinations of one or more of the related listed items.

[0018] Unless otherwise stated or there are contradictions, the terms or phrases used in the present invention have the following meanings:

[0019] In the present invention, "first" and "second" are only for descriptive purposes and cannot be understood as indicating or implying relative importance or implicitly specifying the quantity of the indicated technical features. Thus, the features defined with "first" and "second" may explicitly or implicitly include at least one of these features.

[0020] In the description of the present invention, the meaning of "a plurality" is at least two, such as two, three, etc., unless otherwise clearly and specifically defined.

[0021] In the present invention, "one or more" refers to any one, any two, or any two or more of the listed items. Among them, "several" refers to any two or more.

[0022] In the present invention, the percentage concentration involved, unless otherwise specified, refers to the final concentration. The final concentration refers to the proportion of the added component in the system after the addition of the component.

[0023] The words "optionally" and the like in the present invention refer to embodiments of the present invention that can provide certain beneficial effects in certain circumstances. However, other embodiments may also be optional under the same circumstances or other circumstances. In addition, the statement of one or more optional embodiments does not imply that other embodiments are not available, nor is it intended to exclude other embodiments from the scope of the present invention.

[0024] When a numerical range is disclosed in the present invention, the above range is considered to be continuous and includes the minimum and maximum values ​​of the range, as well as every value between such minimum and maximum values. Further, when a range refers to an integer, every integer between the minimum and maximum values ​​of the range is included. In addition, when multiple ranges are provided to describe features or characteristics, the ranges can be merged. In other words, unless otherwise indicated, all ranges disclosed in the present invention should be understood to include any and all subranges included therein.

[0025] In the present invention, the technical features described in an open manner include closed technical solutions composed of the listed features, and also include open technical solutions containing the listed features.

[0026] The terms "including" and "having" and any variations thereof in the embodiments of the present invention are intended to cover non-exclusive inclusions. For example, a process, method, system, product, or device that includes a series of steps or units is not limited to the listed steps or units, but may optionally include steps or units that are not listed, or may optionally include other steps or components that are inherent to these processes, methods, products, or devices.

[0027] Reference to "embodiments" in the present invention means that a particular feature, structure, or characteristic described in conjunction with the embodiments may be included in at least one embodiment of the present application. The appearance of the phrase in various places in the specification does not necessarily refer to the same embodiment, nor is it an independent or alternative embodiment that is mutually exclusive with other embodiments. It is explicitly and implicitly understood by those skilled in the art that the embodiments described in the present invention may be combined with other embodiments.

[0028] The first aspect of the present application provides a cooling agent composition, which includes, by mass, 30 to 45 parts of WS-23 (N,2,3-trimethyl-2-isopropylbutanamide), 2 to 8 parts of WS-27 (N,2-diethyl-2-isopropyl-3-methylbutanamide) and 2 to 8 parts of menthol.

[0029] In an alternative example, in the cooling agent composition, the parts by mass of WS-23 can be, but are not limited to, 30 parts, 32 parts, 34 parts, 35 parts, 36 parts, 38 parts, 40 parts, 42 parts, 44 parts, 45 parts, or the range formed by any two of these values. Optionally, in the cooling agent composition, the parts by mass of WS-23 are 35 parts to 42 parts.

[0030] In an alternative example, in the cooling agent composition, the parts by mass of WS-27 can be, but are not limited to, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, or the range formed by any two of these values. Optionally, in the cooling agent composition, the parts by mass of WS-27 are 3 parts to 6 parts.

[0031] In an alternative example, in the cooling agent composition, the parts by mass of menthol can be, but are not limited to, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, or the range formed by any two of these values. Optionally, in the cooling agent composition, the parts by mass of menthol are 3 parts to 6 parts.

[0032] In some embodiments, by parts by mass, the cooling agent composition consists of 30 parts to 45 parts of WS-23, 2 parts to 8 parts of WS-27, and 2 parts to 8 parts of menthol.

[0033] In some embodiments, in the cooling agent composition, the mass ratio of WS-23 to WS-27 is (7 to 12):1. For example, the mass ratio of WS-23 to WS-27 can be, but is not limited to, 7:1, 7.5:1, 8:1, 8.5:1, 9:1, 9.5:1, 10:1, 10.5:1, 11:1, 11.5:1, 12:1, or the range formed by any two of these values.

