Shampoo containing fruit extract and preparation method thereof
Through the scientific combination of a variety of fruit extracts, the shampoo composition formed solves the problem of single anti-detoxification, oil control and anti-dandruff effects, reduces the irritation of chemical additives on the scalp and improves the washing and care effect.
Patent Information
- Application Number
- CN202510596584.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-05-09
- Publication Date
- 2025-07-08
AI Technical Summary
The existing shampoo has single effects on anti-detoxification, oil control and anti-dandruff, and chemical additives are highly irritating to the scalp.
A variety of dry fruit extracts such as pomegranate peel, bergamot and coconut extracts are used to form a combination of conditioning agents, surfactants, preservatives, moisturizers and emulsifiers to reduce the use of chemical additives.
It has achieved a comprehensive improvement in the anti-detachment, oil control and anti-dandruff effects, while reducing the irritation to the scalp and improving the overall washing and care performance of shampoo.
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Abstract
Description
Technical Field
[0001] The present invention belongs to the technical field of daily-use cosmetics, and relates to a shampoo containing fruit extracts and a preparation method thereof. Background Art
[0002] Shampoo, also known as hair shampoo, hair conditioner or shampoo, its main function is to clean the hair and scalp, laying the foundation for hair styling. The purpose of shampooing is to remove the dust on the hair and scalp and wash away the excess oil. Traditional shampoos often rely on chemically synthesized ingredients (such as sulfate surfactants, silicone oil, etc.) to achieve functions such as cleaning and anti-dandruff, but long-term use may cause problems such as scalp irritation and dry hair. In recent years, natural plant extracts have attracted attention due to their high safety and mild efficacy, but single plant ingredients often have limited functions and are difficult to meet the complex requirements of anti-hair loss, oil control and anti-dandruff at the same time. In addition, the application of fruit extracts in shampoos mostly focuses on fragrance or basic moisturization, and the research on the interaction between their active ingredients (such as polyphenols, flavonoids, organic acids, etc.) is insufficient. Summary of the Invention
[0003] The present invention relates to a shampoo containing fruit extracts and a preparation method thereof, belonging to the technical field of daily-use cosmetics. The shampoo containing fruit extracts disclosed by the present invention comprises the following raw materials in parts by weight: 50-70 parts of water, 0.2-0.5 part of conditioner, 8-12 parts of fruit extracts, 10-16 parts of surfactant, 0.05-0.2 part of preservative, 1-4 parts of humectant, 0.1-0.3 part of emulsifier. The shampoo composition with various dried fruit extracts as the core ingredients exerts the synergistic effect of natural ingredients through scientific compatibility, solves the problem of single anti-hair loss, oil control and anti-dandruff effects in the prior art, and reduces the irritation of chemical additives to the scalp at the same time.
[0004] The object of the present invention can be achieved by the following technical solutions:
[0005] A shampoo containing fruit extracts, the shampoo comprises the following raw materials in parts by weight: 50-70 parts of water, 0.2-0.5 part of conditioner, 8-12 parts of fruit extracts, 10-16 parts of surfactant, 0.03-0.05 part of preservative, 1-4 parts of humectant, 0.1-0.3 part of emulsifier.
[0006] Further, the conditioner is composed of hydrolyzed sericin and polyquaternium-22 with a mass ratio of 1:1-2, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:1-2.
[0007] Further, the preservative is phenoxyethanol, the humectant is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
[0008] Further, the fruit extract is composed of pomegranate peel extract, bergamot extract and nata de coco extract with a mass ratio of 1:1 - 2:1.
[0009] Further, the preparation method of the pomegranate peel extract is as follows: Take the pomegranate peel, dry it, crush it into pomegranate peel powder with a particle size below 10 - 800 meshes, mix and stir it with distilled water, then heat for extraction. After solid - liquid separation, the liquid is evaporated and concentrated to obtain the pomegranate peel extract.
