Precipitation reaction tank for wet extraction of lepidolite ore

By designing a precipitation reaction tank for wet extraction of lithium mica ore, and using the combined structure of an electric push rod and a stirring device, the problem of lithium mica ore deposition is solved, achieving sufficient mixing and reaction stability, and improving lithium extraction efficiency.

CN222305824UActive Publication Date: 2025-01-07JIANGXI XINHELEI NEW MATERIAL TECHNOLOGY CO LTD
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Patent Information

Application Number
CN202420659547.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-02
Publication Date
2025-01-07
Estimated Expiration
2034-04-02

AI Technical Summary

Technical Problem

Lithium mica ore is easily deposited at the bottom of the reactor during the extraction process, resulting in insufficient mixing and increasing the difficulty of subsequent extraction.

Method used

A precipitation reaction tank for wet extraction of lithium mica mine is designed, including a support platform, a mixing container, an electric push rod and a stirring device. The mixing container is driven up and down through the electric push rod. The stirring device stirs at the bottom of the mixing container and passes through The motor drive gear and stirring blades achieve uniform mixing, preventing deposition and increasing reaction stability.

Benefits of technology

Effectively prevent lithium mica ore from depositing at the bottom of the mixing container, ensuring sufficient mixing, improving the chemical reaction stability of lithium mica ore with brine and sodium carbonate, and reducing impurity content.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of lithium precipitation and extraction, in particular to a precipitation reaction tank for wet extraction of lepidolite ore, which comprises a support platform, a mixing container, an electric push rod and a stirring device, the electric push rod is fixed on the support platform, a support plate is fixed at the output end of the electric push rod, and the mixing container is fixed on the support plate. A plurality of supporting frames surrounding the periphery of the mixing container are arranged on the supporting platform, the stirring device is located at the top of the mixing container and fixed to the supporting frames, and the stirring end of the stirring device extends into the mixing container and is in sliding connection with the mixing container. The electric push rod pushes the supporting plate to drive the mixing container to move up and down, and the stirring device fixed on the supporting frame stirs lepidolite ore in the mixing container, so that the stirring device can stir the bottom of the mixing container in the stirring process, and the problem that in the prior art, when lithium is extracted from the lepidolite ore, the stirring device cannot stir the bottom of the mixing container is solved. Part of lepidolite ore is easily deposited at the bottom of the reaction kettle, so that the mixing is insufficient.
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Description

Technical Field

[0001] The utility model relates to the technical field of lithium precipitation and extraction, in particular to a precipitation reaction pool for wet extraction of lithium mica ore. Background Art

[0002] Lepidolite is one of the important minerals for lithium extraction. During the extraction process, it is usually necessary to continuously add the chemical agents required for the reaction to the sodium carbonate alkaline solution of the lepidolite. However, the traditional method of adding materials often results in uneven addition, which causes insufficient mixing of brine and alkaline solution, resulting in a high impurity content in the finished lithium carbonate.

[0003] Based on the above problems, the existing patent with publication number CN218393661U discloses a lithium precipitation device for lithium mica, which installs a disperser for uniformly dispersing brine in the reactor, so that the brine is evenly dispersed and added to the alkali solution, and the brine and the sodium carbonate alkali solution are fully mixed through a stirring device, so that the brine, sodium carbonate and lithium mica are fully reacted, thereby improving the quality of the finished lithium carbonate and reducing the impurity content of the finished lithium carbonate.

[0004] However, when implementing the above-mentioned lithium precipitation device for lithium mica, it was found that there were at least the following problems: during the extraction process, the spreader continuously added alkali solution and brine into the reactor, and the stirring rod of the stirring device drove the mixed solution of brine, sodium carbonate and lithium mica ore to mix. However, during the initial mixing of the lithium mica ore, the lithium mica ore contained some impurities, which made the lithium mica ore easily deposited at the bottom of the reactor, resulting in that some of the lithium mica ore deposited at the bottom of the reactor could not be stirred by the stirring rod, which led to insufficient mixing. The lithium carbonate deposited after sufficient reaction was easily mixed in some of the lithium mica ore that was not fully reacted, increasing the difficulty of subsequent extraction. Utility Model Content

[0005] In view of the shortcomings of the prior art, the utility model provides a precipitation reaction pool for wet extraction of lepidolite ore, which can prevent the lepidolite ore from being deposited at the bottom of a mixing container, so as to solve the problem in the prior art that the lepidolite ore is easily deposited at the bottom of a reactor, resulting in insufficient mixing.

