Esterification accelerating device

The acceleration mixer is driven by the transmission shaft and the drive shaft, combined with longitudinal and transverse stirring vortex, the problem of idling the liquid center in the esterification reaction is solved, and the uniform distribution of the catalyst and the improvement of the reaction efficiency are achieved.

CN223249302UActive Publication Date: 2025-08-22SUZHOU FENGBEI BIOTECH CO LTD
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Patent Information

Application Number
CN202422412382.0
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-08
Publication Date
2025-08-22
Estimated Expiration
2034-10-08

AI Technical Summary

Technical Problem

The existing esterification acceleration device is prone to vortex during the stirring process, resulting in the idling of the liquid center, and the catalyst cannot be fully mixed, reducing the reaction efficiency.

Method used

The transmission shaft and the drive shaft are used to drive the acceleration mixer, including the connecting pipe, agitating frame and agitating rod. By combining longitudinal and transverse stirring vortex, one-way vortex is avoided and the catalyst is evenly distributed.

Benefits of technology

The efficiency of liquid esterification reaction is improved, ensuring that the catalyst is fully integrated into the liquid, avoiding the liquid idle phenomenon, and improving the mixing effect.

✦ Generated by Eureka AI based on patent content.

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    Figure CN223249302U_ABST
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Abstract

The utility model provides an esterification accelerating device which comprises a base, two sides of the top of the base are fixedly connected with bearing seats, an esterification kettle body is fixedly connected between the tops of the two bearing seats, and the bottom of the esterification kettle body is fixedly connected with a first case. Compared with the prior art, the esterification kettle has the following beneficial effects that the first motor and the two second motors are started, the first motor drives the connecting pipe, the two dosing pipes and the four stirring rods to transversely rotate in the esterification kettle body through the transmission shaft to generate longitudinal stirring vortexes, and the two second motors drive the two driving shafts to rotate, so that the stirring vortexes are uniformly stirred; the two driving shafts drive the two stirring frames to rotate between the two vertically adjacent stirring rods respectively, and longitudinal vortexes generated by rotation of the dosing pipe and the stirring rods are disordered by generated transverse stirring vortexes, so that the phenomenon that liquid in the esterification kettle body is stirred in an idling manner due to unidirectional stirring vortexes is avoided; the liquid esterification reaction efficiency is effectively improved.
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Description

Technical Field

[0001] The utility model relates to an esterification accelerating device, belonging to the field of stirring equipment. Background Art

[0002] Esterification reaction is a type of organic chemical reaction, which is the reaction between alcohol and carboxylic acid or oxygen-containing inorganic acid to produce ester and water. It is divided into three categories: reaction between carboxylic acid and alcohol, reaction between inorganic oxygen-containing acid and alcohol, and reaction between inorganic strong acid and alcohol. In order to increase the reaction speed, stirring is needed to accelerate the esterification reaction.

[0003] In the prior art, the stirring rod inside the esterification acceleration device is usually horizontal or vertical. During the stirring process of the liquid, a vortex is generated, which makes it impossible for the catalyst in the center of the vortex to be quickly and fully mixed with the liquid at the outer edge of the vortex. The spoiler rod installed inside the kettle body can only disrupt the large vortex into a small vortex, and cannot avoid the phenomenon of idling in the center of the liquid, thereby reducing the efficiency of the liquid esterification reaction.

[0004] In summary, the present invention provides an esterification acceleration device to solve the above problems. Utility Model Content

[0005] In view of the shortcomings of the existing technology, the purpose of the present invention is to provide an esterification acceleration device to solve the problem proposed in the above background technology that vortices are easily generated during the esterification reaction of the stirred liquid, resulting in idling of the liquid center and the inability to fully mix the catalyst.

[0006] In order to achieve the above-mentioned purpose, the present invention is implemented through the following technical solutions: an esterification acceleration device, comprising a base, both sides of the top of the base are fixedly connected to a load-bearing seat, an esterification kettle body is fixedly connected between the tops of the two load-bearing seats, the bottom of the esterification kettle body is fixedly connected to a first chassis, a first motor is fixedly connected inside the first chassis, an output end of the first motor is fixedly connected to a transmission shaft, one end of the transmission shaft sequentially passes through the first chassis and the esterification kettle body and extends to the interior of the esterification kettle body, both sides of the esterification kettle body are fixedly connected to a second chassis, the interiors of the two second chassis are fixedly connected to the second motors, the output ends of the two second motors are fixedly connected to the drive shaft, one end of the drive shaft sequentially passes through the second chassis and the esterification kettle body and extends to the interior of the esterification kettle body, and an acceleration mixer is fixedly connected between the opposite end of the two drive shafts and one end of the transmission shaft.

