Endurance sports nutritious food helpful for relieving physical fatigue
Sports nutrition foods prepared using bottom-spray fluidized bed coating technology and IBC mixers have solved the problems of β-alanine's hygroscopicity and clumping, achieving effective relief of physical fatigue and improving athletic performance and user experience.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- WEIHAI ZIGUANG FIG TECH CO LTD
- Filing Date
- 2024-10-28
- Publication Date
- 2026-04-28
AI Technical Summary
Existing sports nutrition foods lack effective verification in relieving physical fatigue, and products with high β-alanine content are prone to deliquescence and clumping, and have antagonistic effects with vitamins and minerals, affecting user experience.
β-alanine crystals were prepared using bottom-spray fluidized bed coating technology and combined with compound medicinal and edible powders, vitamins and minerals. The bottom-spray fluidized bed coating technology solved the problems of β-alanine's easy hygroscopicity, oxidation and agglomeration. An IBC mixer was used to ensure uniform mixing, thus preparing an endurance sports nutrition food.
It effectively relieves physical fatigue, improves athletic performance, prolongs the swimming time of mice under load, reduces serum urea nitrogen and blood lactate levels, increases liver glycogen reserves, and enhances user experience.
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Abstract
Description
Technical Field
[0001] This invention belongs to the field of sports nutrition foods, specifically relating to an endurance sports nutrition food that helps relieve physical fatigue. Background Technology
[0002] In daily training, the ultimate goal of pursuing higher, faster, and stronger athletic goals, or the targeted improvement of specific physical qualities for a particular sport, is to achieve better athletic performance. Promoting athletes' physical recovery as quickly as possible, enhancing their athletic ability, and improving training effectiveness are major issues for those working in the sports nutrition industry.
[0003] β-Alanine is a precursor to carnosine synthesis. Supplementing with β-alanine can significantly increase the carnosine content in muscles. Carnosine is the main active ingredient in the body, and increased carnosine levels in muscles can alleviate fatigue in competitive athletes. Caffeine has a similar structure to adenosine, a metabolite of adenosine triphosphate (ATP), and can competitively bind to receptors that induce fatigue and sleep signals, thus exerting its biological activity of promoting wakefulness and alleviating fatigue. Numerous interventional, observational, and clinical studies on healthy subjects, both domestically and internationally, have shown that moderate consumption of caffeinated beverages exhibits various benefits in improving alertness and attention, promoting endurance and strength, enhancing athletic performance, alleviating mental and physical fatigue, accelerating fat metabolism, and providing antioxidant effects. Ginseng can regulate multiple core genes, thereby modulating a series of signaling pathways such as TNF and IL-17, thus exerting an anti-fatigue effect. Polygonatum polysaccharide (PCP1), an extract of Polygonatum sibiricum, increases the reserves of energy substances (liver glycogen, muscle glycogen, ATP) in mice by regulating the uptake and metabolism of sugars and lipids, reducing the accumulation of metabolites (lactic acid, urea nitrogen), and decreasing the damage of metabolites to cells and organs. It also reduces MDA content, increases the enzyme activity of SOD and GSH-Px, inhibits oxidation processes, and alleviates fatigue caused by oxidative stress. Lycium barbarum polysaccharide, a major extract of Lycium barbarum, can increase muscle glycogen reserves and improve the phagocytic function of phagocytes, thereby enhancing the anti-hypoxia ability of mice. Zinc plays an important role in the normal function and anti-fatigue ability of skeletal muscle; magnesium supplementation can improve muscle metabolism and work efficiency; chromium's biological function is mainly manifested in its close relationship with insulin, and their combined effect can regulate glucose energy supply.
[0004] Currently, there are numerous sports nutrition products on the market that can alleviate physical fatigue, but these products lack further experimental verification of their efficacy in relieving physical fatigue. Moreover, high-β-alanine products on the market suffer from serious problems of deliquescence and clumping during their shelf life, and have antagonistic effects with other vitamins and minerals, which seriously affects the user experience.
