Clarification reaction kettle for desulfurization in strontium carbonate production

By designing a clarification reactor for desulfurization production in strontium carbonate and utilizing an inner and outer cylinder separation structure and a sludge scraping device, the problems of long cycle and poor effect of the existing clarification process are solved, and fast and efficient clarification effects and convenient equipment maintenance are achieved.

CN223381621UActive Publication Date: 2025-09-26GUIZHOU HONGKAI CHEM CO LTD
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Patent Information

Application Number
CN202422869262.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-22
Publication Date
2025-09-26
Estimated Expiration
2034-11-22

AI Technical Summary

Technical Problem

The existing industrial clarification process has a long cycle and poor effect, making it difficult to clarify alkaline liquids quickly and effectively.

Method used

A clarification reactor for strontium carbonate production and desulfurization is designed, which includes a reactor body and a scraper device. Through the separation structure of the inner and outer cylinders and the rotating cleaning of the scraper, solid-liquid separation and sludge removal are achieved, thereby improving the clarification efficiency.

Benefits of technology

It achieves rapid clarification of alkaline liquid, improves clarification effect, reduces clarification cycle and prolongs equipment service life.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of chemical production equipment, in particular to a clarification reaction kettle for desulfurization in strontium carbonate production, which comprises a reaction kettle body and a mud scraping device, the reaction kettle body is provided with an outer cylinder and an inner cylinder, the lower end of the inner cylinder is opened, and the outer cylinder is divided into a clarification cavity and a precipitation cavity by the inner cylinder; the outer cylinder body is used as a shell of the whole reaction kettle, not only provides physical support, but also plays a role in isolating the external environment. The upper part of the inner cylinder is tightly connected with the top of the outer cylinder, and the lower part of the inner cylinder is open to form an outlet. Through the structural design, the clarification cavity and the precipitation cavity are effectively divided into two relatively independent spaces, so that fluid disturbance caused when external fluid enters the clarification cavity is avoided, and the work of the clarification cavity is prevented from being interfered. Through the structural design, liquid can be quickly clarified, and the clarification effect is good.
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Description

Technical Field

[0001] The utility model relates to the technical field of chemical production equipment, in particular to a clarification reaction kettle for strontium carbonate production and desulfurization. Background Art

[0002] Strontium and strontium salts are widely used in electronics, chemicals, metallurgy, military industry, functional materials and fireworks manufacturing. Celestite is the main strontium ore raw material for the production of various strontium salt compounds. The production process of strontium salts produces a large amount of waste slag and waste gas. The main component of waste gas is SO2. In order to avoid direct emission of SO2 gas and cause air pollution, desulfurization towers are currently commonly used to desulfurize the waste gas. When the desulfurization tower is working, it is necessary to spray alkaline liquid to fully react with the waste gas passing through the desulfurization tower, thereby removing SO2 from the waste gas. Since industrial alkaline liquids are usually prone to precipitating precipitates, the alkaline liquid needs to be clarified when spraying it into the desulfurization tower. The existing industrial clarification process usually uses a clarification tank for static treatment, which not only has a long clarification cycle but also has poor clarification effect. Utility Model Content

[0003] The present invention aims to solve at least one of the technical problems existing in the prior art. To this end, the present invention proposes a clarification reactor for strontium carbonate production and desulfurization, aiming to provide a device that can quickly clarify alkaline liquids and improve the clarification effect.

[0004] According to an embodiment of the present invention, a clarification reactor for strontium carbonate production and desulfurization comprises:

[0005] The reactor body is provided with an outer cylinder, an inner cylinder, a water inlet pipe and a water outlet pipe; the upper end of the inner cylinder is fixedly connected to the top of the outer cylinder, and the lower end of the inner cylinder is open; the inner cylinder divides the outer cylinder into a clarification chamber and a sedimentation chamber; the water inlet pipe is provided at the upper end of the outer cylinder and passes through the outer cylinder to communicate with the sedimentation chamber, and the water outlet pipe is provided on the peripheral wall of the outer cylinder and passes through the outer cylinder and the inner cylinder in sequence to communicate with the clarification chamber;

[0006] The scraper device is provided with a scraper, and the scraper can clean the sludge on the side wall of the outer cylinder.