[0034] In some embodiments, in the cooling agent composition, the mass ratio of WS-23 to menthol is (7 to 12):1. For example, the mass ratio of WS-23 to menthol can be, but is not limited to, 7:1, 7.5:1, 8:1, 8.5:1, 9:1, 9.5:1, 10:1, 10.5:1, 11:1, 11.5:1, 12:1, or the range formed by any two of these values.

[0035] In some embodiments, by parts by mass, the cooling agent composition includes: 35 parts to 42 parts of WS-23, 3 parts to 6 parts of WS-27, and 3 parts to 6 parts of menthol. Further, by parts by mass, the cooling agent composition consists of 35 parts to 42 parts of WS-23, 3 parts to 6 parts of WS-27, and 3 parts to 6 parts of menthol.

[0036] In one embodiment, by mass parts, the cooling agent composition includes 41 parts of WS-23, 5 parts of WS-27 and 4 parts of menthol. In another embodiment, by mass parts, the cooling agent composition includes 35 parts of WS-23, 3 parts of WS-27 and 6 parts of menthol. In yet another embodiment, by mass parts, the cooling agent composition includes 42 parts of WS-23, 6 parts of WS-27 and 3 parts of menthol.

[0037] Currently, the components of current food-grade cooling agents that can be atomized in an electronic atomization device to give a cooling sensation to the human senses are limited, such as: WS-23, WS-3 (N-ethyl-p-menthane-3-carboxamide), WS-5 (N-(ethoxycarbonylmethyl)-p-alkane-3-carboxamide), WS-27 and menthol, etc. The inventors have found through research that the oral cooling sensation of WS-23 is weak; the cooling sensation intensity of WS-27 is slightly weaker than that of WS-23, but it has an unpleasant smell during atomization and suction; the nasal and oral cooling sensations of WS-3 and WS-5 are not obvious; menthol has its special mint aroma and bitter taste. Through a large amount of creative work, the inventors compound WS-23, WS-27 and menthol in a certain proportion, so that the cooling agent composition is suitable for atomization, and improves the richness and comfort of the cooling sensation parts, thereby enhancing the cooling experience of the user's electronic cigarette.

[0038] Among them, the richness of the cooling sensation means that the more the number of cooling sensation parts, the richer it is, that is, the "rich" cooling sensation can be perceived not only in one or a certain part, but in multiple parts. The comfort of the cooling sensation means that the intensity is moderate and the intensity is coordinated, that is, the intensities in different parts are balanced and there is no phenomenon of excessive cooling in individual parts; there is no negative unpleasant smell or other flavors. By adjusting menthol within an appropriate concentration range, the perceived smell is pleasant.

[0039] The second aspect of the present invention provides an electronic atomization liquid, including the above-mentioned cooling agent composition and a solvent.

[0040] In some embodiments, in the electronic atomization liquid, the mass percentage of the cooling agent composition is 0.1% - 10%. In an optional example, in the electronic atomization liquid, the mass percentage of the cooling agent composition is 0.1%, 0.5%, 1%, 2%, 2.5%, 3%, 3.5%, 4%, 4.5%, 5%, 5.5%, 6%, 7%, 8%, 9%, 10% or any range composed of any two of these values. Optionally, in the electronic atomization liquid, the mass percentage of the cooling agent composition is 2% - 6%.

[0041] In some embodiments, the solvent includes but is not limited to one or several of propylene glycol and glycerol.

[0042] In some of these embodiments, based on the mass percentage of the e - liquid being 100%, the e - liquid comprises 0.1% - 10% of a cooling flavor composition, 30% - 70% of propylene glycol, and 20% - 60% of glycerol.

[0043] In an alternative example, in the e - liquid, the mass percentage of propylene glycol can be, but is not limited to, 30%, 35%, 36%, 38%, 40%, 42%, 44%, 45%, 46%, 48%, 50%, 55%, 60%, 65%, 70%, or any range formed by any two of these values. Optionally, in the e - liquid, the mass percentage of propylene glycol is 35% - 50%.

[0044] In an alternative example, in the e - liquid, the mass percentage of glycerol can be, but is not limited to, 20%, 25%, 30%, 35%, 40%, 45%, 48%, 50%, 52%, 54%, 55%, 56%, 58%, 60%, or any range formed by any two of these values. Optionally, in the e - liquid, the mass percentage of glycerol is 48% - 60%.

[0045] In some of these embodiments, based on the mass percentage of the e - liquid being 100%, the e - liquid comprises 2% - 6% of a cooling flavor composition, 35% - 50% of propylene glycol, and 48% - 60% of glycerol.