[0005] This product, formulated using bottom spray coating technology and square cone hopper mixing technology, effectively solves the problems of β-alanine's hygroscopicity, oxidation, clumping, and antagonistic effects with other vitamins and minerals. Animal experiments have shown that it can alleviate physical fatigue in mice, providing important technical support for the vigorous development of sports and the health industry. Summary of the Invention
[0006] A sports nutrition composition for endurance that helps relieve physical fatigue, the composition comprising the following components: highly branched cyclodextrin, coated β-alanine crystal particles, compound medicinal and edible powders (ginseng, amla, wolfberry), beetroot powder, watermelon powder, compound vitamins (thiamine hydrochloride, riboflavin, pyridoxine hydrochloride, cyanocobalamin, niacin, folic acid, biotin, caffeine), compound minerals (magnesium gluconate, zinc gluconate, chromium chloride), and apple polyphenols;
[0007] Preferably, the raw materials of the composition, by weight, include the following components: 300-500g of highly branched cyclodextrin, 300-500g of coated β-alanine crystals, 350-550g of compound medicinal and edible powder, 150-200g of beetroot powder, 200-350g of watermelon powder, 10-30g of compound vitamins, 40-70g of compound minerals, and 30-50g of apple polyphenols.
[0008] Preferably, the compound medicinal and edible powder is prepared by compounding three medicinal and edible extracts in a certain mass ratio, with the following per kilogram addition: 80-130g ginseng extract, 40-65g Polygonatum extract, and 25-45g Lycium barbarum extract. Ginseng can regulate multiple core genes, thereby regulating a series of signaling pathways such as TNF and IL-17, thus exerting an anti-fatigue effect. Polygonatum polysaccharide (PCP1), an extract of Polygonatum, increases the reserves of energy substances (liver glycogen, muscle glycogen, ATP) in mice by regulating the uptake and metabolism of sugars and lipids, reducing the accumulation of metabolites (lactic acid, urea nitrogen), reducing the damage of metabolites to cells and organs, and simultaneously reducing the content of MDA, increasing the enzyme activity of SOD and GSH-Px, inhibiting the oxidation process, and alleviating fatigue caused by oxidative stress. Lycium barbarum polysaccharide is a major extract of Lycium barbarum, which can increase muscle glycogen reserves and improve the phagocytic function of phagocytes, thereby enhancing the anti-hypoxia ability of mice.
[0009] Preferably, the amount of compound minerals added per kilogram is: 200-500g magnesium gluconate, 3-8g zinc gluconate, and 0.2-0.5g chromium chloride. Zinc plays an important role in the normal function and anti-fatigue ability of skeletal muscle, magnesium supplementation can improve muscle metabolism and work efficiency, and the biological function of chromium is mainly manifested in its close relationship with insulin. Their combined effect can adjust the glucose energy supply status.
[0010] Preferably, the amount of compound vitamins added per kilogram is as follows: caffeine 0.01-1g, thiamine hydrochloride 0.02-0.03g, riboflavin 0.02-0.03g, pyridoxine hydrochloride 0.02-0.03g, cyanocobalamin 0.00004-0.00005g, niacin 0.1-0.15g, folic acid 0.001-0.002g, and biotin 0.0001-0.0003g.
[0011] The principle of the bottom-spray fluidized bed coating technology is as follows: Dry powders of drugs and excipients rise from the product collection chamber to the upper boiling expansion chamber under the action of a lower hot air flow. After mixing for a period of time, the spray nozzles in the boiling chamber begin to spray a binder solution counterclockwise. The powder that has absorbed the solution begins to agglomerate into small particles. As the binder is continuously added, the small particles slowly aggregate and form microspheres during the continuous "boiling" process. Due to the larger volume and density of the microspheres, they settle at the bottom of the small particles and powder. Therefore, the powder and small particles that have not yet formed into pellets have more opportunities to absorb the binder and aggregate until they are all pelletized. After stopping the spraying of the binder, the hot air flow rate and temperature are appropriately increased for fluidized drying. The bottom-spray device installs nozzles at the center of a distribution plate, allowing the material to circulate in an orderly manner. The atomized droplets enter the bed in the same direction as the fluidizing gas and come into close contact with the material, reducing atomized liquid loss and improving coating efficiency and quality. This effectively solves problems associated with β-alanine, such as its hygroscopicity, oxidation, agglomeration, and antagonistic effects with other vitamins and minerals. The preparation method employed involves bottom-spray fluidized bed coating technology, selecting fillers and coating materials in specific proportions and according to equipment parameters. The steps include the following:
[0012] (a) Wet granulation: β-alanine crystals are mixed with a filler, and a binder solution (e.g., water) is added to obtain a wet material. The mixing ratio of β-alanine crystal particles to filler ranges from 99:1 to 30:70 (weight to weight or volume to volume); and / or the ratio of the filler to the binder solution is from 1:1 to 1:1.5 (weight to weight or volume to volume). The stirring motor of the wet granulator rotates at a speed of 10–200 r / min, the shear head speed is 50–600 r / min, and / or the feed rate is 5–15 r / min.