[0007] According to some embodiments of the present invention, an hourglass-shaped structure is provided at the lower portion of the inner cylinder.

[0008] According to some embodiments of the present invention, a funnel-shaped cylinder portion is provided at the lower end of the outer cylinder.

[0009] According to some embodiments of the present invention, the mud scraping device includes a rotary drive, a coupling and a control rod. The rotary drive is fixedly connected to the upper end of the outer cylinder, and the rotary drive is connected to the upper end of the control rod through the coupling. The lower end of the control rod passes through the outer cylinder and is detachably connected to the scraper.

[0010] According to some embodiments of the present invention, the scraper includes an extension portion and a working portion, the extension portion and the working portion are fixedly connected, and the length direction of the working portion is parallel to the busbar of the funnel-shaped cylinder portion.

[0011] According to some embodiments of the present invention, a sawtooth structure is provided on the working portion.

[0012] According to some embodiments of the present invention, the outer cylinder is provided with a mud discharge pipe at the lower end of the funnel-shaped cylinder portion, and the mud discharge pipe is provided with a ball valve.

[0013] According to some embodiments of the present invention, a heat-insulating cavity is provided on the peripheral wall of the outer cylinder.

[0014] According to some embodiments of the present invention, a first water pump is provided on the water inlet pipe, and a second water pump is provided on the water outlet pipe.

[0015] According to some embodiments of the present invention, a first solenoid valve is provided on the water inlet pipe, and a second solenoid valve is provided on the water outlet pipe.

[0016] According to the embodiment of the present invention, a clarification reactor for strontium carbonate production and desulfurization has at least the following

[0017] Beneficial effects:

[0018] According to the solution of the present invention, a clarification reactor for strontium carbonate production and desulfurization includes a reactor body and a scraper device, wherein the reactor body is provided with an outer cylinder and an inner cylinder, the lower end of the inner cylinder is open, and the inner cylinder divides the outer cylinder into a clarification chamber and a sedimentation chamber; the outer cylinder serves as the outer shell of the entire reactor, not only providing physical support, but also serving to isolate the external environment. The inner cylinder is placed inside the outer cylinder, closely connected to the top of the outer cylinder at the top, and open at the bottom to form an outlet. The design of this structure effectively divides the clarification chamber and the sedimentation chamber into two relatively independent spaces, avoiding fluid disturbances caused by the entry of external fluids and interference with the operation of the clarification chamber. When the liquid to be clarified enters the sedimentation chamber through the water inlet pipe, the heavier solid particles gradually sink to the bottom under the action of gravity. The inner cylinder limits the flow path of the liquid to be clarified, so that the solid and liquid phases can be more fully separated in the clarification chamber. The clarified liquid is pumped out from the outlet pipe, while the sediment remains in the sedimentation chamber.

[0019] According to the present invention, to maintain the reactor's long-term, efficient operation, sludge accumulated on the outer cylinder's sidewalls must be regularly removed. To this end, a sludge scraping device is configured with rotatable scrapers. These scrapers rotate and slide along the inner wall of the outer cylinder, effectively removing debris from the inner wall, preventing blockage, ensuring internal cleanliness, and extending service life. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] Figure 1 A structural diagram of the utility model;

[0021] Figure 2 This is a schematic cross-sectional view of the utility model;

[0022] Figure 3 For the utility model Figure 2 A structural schematic diagram at A;

[0023] Figure 4 This is a structural diagram of the scraper of the utility model.

[0024] In the picture:

[0025] 100 - reactor body, 101 - clarification chamber, 102 - sedimentation chamber, 103 - hourglass-shaped structure, 104 - insulation chamber, 110 - outer cylinder, 111 - funnel-shaped cylinder, 120 - inner cylinder, 130 - water inlet pipe, 131 - first water pump, 132 - second water pump, 140 - water outlet pipe, 150 - mud discharge pipe, 151 - ball valve;

[0026] 200 - Mud scraping device, 210 - Scraper, 211 - Extension part, 212 - Working part, 213 - Sawtooth structure, 220 - Rotary drive, 230 - Coupling, 240 - Control rod. DETAILED DESCRIPTION

[0027] The following describes embodiments of the present invention in detail. Examples of the embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals throughout represent the same or similar elements or elements having the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary and are intended only to explain the present invention and are not to be construed as limiting the present invention.

