Efficient reaction kettle for pharmaceutical raw material medicine

By introducing a reflux rotating mechanism and cyclone effect into the reactor, combined with heating and ultrasonic vibration, the problem of uneven stirring is solved, uniform mixing and reaction stability of the drug is achieved, and the quality of the drug is improved.

CN222219565UActive Publication Date: 2024-12-24GUANGDONG JIUMING PHARMA
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Patent Information

Application Number
CN202420865501.5
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-24
Publication Date
2024-12-24
Estimated Expiration
2034-04-24

AI Technical Summary

Technical Problem

There is a problem of uneven stirring during the stirring of the existing reactors, which leads to insufficient mixing of drugs and reduces the quality and effect of drugs.

Method used

A high-efficiency reactor including a reactor body, a driving motor, a stirring rack and a reflux rotating mechanism is designed. The bottom material is pumped into the diverting ring tube through a liquid extraction pump, and a cyclone and vortex chamber are used to form a cyclone effect, combined with a heating tube and ultrasonic vibration plate assembly to achieve uniform mixing and heating of materials.

Benefits of technology

The agitation and mixing efficiency of the drug is improved, the uniform distribution of materials in the reactor is ensured, local concentration unevenness is avoided, and the uniformity and stability of the reaction are enhanced.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses an efficient reaction kettle for pharmaceutical raw material medicine, which comprises a reaction kettle body, a driving motor, a stirring frame and a backflow rotating mechanism, and the backflow rotating mechanism comprises an infusion pump, a first backflow pipe, a second backflow pipe, a shunting ring pipe and a rotational flow body. The stirring frame can mix and stir materials, the infusion pump can pump the materials at the inner bottom of the reaction kettle body into the shunting ring pipe, then the materials are shunted and sprayed out into the vortex chamber through the liquid outlet pipe, and a vortex effect can be formed by utilizing the conical umbrella and the vortex channel at the bottom of the vortex body, so that the stirring and mixing efficiency of the materials is improved, and the stirring effect is improved. Moreover, the materials can be more uniformly distributed in the reaction kettle due to the rotational flow effect, so that the situation that the local concentration is too high or too low is avoided, and the uniformity and stability of the reaction are ensured; materials at the bottom are pumped to the top through the infusion pump, so that convection and mixing efficiency of the materials can be promoted, and the mixing effect is improved.
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Description

Technical Field

[0001] The utility model relates to the field of reaction kettles, in particular to a high-efficiency reaction kettle for pharmaceutical raw materials. Background Art

[0002] Reactor is one of the essential main equipment for manufacturing pharmaceutical intermediates. Reactor is a container that provides a place for materials to react. The required materials are placed in the reactor, and the materials react in the reactor to obtain the required target product.

[0003] In the prior art, during the pharmaceutical stirring process of material medicines, many materials will sink to the bottom of the kettle. Since the length of the stirring shaft is limited and cannot reach the bottom of the kettle, common stirring kettles have uneven stirring, which makes it impossible to effectively and fully mix the drugs, thereby reducing the quality and effect of the drugs.

[0004] Therefore, the prior art has defects and needs to be improved. Utility Model Content

[0005] The technical problem to be solved by the utility model is to provide a high-efficiency reaction kettle for pharmaceutical raw materials which can stir evenly and fully mix medicines.

[0006] To achieve this purpose, the utility model adopts the following technical solutions: a high-efficiency reactor for pharmaceutical raw materials, including a reactor body, a driving motor, a stirring frame and a reflux rotating mechanism;

[0007] The reactor body has a containing chamber, the containing chamber is used to contain pharmaceutical materials, the stirring frame is arranged in the containing chamber, the driving motor is arranged on the top of the reactor body, and the output shaft of the driving motor is connected to the stirring frame through a connecting shaft;

[0008] The reflux rotating mechanism comprises a liquid pump, a first reflux pipe, a second reflux pipe, a flow dividing ring pipe and a vortex body, the liquid pump is mounted on the outside of the reactor body, the first reflux pipe is passed through the bottom of the reactor body and connected to the liquid inlet end of the liquid pump;