[0013] (b) Extrusion: The wet material is extruded through an extruder to obtain strips of material with the same diameter. The screen aperture of the extruder is 0.25-0.85 mm, and the screw speed of the extruder is 100-300 r / min.
[0014] (c) Rounding: The obtained strip-shaped material is rounded at high speed by a rounding device to obtain small particles with the same size and the required roundness; the rotation speed of the rounding device is 400-1200 r / min, and / or the rounding time is 15s-10min.
[0015] (d) Coating: The air inlet velocity of the Wurster coating machine is 15-30 Hz, the coating temperature is 20-50 ℃, the feed rate of the coating liquid is 1-20 r / min, and / or the coating weight increases by 0.1%-80%; after coating, the material is dried for 15-25 min, and the moisture content of the final material is controlled to be less than 3.0%, thus obtaining coated β-alanine crystal particles.
[0016] The mixing equipment used is an IBC mixer, which utilizes mechanical force and gravity to uniformly mix two or more materials. This mixing method is widely used in various industrial production processes and daily life. Its parameters include: a loading coefficient of 30%–80% and a working speed of 3–15 r·min⁻¹. The mixed powder is then quantitatively filled and heat-sealed using a fully automatic drum food canning machine, controlling the filling amount to 150±1.5g / drum with a quantitative filling accuracy of over 99.9%, resulting in an endurance sports nutrition food that helps alleviate physical fatigue. Attached Figure Description
[0017] Figure 1 compared Compare serum urea nitrogen levels before and after exercise in each group, and the serum urea nitrogen (mmol / L) content between the positive control and the blank control.
[0018] Figure 2 The levels of liver glycogen (mg / g) were compared between positive and blank control mice after exercise.
[0019] Figure 3 The levels of blood lactate were compared between positive and blank control mice after exercise.
[0020] Figure 4 Compare the swimming time (s) of positive control and blank control mice under load. Detailed Implementation
[0021] The present invention will now be described in further detail with reference to practical examples, but the embodiments of the invention are not limited thereto. Unless otherwise specified, the reagents, methods, and equipment used in the present invention are conventional reagents, methods, and equipment in this technical field. Test methods in the following examples that do not specify specific experimental conditions are generally performed under conventional experimental conditions. Unless otherwise specified, the reagents and raw materials used in the present invention are all commercially available.
[0022] Example 1:
[0023] A method for preparing an endurance sports nutrition food composition that helps relieve physical fatigue:
[0024] Table 1 shows the component names and content ratios in Example 1.
[0025] Component Name Mass (kg) Quality percentage (%) β-alanine crystals 50 73.40% microcrystalline cellulose 4 5.88% resistant dextrin 4 5.88% Coating material 10 14.84%
[0026] The preparation method of these coated β-alanine crystal particles includes:
[0027] (1) Wet granulation: Take 50 kg of β-alanine crystals, mix with 4 kg of microcrystalline cellulose and 4 kg of resistant dextrin, add 8.4 kg of water to obtain wet material. The stirring motor speed of the wet granulator is 50 r / min, the speed of the shear head is 300 r / min, and the feed rate of the binder is 6 r / min.
[0028] (2) Extrusion: The wet material described in step (1) is extruded through an extruder with a sieve aperture of 0.4 mm to obtain strip-shaped materials of the same diameter. The screw speed of the extruder is 130 r / min.
[0029] (3) Rounding: The strip material obtained in step (2) is rounded at high speed through a rounding device to obtain small particles with the same size and the required roundness; the rotation speed of the rounding device is 700 r / min and the rounding time is 50 s.
[0030] (4) Drying: Dry the small particles obtained in step (3). The drying temperature is 45 degrees and the drying time is 30 minutes.
[0031] (5) Coating: The β-alanine crystal particles obtained in step (4) were coated with a coating material using a Wurster coating machine. The coating material was dissolved in water or ethanol with a solids content of 20%. The air inlet velocity of the Wurster coating machine was 19 Hz, the coating temperature was 40 °C, and the feed rate of the coating solution was 7 r / min. After coating, the particles were dried for 15 min to obtain coated β-alanine crystal particles.