[0028] In the description of the present invention, it should be understood that descriptions involving orientation, such as the orientation or positional relationship indicated by up, down, etc., are based on the orientation or positional relationship shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0029] In the description of this utility model, "a plurality" means more than two. The use of "first" or "second" is solely for the purpose of distinguishing technical features and should not be construed as indicating or implying relative importance, or implicitly indicating the number of technical features indicated, or implicitly indicating the order of the technical features indicated.

[0030] In the description of the present invention, unless otherwise clearly defined, terms such as setting, installing, and connecting should be understood in a broad sense, and technicians in the relevant technical field can reasonably determine the specific meanings of the above terms in the present invention based on the specific content of the technical solution.

[0031] Reference Figures 1 to 4 As shown, the utility model discloses a clarification reactor for strontium carbonate production and desulfurization, comprising a reactor body 100 and a mud scraping device 200, wherein the reactor body 100 is provided with an outer cylinder 110, an inner cylinder 120, an inlet pipe 130 and a water outlet pipe 140; the upper end of the inner cylinder 120 is fixedly connected to the top of the outer cylinder 110, and the lower end of the inner cylinder 120 is open; the inner cylinder 120 divides the outer cylinder 110 into a clarification chamber 101 and a sedimentation chamber 102; the inlet pipe 130 is provided at the upper end of the outer cylinder 110 and passes through the outer cylinder 110 and is connected to the sedimentation chamber 102, and the outlet pipe 140 is provided on the peripheral wall of the outer cylinder 110 and passes through the outer cylinder 110 and the inner cylinder 120 in sequence and is connected to the clarification chamber 101; the mud scraping device 200 is provided with a scraper 210, which can clean the sludge on the side wall of the outer cylinder 110.

[0032] Specifically, in this embodiment, the reactor body 100 is provided with an outer cylinder 110 and an inner cylinder 120. The lower end of the inner cylinder 120 is open, and the inner cylinder 120 divides the outer cylinder 110 into a clarification chamber 101 and a sedimentation chamber 102. The outer cylinder 110 serves as the outer shell of the entire reactor, providing not only physical support but also isolating the reactor from the external environment. The inner cylinder 120 is placed inside the outer cylinder 110, closely connected to the top of the outer cylinder 110 at the top, and open at the bottom to form an outlet. Located at the top of the outer cylinder 110, it directly connects to the sedimentation chamber 102 and is responsible for introducing the solution to be clarified. The outlet pipe 140 is sequentially interspersed between the outer cylinder 110 and the inner cylinder 120, ultimately connecting to the clarification chamber 101, ensuring the safe discharge of the purified liquid. This structural design effectively divides the clarification chamber 101 and the sedimentation chamber 102 into two relatively independent spaces, preventing fluid disturbance caused by the entry of external fluid from interfering with the operation of the clarification chamber 101. When the liquid to be clarified enters the sedimentation chamber 102 through the water inlet pipe 130, the heavier solid particles gradually sink to the bottom under the action of gravity. The inner cylinder 120 limits the flow path of the liquid to be clarified, so that the solid and liquid phases can be more fully separated in the clarification chamber 101. The clarified liquid is extracted from the outlet pipe 140, and the sedimentation material remains in the sedimentation chamber 102. Furthermore, in order to maintain the long-term and efficient operation of the reactor, the sludge accumulated on the side wall of the outer cylinder 110 must be regularly removed. To this end, a rotatable scraper 210 is configured through the scraping device 200. The scraper 210 can rotate and slide along the inner wall of the outer cylinder 110, effectively removing attachments on the inner wall of the outer cylinder 110, preventing blockage, and ensuring the internal cleanliness of the inner wall of the outer cylinder 110, thereby extending the service life.

[0033] In some embodiments of the present invention, an hourglass-shaped structure 103 is provided at the lower portion of the inner cylinder 120. The hourglass-shaped structure 103 is designed to guide the water flow upward, first converging and then slowly diffusing, thereby reducing the chance of the supernatant being disturbed and improving the purity of the liquid in the clarification chamber 101.