[0007] Furthermore, the transmission shaft is rotatably connected to the first chassis, and the transmission shaft is rotatably connected to the esterification kettle body.

[0008] Furthermore, the drive shaft is rotatably connected to the second chassis, and the second chassis is rotatably connected to the esterification kettle body.

[0009] Furthermore, the bottom of one side of the esterification kettle body is connected to a liquid inlet pipe, the bottom of the other side of the esterification kettle body is connected to a liquid outlet pipe, and the top of one side of the esterification kettle body is connected to a discharge pipe.

[0010] Furthermore, the acceleration mixer includes a connecting pipe and two stirring frames, the two stirring frames are respectively fixedly connected to the opposite ends of the two driving shafts, and the opposite sides of the two stirring frames are open. The connecting pipe is fixedly connected to the top of the transmission shaft and is located between the opposite sides of the two stirring frames. The top of the connecting pipe passes through the top of the inner wall of the esterification kettle body and extends to the top of the esterification kettle body. Both sides of the connecting pipe surface and the openings located on the opposite sides of the two stirring frames are connected with dosing pipes. The front sides of the two dosing pipes are evenly connected with multiple one-way valves from left to right. Stirring rods are fixedly connected to both sides of the connecting pipe and located directly above and directly below the two stirring frames.

[0011] Furthermore, the top end of the connecting tube is rotatably connected to the infusion tube, and the connecting tube is communicated with the infusion tube.

[0012] Furthermore, the connecting pipe is rotatably connected to the esterification kettle body, and the separated ends of the two dosing pipes extend into the interiors of the two stirring frames respectively through openings on opposite sides of the two stirring frames.

[0013] Beneficial effects of the utility model:

[0014] By starting the first motor and the two second motors, the first motor drives the connecting pipe, the two dosing pipes and the four stirring rods to rotate horizontally inside the esterification kettle body through the transmission shaft, thereby generating a longitudinal stirring vortex. The two second motors drive the two drive shafts to rotate, and the two drive shafts drive the two stirring frames to rotate between two upper and lower adjacent stirring rods respectively. The generated transverse stirring vortex will disrupt the longitudinal vortex generated by the rotation of the dosing pipes and the stirring rods, thereby avoiding the phenomenon of idling stirring of the liquid inside the esterification kettle body caused by the occurrence of a unidirectional stirring vortex, thereby effectively improving the efficiency of the liquid esterification reaction.

[0015] The catalyst is transported to the interior of the connecting tube through the infusion tube. The bottom end of the cavity inside the connecting tube is located below the port of the dosing tube, so that the catalyst transported inside the connecting tube can be completely transported to the interior of the two dosing tubes. The water pressure can open the one-way valve and discharge the catalyst from the two dosing tubes to the interior of the esterification kettle body and mix with the liquid, thereby avoiding the phenomenon of the catalyst floating on the surface of the liquid inside the esterification kettle body and accelerating the efficiency of the catalyst being integrated into various parts of the liquid. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Other features, objects and advantages of the present invention will become more apparent from the detailed description of the non-limiting embodiments with reference to the following drawings:

[0017] Figure 1 This is a schematic structural perspective diagram of an esterification acceleration device of the present invention;

[0018] Figure 2 This is a schematic structural front view of an esterification acceleration device of the utility model;

[0019] Figure 3 This is a schematic main cross-sectional view of the structure of an esterification acceleration device of the present invention;

[0020] Figure 4 for Figure 3 The main cross-sectional view of the structure of the connecting pipe shown is a schematic diagram.

[0021] In the figure: 1. Base; 2. Load-bearing seat; 3. Esterification kettle body; 4. First chassis; 5. First motor; 6. Transmission shaft; 7. Second chassis; 8. Second motor; 9. Accelerator mixer; 10. Drive shaft; 11. Liquid inlet pipe; 12. Liquid outlet pipe; 13. Discharge pipe; 14. Liquid infusion pipe; 91. Connecting pipe; 92. Stirring frame; 93. Dosing pipe; 94. Stirring rod; 95. One-way valve. DETAILED DESCRIPTION

[0022] In order to make the technical means, creative features, objectives and effects achieved by the present invention easier to understand, the present invention is further described below in conjunction with specific implementation methods.