[0009] The cyclone body is arranged on the connecting shaft above the stirring frame, the flow dividing ring pipe is arranged above the cyclone body, and is connected to the liquid outlet end of the liquid pump through the second reflux pipe;

[0010] The liquid pump is used to pump the material at the bottom of the accommodating chamber into the diverter annular pipe through the first reflux pipe; the diverter annular pipe is provided with a plurality of liquid outlet pipes along the circumferential direction, and a plurality of vortex chambers are provided at the top of the cyclone body along the circumferential direction, and the liquid outlet of the liquid outlet pipe faces the vortex chamber, and the liquid outlet pipe is used to divert and spray the material in the second reflux pipe into the vortex chamber;

[0011] A conical umbrella is provided at the bottom of the cyclone body, and a plurality of cyclone channels are provided on the conical umbrella along the circumferential direction. A guide hole is provided in the vortex chamber, and the guide hole is used to guide the material into the cyclone channel. The cyclone channel is used to apply centrifugal force to the material as the connecting shaft rotates.

[0012] By adopting the above technical solution, the pharmaceutical raw material high-efficiency reactor further includes a heating tube, which is arranged at the bottom of the reactor body and is used to heat the material in the accommodating chamber.

[0013] By adopting the above-mentioned technical solutions, the pharmaceutical raw material medicinal high-efficiency reactor also includes an ultrasonic vibration plate assembly;

[0014] An embedding groove is provided on the side wall of the reactor body, and the ultrasonic vibration plate assembly is arranged in the embedding groove. The ultrasonic vibration plate assembly is used to generate high-frequency vibration for the material in the accommodating chamber.

[0015] By adopting the above-mentioned technical solutions, in the pharmaceutical raw material high-efficiency reactor, the cyclone channel is gradually expanded from the inside to the outside.

[0016] By adopting the above-mentioned technical solutions, in the pharmaceutical raw material high-efficiency reactor, a liquid guide tube is provided at the bottom of the reactor body, and an electric valve is provided on the liquid guide tube, and the electric valve is used to control the conduction or cutoff of the liquid guide tube.

[0017] By adopting the above-mentioned technical solutions, the pharmaceutical raw material medicinal high-efficiency reactor also includes a temperature sensor;

[0018] The temperature sensor is arranged on the inner wall of the reactor body, the temperature sensor is electrically connected to the heating tube, and the temperature sensor is used to detect the temperature of the material in the accommodating chamber.

[0019] By adopting the above-mentioned technical solutions, in the pharmaceutical raw material high-efficiency reactor, a liquid inlet pipe is provided on the top of the reactor body, and the liquid inlet pipe is used to introduce the material into the accommodating chamber.

[0020] By adopting the above-mentioned technical solutions, the pharmaceutical raw material high-efficiency reactor further includes a support frame, which is connected to the reactor body to support the reactor body.

[0021] Compared with the prior art, the utility model has the following beneficial effects:

[0022] The reactor body of the utility model contains materials for pharmaceutical preparation, the stirring frame can mix and stir the materials, the liquid pump can pump the materials at the bottom of the reactor body into the diversion ring pipe, and then the materials are diverted and sprayed into the vortex chamber through the liquid outlet pipe. The conical umbrella and the vortex channel at the bottom of the vortex body can form a vortex effect, thereby increasing the stirring and mixing efficiency of the materials. In addition, the vortex effect can make the materials more evenly distributed in the reactor, avoid the situation where the local concentration is too high or too low, and ensure the uniformity and stability of the reaction; the materials at the bottom are pumped to the top by the liquid pump, which can promote the convection and mixing efficiency of the materials and improve the mixing effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] In order to more clearly illustrate the embodiments of the utility model or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative labor.

