Dimethyl carbonate dehydrator

By designing a rotatable plate body and inner cavity structure in a dimethyl carbonate dehydrator, the silicone dehydrating agent is evenly distributed from top to bottom, the problem of uneven distribution of dehydrating agents in the prior art is solved, the dehydration efficiency of dimethyl carbonate is improved, and the regeneration of dehydrating agent is realized.

CN222677243UActive Publication Date: 2025-03-28WEIFANG AOTONG PHARM CO LTD
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Patent Information

Application Number
CN202421247804.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-06-03
Publication Date
2025-03-28
Estimated Expiration
2034-06-03

AI Technical Summary

Technical Problem

In the existing dimethyl carbonate dehydrator, the dehydrating agent cannot be evenly distributed from top to bottom, resulting in low dehydration efficiency of dimethyl carbonate.

Method used

A dimethyl carbonate dehydrator is designed, including a shell, a rotating shaft, a plate body and an inner cavity. The plate body is distributed with respect to the rotating shaft and other angles. A silicone dehydrating agent is installed inside the inner cavity. The motor drives the rotating shaft and a plate body to rotate, so that the silicone dehydrating agent is evenly distributed from top to bottom.

Benefits of technology

Through the uniformly distributed silicone dehydrating agent, the area of ​​absorbing the internal moisture of dimethyl carbonate is increased, the dehydration efficiency is improved, and the water inside the dehydrating agent is evaporated and discharged through an electric heating rod, realizing the regeneration of the dehydrating agent.

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Abstract

The utility model discloses a dimethyl carbonate dehydrator which comprises a shell, a rotating shaft is rotatably mounted in the shell, plate bodies are fixed on the outer wall of the rotating shaft and are distributed at equal angles relative to the central axis of the rotating shaft, an inner cavity is formed in each plate body, water permeable holes are uniformly formed in the side of each plate body, and the water permeable holes are communicated with the inner cavity. The dimethyl carbonate dehydrator is provided with the plate body and the inner cavity, so that the silica gel dehydrating agent can be uniformly distributed in the dehydrator from top to bottom, the dehydration effect of the dehydrator is improved, and the dehydration effect of the dehydrator is improved. The area of the silica gel dehydrating agent for absorbing moisture in dimethyl carbonate is increased, dehydration of the dimethyl carbonate is facilitated, meanwhile, the motor is started to drive the silica gel dehydrating agent to rotate, so that the silica gel dehydrating agent can be in contact with more dimethyl carbonate, and the dehydration efficiency of the dimethyl carbonate is further improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of dimethyl carbonate processing, in particular to a dimethyl carbonate dehydrator. Background Art

[0002] Dimethyl carbonate is an organic compound with the chemical formula C3H6O3. It is a low-toxic, environmentally friendly, and widely used chemical raw material. It is an important organic synthesis intermediate. Its molecular structure contains functional groups such as carbonyl, methyl, and methoxy. It has a variety of reaction properties. It is safe, convenient, less polluting, and easy to transport in production. In order to improve the purity of dimethyl carbonate, a dehydrator is used to dehydrate dimethyl carbonate.

[0003] However, the dehydrating agent in the existing dimethyl carbonate dehydrator cannot be evenly distributed in the dehydrator from top to bottom, resulting in the inability to efficiently dehydrate the dimethyl carbonate in the dehydrator. In view of the above problems, it is urgent to carry out innovative design based on the original dimethyl carbonate dehydrator. Utility Model Content

[0004] The purpose of the utility model is to provide a dimethyl carbonate dehydrator to solve the problems raised by the above background technology.

[0005] To achieve the above-mentioned purpose, the utility model provides the following technical scheme: a dimethyl carbonate dehydrator, comprising a shell, a rotating shaft is rotatably installed inside the shell, a plate body is fixed to the outer wall of the rotating shaft, and the plate body is distributed at equal angles about the central axis of the rotating shaft, an inner cavity is opened inside the plate body, and water-permeable holes are evenly opened on the sides of the plate body, the water-permeable holes and the inner cavity are interconnected, a silica gel dehydrating agent is installed inside the inner cavity, a motor is fixed on the top of the rotating shaft passing through the top of the shell, and the outer wall of the motor is fixed to the top of the shell through a machine cover.

[0006] Preferably, a heating cavity is opened on the side of the shell, and electric heating rods are installed inside the heating cavity. The electric heating rods are distributed at equal angles with respect to the central axis of the shell.

[0007] Preferably, an exhaust pipe is provided on one side of the top of the shell, and the exhaust pipe is designed to be a "U"-shaped structure. A bottom cover is threadedly installed on the bottom of the exhaust pipe, and a dust filter is clamped inside the bottom cover. The top of the dust filter fits with the bottom of the exhaust pipe, and a through hole is opened at the bottom of the bottom cover.