[0006] In order to achieve the above-mentioned purpose, the utility model provides a precipitation reaction tank for wet extraction of lithium mica ore, including a supporting platform, a mixing container, an electric push rod and a stirring device, the electric push rod is fixed on the supporting platform, and a supporting plate is fixed at its output end, the mixing container is fixed on the supporting plate, and a plurality of supporting frames surrounding the periphery of the mixing container are provided on the supporting platform, the stirring device is located on the top of the mixing container and is fixed to the plurality of supporting frames, and the stirring end of the stirring device extends into the mixing container and is slidably connected to the mixing container.

[0007] Optionally, the stirring device includes a motor fixed to the multiple supporting frames and a T-shaped fixed tube, the fixed tube is slidably connected to the mixing container, one end of the single head is fixed to the supporting frame, the output end of the motor is fixed to a rotating shaft, the rotating shaft is rotatably connected in the fixed tube, a gear 1 is provided at the bottom of the rotating shaft, one end of the double heads of the fixed tube is rotatably connected to the output shaft, one end of the output shaft facing the gear is fixed with a gear 2 meshing with the gear, and one end of the output shaft protruding from the fixed tube is fixed with multiple stirring blades.

[0008] Optionally, a plurality of the support frames are provided with sliding grooves, a plurality of fixed blocks are fixed outside the mixing container, and the plurality of fixed blocks are slidably connected in the sliding grooves.

[0009] Optionally, a limited support column is provided between the support plate and the support platform, and one end of the limited support column is fixed to the support plate.

[0010] Optionally, it further comprises a plurality of material adding containers located on the top of the mixing container and fixed to the supporting frame, wherein the plurality of material adding containers are connected to the mixing container via a hose, and a booster pump is provided on the top of the material adding container.

[0011] Optionally, it further comprises an annular liquid spraying member, the interior of which is hollow and connected to the hose, the liquid spraying member is fixed to the inner wall of the mixing container and is provided with a plurality of spraying holes on the side facing the stirring device.

[0012] Compared with the prior art, the utility model provides a precipitation reaction tank for wet extraction of lepidolite ore, which has the following beneficial effects:

[0013] The utility model drives the mixing container to move up and down by pushing the support plate through the electric push rod, and the stirring device fixed on the support frame stirs the lithium mica ore in the mixing container, so that the stirring device can stir the bottom of the mixing container during the stirring process, thereby solving the problem in the prior art that part of the lithium mica ore is easily deposited at the bottom of the reactor when lithium is extracted from the lithium mica ore, resulting in insufficient mixing;

[0014] The utility model drives the rotating shaft to rotate through the output end of the motor so that the gear 1 drives the stirring blades on the two output shafts to rotate in the opposite direction, so that during the mixing process, the stirring device can more evenly mix and contact the lepidolite ore with the brine and the sodium carbonate, thereby increasing the stability of the chemical reaction between the lepidolite ore, the brine and the sodium carbonate when the lepidolite ore is extracted for lithium;

[0015] The utility model increases the support for the support plate by arranging the limit support column, and can prevent the output end of the electric push rod from sliding down after the electric push rod stops running, limit the support plate, and thus protect the electric push rod. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0017] Figure 2 Shows Figure 1 A front view structural diagram of

[0018] Figure 3 A partial structural schematic diagram is shown;

[0019] Figure 4 Shows Figure 3 Schematic diagram of the internal structure.