[0032] The product mixing method includes: weighing out 32.0 kg of highly branched cyclodextrin, 31.0 kg of coated β-alanine crystals, 39.6 kg of compound medicinal and edible powder, 17.2 kg of beetroot powder, 21.0 kg of watermelon powder, 1.52 kg of compound vitamins, 4.73 kg of compound minerals, and 3.35 kg of apple polyphenols, totaling 150.0 kg; and adding all the above raw materials into the IBC mixer tank at a loading coefficient of 60% and a working speed of 12 r·min. -1 The mixed powder is quantitatively filled and heat-sealed using a fully automatic drum food filling machine, with the filling amount controlled at 150±1.5g / drum and the quantitative filling accuracy at over 99.9%, resulting in an endurance sports nutrition food that helps relieve physical fatigue.
[0033] Table 2 shows the comparative experiments on the stability of the products of the present invention in Example 1.
[0034]
[0035] Example 2:
[0036] A method for preparing an endurance sports nutrition food composition that helps relieve physical fatigue:
[0037] Table 3 shows the component names and content ratios in Example 2.
[0038]
[0039]
[0040] The preparation method of these coated β-alanine crystal particles includes:
[0041] (1) Wet granulation: Take 60kg of β-alanine crystals, mix with 3kg of microcrystalline cellulose and 4kg of β-cyclodextrin, add 7kg of water to obtain wet material. The stirring motor speed of the wet granulator is 45r / min, the speed of the shear head is 200r / min, and the feed rate of the binder is 5r / min.
[0042] (2) Extrusion: The wet material described in step (1) is extruded through an extruder with a sieve aperture of 0.8 mm to obtain strip-shaped materials of the same diameter. The screw speed of the extruder is 210 r / min.
[0043] (3) Rounding: The strip material obtained in step (2) is rounded at high speed through a rounding device to obtain small particles with the same size and the required roundness; the rotation speed of the rounding device is 500 r / min and the rounding time is 30 s.
[0044] (4) Drying: Dry the small particles obtained in step (3). The drying temperature is 35 degrees and the drying time is 40 minutes.
[0045] (5) Coating: The β-alanine crystal particles obtained in step (4) were coated with a coating material using a Wurster coating machine. The coating material was dissolved in water or ethanol with a solids content of 20%. The air inlet velocity of the Wurster coating machine was 25 Hz, the coating temperature was 38 °C, and the feed rate of the coating solution was 5 r / min. After coating, the particles were dried for 20 min to obtain coated β-alanine crystal particles.
[0046] The product mixing method includes: weighing out 40.0 kg of highly branched cyclodextrin, 40.0 kg of coated β-alanine crystals, 54.6 kg of compound medicinal and edible powder, 15.2 kg of beetroot powder, 25.0 kg of watermelon powder, 1.93 kg of compound vitamins, 5.45 kg of compound minerals, and 4.82 kg of apple polyphenols, totaling 187.0 kg; and adding all the above raw materials into the IBC mixer tank at a loading coefficient of 70% and a working speed of 9 r·min. -1The mixed powder is quantitatively filled and heat-sealed using a fully automatic drum food filling machine, with the filling amount controlled at 150±1.5g / drum and the quantitative filling accuracy at over 99.9%, resulting in an endurance sports nutrition food that helps relieve physical fatigue.
[0047] Table 4 shows the comparative experiments on the stability of the products of the present invention in Example 2.
[0048]
[0049] Test Example 1
[0050] An evaluation experiment on the effects of an endurance sports nutrition food that helps relieve physical fatigue (prepared in Example 1).
[0051] Materials Preparation: Dissolve 11-15 grams of the prepared endurance sports nutrition food in 200 ml of water for later use. Experimental animals used were male ICR mice weighing 18-20 g (Tables 5 and 6).
[0052] Observation indicators: mouse body weight, blood urea nitrogen, liver glycogen, blood lactate before and after exercise, and the time to swim to exhaustion with a load of 5% of the mouse body weight.
[0053] Statistical methods: All data are expressed as mean ± standard deviation. Statistical analysis was performed using SPSS 11.0. Analysis of variance was used for comparisons between groups. P < 0.05 was considered statistically significant. For data in the same group labeled with different letters, P ≤ 0.05; for data labeled with the same letter, P > 0.05.