[0010] Further, the mass ratio of the pomegranate peel powder to distilled water is 1:15 - 20, the temperature and time of the heating extraction are 70°C - 85°C and 2 - 3h respectively, and the solid content of the pomegranate peel extract is 20 - 30%.
[0011] Further, the preparation method of the bergamot extract is as follows: Cut the bergamot into slices, soak it in an ethanol solution, and then take the soaking solution for evaporation and concentration to obtain the bergamot extract.
[0012] Further, the mass ratio of the bergamot to the ethanol solution is 1:5 - 6, where the mass fraction of the ethanol solution is 60 - 75%, the temperature and time of the soaking are 40 - 50°C and 4 - 6h respectively, and the solid content of the bergamot extract is 20 - 35%.
[0013] Further, the preparation method of the nata de coco extract is as follows: Dry the nata de coco and crush it into powder, add distilled water with a solid - liquid ratio of 1 - 5g:200 - 500mL to the powder, add Gluconacetobacter xylinus with a mass ratio of 1:0.01 - 0.03 to the powder and ferment at room temperature, then add a complex enzyme with a mass ratio of 1:0.02 - 0.05 to the powder for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:1 - 3. The temperature, time and pH of the enzymatic hydrolysis are 45 - 55°C, 12 - 24h and 4.5 - 5.5 respectively. After enzymatic hydrolysis, filter, and evaporate and concentrate the filtrate into a nata de coco extract with a solid content of 30 - 50%.
[0014] Further, the preparation method of the shampoo containing the fruit extract is as follows: Mix and stir all the raw materials except the preservative, and then add the preservative and stir to complete the whole process.
[0015] Advantages of the present invention:
[0016] The shampoo composition of the present invention with various dried - fruit extracts as the core components exerts the synergistic effect of natural components through scientific compatibility, solves the problem of single anti - hair - loss, oil - control and anti - dandruff effects in the prior art, and at the same time reduces the irritation of chemical additives to the scalp. Specific embodiments
[0017] To further elaborate on the technical means and effects adopted by the present invention to achieve the intended invention purpose, the following, in combination with embodiments, details the specific implementation manners, structures, features and their effects of the present invention as follows.
[0018] The hydrolyzed sericin protein involved in the present invention was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.; glyceryl cocoate was purchased from Hubei Xingyan New Materials Technology Co., Ltd., with the CAS number of 68201-46-7; fatty alcohol polyoxyethylene ether was purchased from Shanghai Yushicheng Chemical Technology Co., Ltd.; the preservation number of Gluconacetobacter xylinus is: CGMCC1.2706, purchased from Shanghai Preservation Biotechnology Center, and the active concentration of Gluconacetobacter xylinus is 3×10 8 CFU / g; cellulase and pectinase were purchased from Nanning Donghenghuadao Biotechnology Co., Ltd., and the enzyme activities of both are 10,000 U / G.
[0019] Example 1
[0020] A shampoo containing fruit extract, and the shampoo comprises the following raw materials in parts by weight: 50 parts of water, 0.2 part of conditioner, 8 parts of fruit extract, 10 parts of surfactant, 0.05 part of preservative, 1 part of moisturizer, and 0.1 part of emulsifier.
[0021] The conditioner is composed of hydrolyzed sericin protein and polyquaternium-22 with a mass ratio of 1:1, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:1.
[0022] The preservative is phenoxyethanol, the moisturizer is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
[0023] The fruit extract is composed of pomegranate peel extract, lemon extract and nata de coco extract with a mass ratio of 1:1:1.
[0024] The preparation method of the pomegranate peel extract is as follows: take the pomegranate peel, dry it, crush it into pomegranate peel powder with a particle size below 100 mesh, mix and stir it with distilled water, then heat and extract it, and after solid-liquid separation, evaporate and concentrate the liquid to obtain the pomegranate peel extract.
[0025] The mass ratio of the pomegranate peel powder to distilled water is 1:15, the temperature and time of the heating extraction are 70°C and 2 h respectively, and the solid content of the pomegranate peel extract is 20%.