[0024] The structures, proportions, sizes, etc. illustrated in the drawings of this specification are only used to match the contents disclosed in the specification so as to facilitate understanding and reading by persons familiar with this technology. They are not used to limit the conditions under which the present invention can be implemented, and therefore have no substantive technical significance. Any structural modification, change in proportion or adjustment of size, without affecting the effects and purposes that can be achieved by the present invention, should still fall within the scope of the technical contents disclosed by the present invention.

[0025] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0026] Figure 2 This is a schematic diagram of the structure of the reflux rotating mechanism of the utility model;

[0027] Figure 3 This is a schematic diagram of the bottom structure of the utility model;

[0028] Figure 4 This is a schematic diagram of the cyclone structure of the utility model;

[0029] Figure 5 This is a schematic structural diagram of the cyclone fluid of the utility model from another perspective;

[0030] Figure 6 This is a schematic diagram of the structure of the ultrasonic vibration plate assembly of the utility model. DETAILED DESCRIPTION

[0031] In order to make the utility model's purpose, features, and advantages more obvious and easy to understand, the following will be combined with the drawings in the utility model embodiments to clearly and completely describe the technical solutions in the utility model embodiments. Obviously, the embodiments described below are only part of the utility model embodiments, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0032] In the description of the present invention, it should be understood that the terms "upper", "lower", "top", "bottom", "inside", "outside", etc., indicating the orientation or positional relationship, are based on the orientation or positional relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention. It should be noted that when a component is considered to be "connected" to another component, it may be directly connected to the other component or there may be a centrally arranged component at the same time.

[0033] The technical solution of the utility model is further explained below with reference to the accompanying drawings and through specific implementation methods.

[0034] like Figures 1 to 6 As shown, the embodiment of the utility model provides a high-efficiency reactor for pharmaceutical raw materials, including a reactor body 1, a driving motor 2, a stirring frame 3 and a reflux rotating mechanism 4;

[0035] The reactor body 1 has a containing chamber, which is used to contain pharmaceutical materials. The stirring frame 3 is arranged in the containing chamber, and the driving motor 2 is arranged on the top of the reactor body 1. The output shaft of the driving motor 2 is connected to the stirring frame 3 through the connecting shaft 21; the stirring frame 3 can play a role in mixing and stirring the materials in the reactor body 1. Specifically, the stirring frame 3 is connected to the driving motor 2 through the connecting shaft 21. When the driving motor 2 is started, it will drive the connecting shaft 21 to rotate, and then the stirring frame 3 will rotate in the containing chamber, so as to mix the materials evenly, ensure that the various raw materials of the materials can fully contact and react during the reaction process, and improve the reaction efficiency.

[0036] like Figure 1 and Figure 2As shown, the reflux rotating mechanism 4 includes a liquid pump 41, a first reflux pipe 42, a second reflux pipe 43, a flow splitting ring pipe 44 and a cyclone 45. The liquid pump 41 is mounted on the outside of the reactor body 1, the first reflux pipe 42 is passed through the bottom of the reactor body 1, and is connected to the liquid inlet end of the liquid pump 41; the cyclone 45 is arranged on the connecting shaft 21 above the stirring frame 3, the flow splitting ring pipe 44 is arranged above the cyclone 45, and is connected to the liquid outlet end of the liquid pump 41 through the second reflux pipe 43;

[0037] The liquid pump 41 is used to pump the material at the bottom of the accommodating chamber into the diverter annular pipe 44 through the first reflux pipe 42; the diverter annular pipe 44 is provided with a plurality of liquid outlet pipes 441 along the circumferential direction, and a plurality of vortex chambers 451 are provided at the top of the cyclone body 45 along the circumferential direction, and the liquid outlet of the liquid outlet pipe 441 faces the vortex chamber 451, and the liquid outlet pipe 441 is used to divert and spray the material in the second reflux pipe 43 into the vortex chamber 451; the material at the bottom of the reactor body 1 is difficult to be stirred by the stirring frame 3, which will cause sedimentation and uneven mixing of the raw materials. By pumping the material at the bottom to the top, convection and mixing efficiency can be promoted, and the mixing effect can be improved.