[0020] In the figure: 1. Support platform; 2. Mixing container; 3. Electric push rod; 4. Stirring device; 41. Motor; 42. Fixed pipe; 43. Rotating shaft; 44. Gear 1; 45. Output shaft; 46. Gear 2; 47. Stirring blade; 5. Support plate; 6. Support frame; 7. Fixed block; 8. Sliding groove; 9. Limit support column; 10. Feeding container; 11. Hose; 12. Booster pump; 13. Spraying part; 14. Spraying hole. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0022] Example: See Figures 1 to 4 According to an embodiment of the utility model, a technical solution is provided: a precipitation reaction tank for wet extraction of lithium mica ore, comprising a supporting platform 1, a mixing container 2, an electric push rod 3 and a stirring device 4, the electric push rod 3 is fixed on the supporting platform 1, and a supporting plate 5 is fixed at its output end, the mixing container 2 is fixed on the supporting plate 5, a plurality of supporting frames 6 surrounding the periphery of the mixing container 2 are provided on the supporting platform 1, the stirring device 4 is located on the top of the mixing container 2 and is fixed to the plurality of supporting frames 6, and the stirring end of the stirring device 4 extends into the mixing container 2 and is slidably connected to the mixing container 2.

[0023] The sedimentation reaction tank for wet extraction of lepidolite ore with the above structure is adopted. The electric push rod 3 pushes the support plate 5 to drive the mixing container 2 to move up and down. The stirring device 4 fixed on the support frame 6 stirs the lepidolite ore in the mixing container 2, so that the stirring device 4 can stir the bottom of the mixing container 2 during the stirring process, thereby solving the problem in the prior art that part of the lepidolite ore is easily deposited at the bottom of the reactor when lithium is extracted from the lepidolite ore, resulting in insufficient mixing.

[0024] In this embodiment, the stirring device 4 includes a motor 41 fixed to multiple support frames 6 and a T-shaped fixed tube 42. The fixed tube 42 is slidably connected to the mixing container 2, and one end of its single head is fixed to the support frame 6. The output end of the motor 41 is fixed to a rotating shaft 43, and the rotating shaft 43 is rotatably connected in the fixed tube 42. A gear 1 44 is provided at the bottom of the rotating shaft 43. One end of the double head of the fixed tube 42 is rotatably connected to an output shaft 45. The output shaft 45 is fixed with a gear 2 46 meshing with the gear at one end facing the gear. A plurality of stirring blades 47 are fixed to one end of the output shaft 45 protruding from the fixed tube 42. The rotating shaft 43 is driven to rotate by the output end of the motor 41 so that the gear 1 44 drives the stirring blades 47 on the two output shafts 45 to rotate in the opposite direction, so that during the mixing process, the stirring device 4 can more evenly mix and contact the lithium mica ore with brine and sodium carbonate, thereby increasing the stability of the chemical reaction between the lithium mica ore, brine and sodium carbonate when lithium is extracted from the lithium mica ore.

[0025] In this embodiment, sliding grooves 8 are provided on multiple support frames 6, and multiple fixed blocks 7 are fixed outside the mixing container 2. The multiple fixed blocks 7 are slidably connected in the sliding grooves 8. By providing multiple fixed blocks 7 slidably connected to the sliding grooves 8, the electric push rod 3 is reduced in the process of pushing the support plate 5 and then driving the mixing container 2 to move up and down, thereby increasing the stability of the mixing container 2 and preventing the mixing container 2 from being offset and tilted, thereby preventing the mixing container 2 from tipping over.

[0026] In this embodiment, a limiting support column 9 is arranged between the support plate 5 and the support platform 1, and one end of the limiting support column 9 is fixed to the support plate 5. By providing the limiting support column 9, the support for the support plate 5 is increased, and after the electric push rod 3 stops running, the output end of the electric push rod 3 can be prevented from sliding down, and the support plate 5 can be limited, thereby protecting the electric push rod 3.

[0027] In this embodiment, it also includes a plurality of adding containers 10 located on the top of the mixing container 2 and fixed to the supporting frame 6. The plurality of adding containers 10 are connected to the mixing container 2 through a hose 11. A booster pump 12 is provided on the top of the adding container 10. By adding brine and sodium carbonate into the adding container 10 and passing through the booster pump 12, the brine and sodium carbonate are sprayed into the mixing container 2 along the hose 11.