[0026] The preparation method of the lemon extract is as follows: slice the lemon, soak it in an ethanol solution, and then take the soaking solution and evaporate and concentrate it to obtain the lemon extract.
[0027] The mass ratio of the lemon to the ethanol solution is 1:5, where the mass fraction of the ethanol solution is 60%. The temperature and time of the soaking are 40°C and 4 h respectively, and the solid content of the lemon extract is 20%.
[0028] The preparation method of the nata de coco extract is as follows: The nata de coco is dried and crushed into powder, distilled water with a solid-liquid ratio of 1 g:200 mL to the powder is added, and gluconacetobacter xylinus with a mass ratio of 1:0.01 to the powder is added and fermented at room temperature for 105 h, sterilized, and a complex enzyme with a mass ratio of 1:0.02 to the powder is added for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:1. The temperature, time and pH of the enzymatic hydrolysis are 45°C, 12 h and 4.5 respectively. After enzymatic hydrolysis, it is filtered, and the filtrate is evaporated and concentrated into a nata de coco extract with a solid content of 30%.
[0029] The preparation method of the shampoo containing fruit extract is as follows: All raw materials in parts by weight are mixed and stirred except for the preservative, and then the preservative is added and stirred to complete the whole process.
[0030] Example 2
[0031] A shampoo containing fruit extract, the shampoo comprises the following raw materials in parts by weight: 60 parts of water, 0.4 part of conditioner, 10 parts of fruit extract, 13 parts of surfactant, 0.1 part of preservative, 3 parts of moisturizer, 0.2 part of emulsifier.
[0032] The conditioner is composed of hydrolyzed sericin and polyquaternium-22 with a mass ratio of 1:1.5, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:1.5.
[0033] The preservative is phenoxyethanol, the moisturizer is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
[0034] The fruit extract is composed of pomegranate peel extract, lemon extract and nata de coco extract with a mass ratio of 1:1.5:1.
[0035] The preparation method of the pomegranate peel extract is as follows: The pomegranate peel is taken, dried, and crushed into pomegranate peel powder with a particle size below 100 meshes, mixed and stirred with distilled water, and then heated for extraction. After solid-liquid separation, the liquid is evaporated and concentrated to obtain the pomegranate peel extract.
[0036] The mass ratio of the pomegranate peel powder to the distilled water is 1:17, the temperature and time of the heating extraction are 77°C and 2.5 h respectively, and the solid content of the pomegranate peel extract is 25%.
[0037] The preparation method of the bergamot extract is as follows: slice the bergamot, soak it in an ethanol solution, and then take the soaking solution for evaporation and concentration to obtain the bergamot extract.
[0038] The mass ratio of the bergamot to the ethanol solution is 1:5.5, where the mass fraction of the ethanol solution is 70%, the soaking temperature and time are 45°C and 5 h respectively, and the solid content of the bergamot extract is 28%.
[0039] The preparation method of the nata de coco extract is as follows: dry the nata de coco and crush it into powder, add distilled water with a solid-liquid ratio of 3 g:350 mL to the powder, add Gluconacetobacter xylinus with a mass ratio of 1:0.02 to the powder and ferment at room temperature for 110 h, heat up to 60°C for sterilization, and after cooling to room temperature, add a complex enzyme with a mass ratio of 1:0.03 to the powder for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:2. The enzymatic hydrolysis temperature, time and pH are 50°C, 18 h and 5 respectively. After enzymatic hydrolysis, filter, and evaporate and concentrate the filtrate into a nata de coco extract with a solid content of 40%.
[0040] The preparation method of the shampoo containing fruit extract is as follows: mix and stir all the raw materials in parts by weight except the preservative, and then add the preservative and stir to complete the whole process.
[0041] Example 3
[0042] A shampoo containing fruit extract, the shampoo comprises the following raw materials in parts by weight: 70 parts of water, 0.5 part of conditioner, 12 parts of fruit extract, 16 parts of surfactant, 0.2 part of preservative, 4 parts of moisturizer, 0.3 part of emulsifier.