[0046] In some embodiments, the e - liquid further comprises one or several of essence, sweetener, and nicotine salt.

[0047] Specifically, based on the mass percentage of the e - liquid being 100%, the mass percentage of essence is 0 - 30%, the mass percentage of sweetener is 0 - 8%, and the mass percentage of nicotine salt is 0 - 10%.

[0048] For example, in the e - liquid, the mass percentage of essence can be, but is not limited to, 0, 1%, 5%, 10%, 15%, 20%, 25%, 30%, or any range formed by any two of these values. In the e - liquid, the mass percentage of sweetener can be, but is not limited to, 0, 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, or any range formed by any two of these values. In the e - liquid, the mass percentage of nicotine salt can be, but is not limited to, 0, 1%, 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, or any range formed by any two of these values.

[0049] In an optional example, the essence includes one or more of, but is not limited to, strawberry essence, watermelon essence, lemon essence, peach essence, mango essence, papaya essence, orange essence, grape essence, litchi essence, pitaya essence, pomelo essence, apple essence, banana essence, and coconut essence.

[0050] In an optional example, the sweetener includes one or more of, but is not limited to, neotame, advantame, sucralose, acesulfame potassium, stevioside, glucosyl stevioside, and aspartame.

[0051] In an optional example, the nicotine salt can be a salt formed by nicotine and an organic acid, and the organic acid can be, but is not limited to, benzoic acid, tartaric acid, etc.

[0052] In some of these embodiments, taking the mass percentage of the e - liquid as 100%, the e - liquid includes 0.1% - 10% of the cooling agent composition, 30% - 70% of propylene glycol, 20% - 60% of glycerol, 0 - 30% of essence, 0 - 8% of sweetener, and 0 - 10% of nicotine salt. Further, taking the mass percentage of the e - liquid as 100%, the e - liquid includes 2% - 6% of the cooling agent composition, 35% - 50% of propylene glycol, 48% - 60% of glycerol, 0 - 30% of essence, 0 - 8% of sweetener, and 0 - 10% of nicotine salt.

[0053] The above - mentioned e - liquid can improve the richness and comfort of the cooling sensation area, thereby enhancing the user's experience of the e - cigarette.

[0054] In some embodiments, the preparation steps of the e - liquid include: stirring the cooling agent composition and the solvent evenly to obtain the e - liquid. The specific stirring steps are not particularly limited, as long as the components can be mixed evenly.

[0055] The third aspect of the present invention provides an e - atomization device, including the above - mentioned e - liquid.

[0056] Specifically, the above - mentioned e - liquid is filled into the e - atomization device for inhalation. Among them, the e - atomization device includes an atomization core. For example, the atomization core can be, but is not limited to, a ceramic heating core.

[0057] In order to make the purpose and advantages of the present invention clearer, the following further details the cooling agent composition of the present invention and its effects with specific embodiments. It should be understood that the specific embodiments described here are only used to explain the present invention and shall not be used to limit the present invention. Unless otherwise specified, the following embodiments do not include other components except inevitable impurities. The drugs and instruments used in the embodiments are all conventional selections in the art unless otherwise specified. The experimental methods without specific conditions in the embodiments are carried out according to conventional conditions, such as the conditions described in literature, books, or the methods recommended by the manufacturers.

[0058] Example 1

[0059] This example provides a cooling agent composition, by mass, including: 41 parts of WS-23, 5 parts of WS-27, and 4 parts of menthol, totaling 50 parts.

[0060] This example also provides an e-liquid. Based on the total mass percentage of the e-liquid being 100%, the e-liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0061] The preparation steps of the above e-liquid include: uniformly stirring the cooling agent composition, glycerol, and propylene glycol to prepare the e-liquid.

[0062] Example 2

[0063] This example provides a cooling agent composition, by mass, including: 30 parts of WS-23, 8 parts of WS-27, and 8 parts of menthol, totaling 46 parts.

[0064] This example also provides an e-liquid. Based on the total mass percentage of the e-liquid being 100%, the e-liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0065] The preparation steps of the above e-liquid include: uniformly stirring the cooling agent composition, glycerol, and propylene glycol to prepare the e-liquid.

[0066] Example 3

[0067] This example provides a cooling agent composition, by mass, including: 45 parts of WS-23, 2 parts of WS-27, and 2 parts of menthol, totaling 49 parts.