[0008] Preferably, a feeding bin is provided on one side of the top of the shell body away from the exhaust pipe, and a top cover is threadedly mounted on the top of the feeding bin.

[0009] Preferably, a discharge pipe is provided at the bottom of one side of the shell, and a manual valve is installed on the discharge pipe.

[0010] Preferably, the diameter of the silica gel dehydrating agent is larger than the diameter of the water permeable hole.

[0011] Preferably, a heat insulation board is fixed to the outer wall of the shell, and the heat insulation board is designed as a hollow cylindrical structure.

[0012] Compared with the prior art, the utility model has the following beneficial effects: the dimethyl carbonate dehydrator is provided with a plate body and an inner cavity, so that the silica gel dehydrating agent can be evenly distributed from top to bottom inside the dehydrator, increasing the area of ​​the silica gel dehydrating agent absorbing the internal moisture of the dimethyl carbonate, which is beneficial to the dehydration of the dimethyl carbonate. At the same time, starting the motor can drive the silica gel dehydrating agent to rotate, so that the silica gel dehydrating agent can contact more dimethyl carbonate, further improving the efficiency of the dehydration of the dimethyl carbonate.

[0013] Under the obstruction of the plate body and the water-permeable holes, dimethyl carbonate can be separated from the silica gel dehydrating agent, so that dimethyl carbonate can be directly discharged quickly from the discharge pipe, thereby improving the rapid discharge of dimethyl carbonate after dehydration;

[0014] By starting the electric heating rod, the inside of the shell is heated, so that the temperature inside the shell increases. The high temperature inside the shell heats the silica gel dehydrating agent, so that the water inside the silica gel dehydrating agent evaporates and is discharged through the exhaust pipe, so that the silica gel dehydrating agent can be used again. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 This is a schematic diagram of the front cross-sectional structure of the utility model;

[0016] Figure 2 This is a schematic diagram of the cross-sectional structure of the utility model from top view;

[0017] Figure 3 For this utility model Figure 2 A schematic diagram of the enlarged structure of the middle plate;

[0018] Figure 4 For this utility model Figure 1 The enlarged structural diagram at A in the middle;

[0019] Figure 5 For this utility model Figure 4 Schematic diagram of the structure of the midsole cover from a top view.

[0020] In the figure: 1. Shell; 2. Rotating shaft; 3. Plate; 4. Inner cavity; 5. Water permeable hole; 6. Silica gel dehydrating agent; 7. Motor; 8. Heating cavity; 9. Electric heating rod; 10. Exhaust pipe; 11. Bottom cover; 12. Dust filter; 13. Through hole; 14. Feed bin; 15. Top cover; 16. Discharge pipe; 17. Manual valve; 18. Heat insulation board. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0022] See also Figure 1-5 The utility model provides a technical solution: a dimethyl carbonate dehydrator, comprising a shell 1, a rotating shaft 2 is rotatably installed inside the shell 1, a plate body 3 is fixed on the outer wall of the rotating shaft 2, and the plate body 3 is distributed at equal angles about the central axis of the rotating shaft 2, an inner cavity 4 is opened inside the plate body 3, and water-permeable holes 5 are evenly opened on the sides of the plate body 3, the water-permeable holes 5 and the inner cavity 4 are interconnected, a silica gel dehydrating agent 6 is installed inside the inner cavity 4, a motor 7 is fixed on the top of the shell 1 through the top of the rotating shaft 2, and the outer wall of the motor 7 is fixed to the top of the shell 1 through a machine cover, so that the silica gel dehydrating agent 6 can be evenly distributed from top to bottom inside the dehydrator, increasing the area of ​​the silica gel dehydrating agent 6 absorbing the internal moisture of dimethyl carbonate, which is beneficial to the dehydration of dimethyl carbonate, and starting the motor 7 at the same time can drive the silica gel dehydrating agent 6 to rotate, so that the silica gel dehydrating agent 6 can contact more dimethyl carbonate, further improving the efficiency of dimethyl carbonate dehydration.

[0023] A heating chamber 8 is provided on the side of the shell 1 , and electric heating rods 9 are installed inside the heating chamber 8 . The electric heating rods 9 are distributed at equal angles with respect to the central axis of the shell 1 , which is beneficial for the dimethyl carbonate inside the shell 1 to be heated quickly.

[0024] An exhaust pipe 10 is arranged on one side of the top of the shell 1. The exhaust pipe 10 is designed as a "U"-shaped structure. A bottom cover 11 is threadedly installed on the bottom of the exhaust pipe 10. A dust filter 12 is clamped inside the bottom cover 11. The top of the dust filter 12 fits with the bottom of the exhaust pipe 10. A through hole 13 is provided at the bottom of the bottom cover 11. The dust filter 12 prevents external dust from entering the interior of the shell 1 through the exhaust pipe 10, thereby ensuring the cleanliness of the interior of the shell 1 and allowing the dust filter 12 to be removed for cleaning.