[0038] like Figure 4 and Figure 5 As shown, a conical umbrella 452 is provided at the bottom of the cyclone body 45, and a plurality of cyclone channels 453 are provided in the circumferential direction of the conical umbrella 452. A guide hole 454 is provided in the vortex chamber 451, and the guide hole 454 is used to guide the material into the cyclone channel 453. The cyclone channel 453 is used to apply centrifugal force to the material as the connecting shaft 21 rotates. The material at the bottom of the reactor body 1 is pumped into the diversion ring pipe 44 by the liquid pump 41, and then the material is diverted and sprayed into the vortex chamber 451 through the liquid outlet pipe 441. The conical umbrella 452 and the cyclone channel 453 at the bottom of the cyclone body 45 can form a cyclone effect on the material, thereby increasing the stirring and mixing efficiency of the material. In addition, the cyclone effect can make the material more evenly distributed in the reactor, avoiding the situation of excessively high or low local concentration, and ensuring the uniformity and stability of the reaction.

[0039] like Figure 1 and Figure 3 As shown, further, a heating tube 5 is included, and the heating tube 5 is arranged at the bottom of the reactor body 1, and the heating tube 5 is used to heat the material in the accommodating chamber. By heating the material through the heating tube 5, the material in the reactor can reach the required reaction temperature, promote the reaction rate, and accelerate the reaction process.

[0040] like Figure 1 and Figure 6As shown, further, an ultrasonic vibration plate assembly 6 is included. An embedding groove is provided on the side wall of the reactor body 1. The ultrasonic vibration plate assembly 6 is arranged in the embedding groove. The ultrasonic vibration plate assembly 6 is used to generate high-frequency vibration for the material in the accommodating chamber. Ultrasonic vibration can generate tiny bubbles and micro-flows in the material, thereby increasing the disturbance and mixing efficiency inside the material, so as to fully mix the raw materials of different components and promote the contact and reaction rate between the reaction substances.

[0041] like Figure 4 and Figure 5 As shown, further, the swirl channel 453 is gradually expanded from the inside to the outside. Such a configuration can reduce the flow resistance of the liquid in the channel, reduce the pressure loss of the liquid when flowing through the channel, increase the flow speed of the liquid in the channel, and improve the mixing efficiency and mass transfer rate.

[0042] like Figure 1 and Figure 3 As shown, further, a liquid conduit 11 is provided at the bottom of the reactor body 1, and an electric valve 12 is provided on the liquid conduit 11, and the electric valve 12 is used to control the conduction or cutoff of the liquid conduit 11. Through the electric valve 12, the operator can control the conduction or cutoff of the liquid conduit 11 at the bottom of the reactor body 1, thereby controlling the discharge of materials.

[0043] Furthermore, a temperature sensor (not shown) is included, which is arranged on the inner wall of the reactor body 1, and is electrically connected to the heating tube 5, and is used to detect the temperature of the material in the accommodating chamber. The temperature sensor can monitor the temperature of the reaction material in real time, and adjust the heating power of the heating tube 5 according to the actual situation, so as to accurately control the temperature inside the reactor body 1 and ensure that the reaction is carried out within a suitable temperature range.

[0044] like Figure 1 As shown, further, a liquid inlet pipe 13 is provided on the top of the reactor body 1, and the liquid inlet pipe 13 is used to introduce materials into the accommodating chamber. The setting of the liquid inlet pipe 13 can facilitate the real-time addition of supplementary raw materials to the reactor body 1 during the mixing reaction process.

[0045] like Figure 1 As shown, further, a support frame 14 is included, and the support frame 14 is connected to the reactor body 1 to support the reactor body 1. The setting of the support frame 14 can improve the support stability of the reactor body 1 and prevent the heating pipe 5 from contacting the ground.