[0054] Table 5. Effects of the present invention on weekly body weight of mice.
[0055]
[0056] Table 6 Test Grouping Information
[0057]
[0058] The effects of the endurance sports nutrition product described in this invention, which helps alleviate physical fatigue, on serum urea nitrogen levels in mice before and after exercise: After exercise, serum urea nitrogen levels in the blank control and positive control groups were significantly higher than before exercise, while there were no significant differences in the three dosage groups compared to before exercise. Comparing serum urea nitrogen levels after exercise, there was no significant difference between the positive control and blank control groups, while the three dosage groups were significantly lower than the two control groups. Figure 1) This invention demonstrates that the sports solid beverage described in this invention can promote amino acid utilization and / or prevent excessive protein breakdown caused by exercise.
[0059] The effects of the endurance sports nutrition food described in this invention, which helps alleviate physical fatigue, on liver glycogen: The liver glycogen levels in the positive control and all three experimental groups were significantly higher than those in the blank control; there were no significant differences between the three experimental groups and the positive control. Figure 2) .
[0060] The effect of the endurance sports nutrition food described in this invention, which helps alleviate physical fatigue, on blood lactate: This indicator was determined by calculating the area under the blood lactate curve at three time points: rest, immediately after exercise, and after weighted swimming. There was no significant difference in blood lactate levels between the positive control and the blank control group. The low-dose experimental group was significantly lower than the blank control group, while both the medium- and high-dose experimental groups were significantly lower than the blank control and the positive control group, respectively. Figure 3) .
[0061] The effect of the endurance sports nutrition food described in this invention, which helps relieve physical fatigue, on the weight-bearing swimming time of mice: the weight-bearing swimming time of mice in both the medium and high dose experimental groups was significantly longer than that of the blank control group, while there was no significant difference between the two control groups. Figure 4) .
[0062] Conclusion: The endurance sports nutrition food described in this invention, which helps relieve physical fatigue, can significantly prolong the swimming time of mice under load, and has the effects of enhancing endurance and delaying exercise fatigue. Its mechanism may be related to its reduction of serum urea nitrogen and blood lactate levels and increase of liver glycogen.
[0063] The above description of the disclosed embodiments enables those skilled in the art to make or use the invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the invention. Therefore, the invention is not to be limited to the embodiments shown herein, but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims
1. A sports nutrition food for endurance that helps relieve physical fatigue, characterized in that, The endurance sports nutrition food mentioned above is made from coated β-alanine crystal particles and highly branched cyclodextrin as the main raw materials, with the addition of 3 kinds of food and medicine homologous ingredients, 7 kinds of vitamins, 3 kinds of minerals, 4 kinds of natural plant ingredients and other ingredients. The β-alanine crystals are treated with bottom spray coating technology and mixed with square cone hopper technology. The components include highly branched cyclodextrin, coated β-alanine crystal particles, compound medicinal and edible powders (ginseng, amla, and wolfberry), beetroot powder, watermelon powder, compound vitamins (thiamine hydrochloride, riboflavin, pyridoxine hydrochloride, cyanocobalamin, niacin, folic acid, biotin, and caffeine), compound minerals (magnesium gluconate, zinc gluconate, and chromium chloride), and apple polyphenols. By measuring mouse body weight, blood urea nitrogen, liver glycogen, blood lactate, and the time required for mice to swim to exhaustion with a load of 5% of their body weight before and after exercise, it was demonstrated that this invention effectively helps to relieve physical fatigue and prolong exercise time. Furthermore, the coated β-alanine crystal particles have good anti-caking and anti-hygroscopic properties, significantly improving product stability.
2. A sports nutrition food for endurance that helps relieve physical fatigue, characterized in that, Added per kilogram: 300-500g of highly branched cyclodextrin, 300-500g of coated β-alanine crystals, 350-550g of compound medicinal and edible powder, 150-200g of beetroot powder, 200-350g of watermelon powder, 10-30g of compound vitamins, 40-70g of compound minerals, and 30-50g of apple polyphenols.