[0025] A feeding bin 14 is provided on one side of the top of the shell 1 away from the exhaust pipe 10 , and a top cover 15 is threadedly mounted on the top of the feeding bin 14 , through which dimethyl carbonate can be fed into the interior of the shell 1 .

[0026] A discharge pipe 16 is provided at the bottom of one side of the shell 1 , and a manual valve 17 is installed on the discharge pipe 16 , through which the dimethyl carbonate in the shell 1 can be discharged.

[0027] The diameter of the silica gel dehydrating agent 6 is larger than the diameter of the water permeable hole 5 , thereby preventing the silica gel dehydrating agent 6 from coming out of the inner cavity 4 through the water permeable hole 5 .

[0028] An insulation board 18 is fixed to the outer wall of the shell 1 . The insulation board 18 is designed as a hollow cylindrical structure. The material of the insulation board 18 is rock wool, which reduces the probability of the shell 1 scalding the user.

[0029] Working principle: When using the dimethyl carbonate dehydrator, firstly, the dimethyl carbonate to be dehydrated is fed into the shell 1 through the feeding bin 14. Under the action of the plate 3 and the inner cavity 4, the silica gel dehydrating agent 6 can be evenly distributed from top to bottom in the shell 1, increasing the area of ​​the silica gel dehydrating agent 6 to absorb the water inside the dimethyl carbonate, so that the water in the dimethyl carbonate enters the inner cavity 4 through the water-permeable hole 5 and is absorbed by the silica gel dehydrating agent 6 inside the inner cavity 4. By starting the motor 7, the rotating shaft 2, the plate 3 and the silica gel dehydrating agent 6 inside the plate 3 can be driven to rotate, so that the silica gel dehydrating agent 6 can absorb more water in the dimethyl carbonate;

[0030] The discharge pipe 16 is opened through the manual valve 17, so that the dehydrated dimethyl carbonate in the shell 1 is discharged through the discharge pipe 16. Under the obstruction of the water-permeable hole 5, the silica gel dehydrating agent 6 remains in the inside of the plate body 3. Then the electric heating rod 9 is started to heat the inside of the shell 1, so that the temperature inside the shell 1 increases. The high temperature inside the shell 1 heats the silica gel dehydrating agent 6, so that the water inside the silica gel dehydrating agent 6 evaporates and is discharged through the exhaust pipe 10, so that the silica gel dehydrating agent 6 can be used again.

[0031] Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art may still modify the technical solutions described in the aforementioned embodiments, or make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention shall be included in the protection scope of the present invention.

Claims

1. A dimethyl carbonate dehydrator, comprising a housing (1), characterized in that: A rotating shaft (2) is rotatably mounted inside the shell (1), a plate body (3) is fixed to the outer wall of the rotating shaft (2), and the plate bodies (3) are distributed at equal angles with respect to the central axis of the rotating shaft (2), an inner cavity (4) is provided inside the plate body (3), water-permeable holes (5) are evenly provided on the sides of the plate body (3), the water-permeable holes (5) and the inner cavity (4) are interconnected, a silica gel dehydrating agent (6) is installed inside the inner cavity (4), the top of the rotating shaft (2) passes through the top of the shell (1), and a motor (7) is fixed thereto, and the outer wall of the motor (7) is fixed to the top of the shell (1) via a machine cover.

2. A dimethyl carbonate dehydrator according to claim 1, characterized in that: A heating cavity (8) is provided on the side of the shell (1), and electric heating rods (9) are installed inside the heating cavity (8). The electric heating rods (9) are distributed at equal angles with respect to the central axis of the shell (1).

3. A dimethyl carbonate dehydrator according to claim 1, characterized in that: An exhaust pipe (10) is arranged on one side of the top of the shell (1), the exhaust pipe (10) being designed as a "U"-shaped structure, a bottom cover (11) being threadedly mounted on the bottom of the exhaust pipe (10), a dust filter (12) being clamped inside the bottom cover (11), the top of the dust filter (12) being in contact with the bottom of the exhaust pipe (10), and a through hole (13) being provided at the bottom of the bottom cover (11).

4. A dimethyl carbonate dehydrator according to claim 1, characterized in that: A feeding bin (14) is provided on one side of the top of the housing (1) away from the exhaust pipe (10), and a top cover (15) is threadedly mounted on the top of the feeding bin (14).

5. A dimethyl carbonate dehydrator according to claim 1, characterized in that: A discharge pipe (16) is provided at the bottom of one side of the housing (1), and a manual valve (17) is installed on the discharge pipe (16).

6. A dimethyl carbonate dehydrator according to claim 1, characterized in that: The diameter of the silica gel dehydrating agent (6) is larger than the diameter of the water permeable hole (5).

7. A dimethyl carbonate dehydrator according to claim 1, characterized in that: A heat insulation board (18) is fixed to the outer wall of the shell (1), and the heat insulation board (18) is designed as a hollow cylindrical structure.