[0034] In some embodiments of the present invention, a funnel-shaped cylinder 111 is provided at the lower end of the outer cylinder 110. In this embodiment, the design of the funnel-shaped cylinder 111 increases the bottom slope angle of the outer cylinder 110, accelerates the sliding speed of solid particles, promotes rapid sedimentation, and effectively improves the separation efficiency. The inclined funnel wall makes it difficult for residual matter to be retained, reduces the possibility of bottom accumulation, facilitates regular cleaning, and makes maintenance simple and quick. It can prevent sediment from silting. Furthermore, the design of the funnel-shaped cylinder 111 forms a streamlined channel that helps the liquid transition smoothly, avoids turbulence, protects the liquid in the clarification cavity 101 from secondary contamination, and maintains a high-quality clarification effect.

[0035] In some embodiments of the present invention, the scraper device 200 includes a rotary drive 220, a coupling 230, and a control rod 240. The rotary drive 220 is fixedly connected to the upper end of the outer cylinder 110. The rotary drive 220 is connected to the upper end of the control rod 240 through the coupling 230. The lower end of the control rod 240 extends through the outer cylinder 110 and is removably connected to the scraper 210. In this embodiment, the rotary drive 220 is mounted on the upper end of the outer cylinder 110 and serves as a power source, providing stable rotational force for the scraping action. The coupling 230 ensures smooth and efficient power transmission, connecting the rotary drive 220 and the control rod 240 to ensure precise connection during energy conversion. The upper end of the control rod 240 is tightly connected to the coupling 230, while the lower end of the control rod 240 extends into the interior of the reactor. The scraping action is implemented and adjusted through a removable connection with the scraper 210. This structural design allows the start and stop of the rotary drive 220 to be controlled by a preset program or manual command, enabling it to be activated as needed without human intervention, saving time and labor. The length of the control rod 240 and the rotation radius of the scraper 210 ensure that the scraper 210 reaches every part of the outer cylinder 110, leaving no blind spots and thoroughly removing dirt.

[0036] In some embodiments of the present invention, the scraper 210 includes an extension portion 211 and a working portion 212. The extension portion 211 and the working portion 212 are fixedly connected, and the length direction of the working portion 212 is parallel to the generatrix of the funnel-shaped cylinder 111. In this embodiment, the extension portion 211 serves as a connecting portion and is tightly integrated with the control rod 240, thereby achieving power transmission while increasing the operating distance and ensuring that the scraper 210 reaches every corner of the reactor. The working portion 212 is fixedly connected to the extension portion 211, and its length direction is parallel to the generatrix of the funnel-shaped cylinder 111. This design maximizes the coverage of the cleaning area, follows the principles of fluid mechanics, and avoids leaving any residue.

[0037] In some embodiments of the present invention, a serrated structure 213 is provided on the working portion 212. In this embodiment, the serrated structure 213 provided on the working portion 212 can improve the cleaning efficiency of the scraper device 200 and its ability to remove stubborn stains. The serrated structure 213 is introduced on the working portion 212 to increase friction and cutting force, ensuring a deep cleaning effect.

[0038] In some embodiments of the present invention, the outer cylinder 110 is provided with a mud discharge pipe 150 at the lower end of the funnel-shaped cylinder 111. This pipe is equipped with a ball valve 151. In this embodiment, the mud discharge pipe 150 directly connects to the lowest point of the funnel-shaped cylinder 111, utilizing gravity to smoothly discharge sediment, ensuring unobstructed flow within the interior and reducing the risk of clogging. The ball valve 151 serves as a control element within the mud discharge pipe 150. By turning a handle, the internal passageway's state is altered, enabling immediate control of material discharge, ensuring both efficient cleaning and ease of operation.

[0039] In some embodiments of the present invention, an insulating cavity 104 is provided on the peripheral wall of the outer cylinder 110. In this embodiment, by providing the insulating cavity 104 on the peripheral wall of the outer cylinder 110, antifreeze liquid can be injected into the insulating cavity 104 when the ambient temperature is too low to prevent the liquid inside the outer cylinder 110 from freezing.