[0043] The conditioner is composed of hydrolyzed sericin and polyquaternium-22 with a mass ratio of 1:2, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:2.
[0044] The preservative is phenoxyethanol, the moisturizer is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
[0045] The fruit extract is composed of pomegranate peel extract, bergamot extract and nata de coco extract with a mass ratio of 1:2:1.
[0046] The preparation method of the pomegranate peel extract is as follows: take the pomegranate peel and dry it, crush it into pomegranate peel powder with a particle size less than 100 mesh, mix and stir it with distilled water, and then heat for extraction. After solid-liquid separation, the liquid is evaporated and concentrated to obtain the pomegranate peel extract.
[0047] The mass ratio of the pomegranate peel powder to distilled water is 1:20. The temperature and time for heating extraction are 85°C and 3 h respectively, and the solid content of the pomegranate peel extract is 30%.
[0048] The preparation method of the lemon extract is as follows: slice the lemon, soak it in an ethanol solution, and then evaporate and concentrate the soaking solution to obtain the lemon extract.
[0049] The mass ratio of the lemon to the ethanol solution is 1:6, where the mass fraction of the ethanol solution is 75%. The temperature and time for soaking are 50°C and 6 h respectively, and the solid content of the lemon extract is 35%.
[0050] The preparation method of the nata de coco extract is as follows: after drying the nata de coco, crush it into powder, add distilled water with a solid-liquid ratio of 5 g:500 mL to the powder, add Gluconacetobacter xylinus with a mass ratio of 1:0.03 to the powder, ferment at room temperature for 105 h, raise the temperature to 60°C for sterilization, and after cooling to room temperature, add a complex enzyme with a mass ratio of 1:0.05 to the powder for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:3. The temperature, time and pH for enzymatic hydrolysis are 55°C, 24 h and 5.5 respectively. After enzymatic hydrolysis, filter, and evaporate and concentrate the filtrate into a nata de coco extract with a solid content of 50%.
[0051] The preparation method of the shampoo containing fruit extract is as follows: mix and stir all the raw materials in parts by weight except the preservative, and then add the preservative and stir to complete the whole process.
[0052] Comparative Example 1
[0053] Based on Example 2, a shampoo containing fruit extract, the shampoo comprises the following raw materials in parts by weight: 60 parts of water, 0.4 part of conditioner, 10 parts of fruit extract, 13 parts of surfactant, 0.1 part of preservative, 3 parts of moisturizer, 0.2 part of emulsifier.
[0054] The conditioner is composed of hydrolyzed sericin and polyquaternium-22 with a mass ratio of 1:1.5, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:1.5.
[0055] The preservative is phenoxyethanol, the moisturizer is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
[0056] The fruit extract is composed of pomegranate peel extract, lemon extract and nata de coco extract with a mass ratio of 1:1.5:1.
[0057] The preparation method of the pomegranate peel extract is as follows: Take dried pomegranate peel, crush it into pomegranate peel powder with a mesh size of up to 100, mix and stir it with distilled water, then heat for extraction. After solid-liquid separation, the liquid is evaporated and concentrated to obtain the pomegranate peel extract.
[0058] The mass ratio of the pomegranate peel powder to distilled water is 1:17. The temperature and time of the heating extraction are 77°C and 2.5 h respectively. The solid content of the pomegranate peel extract is 25%.
[0059] The preparation method of the lemon extract is as follows: Slice the lemon, soak it in an ethanol solution, and then take the soaking solution for evaporation and concentration to obtain the lemon extract.
[0060] The mass ratio of the lemon to the ethanol solution is 1:5.5, where the mass fraction of the ethanol solution is 70%. The temperature and time of the soaking are 45°C and 5 h respectively. The solid content of the lemon extract is 28%.