[0068] This example also provides an e-liquid. Based on the total mass percentage of the e-liquid being 100%, the e-liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0069] The preparation steps of the above e-liquid include: uniformly stirring the cooling agent composition, glycerol, and propylene glycol to prepare the e-liquid.

[0070] Example 4

[0071] This example provides a cooling agent composition, by mass, including: 35 parts of WS-23, 3 parts of WS-27, and 6 parts of menthol, totaling 44 parts.

[0072] This embodiment also provides an e - liquid. Based on the total mass percentage of the e - liquid being 100%, the e - liquid includes 3% of the above - mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0073] The preparation steps of the above - mentioned e - liquid include: stirring the cooling agent composition, glycerol, and propylene glycol evenly to obtain the e - liquid.

[0074] Example 5

[0075] This embodiment provides a cooling agent composition, by mass parts, including: 42 parts of WS - 23, 6 parts of WS - 27, and 3 parts of menthol, totaling 51 parts.

[0076] This embodiment also provides an e - liquid. Based on the total mass percentage of the e - liquid being 100%, the e - liquid includes 3% of the above - mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0077] The preparation steps of the above - mentioned e - liquid include: stirring the cooling agent composition, glycerol, and propylene glycol evenly to obtain the e - liquid.

[0078] Comparative Example 1

[0079] Comparative Example 1 provides a cooling agent composition, by mass parts, including: 30 parts of WS - 23, 8 parts of WS - 27, and 9 parts of menthol, totaling 47 parts.

[0080] Comparative Example 1 also provides an e - liquid. Based on the total mass percentage of the e - liquid being 100%, the e - liquid includes 3% of the above - mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0081] The preparation steps of the above - mentioned e - liquid include: stirring the cooling agent composition, glycerol, and propylene glycol evenly to obtain the e - liquid.

[0082] Comparative Example 2

[0083] Comparative Example 2 provides a cooling agent composition, by mass parts, including: 30 parts of WS - 23, 9 parts of WS - 27, and 8 parts of menthol, totaling 47 parts.

[0084] Comparative Example 2 also provides an e - liquid. Based on the total mass percentage of the e - liquid being 100%, the e - liquid includes 3% of the above - mentioned cooling agent composition, 40% of glycerol, and 57% of propylene glycol.

[0085] The preparation steps of the above - mentioned e - liquid include: stirring the cooling agent composition, glycerol, and propylene glycol evenly to obtain the e - liquid.

[0086] Comparative Example 3

[0087] Comparative Example 3 provides a cooling agent composition, which includes, by weight, 29 parts of WS-23, 8 parts of WS-27 and 8 parts of menthol, totaling 45 parts.

[0088] Comparative Example 3 also provides an electronic atomization liquid. Taking the total mass percentage of the electronic atomization liquid as 100%, the electronic atomization liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol and 57% of propylene glycol.

[0089] The preparation steps of the electronic atomization liquid include: uniformly stirring the cooling agent composition, glycerin and propylene glycol to prepare the electronic atomization liquid.

[0090] Comparative Example 4

[0091] Comparative Example 4 provides a cooling agent composition, which comprises, by weight, 45 parts of WS-23, 2 parts of WS-27 and 1 part of menthol, for a total of 48 parts.

[0092] Comparative Example 4 also provides an electronic atomization liquid. Taking the total mass percentage of the electronic atomization liquid as 100%, the electronic atomization liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol and 57% of propylene glycol.

[0093] The preparation steps of the electronic atomization liquid include: uniformly stirring the cooling agent composition, glycerin and propylene glycol to prepare the electronic atomization liquid.

[0094] Comparative Example 5

[0095] Comparative Example 5 provides a cooling agent composition, which includes, by weight, 45 parts of WS-23, 1 part of WS-27 and 2 parts of menthol, for a total of 48 parts.

[0096] Comparative Example 5 also provides an electronic atomization liquid. Taking the total mass percentage of the electronic atomization liquid as 100%, the electronic atomization liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol and 57% of propylene glycol.

[0097] The preparation steps of the electronic atomization liquid include: uniformly stirring the cooling agent composition, glycerin and propylene glycol to prepare the electronic atomization liquid.

[0098] Comparative Example 6

[0099] Comparative Example 6 provides a cooling agent composition, which includes, by weight, 46 parts of WS-23, 2 parts of WS-27 and 2 parts of menthol, for a total of 50 parts.