3. The endurance sports nutrition food that helps relieve physical fatigue according to claim 1, characterized in that: (a) The compound medicinal and edible powder is prepared by compounding three kinds of medicinal and edible powders in a certain mass ratio, with the following addition per kilogram: ginseng 80-130 g, wolfberry 40-65 g, and amla 25-45 g; (b) The compound mineral is prepared by compounding three kinds of mineral nutritional fortifiers in a certain mass ratio, with the following addition per kilogram: magnesium gluconate 200-500 g, zinc gluconate 3-8 g, and chromium chloride 0.2-0.5 g. (c) The compound vitamin is prepared by compounding seven vitamin fortifiers in a certain mass ratio, with the following amounts added per kilogram: caffeine 0.01-1g, thiamine hydrochloride 0.02-0.03g, riboflavin 0.02-0.03g, pyridoxine hydrochloride 0.02-0.03g, cyanocobalamin 0.00004-0.00005g, niacin 0.1-0.15g, folic acid 0.001-0.002g, and biotin 0.0001-0.0003g.
4. A sports nutrition food for endurance that helps relieve physical fatigue, characterized in that, The β-alanine crystal particles in claim 1 are coated and embedded by a Wurster bottom spray coating equipment, the process steps of which include (a) wet granulation, (b) extrusion, (c) spheronization, and (d) coating.
5. The wet granulation process described in claim 4 (a) comprises mixing β-alanine crystals with a filler and adding a binder solution (e.g., ethanol) to obtain a wet material, wherein the mixing ratio of β-alanine crystal particles to filler ranges from 99:1 to 30:70 (weight to weight or volume to volume); and / or the ratio of the filler to the binder solution is from 1:1 to 1:1.5 (weight to weight or volume to volume); (b) the extrusion process comprises extruding the wet material through an extruder to obtain strips of the same diameter. The wet granulator has a stirring motor speed of 10–200 r / min, a shear head speed of 50–600 r / min, and / or a feed rate of 5–15 r / min. The screen plate aperture of the extruder is 0.25-0.85 mm, and the screw speed of the extruder is 100-300 r / min; (c) the rounding process includes, the obtained strip material is rounded at high speed by a rounding device to obtain small particles with the same size and the required roundness; the rotation speed of the rounding device is 400-1200 r / min, and / or the rounding time is 15 s-10 min; (d) the coating process includes, the air inlet speed of the Wurster coating machine is 15-30 Hz, the coating temperature is 20-50 ℃, the feed rate of the coating liquid is 1-20 r / min, and / or the coating weight increases by 0.1%-80%; after the coating is completed and dried for 15-25 min, the moisture content of the final material is controlled to be less than 5.0%, and coated β-alanine crystal particles are obtained.
6. The coated β-alanine crystal particles as described in claim 4 are made from the following raw materials: 55.00% to 95.00% by mass of the β-alanine crystals, 1.00% to 35.00% by mass of the filler, and 0.70% to 40% by mass of the coating material.
7. The coated β-alanine crystal particles as described in claim 4, characterized in that, (a) The filler comprises microcrystalline cellulose, sodium octenyl succinate starch, pregelatinized starch, sodium carboxymethyl cellulose, sodium carboxymethyl starch, cross-linked sodium carboxymethyl starch, resistant dextrin, methyl cellulose, hydroxypropyl methyl cellulose, hydroxyethyl cellulose, β-cyclodextrin, or mixtures thereof; (b) The coating material comprises hydroxypropyl methyl cellulose, carrageenan, xanthan gum, gum arabic, modified starch, polyvinyl alcohol, titanium dioxide, silicon dioxide, triacetin, calcium silicate, or mixtures thereof; (c) The particle size of the coated β-alanine crystal particles is 20 to 60 mesh, and the effective content of β-alanine in the coated β-alanine crystal particles is adjustable, up to a maximum of 99.00%.
8. The method according to any one of claims 4 to 7, characterized in that, The coated β-alanine crystal particles prepared by the method effectively prevent β-alanine crystals from absorbing moisture from the environment, prevent self-polymerization, improve storage stability, prevent the deliquescence problem of β-alanine, and extend shelf life; they also improve the flowability of β-alanine, making it easier to process and package.
9. The mixing equipment used is an IBC mixer, and its parameters include: With a loading coefficient of 30% to 80% and a working speed of 3 to 15 r·min-1, the mixed powder is quantitatively filled and heat-sealed by a fully automatic barrel food canning machine, controlling the filling amount to 150±1.5 g / barrel, and the quantitative filling accuracy to be above 99.9%, resulting in an endurance sports nutrition food that helps relieve physical fatigue.