[0061] The preparation method of the nata de coco extract is as follows: Dry the nata de coco and crush it into powder, add distilled water with a solid-liquid ratio of 3 g:350 mL to the powder, and then add a complex enzyme with a mass ratio of 1:0.03 to the powder for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:2. The temperature, time and pH of the enzymatic hydrolysis are 50°C, 18 h and 5 respectively. After enzymatic hydrolysis, filter, and evaporate and concentrate the filtrate into a nata de coco extract with a solid content of 40%.
[0062] The preparation method of the shampoo containing fruit extract is as follows: Mix and stir all the raw materials in parts by weight except the preservative, and then add the preservative and stir to complete the whole process.
[0063] Comparative Example 2
[0064] On the basis of Example 2, remove the pomegranate peel extract from the fruit extract and replace it with an equal mass of lemon extract, and other conditions are the same as those in Example 2.
[0065] Comparative Example 3
[0066] On the basis of Example 2, remove the lemon extract from the fruit extract and replace it with an equal mass of pomegranate peel extract, and other conditions are the same as those in Example 2.
[0067] Comparative Example 4
[0068] On the basis of Example 2, remove the nata de coco extract from the fruit extract and replace it with an equal mass of lemon extract, and other conditions are the same as those in Example 2.
[0069] Comparative Example 5
[0070] On the basis of Example 2, the cellulase in the preparation of coconut fruit extract was removed and replaced with an equal mass of pectinase, and other conditions were the same as those in Example 2.
[0071] Comparative Example 6
[0072] On the basis of Example 2, the pectinase in the preparation of coconut fruit extract was removed and replaced with an equal mass of cellulase, and other conditions were the same as those in Example 2.
[0073] Performance test
[0074] The shampoos containing fruit extracts prepared in Examples 1-3 and Comparative Examples 1-6 were used as samples; 900 testers aged between 18 and 60 years old were randomly divided into 9 groups, with 100 people in each group using the samples to wash their hair respectively. The usage amount for each test subject was 5-8 g each time. When using, gently knead the hair and scalp. The usage effect was evaluated after 1 month of use. The evaluation criteria for the usage effect refer to Table 1, and the evaluation results of the samples are shown in Tables 2-3;
[0075] Antibacterial test: The minimum inhibitory concentration of the antidandruff agent in the sample was detected according to the method in the "Disinfection Technical Specification" 2002 edition. The standard bacterium was Malassezia furfur, purchased from the Wuhan University Culture Collection Center. The test results are shown in Table 4.
[0076] Table 1: Evaluation criteria
[0077]
[0078] Table 2 Usage effect evaluation results
[0079]
[0080]
[0081] Table 3 Usage effect evaluation results
[0082]
[0083] Table 4: Minimum inhibitory concentration of Malassezia furfur
[0084]
[0085]
[0086] Note: The minimum inhibitory concentration refers to the lowest concentration that can inhibit the growth of bacteria, that is, the smaller the minimum inhibitory concentration, the better the antibacterial effect of the substance.
[0087] From the analysis of the evaluation results in Table 2-3, the evaluation grades of Examples 1-3 are all Grade I, and Grade III appears in Comparative Examples 2-4. In Comparative Example 1, Acetobacter xylinum was not used for fermentation, resulting in a reduction in the extraction of effective components in nata de coco, and thus the effect of the shampoo was also reduced; in Comparative Examples 2-4, one of the pomegranate peel extract, nata de coco extract and lemon extract was removed, and the anti-dandruff, repair and breathability of the shampoo were all poor. The effect was the best when the three extracts were used simultaneously. The interaction between phenols, flavonoids and acids in the three fruit extracts improved the washing and care effect of the shampoo; in Comparative Examples 5-6, a single enzyme was used, and the release of effective components in nata de coco decreased, thus affecting the washing and care performance of the shampoo. Combining the data analysis in Table 4, the minimum inhibitory concentration of Examples 1-3 is the smallest, and its antibacterial effect is better than that of Comparative Examples 1-6. Therefore, the washing and care of the scalp in the examples are cleaner and there will be no scalp itching.