[0100] Comparative Example 6 also provides an electronic atomization liquid. Taking the total mass percentage of the electronic atomization liquid as 100%, the electronic atomization liquid includes 3% of the above-mentioned cooling agent composition, 40% of glycerol and 57% of propylene glycol.

[0101] The preparation steps of the above e-liquid include: uniformly stirring the cooling flavorant composition, glycerol and propylene glycol to obtain the e-liquid.

[0102] Comparative Example 7

[0103] Comparative Example 7 provides an e-liquid. Based on 100% of the total mass percentage of the e-liquid, the e-liquid includes 3% of cooling flavorant WS-23, 40% of glycerol, and 57% of propylene glycol.

[0104] The preparation steps of the above e-liquid include: uniformly stirring the cooling flavorant WS-23, glycerol and propylene glycol to obtain the e-liquid.

[0105] Comparative Example 8

[0106] Comparative Example 8 provides an e-liquid. Based on 100% of the total mass percentage of the e-liquid, the e-liquid includes 3% of cooling flavorant WS-27, 40% of glycerol, and 57% of propylene glycol.

[0107] The preparation steps of the above e-liquid include: uniformly stirring the cooling flavorant WS-27, glycerol and propylene glycol to obtain the e-liquid.

[0108] Comparative Example 9

[0109] Comparative Example 9 provides an e-liquid. Based on 100% of the total mass percentage of the e-liquid, the e-liquid includes 3% of cooling flavorant WS-3, 40% of glycerol, and 57% of propylene glycol.

[0110] The preparation steps of the above e-liquid include: uniformly stirring the cooling flavorant WS-3, glycerol and propylene glycol to obtain the e-liquid.

[0111] Comparative Example 10

[0112] Comparative Example 10 provides an e-liquid. Based on 100% of the total mass percentage of the e-liquid, the e-liquid includes 3% of cooling flavorant WS-5, 40% of glycerol, and 57% of propylene glycol.

[0113] The preparation steps of the above e-liquid include: uniformly stirring the cooling flavorant WS-5, glycerol and propylene glycol to obtain the e-liquid.

[0114] Comparative Example 11

[0115] Comparative Example 11 provides an e-liquid. Based on 100% of the total mass percentage of the e-liquid, the e-liquid includes 3% of cooling flavorant menthol, 40% of glycerol, and 57% of propylene glycol.

[0116] The preparation steps of the above-mentioned e-liquid include: stirring menthol (a cooling agent), glycerol, and propylene glycol evenly to obtain the e-liquid.

[0117] The proportion of the cooling agent composition in the e-liquids of the above-mentioned examples and comparative examples is shown in Table 1 below. The dosage unit of each component in Table 1 is parts by mass:

[0118] Table 1 Cooling agent compositions of each example and comparative example

[0119]

[0120] Load the e-liquids prepared in the above examples and comparative examples into the same atomizer and provide them to 30 professional sensory evaluators for blind sampling evaluation. According to the sensory indicators and grade standards, determine the sensory scores of the samples. Among them, the sensory indicators include the degree of coolness in the oral cavity, larynx (also called the laryngeal ventricle), lower larynx, and nasal cavity, as well as abnormal odors. The professional sensory evaluators score according to the intensity of the coolness they feel. 0 points means no coolness, and 5 points means extremely strong coolness. The specific coolness scoring indicators are shown in Table 2 below. For abnormal odors, 0 points means no abnormal odor, and 5 points means extremely strong abnormal odor. The specific abnormal odor scoring indicators are shown in Table 3 below.

[0121] Table 2 Scoring criteria for coolness intensity

[0122]

[0123] Table 3 Scoring criteria for the intensity of abnormal odors

[0124]

[0125] Thirty professional evaluators first study the evaluation results of various standard samples and use them as a reference to blindly sample the e-liquids of the examples and comparative examples. According to the sensory indicators and the intensity of coolness, determine the scores of each sensory indicator of the samples. Take the average score of the 30 professional sensory evaluators as the score of each sensory indicator. The specific results are shown in Table 4. In Table 4, the coolness richness is the average of the degrees of coolness in the oral cavity, larynx, lower larynx, and nasal cavity. Among them, when the coolness score of the lower larynx is greater than 1, the experience is not good. The effect is better when the score of the coolness richness is around 3. Being much higher than 3 will produce an overly cool effect, and being much lower than 3 will produce a less cool effect.