[0040] In some embodiments of the present invention, a first water pump 131 is provided on the water inlet pipe 130, and a second water pump 132 is provided on the water outlet pipe 140. In this embodiment, the first water pump 131 is responsible for directing water into the outer cylinder 110, providing sufficient pressure to ensure a stable and even flow of water into the sedimentation chamber 102. The second water pump 132 is responsible for output, delivering the treated clarified liquid to its destination, thus providing both transportation and pressure boosting.

[0041] In some embodiments of the present invention, a first solenoid valve is provided on the water inlet pipe 130, and a second solenoid valve is provided on the water outlet pipe 140. The flow rate and opening state of the water inlet pipe 130 and the water outlet pipe 140 are intelligently controlled by the first solenoid valve and the second solenoid valve.

[0042] The embodiments of the present invention are described in detail above with reference to the accompanying drawings. However, the present invention is not limited to the above embodiments. Various changes can be made within the scope of knowledge possessed by ordinary technicians in the relevant technical field without departing from the purpose of the present invention.

Claims

1. A clarification reactor for strontium carbonate production and desulfurization, characterized in that: include: A reactor body (100) is provided with an outer cylinder (110), an inner cylinder (120), a water inlet pipe (130) and a water outlet pipe (140); the upper end of the inner cylinder (120) is fixedly connected to the top of the outer cylinder (110), and the lower end of the inner cylinder (120) is open; the inner cylinder (120) divides the outer cylinder (110) into a clarification chamber (101) and a sedimentation chamber (102); the water inlet pipe (130) is provided at the upper end of the outer cylinder (110) and passes through the outer cylinder (110) to communicate with the sedimentation chamber (102); the water outlet pipe (140) is provided on the peripheral wall of the outer cylinder (110) and passes through the outer cylinder (110) and the inner cylinder (120) in sequence to communicate with the clarification chamber (101); A mud scraping device (200) is provided with a scraper (210), and the scraper (210) can clean the mud on the side wall of the outer cylinder (110).

2. The clarification reactor for strontium carbonate production and desulfurization according to claim 1, wherein: An hourglass-shaped structure (103) is provided at the lower portion of the inner cylinder (120).

3. The clarification reactor for strontium carbonate production and desulfurization according to claim 1, wherein: A funnel-shaped cylindrical portion (111) is provided at the lower end of the outer cylindrical body (110).

4. The clarification reactor for desulfurization of strontium carbonate production according to claim 3, characterized in that: The mud scraping device (200) comprises a rotary drive (220), a coupling (230) and a control rod (240); the rotary drive (220) is fixedly connected to the upper end of the outer cylinder (110); the rotary drive (220) is transmission-connected to the upper end of the control rod (240) via the coupling (230); and the lower end of the control rod (240) passes through the outer cylinder (110) and is detachably connected to the scraper (210).

5. The clarification reactor for strontium carbonate production and desulfurization according to claim 4, characterized in that: The scraper (210) comprises an extension portion (211) and a working portion (212), wherein the extension portion (211) and the working portion (212) are fixedly connected, and the length direction of the working portion (212) is parallel to the generatrix of the funnel-shaped cylinder portion (111).

6. The clarification reactor for strontium carbonate production and desulfurization according to claim 5, characterized in that: The working portion (212) is provided with a sawtooth structure (213).

7. The clarification reactor for strontium carbonate production and desulfurization according to claim 3, characterized in that: The outer cylinder (110) is provided with a mud discharge pipe (150) at the lower end of the funnel-shaped cylinder portion (111), and a ball valve (151) is provided on the mud discharge pipe (150).

8. The clarification reactor for strontium carbonate production and desulfurization according to claim 1, characterized in that: A heat-insulating cavity (104) is provided on the peripheral wall of the outer cylinder (110).

9. The clarification reactor for strontium carbonate production and desulfurization according to claim 1, characterized in that: The water inlet pipe (130) is provided with a first water pump (131), and the water outlet pipe (140) is provided with a second water pump (132).

10. The clarification reactor for strontium carbonate production and desulfurization according to claim 9, characterized in that: The water inlet pipe (130) is provided with a first solenoid valve, and the water outlet pipe (140) is provided with a second solenoid valve.