Ammonium bifluoride self-separation device
Through the design of the feed barrel, centrifugal barrel and spiral blade, the problem of the existing device requiring the separation operation is solved, and the continuous separation and efficient production of ammonium hydrogen fluoride are achieved.
Patent Information
- Application Number
- CN202421720707.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-19
- Publication Date
- 2025-09-02
- Estimated Expiration
- 2034-07-19
AI Technical Summary
The existing ammonium hydrogen fluoride separation device needs to stop the separation operation when the solid material is discharged, which reduces the production efficiency.
The design of feed barrel, centrifugal barrel, discharge barrel and spiral blade is adopted, and the centrifugal force and spiral blade are used to achieve continuous separation of mother liquor and crystallization, so as to avoid crystallization gathering and blockage in the discharge tube.
The continuous separation of mother liquor and crystallization is achieved, production efficiency is improved, crystallization is blocked, and the structure is compact.
Smart Images

Figure CN223287750U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of ammonium bifluoride production equipment, in particular to an ammonium bifluoride self-separation device. Background Art
[0002] Ammonium bifluoride is a white or colorless, transparent, orthorhombic crystal that is easily deliquescent and agglomerated in air but readily soluble in water. It is primarily used as a glass etchant, preservative, and solvent for the production of metallic beryllium from beryllium oxide. During its production, a separation device is required to separate the ammonium bifluoride crystals from the mother liquor.
[0003] After searching, the Chinese patent publication number CN207238271U discloses a solid-liquid separator specifically for ammonium bifluoride production, including a separation tank, a motor, a rotating shaft, an impeller, a separation net, a centrifugal layer, a liquid layer, a transverse pusher, an inclined pusher, a feeder, a high-frequency vibrator, a liquid collector, an insulation layer and a pressurizer.
[0004] This patent sets up an inclined pusher and a horizontal pusher. When the solid-liquid separation of the material is completed, the inclined pusher pushes up the left side of the separation tank through the second push plate, causing the separation tank to tilt, which is conducive to the discharge of the separated solids and liquids. The horizontal pusher pushes out the solid material remaining in the centrifugal layer through the first push plate, making the separator convenient and efficient in discharging. However, the separation operation needs to be stopped every time the solid material is discharged, which reduces production efficiency. Utility Model Content
[0005] The purpose of the utility model is to solve the shortcomings of the prior art and to propose an ammonium bifluoride self-separation device.
[0006] In order to achieve the above purpose, the present invention adopts the following technical solutions:
[0007] An ammonium bifluoride self-separation device includes a shell supported on the ground by a base, wherein the two ends of the inner wall of the shell are respectively connected to a feed cylinder and a discharge cylinder, a centrifugal cylinder is arranged between the feed cylinder and the discharge cylinder, the outer wall of the centrifugal cylinder is a screening plate, the two ends of the centrifugal cylinder are respectively rotatably connected to the feed cylinder and the discharge cylinder, a liquid cavity exists between the combination of the centrifugal cylinder and the discharge cylinder and the inner wall of the shell, a feed hopper connected to the feed cylinder is provided at one end of the outer wall of the top end of the shell, and the bottom end of the discharge cylinder is connected to a solid discharge pipe.
[0008] As a further solution of the present invention: one end of the liquid cavity is connected to a liquid outlet pipe.
[0009] As a further solution of the present invention: a cavity is provided inside the base, and a motor is fixed to the inner wall of the cavity.
[0010] As a further solution of the present invention: the motor output shaft is connected to a driving gear.
[0011] As a further solution of the present invention: the outer wall of the centrifugal cylinder is provided with a driven gear that meshes with the driving gear.
[0012] As a further solution of the present invention: the bottom end of the solid discharge pipe is rotatably connected to a driven bevel gear, and one side of the driven bevel gear is transmission-engaged with a driving bevel gear.
[0013] As a further solution of the present invention: one side of the active bevel gear is connected to the motor output shaft through a transmission shaft.
[0014] As a further solution of the present invention: the inner wall of the driven bevel gear is connected with a spiral blade via a connecting rod, and the spiral blade is located inside the solid discharge pipe.
[0015] Compared with the prior art, the present invention provides an ammonium bifluoride self-separation device with the following beneficial effects:
[0016] 1. The utility model realizes continuous separation of mother liquor and crystals by providing a feed cylinder, a centrifugal cylinder, a feed hopper and a discharge cylinder, thereby improving production efficiency.
[0017] 2. The utility model is provided with spiral blades, which can transport the crystals entering the solid discharge pipe outwards during crystal discharge, thus preventing crystals from accumulating and clogging in the solid discharge pipe.
