A method for preparing micro-nano silicon phase Al-50Si alloy based on multi-level high-speed ball milling and spark plasma sintering

By employing multi-stage high-speed ball milling and spark plasma sintering processes, the problems of silicon phase coarsening and non-dense microstructure in Al-50Si alloys were solved, enabling the preparation of high-performance alloys, simplifying the process flow and reducing costs.

CN122406013APending Publication Date: 2026-07-17

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Filing Date
2026-05-25
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Traditional processes for preparing Al-50Si alloys result in coarsening of the silicon phase, non-dense microstructure, and deterioration of performance. Furthermore, the processes are complex, costly, and difficult to achieve uniform and precise control of the silicon phase size.

Method used

A multi-stage high-speed ball milling and spark plasma sintering method was adopted to prepare micro-nano silicon powder by graded ball milling with high-energy WC balls and medium-energy steel balls, and combined with a segmented temperature and pressure controlled spark plasma sintering process to prepare a dense Al-50Si alloy with excellent performance.

Benefits of technology

It achieves precise control of silicon phase size, has a uniform internal structure, excellent mechanical and thermal conductivity, reduces raw material costs and preparation complexity, and is suitable for large-scale production.

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Abstract

本发明公开的一种基于多层级高速球磨与放电等离子烧结的微纳米硅相Al‑50Si合金制备方法,以铝粉和硅块为原料,先通过高能量WC球破碎硅块制备微米级硅粉,再通过中能量钢球分散破碎制备微纳米级硅粉,经酸洗纯化后与铝粉通过低能量氧化锆球混合球磨得到复合粉末,最终通过分段控温控压的放电等离子烧结工艺制得Al‑50Si合金。本发明通过多层级分级球磨从原料端实现硅相尺寸的精准调控,配合优化的放电等离子烧结工艺,有效解决了传统工艺中Al‑50Si合金硅相粗化、组织不致密、性能劣化的问题。
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