[0023] See also Figure 1-4The utility model provides a technical solution: an esterification acceleration device, comprising a base 1, both sides of the top of the base 1 are fixedly connected to a load-bearing seat 2, an esterification kettle body 3 is fixedly connected between the tops of the two load-bearing seats 2, the bottom of the esterification kettle body 3 is fixedly connected to a first chassis 4, the interior of the first chassis 4 is fixedly connected to a first motor 5, the output end of the first motor 5 is fixedly connected to a transmission shaft 6, one end of the transmission shaft 6 sequentially passes through the first chassis 4 and the esterification kettle body 3 and extends to the interior of the esterification kettle body 3, both sides of the esterification kettle body 3 are fixedly connected to a second chassis 7, the interiors of the two second chassis 7 are fixedly connected A second motor 8 is connected, and the output ends of the two second motors 8 are fixedly connected to a drive shaft 10. One end of the drive shaft 10 sequentially passes through the second chassis 7 and the esterification kettle body 3 and extends to the interior of the esterification kettle body 3. An acceleration mixer 9 is fixedly connected between the opposite end of the two drive shafts 10 and one end of the transmission shaft 6. The first motor 5 and the two second motors 8 are connected to an external power supply and are provided with the same power control switch. The transmission shaft 6 is rotatably connected to the first chassis 4, the transmission shaft 6 is rotatably connected to the esterification kettle body 3, the drive shaft 10 is rotatably connected to the second chassis 7, and the second chassis 7 is rotatably connected to the esterification kettle body 3.

[0024] See also Figure 2-4 The bottom of one side of the esterification kettle body 3 is connected to a liquid inlet pipe 11, and a solenoid valve is provided on the liquid inlet pipe 11. By opening the liquid inlet pipe 11, the unesterified liquid can be transported to the interior of the esterification kettle body 3 for esterification reaction processing. The bottom of the other side of the esterification kettle body 3 is connected to a liquid outlet pipe 12, and the top of one side of the esterification kettle body 3 is connected to a discharge pipe 13. A solenoid valve is installed on the discharge pipe 13, which is connected to an external power supply and provided with a power control switch. By opening the discharge pipe 13, the grease produced by the esterification reaction above the interior of the esterification kettle body 3 can be discharged in a centralized manner. The liquid outlet pipe 12 is provided with a solenoid valve, which is connected to an external power supply and provided with a power control switch. By opening the liquid outlet pipe 12, the sewage separated by the esterification reaction at the bottom of the esterification kettle body 3 can be discharged in a centralized manner.

[0025] See also Figure 2-4The accelerating mixer 9 includes a connecting pipe 91 and two stirring frames 92. The two stirring frames 92 are respectively fixedly connected to the opposite ends of the two driving shafts 10. The opposite sides of the two stirring frames 92 are open. The connecting pipe 91 is fixedly connected to the top of the transmission shaft 6 and is located between the opposite sides of the two stirring frames 92. The top of the connecting pipe 91 passes through the top of the inner wall of the esterification kettle body 3 and extends to the top of the esterification kettle body 3. Both sides of the connecting pipe 91 and the openings on the opposite sides of the two stirring frames 92 are connected with dosing pipes 93. The front faces of the two dosing pipes 93 are evenly connected with multiple one-way valves 95 from left to right. Stirring rods 94 are fixedly connected to both sides of the connecting pipe 91 and located just above and just below the two stirring frames 92. The bottom end of the cavity inside 1 is located below the port of the dosing tube 93, so that the catalyst transported inside the connecting tube 91 can be fully transported to the interior of the two dosing tubes 93. The water pressure can open the one-way valve 95 and discharge the catalyst from the two dosing tubes 93 to the interior of the esterification kettle body 3 and mix with the liquid. The top of the connecting tube 91 is rotatably connected to the infusion tube 14. The connecting tube 91 is connected to the infusion tube 14. The other end of the infusion tube 14 is connected to the external pump body. The catalyst used in the esterification reaction can be pumped from the infusion tube 14 to the interior of the connecting tube 91. The connecting tube 91 is rotatably connected to the esterification kettle body 3. The separated ends of the two dosing tubes 93 extend to the interior of the two stirring frames 92 through the openings on the opposite sides of the two stirring frames 92.

[0026] Specific implementation method: By opening the liquid inlet pipe 11, the liquid that has not been esterified is pumped from the liquid inlet pipe 11 to the inside of the esterification kettle body 3, and then the catalyst is transported to the inside of the connecting pipe 91 through the liquid infusion pipe 14. The bottom end of the cavity inside the connecting pipe 91 is located below the port of the dosing pipe 93, so that the catalyst transported inside the connecting pipe 91 can be completely transported to the inside of the two dosing pipes 93. The water pressure can open the one-way valve 95, and the catalyst is discharged from the two dosing pipes 93 to the inside of the esterification kettle body 3 and mixed with the liquid, thereby avoiding the phenomenon of the catalyst floating on the water surface of the liquid inside the esterification kettle body 3, and accelerating the efficiency of the catalyst integrating into various parts of the liquid.