[0088] The above are only the preferred embodiments of the present invention, and do not impose any form of limitation on the present invention. Although the present invention has been disclosed as above with the preferred embodiments, it is not intended to limit the present invention. Any person skilled in the art can make some changes or modifications to the equivalent embodiments with equivalent changes within the scope of the technical solution of the present invention. However, as long as it does not depart from the content of the technical solution of the present invention, any brief modifications, equivalent changes and modifications made to the above embodiments based on the technical essence of the present invention still fall within the scope of the technical solution of the present invention.
Claims
1. A shampoo containing fruit extract, characterized in that, The shampoo comprises the following raw materials in parts by weight: 50 - 70 parts of water, 0.2 - 0.5 part of conditioner, 8 - 12 parts of fruit extract, 10 - 16 parts of surfactant, 0.05 - 0.2 part of preservative, 1 - 4 parts of humectant, and 0.1 - 0.3 part of emulsifier.
2. The shampoo containing fruit extract according to claim 1, characterized in that, The conditioner is composed of hydrolyzed sericin and polyquaternium - 22 with a mass ratio of 1:1 - 2, and the surfactant is composed of sodium lauroyl sarcosinate and potassium cocoyl glycinate with a mass ratio of 1:1 - 2.
3. The shampoo containing fruit extract according to claim 1, characterized in that, The preservative is phenoxyethanol, the humectant is glyceryl cocoate, and the emulsifier is fatty alcohol polyoxyethylene ether.
4. The shampoo containing fruit extract according to claim 1, characterized in that, The fruit extract is composed of pomegranate peel extract, bergamot extract, and nata de coco extract with a mass ratio of 1:1 - 2:
1.
5. The shampoo containing fruit extract according to claim 4, characterized in that, The preparation method of the pomegranate peel extract is as follows: Take dried pomegranate peel, crush it into pomegranate peel powder with a mesh size below 10 - 800, mix and stir it with distilled water, then heat for extraction. After solid - liquid separation, the liquid is evaporated and concentrated to obtain pomegranate peel extract.
6. The shampoo containing fruit extract according to claim 5, characterized in that, The mass ratio of the pomegranate peel powder to distilled water is 1:15 - 20, the temperature and time of the heating extraction are 70℃ - 85℃ and 2 - 3h respectively, and the solid content of the pomegranate peel extract is 20 - 30%.
7. The shampoo containing fruit extract according to claim 4, characterized in that, The preparation method of the bergamot extract is as follows: Cut the bergamot into slices, soak it in an ethanol solution, and then take the soaking solution for evaporation and concentration to obtain bergamot extract.
8. The shampoo containing fruit extract according to claim 7, characterized in that, The mass ratio of the bergamot to the ethanol solution is 1:5 - 6, where the mass fraction of the ethanol solution is 60 - 75%, the temperature and time of the soaking are 40 - 50℃ and 4 - 6h respectively, and the solid content of the bergamot extract is 20 - 35%.
9. The shampoo containing fruit extract according to claim 4, wherein, The preparation method of the nata de coco extract is as follows: Dry the nata de coco and crush it into powder, add distilled water with a solid - liquid ratio of 1 - 5g:200 - 500mL to the powder, add gluconacetobacter xylinus with a mass ratio of 1:0.01 - 0.03 to the powder and ferment at room temperature, then add a complex enzyme with a mass ratio of 1:0.02 - 0.05 to the powder for enzymatic hydrolysis. The complex enzyme is composed of cellulase and pectinase with a mass ratio of 1:1 - 3. The temperature, time, and pH of the enzymatic hydrolysis are 45 - 55℃, 12 - 24h, and 4.5 - 5.5 respectively. After enzymatic hydrolysis, filter, and evaporate and concentrate the filtrate to obtain nata de coco extract with a solid content of 30 - 50%.
10. The shampoo containing fruit extract according to claim 1, characterized in that, The preparation method of the shampoo containing fruit extract solution is as follows: Mix and stir all components except the preservative, and then add the preservative and stir to complete the whole process.