[0126] Table 4 Sensory scores of the e-liquids of each example and comparative example

[0127]

[0128] As can be seen from Table 4 above, compounding WS-23 with WS-27 and menthol to prepare a cooling agent and using it in the e-liquid can increase the intensity of coolness in the oral cavity and larynx and increase the richness of the coolness during the puffing of the e-cigarette.

[0129] As can be seen from the e-liquids of Example 1, Example 4 and Example 5, the coolness scores in the oral cavity, larynx and nasal cavity parts of their senses are not abnormally high or low, and the coolness comfort is better than that of the e-liquids of any comparative example.

[0130] As can be seen from the comparison between Comparative Example 1 to Comparative Example 2 and Example 2, in the cool flavor agent composition, the dosages of WS-23, WS-27 and menthol are not within the range, the sensory effect evaluation is not good, abnormal odors are prominent, and the coolness in the lower larynx is weak. As can be seen from the comparison between Comparative Example 3 and Example 2, the nasal cavity coolness of the cool flavor agent composition of Comparative Example 3 is significantly insufficient, and the coolness richness is poor.

[0131] As can be seen from the comparison between Example 3 and Comparative Example 4 to Comparative Example 6, in the flavor agent composition, the dosages of WS-23, WS-27 and menthol are not within the range, the sensory effect evaluation is not good, the coolness richness of the cool flavor agent composition of Comparative Example 4 is insufficient, the larynx coolness degree of the cool flavor agent composition of Comparative Example 5 is not enough, and the nasal cavity coolness degree of the cool flavor agent composition of Comparative Example 6 is too high.

[0132] The technical features of the above-described embodiments can be combined arbitrarily. For the sake of brevity of description, not all possible combinations of the technical features in the above embodiments are described. However, as long as there is no contradiction in the combination of these technical features, it should be considered to be within the scope described in this specification.

[0133] The above-described embodiments only represent several implementation manners of the present invention, which are convenient for understanding the technical solutions of the present invention specifically and in detail, but should not be construed as a limitation on the protection scope of the invention patent. It should be noted that for those of ordinary skill in the art, without departing from the concept of the present invention, several deformations and improvements can still be made, and these all belong to the protection scope of the present invention. It should be understood that the technical solutions obtained by those skilled in the art through logical analysis, reasoning or limited experiments based on the technical solutions provided by the present invention are all within the protection scope of the appended claims of the present invention. Therefore, the protection scope of the present invention patent should be subject to the content of the appended claims, and the specification can be used to explain the content of the claims.

Claims

1. A cooling agent composition, characterized in that, By mass parts, it includes: 30 parts to 45 parts of WS-23, 2 parts to 8 parts of WS-27, and 2 parts to 8 parts of menthol.

2. The cooling agent composition according to claim 1, characterized in that, By mass parts, it includes: 35 parts to 42 parts of WS-23, 3 parts to 6 parts of WS-27, and 3 parts to 6 parts of menthol.

3. The cooling agent composition according to claim 1 or 2, characterized in that, The mass ratio of the said WS-23 to the said WS-27 is (7 to 12):1; and / or, The mass ratio of the said WS-23 to the said menthol is (7 to 12):

1.

4. An electronic atomization liquid, characterized in that, It includes a solvent and the cooling flavor composition according to any one of claims 1 to 3.

5. The electronic atomization liquid according to claim 4, wherein The said solvent includes one or several of propylene glycol and glycerol.

6. The electronic atomization liquid according to claim 5, wherein, Based on the mass percentage of the e-liquid being 100%, the e-liquid includes 0.1% to 10% of the cooling flavor composition, 30% to 70% of propylene glycol, and 20% to 60% of glycerol.

7. The electronic atomization liquid according to claim 6, characterized in that, Based on the mass percentage of the e-liquid being 100%, the e-liquid includes 2% to 6% of the cooling flavor composition, 35% to 50% of propylene glycol, and 48% to 60% of glycerol.

8. The electronic atomization liquid according to any one of claims 4 to 7, characterized in that The said e-liquid further includes one or several of essence, sweetener, and nicotine salt.

9. The electronic atomization liquid according to claim 8, wherein, Based on the mass percentage of the e-liquid being 100%, the mass percentage of the essence is 0 to 30%, the mass percentage of the sweetener is 0 to 8%, and the mass percentage of the nicotine salt is 0 to 10%.

10. An electronic atomization device, characterized in that, It includes the e-liquid according to any one of claims 4 to 9.