[0027] The first motor 5 and the two second motors 8 are started at the same time. The first motor 5 drives the connecting pipe 91 to rotate through the transmission shaft 6. The connecting pipe 91 can simultaneously drive the two dosing pipes 93 and the four stirring rods 94 to rotate horizontally inside the esterification kettle body 3, thereby generating a longitudinal stirring vortex and stirring the liquid inside the esterification kettle body 3 to accelerate the mixing of the catalyst. The two second motors 8 drive the two drive shafts 10 to rotate. The two drive shafts 10 simultaneously drive the two stirring frames 92 to rotate between the two upper and lower adjacent stirring rods 94, respectively. The generated transverse stirring vortex will disrupt the longitudinal vortex generated by the rotation of the dosing pipe 93 and the stirring rod 94, thereby avoiding the phenomenon of idling stirring of the liquid inside the esterification kettle body 3, effectively improving the efficiency of the liquid esterification reaction, and the bayonet between the opposite sides of the two stirring frames 92 does not affect the normal rotation of the two dosing pipes 93.

[0028] After the esterification reaction, the grease and water in the liquid will produce a water-oil separation phenomenon, and the grease will float on the water surface. The liquid is continuously transported to the interior of the esterification kettle body 3 through the liquid inlet pipe 11. As the water level inside the esterification kettle body 3 rises, the grease can be pushed upward. The valve on the discharge pipe 13 is opened to discharge the grease in a centralized manner. After the discharge is completed, the valve on the liquid outlet pipe 12 can be opened to discharge the wastewater containing residual grease for secondary filtration.

[0029] In addition, it should be understood that although this specification is described in terms of implementation methods, not every implementation method contains only one independent technical solution. This narrative method of the specification is only for the sake of clarity. Those skilled in the art should regard the specification as a whole. The technical solutions in each embodiment can also be appropriately combined to form other implementation methods that can be understood by those skilled in the art.

Claims

1. An esterification acceleration device, comprising a base (1), characterized in that: Both sides of the top of the base (1) are fixedly connected to the bearing seats (2), the tops of the two bearing seats (2) are fixedly connected to the esterification kettle body (3), the bottom of the esterification kettle body (3) is fixedly connected to the first chassis (4), the interior of the first chassis (4) is fixedly connected to the first motor (5), the output end of the first motor (5) is fixedly connected to the transmission shaft (6), one end of the transmission shaft (6) passes through the first chassis (4) and the esterification kettle body (3) in sequence and extends to the interior of the esterification kettle body (3) , both sides of the esterification kettle body (3) are fixedly connected to a second chassis (7), the interiors of the two second chassis (7) are fixedly connected to a second motor (8), the output ends of the two second motors (8) are fixedly connected to a drive shaft (10), one end of the drive shaft (10) sequentially passes through the second chassis (7) and the esterification kettle body (3) and extends to the interior of the esterification kettle body (3), and an acceleration mixer (9) is fixedly connected between the opposite end of the two drive shafts (10) and one end of the transmission shaft (6); The accelerating mixer (9) comprises a connecting pipe (91) and two stirring frames (92), the two stirring frames (92) being fixedly connected to opposite ends of the two driving shafts (10), and opposite sides of the two stirring frames (92) being open. The connecting pipe (91) is fixedly connected to the top end of the transmission shaft (6) and is located between opposite sides of the two stirring frames (92). The top end of the connecting pipe (91) passes through the top of the inner wall of the esterification kettle body (3) and extends to the top of the esterification kettle body (3). Both sides of the pipe surface of the connecting pipe (91) and the openings located on the opposite sides of the two stirring frames (92) are connected with dosing pipes (93). The front faces of the two dosing pipes (93) are evenly connected with a plurality of one-way valves (95) from left to right. Both sides of the connecting pipe (91) and the openings located directly above and directly below the two stirring frames (92) are fixedly connected with stirring rods (94).

2. The esterification acceleration device according to claim 1, characterized in that: The transmission shaft (6) is rotatably connected to the first chassis (4), and the transmission shaft (6) is rotatably connected to the esterification kettle body (3).

3. The esterification acceleration device according to claim 1, characterized in that: The drive shaft (10) is rotatably connected to the second chassis (7), and the second chassis (7) is rotatably connected to the esterification kettle body (3).

4. The esterification acceleration device according to claim 1, characterized in that: The bottom of one side of the esterification kettle body (3) is connected to a liquid inlet pipe (11), the bottom of the other side of the esterification kettle body (3) is connected to a liquid outlet pipe (12), and the top of one side of the esterification kettle body (3) is connected to a discharge pipe (13).

5. The esterification acceleration device according to claim 1, characterized in that: The top end of the connecting tube (91) is rotatably connected to the infusion tube (14), and the connecting tube (91) is in communication with the infusion tube (14).

6. The esterification acceleration device according to claim 1, characterized in that: The connecting pipe (91) is rotatably connected to the esterification kettle body (3), and the separated ends of the two dosing pipes (93) extend into the interior of the two stirring frames (92) through openings on opposite sides of the two stirring frames (92).