[0046] The reactor body 1 of the utility model contains materials for pharmaceutical preparation, the stirring frame 3 can mix and stir the materials, the liquid pump 41 can pump the materials at the bottom of the reactor body 1 into the diversion ring pipe 44, and then the materials are diverted and sprayed into the vortex chamber 451 through the liquid outlet pipe 441. The conical umbrella 452 and the vortex channel 453 at the bottom of the vortex body 45 can form a vortex effect, thereby increasing the stirring and mixing efficiency of the materials, and the vortex effect can make the materials more evenly distributed in the reactor, avoid the situation where the local concentration is too high or too low, and ensure the uniformity and stability of the reaction; the material at the bottom is pumped to the top by the liquid pump 41, which can promote the convection and mixing efficiency of the materials and improve the mixing effect.

[0047] As described above, the above embodiments are only used to illustrate the technical solutions of the utility model, rather than to limit it. Although the utility model has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that the technical solutions described in the aforementioned embodiments can still be modified, or some of the technical features can be replaced by equivalents. However, these modifications or replacements do not deviate the essence of the corresponding technical solutions from the spirit and scope of the technical solutions of the various embodiments of the utility model.

Claims

1. A high-efficiency reactor for pharmaceutical raw materials, characterized in that: It includes a reactor body, a driving motor, a stirring frame and a reflux rotating mechanism; The reactor body has a containing chamber, the containing chamber is used to contain pharmaceutical materials, the stirring frame is arranged in the containing chamber, the driving motor is arranged on the top of the reactor body, and the output shaft of the driving motor is connected to the stirring frame through a connecting shaft; The reflux rotating mechanism comprises a liquid pump, a first reflux pipe, a second reflux pipe, a flow dividing ring pipe and a vortex body, the liquid pump is mounted on the outside of the reactor body, the first reflux pipe is passed through the bottom of the reactor body and connected to the liquid inlet end of the liquid pump; The cyclone body is arranged on the connecting shaft above the stirring frame, the flow dividing ring pipe is arranged above the cyclone body, and is connected to the liquid outlet end of the liquid pump through the second reflux pipe; The liquid pump is used to pump the material at the bottom of the accommodating chamber into the diverter annular pipe through the first reflux pipe; the diverter annular pipe is provided with a plurality of liquid outlet pipes along the circumferential direction, and a plurality of vortex chambers are provided at the top of the cyclone body along the circumferential direction, and the liquid outlet of the liquid outlet pipe faces the vortex chamber, and the liquid outlet pipe is used to divert and spray the material in the second reflux pipe into the vortex chamber; A conical umbrella is provided at the bottom of the cyclone body, and a plurality of cyclone channels are provided on the conical umbrella along the circumferential direction. A guide hole is provided in the vortex chamber, and the guide hole is used to guide the material into the cyclone channel. The cyclone channel is used to apply centrifugal force to the material as the connecting shaft rotates.

2. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: It also includes a heating tube, which is arranged at the bottom of the reactor body and is used to heat the material in the accommodating chamber.

3. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: Also included is an ultrasonic vibration plate assembly; An embedding groove is provided on the side wall of the reactor body, and the ultrasonic vibration plate assembly is arranged in the embedding groove. The ultrasonic vibration plate assembly is used to generate high-frequency vibration for the material in the accommodating chamber.

4. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: The swirl channel is arranged to expand gradually from the inside to the outside.

5. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: A liquid guide tube is provided at the bottom of the reactor body, and an electric valve is provided on the liquid guide tube. The electric valve is used to control the conduction or cutoff of the liquid guide tube.

6. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 2, characterized in that: Also includes a temperature sensor; The temperature sensor is arranged on the inner wall of the reactor body, the temperature sensor is electrically connected to the heating tube, and the temperature sensor is used to detect the temperature of the material in the accommodating chamber.

7. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: A liquid inlet pipe is provided on the top of the reactor body, and the liquid inlet pipe is used to introduce materials into the accommodating chamber.

8. The pharmaceutical raw material medicinal high-efficiency reactor according to claim 1, characterized in that: A support frame is also included, and the support frame is connected to the reactor body to support the reactor body.

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