[0018] 3. The utility model is provided with a transmission shaft, a driving bevel gear and a driven bevel gear, and utilizes the motor that drives the centrifugal drum to rotate to drive the spiral blade to rotate, thereby reducing the setting of the power source and making the structure more compact.
[0019] The parts not involved in the device are the same as those in the prior art or can be implemented by using the prior art. The utility model has a simple structure and is easy to operate. BRIEF DESCRIPTION OF THE DRAWINGS
[0020] Figure 1 This is a schematic diagram of the overall structure of the ammonium bifluoride self-separation device proposed in the utility model;
[0021] Figure 2 This is a schematic diagram of the internal structure of the ammonium bifluoride self-separation device proposed in the present invention;
[0022] Figure 3 This is a side structural diagram of the ammonium bifluoride self-separation device proposed in the utility model;
[0023] Figure 4 This is a schematic diagram of the transmission structure of the driving gear and the driven gear of the ammonium bifluoride self-separation device proposed in the utility model;
[0024] Figure 5 This is a schematic diagram of the internal structure of the discharge pipe of the ammonium bifluoride self-separation device proposed in the utility model.
[0025] In the figure: 1. Base; 2. Shell; 3. Feed cylinder; 4. Centrifugal cylinder; 5. Feed hopper; 6. Discharge cylinder; 7. Screw shaft; 8. Cavity; 9. Motor; 10. Driving gear; 11. Driven gear; 12. Liquid cavity; 13. Liquid discharge pipe; 14. Solid discharge pipe; 15. Driven bevel gear; 16. Spiral blade; 17. Driving bevel gear; 18. Transmission shaft. DETAILED DESCRIPTION
[0026] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.
[0027] In the description of the present invention, it should be understood that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating directions or positional relationships, are based on the directions or positional relationships shown in the accompanying drawings. They are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operated in a specific direction. Therefore, they cannot be understood as limitations on the present invention.
[0028] Example 1
[0029] Ammonium bifluoride self-separation device, such as Figures 1 to 4 As shown, it includes a shell 2 supported on the ground by a base 1, and the two ends of the inner wall of the shell 2 are respectively connected to a feed cylinder 3 and a discharge cylinder 6, a centrifuge cylinder 4 is arranged between the feed cylinder 3 and the discharge cylinder 6, and the outer wall of the centrifuge cylinder 4 is a screening plate, and the two ends of the centrifuge cylinder 4 are rotatably connected to the feed cylinder 3 and the discharge cylinder 6 respectively, and there is a liquid cavity 12 between the combination of the centrifuge cylinder 4 and the discharge cylinder 6 and the inner wall of the shell 2, and a feed hopper 5 connected to the feed cylinder 3 is provided at one end of the outer wall of the top end of the shell 2, and a solid discharge pipe 14 is connected to the bottom end of the discharge cylinder 6, and a liquid discharge pipe 13 is connected to one end of the liquid cavity 12, and a cavity 8 is opened inside the base 1, and a motor 9 is fixed to the inner wall of the cavity 8, and the output shaft of the motor 9 is connected to a driving gear 10, and the outer wall of the centrifuge cylinder 4 is provided with a driven gear 11 engaged with the driving gear 10.
[0030] During production, the mixture of mother liquor and crystals is fed into the combination of feed cylinder 3, centrifugal cylinder 4 and discharge cylinder 6 through feed hopper 5. Motor 9 drives driving gear 10 to rotate, and the centrifugal cylinder 4 is rotated through the transmission of driving gear 10 and driven gear 11. The centrifugal force generated by the rotation of centrifugal cylinder 4 separates the mother liquor from the crystals. The mother liquor passes through centrifugal cylinder 4 and flows out through liquid discharge pipe 13. The separated crystals move toward discharge cylinder 6 through relative rotation of centrifugal cylinder 4 and screw shaft 7, and flow out through solid discharge pipe 14.
[0031] By providing the feed cylinder 3, the centrifugal cylinder 4, the feed hopper 5 and the discharge cylinder 6, continuous separation of the mother liquor and the crystals is achieved, thereby improving production efficiency.
[0032] Example 2
[0033] Ammonium bifluoride self-separation device, this embodiment makes the following improvements on the basis of embodiment 1, such as Figure 2 、 Figure 5 As shown, the bottom end of the solid discharge pipe 14 is rotatably connected to a driven bevel gear 15, and one side of the driven bevel gear 15 is engaged with a driving bevel gear 17, and one side of the driving bevel gear 17 is connected to the output shaft of the motor 9 through a transmission shaft 18. The inner wall of the driven bevel gear 15 is connected to a spiral blade 16 through a connecting rod, and the spiral blade 16 is located inside the solid discharge pipe 14.