[0028] In this embodiment, an annular liquid spraying member 13 is further included. The interior of the liquid spraying member 13 is hollow and connected to the hose 11. The liquid spraying member 13 is fixed to the inner wall of the mixing container 2 and a plurality of spraying holes 14 are provided on the side facing the stirring device 4. By providing the annular liquid spraying member 13, the brine and sodium carbonate can be sprayed along the periphery of the stirring device 4, so that the brine and sodium carbonate can be quickly stirred by the stirring device 4, thereby increasing the mixing efficiency and the mixing stability.

[0029] Working principle: the mixed liquid of lithium mica ore and water is introduced into the mixing container 2, and brine and sodium carbonate are added to multiple feeding containers 10, and the brine and sodium carbonate are punched into the spray part 13 along the hose 11 through the booster pump 12, and sprayed toward the stirring blades 47. In this process, the output end of the motor 41 drives the rotating shaft 43 to rotate so that the gear 1 44 drives the stirring blades 47 on the two output shafts 45 to rotate in the opposite direction, and the electric push rod 3 pushes the support plate 5 to drive the mixing container 2 to move up and down, and the stirring device 4 fixed on the support frame 6 stirs the lithium mica ore in the mixing container 2. In this up and down lifting process, because a plurality of fixed blocks 7 slidably connected to the sliding groove 8 are provided, the mixing container 2 can be prevented from being offset and tilted. When the mixing stops, the electric push rod 3 is retracted to drive the mixing container 2 to move downward, and the support plate 5 is supported by the limit support column 9.

[0030] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A precipitation reaction tank for wet extraction of lepidolite ore, characterized in that: include: A support platform (1), a mixing container (2), an electric push rod (3) and a stirring device (4), wherein the electric push rod (3) is fixed on the support platform (1), and a support plate (5) is fixed to the output end of the electric push rod (3), the mixing container (2) is fixed on the support plate (5), a plurality of support frames (6) surrounding the periphery of the mixing container (2) are provided on the support platform (1), the stirring device (4) is located on the top of the mixing container (2) and is fixed to the plurality of support frames (6), and the stirring end of the stirring device (4) extends into the mixing container (2) and is slidably connected to the mixing container (2).

2. A precipitation reaction tank for wet extraction of lepidolite according to claim 1, characterized in that: The stirring device (4) comprises a motor (41) fixed to a plurality of the supporting frames (6) and a T-shaped fixed tube (42); the fixed tube (42) is slidably connected to the mixing container (2); one end of the fixed tube (42) is fixed to the supporting frame (6); the output end of the motor (41) is fixed to a rotating shaft (43); the rotating shaft (43) is rotatably connected to the fixed tube (42); a gear 1 (44) is provided at the bottom of the rotating shaft (43); one end of the double ends of the fixed tube (42) is rotatably connected to an output shaft (45); a gear 2 (46) meshing with the gear is fixed to one end of the output shaft (45) facing the gear; and a plurality of stirring blades (47) are fixed to one end of the output shaft (45) protruding from the fixed tube (42).

3. A precipitation reaction tank for wet extraction of lepidolite according to claim 1, characterized in that: A plurality of the support frames (6) are each provided with a sliding groove (8), a plurality of fixed blocks (7) are fixed outside the mixing container (2), and the plurality of fixed blocks (7) are slidably connected in the sliding groove (8).

4. A precipitation reaction tank for wet extraction of lepidolite according to claim 1, characterized in that: A limited support column (9) is provided between the support plate (5) and the support platform (1), and one end of the limited support column (9) is fixed to the support plate (5).

5. A precipitation reaction tank for wet extraction of lepidolite according to claim 1, characterized in that: It also includes a plurality of material adding containers (10) located on the top of the mixing container (2) and fixed to the supporting frame (6); the plurality of material adding containers (10) are connected to the mixing container (2) via a hose (11); and a booster pump (12) is provided on the top of the material adding container (10).

6. A precipitation reaction tank for wet extraction of lepidolite according to claim 5, characterized in that: It also comprises an annular liquid spraying member (13), the interior of which is hollow and connected to the hose (11), and the liquid spraying member (13) is fixed to the inner wall of the mixing container (2) and is provided with a plurality of spraying holes (14) on one side facing the stirring device (4).

Citation Information

Patent Citations

  • Lithium precipitation device for lepidolite

    CN218393661U