[0034] When the motor 9 rotates, the driving bevel gear 17 is driven to rotate through the transmission shaft 18, and the spiral blade 16 is driven by the transmission of the driving bevel gear 17 and the driven bevel gear 15 to rotate and transport the crystals entering the solid discharge pipe 14 outward to prevent the crystals from gathering and clogging in the solid discharge pipe 14.
[0035] By providing the spiral blades 16 , the crystals entering the solid discharge pipe 14 are transported outwards during crystal discharge, thereby preventing the crystals from accumulating and clogging in the solid discharge pipe 14 .
[0036] By providing the transmission shaft 18, the driving bevel gear 17 and the driven bevel gear 15, the motor 9 that drives the centrifugal drum 4 to rotate drives the spiral blade 16 to rotate, thereby reducing the number of power sources and making the structure more compact.
[0037] Working principle: During production, the mixture of mother liquor and crystals is input into the combination of feed cylinder 3, centrifugal cylinder 4 and discharge cylinder 6 through feed hopper 5, and motor 9 drives driving gear 10 to rotate. The centrifugal cylinder 4 is rotated by the transmission of driving gear 10 and driven gear 11. The centrifugal force generated by the rotation of centrifugal cylinder 4 separates the mother liquor from the crystals. The mother liquor passes through the centrifugal cylinder 4 and flows out through the liquid discharge pipe 13. The separated crystals move toward the discharge cylinder 6 through the relative rotation of centrifugal cylinder 4 and spiral shaft 7, and flow out through the solid discharge pipe 14. At the same time, the transmission shaft 18 drives the driving bevel gear 17 to rotate, and the spiral blade 16 is driven by the transmission of driving bevel gear 17 and driven bevel gear 15 to rotate to transport the crystals entering the solid discharge pipe 14 outward to avoid crystal accumulation and blockage in the solid discharge pipe 14.
[0038] The above is only a preferred specific implementation method of the present invention, but the protection scope of the present invention is not limited to this. Any technician familiar with the technical field within the technical scope disclosed by the present invention can make equivalent replacements or changes based on the technical solution and utility model concept of the present invention, which should be covered by the protection scope of the present invention.
Claims
1. An ammonium bifluoride self-separation device, comprising a housing (2) supported on the ground by a base (1), characterized in that: The two ends of the inner wall of the shell (2) are respectively connected to a feed cylinder (3) and a discharge cylinder (6); a centrifugal cylinder (4) is arranged between the feed cylinder (3) and the discharge cylinder (6); the outer wall of the centrifugal cylinder (4) is a screening plate; the two ends of the centrifugal cylinder (4) are respectively rotatably connected to the feed cylinder (3) and the discharge cylinder (6); a liquid cavity (12) exists between the combination of the centrifugal cylinder (4) and the discharge cylinder (6) and the inner wall of the shell (2); a feed hopper (5) connected to the feed cylinder (3) is arranged at one end of the outer wall of the top end of the shell (2); and a solid discharge pipe (14) is connected to the bottom end of the discharge cylinder (6).
2. The ammonium bifluoride self-separation device according to claim 1, wherein One end of the liquid cavity (12) is connected to a liquid outlet pipe (13).
3. The ammonium bifluoride self-separation device according to claim 1, wherein A cavity (8) is provided inside the base (1), and a motor (9) is fixed to the inner wall of the cavity (8).
4. The ammonium bifluoride self-separation device according to claim 3, characterized in that The output shaft of the motor (9) is connected to a driving gear (10).
5. The ammonium bifluoride self-separation device according to claim 1, characterized in that The outer wall of the centrifugal cylinder (4) is provided with a driven gear (11) that is in transmission meshing engagement with the driving gear (10).
6. The ammonium bifluoride self-separation device according to claim 1, characterized in that The bottom end of the solid discharge pipe (14) is rotatably connected to a driven bevel gear (15), and one side of the driven bevel gear (15) is transmission-engaged with a driving bevel gear (17).
7. The ammonium bifluoride self-separation device according to claim 6, characterized in that One side of the active bevel gear (17) is connected to the output shaft of the motor (9) via a transmission shaft (18).
8. The ammonium bifluoride self-separation device according to claim 6, characterized in that The inner wall of the driven bevel gear (15) is connected to a spiral blade (16) via a connecting rod, and the spiral blade (16) is located inside the solid discharge pipe (14).
Citation Information
Patent Citations
Ammonium bifluoride produces special solid -liquid separation ware
CN207238271U